#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2216331.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2216331_Fobs loop_ _publ_author_name 'Pu, Shou-Cheng' 'Gao, Wen-Yuan' 'Deng, Yi' 'Tu, Chun-Ling' _publ_section_title ; 4-Hydroxy-2,2,6,6-tetramethylpiperidinium nitrate ; _journal_coeditor_code BT2639 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o4896 _journal_volume 63 _journal_year 2007 _space_group_IT_number 36 _symmetry_space_group_name_Hall 'C 2c -2' _symmetry_space_group_name_H-M 'C m c 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 11.6721 _cell_length_b 10.5156 _cell_length_c 9.6565 _exptl_crystal_F_000 480.00 _reflns_d_resolution_high 0.7584 _[local]_cod_data_source_file bt2639Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' _R071115b' _shelx_refln_list_code 4 _shelx_f_calc_maximum 144.08 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, z' 'x, -y, z+1/2' '-x, -y, z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, z' 'x+1/2, -y+1/2, z+1/2' '-x+1/2, -y+1/2, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 20759.48 22756.93 756.10 o 4 0 0 3567.08 3388.84 50.52 o 6 0 0 4564.83 4408.55 162.42 o 8 0 0 3416.66 3251.40 81.90 o 12 0 0 3.26 24.07 10.28 o 14 0 0 25.99 0.79 10.47 o 1 1 0 1521.08 1298.99 12.87 o 3 1 0 82.34 77.50 3.43 o 5 1 0 18.53 18.08 2.53 o 7 1 0 122.63 115.70 4.53 o 9 1 0 135.91 116.74 4.03 o 11 1 0 31.83 21.55 4.91 o 13 1 0 38.21 38.60 10.02 o 15 1 0 0.17 6.81 8.90 o 0 2 0 14197.49 13913.16 338.32 o 2 2 0 1450.62 1246.58 17.81 o 4 2 0 455.47 409.55 7.96 o 6 2 0 559.96 483.39 9.48 o 8 2 0 591.88 612.85 20.17 o 10 2 0 254.26 239.16 8.85 o 12 2 0 0.48 0.92 2.36 o 14 2 0 7.57 18.16 8.43 o 1 3 0 368.05 363.09 5.32 o 3 3 0 196.55 165.51 5.20 o 5 3 0 0.06 3.32 1.57 o 7 3 0 296.07 279.80 12.46 o 9 3 0 322.69 345.01 11.41 o 11 3 0 50.45 43.33 7.59 o 13 3 0 82.18 96.95 14.22 o 0 4 0 15607.66 16322.03 482.29 o 2 4 0 821.54 791.56 11.02 o 4 4 0 249.29 251.65 6.34 o 6 4 0 388.87 425.06 9.43 o 8 4 0 125.65 123.95 6.82 o 10 4 0 101.61 99.09 5.98 o 12 4 0 9.35 15.94 5.22 o 14 4 0 12.12 13.50 8.20 o 1 5 0 1080.33 1239.97 24.50 o 3 5 0 190.41 149.87 4.64 o 5 5 0 36.18 37.25 3.85 o 7 5 0 82.40 84.40 5.18 o 9 5 0 165.72 176.89 10.94 o 11 5 0 0.32 5.13 3.20 o 13 5 0 3.97 1.66 3.17 o 0 6 0 2993.38 3252.18 102.72 o 2 6 0 26.44 25.09 3.10 o 4 6 0 173.01 164.26 6.36 o 6 6 0 359.68 373.92 17.15 o 8 6 0 116.32 121.65 8.74 o 10 6 0 76.15 78.01 8.78 o 12 6 0 0.24 10.74 8.25 o 1 7 0 1516.01 1554.19 35.76 o 3 7 0 408.77 388.47 10.43 o 5 7 0 16.71 32.02 5.33 o 7 7 0 631.66 599.61 16.42 o 9 7 0 43.13 27.05 5.23 o 11 7 0 12.37 22.51 7.72 o 13 7 0 0.91 5.88 4.57 o 0 8 0 19.81 23.43 6.47 o 2 8 0 163.58 147.43 9.07 o 4 8 0 349.82 346.12 12.47 o 6 8 0 194.17 157.23 10.58 o 8 8 0 50.57 43.54 8.62 o 10 8 0 2.97 4.66 4.19 o 12 8 0 24.39 29.45 11.31 o 1 9 0 7.52 6.47 2.83 o 3 9 0 386.02 316.70 10.64 o 5 9 0 482.93 530.82 13.67 o 7 9 0 24.93 22.45 6.45 o 9 9 0 1.20 4.66 3.53 o 11 9 0 2.10 8.41 6.69 o 0 10 0 0.35 3.64 5.01 o 2 10 0 181.73 162.95 25.55 o 4 10 0 7.34 9.80 3.79 o 6 10 0 0.18 6.46 5.70 o 8 10 0 87.80 99.49 15.76 o 10 10 0 23.82 25.11 7.67 o 1 11 0 108.22 94.77 19.91 o 3 11 0 230.79 216.94 11.47 o 5 11 0 124.97 124.14 29.57 o 7 11 0 112.46 117.33 19.75 o 9 11 0 2.28 6.44 4.71 o 0 12 0 172.25 128.88 41.14 o 2 12 0 66.04 53.55 14.91 o 4 12 0 80.52 69.58 14.83 o 6 12 0 31.74 32.35 8.07 o 1 13 0 3.51 7.91 4.32 o 3 13 0 83.73 69.59 29.64 o 5 13 0 114.59 146.30 31.02 o 1 1 1 1152.63 944.51 6.46 o 3 1 1 12485.48 12670.00 117.62 o 5 1 1 3642.10 3679.87 40.17 o 7 1 1 55.57 47.28 2.38 o 9 1 1 189.90 215.33 4.72 o 11 1 1 34.70 24.77 3.48 o 13 1 1 72.77 74.03 8.81 o 15 1 1 23.06 23.78 6.85 o 0 2 1 7963.34 7417.17 98.60 o 2 2 1 4915.36 4752.12 36.83 o 4 2 1 1049.86 1049.56 11.99 o 6 2 1 57.59 47.84 2.51 o 8 2 1 247.79 240.69 5.37 o 10 2 1 691.21 707.99 13.81 o 12 2 1 14.61 11.66 2.98 o 14 2 1 17.77 35.55 7.87 o 1 3 1 1618.99 1548.86 17.24 o 3 3 1 1097.81 1110.44 16.01 o 5 3 1 79.88 72.83 2.60 o 7 3 1 143.30 136.30 4.19 o 9 3 1 90.79 92.46 4.02 o 11 3 1 14.67 8.30 2.01 o 13 3 1 0.61 5.34 2.19 o 0 4 1 3830.59 3823.00 33.60 o 2 4 1 650.60 684.07 7.61 o 4 4 1 598.96 588.21 7.62 o 6 4 1 67.17 77.13 3.15 o 8 4 1 206.14 176.01 5.24 o 10 4 1 395.00 407.23 10.07 o 12 4 1 5.91 11.07 2.59 o 14 4 1 4.08 11.55 4.64 o 1 5 1 69.62 73.28 1.95 o 3 5 1 1749.25 1757.15 19.08 o 5 5 1 455.48 444.76 9.29 o 7 5 1 29.15 31.73 2.97 o 9 5 1 1.11 3.98 2.04 o 11 5 1 34.06 35.57 4.23 o 13 5 1 2.33 8.38 3.30 o 0 6 1 675.08 723.35 13.33 o 2 6 1 520.56 529.59 7.56 o 4 6 1 532.20 551.96 9.65 o 6 6 1 26.71 26.69 2.93 o 8 6 1 188.04 175.94 5.83 o 10 6 1 11.50 6.88 2.40 o 12 6 1 6.71 5.30 2.76 o 1 7 1 111.73 130.98 4.15 o 3 7 1 62.21 67.01 4.07 o 5 7 1 23.93 24.89 2.69 o 7 7 1 9.13 10.36 2.22 o 9 7 1 59.13 60.30 6.29 o 11 7 1 13.36 11.40 4.13 o 13 7 1 3.49 6.11 2.96 o 0 8 1 6.43 3.52 2.17 o 2 8 1 70.96 85.03 4.39 o 4 8 1 612.21 599.29 12.51 o 6 8 1 6.65 5.83 2.25 o 8 8 1 102.10 128.67 9.22 o 10 8 1 24.73 13.89 3.92 o 12 8 1 15.39 14.12 3.50 o 1 9 1 152.96 153.56 6.91 o 3 9 1 30.61 34.59 4.39 o 5 9 1 16.42 20.09 3.04 o 7 9 1 59.35 56.91 5.67 o 9 9 1 50.31 55.40 6.74 o 11 9 1 19.30 30.61 6.05 o 0 10 1 306.97 254.39 18.70 o 2 10 1 65.82 54.35 6.88 o 4 10 1 57.96 48.52 5.30 o 6 10 1 16.11 11.16 3.62 o 8 10 1 14.10 19.69 5.71 o 10 10 1 8.07 12.91 3.81 o 1 11 1 206.20 208.76 15.49 o 3 11 1 290.11 278.38 15.49 o 5 11 1 286.52 342.18 16.33 o 7 11 1 76.32 86.85 8.97 o 9 11 1 44.46 49.76 9.08 o 0 12 1 51.68 40.79 9.67 o 2 12 1 103.22 91.81 8.71 o 4 12 1 48.62 36.05 9.68 o 6 12 1 19.64 22.27 6.18 o 1 13 1 18.77 18.43 5.50 o 3 13 1 56.97 48.01 10.90 o 5 13 1 139.91 150.21 17.08 o 0 0 2 10144.57 9799.55 183.02 o 2 0 2 2495.86 2471.20 44.92 o 4 0 2 2504.91 2659.25 35.74 o 6 0 2 246.74 243.85 5.31 o 8 0 2 1026.22 1112.26 25.60 o 10 0 2 80.38 86.02 5.63 o 12 0 2 32.59 30.72 6.28 o 14 0 2 45.59 52.13 15.59 o 3 1 2 317.46 313.29 5.44 o 5 1 2 1714.24 1761.13 19.37 o 7 1 2 116.06 108.73 2.52 o 9 1 2 1.24 2.51 1.08 o 11 1 2 0.01 2.43 1.53 o 13 1 2 14.03 8.59 3.58 o 15 1 2 23.04 16.38 5.40 o 0 2 2 4191.85 4026.75 56.20 o 2 2 2 1464.70 1390.68 14.64 o 4 2 2 263.75 237.81 4.41 o 6 2 2 166.81 158.37 3.30 o 8 2 2 283.13 289.73 7.42 o 10 2 2 58.24 58.61 3.84 o 12 2 2 10.00 10.08 3.79 o 14 2 2 1.79 8.30 3.85 o 1 3 2 217.15 179.48 3.75 o 3 3 2 57.30 74.78 2.70 o 5 3 2 852.04 863.01 10.64 o 7 3 2 138.92 152.20 4.69 o 9 3 2 81.69 69.73 4.02 o 11 3 2 0.81 4.22 2.86 o 13 3 2 49.84 40.60 5.90 o 0 4 2 304.33 317.18 5.98 o 2 4 2 523.27 530.59 8.19 o 4 4 2 582.55 587.74 9.46 o 6 4 2 132.62 113.46 3.60 o 8 4 2 123.58 126.71 4.00 o 10 4 2 17.79 14.29 2.85 o 12 4 2 3.89 7.90 3.02 o 14 4 2 40.24 34.15 7.07 o 1 5 2 549.37 583.11 9.56 o 3 5 2 189.88 211.95 6.07 o 5 5 2 166.52 169.72 4.79 o 7 5 2 42.28 33.49 2.86 o 9 5 2 280.58 290.56 8.14 o 11 5 2 18.19 21.19 3.41 o 13 5 2 30.02 32.50 6.52 o 0 6 2 1316.30 1334.64 22.94 o 2 6 2 907.48 868.87 11.45 o 4 6 2 70.49 84.81 5.37 o 6 6 2 213.60 223.86 6.60 o 8 6 2 128.82 144.17 5.24 o 10 6 2 7.65 11.95 3.16 o 12 6 2 18.48 16.34 3.83 o 1 7 2 881.95 891.87 15.24 o 3 7 2 310.26 303.54 6.11 o 5 7 2 87.83 86.61 5.31 o 7 7 2 295.32 309.18 7.92 o 9 7 2 144.84 171.79 14.02 o 11 7 2 36.09 32.41 5.25 o 13 7 2 11.04 20.31 7.79 o 0 8 2 428.46 442.17 13.64 o 2 8 2 74.46 74.60 5.39 o 4 8 2 160.46 158.52 6.63 o 6 8 2 69.79 66.57 5.86 o 8 8 2 57.83 59.04 6.98 o 10 8 2 29.66 28.50 5.89 o 12 8 2 3.08 14.07 4.30 o 1 9 2 281.91 266.41 8.74 o 3 9 2 62.46 65.31 8.84 o 5 9 2 6.38 8.39 2.21 o 7 9 2 87.74 103.60 8.47 o 9 9 2 39.65 29.34 5.78 o 11 9 2 0.46 6.29 2.54 o 0 10 2 101.23 92.29 11.87 o 2 10 2 136.44 132.93 5.68 o 4 10 2 79.17 74.47 11.67 o 6 10 2 10.21 13.90 3.33 o 8 10 2 44.22 36.91 6.22 o 10 10 2 61.22 64.10 13.16 o 1 11 2 107.05 111.14 10.44 o 3 11 2 34.93 35.39 7.38 o 5 11 2 5.89 5.59 2.44 o 7 11 2 36.83 37.08 6.33 o 9 11 2 54.06 37.05 10.24 o 0 12 2 245.97 243.77 13.47 o 2 12 2 85.10 72.24 12.75 o 4 12 2 2.23 5.99 2.77 o 6 12 2 6.69 9.64 3.95 o 1 13 2 195.90 218.37 20.16 o 3 13 2 64.90 41.86 9.62 o 1 1 3 1959.44 1837.49 13.98 o 3 1 3 1694.87 1622.60 12.39 o 5 1 3 2889.05 3070.24 42.48 o 7 1 3 340.56 373.47 7.12 o 9 1 3 152.63 126.93 5.26 o 11 1 3 137.11 142.41 5.12 o 13 1 3 34.50 35.39 5.18 o 0 2 3 6651.01 6949.62 326.82 o 2 2 3 790.87 864.48 13.84 o 4 2 3 2501.81 2663.30 30.09 o 6 2 3 568.01 639.19 9.47 o 8 2 3 21.99 23.36 2.78 o 10 2 3 48.91 46.28 5.13 o 12 2 3 6.23 9.31 2.55 o 14 2 3 44.28 27.52 5.36 o 1 3 3 2294.40 2388.23 18.12 o 3 3 3 1415.35 1475.15 15.89 o 5 3 3 428.64 462.90 7.39 o 7 3 3 288.38 271.38 7.47 o 9 3 3 236.32 249.57 7.48 o 11 3 3 30.57 40.37 4.81 o 13 3 3 28.41 20.60 4.62 o 0 4 3 2610.86 2752.34 54.07 o 2 4 3 260.94 287.44 6.11 o 4 4 3 521.66 558.55 7.88 o 6 4 3 320.82 313.14 6.79 o 8 4 3 105.32 101.87 4.62 o 10 4 3 75.80 70.68 5.30 o 12 4 3 18.12 17.16 3.26 o 14 4 3 37.53 23.62 5.51 o 1 5 3 366.83 401.25 6.54 o 3 5 3 258.55 285.14 5.38 o 5 5 3 425.71 434.93 9.86 o 7 5 3 65.63 53.16 4.86 o 9 5 3 97.54 108.55 5.96 o 11 5 3 86.96 100.95 9.80 o 13 5 3 12.34 17.74 5.41 o 0 6 3 2169.38 2162.56 78.08 o 2 6 3 91.89 93.91 4.18 o 4 6 3 453.49 430.02 7.78 o 6 6 3 46.57 53.90 4.06 o 8 6 3 154.83 137.31 6.14 o 10 6 3 72.01 62.17 5.99 o 12 6 3 47.40 70.19 10.69 o 1 7 3 1374.08 1318.02 17.70 o 3 7 3 608.13 624.50 11.45 o 5 7 3 421.35 463.94 10.74 o 7 7 3 171.16 189.82 8.70 o 9 7 3 252.23 294.21 8.74 o 11 7 3 38.27 30.28 6.11 o 0 8 3 1142.19 1129.94 31.28 o 2 8 3 19.25 24.71 3.14 o 4 8 3 140.18 131.99 7.30 o 6 8 3 31.08 24.84 3.84 o 8 8 3 51.44 40.55 4.45 o 10 8 3 15.61 15.34 4.13 o 12 8 3 23.08 23.13 8.77 o 1 9 3 1233.70 1254.19 20.89 o 3 9 3 344.30 353.30 13.15 o 5 9 3 42.28 39.50 4.84 o 7 9 3 290.35 284.01 12.06 o 9 9 3 244.95 280.71 9.66 o 11 9 3 59.75 49.73 9.48 o 0 10 3 165.29 160.80 11.42 o 2 10 3 59.21 51.40 8.00 o 4 10 3 25.88 25.80 4.53 o 6 10 3 8.76 7.96 2.93 o 8 10 3 6.95 14.29 3.81 o 10 10 3 15.48 10.12 5.92 o 1 11 3 5.89 9.85 3.07 o 3 11 3 52.48 40.26 7.56 o 5 11 3 5.19 6.67 3.30 o 7 11 3 51.55 47.85 7.94 o 0 12 3 56.68 66.72 16.02 o 2 12 3 22.85 19.44 4.68 o 4 12 3 35.79 34.01 6.80 o 6 12 3 2.06 5.20 4.09 o 1 13 3 60.91 44.25 10.13 o 3 13 3 8.45 15.92 4.16 o 0 0 4 1038.31 1062.23 16.81 o 2 0 4 137.04 122.84 3.54 o 4 0 4 1188.93 1315.98 22.45 o 6 0 4 29.88 31.36 3.75 o 8 0 4 69.49 95.14 9.74 o 10 0 4 271.97 269.22 13.71 o 12 0 4 10.75 9.34 4.33 o 14 0 4 11.00 17.73 6.27 o 1 1 4 2314.87 2401.04 15.69 o 3 1 4 642.23 637.90 8.18 o 5 1 4 224.17 245.71 5.78 o 7 1 4 58.72 63.54 4.12 o 9 1 4 67.17 77.22 6.32 o 11 1 4 2.81 7.52 2.36 o 13 1 4 1.24 6.59 2.03 o 0 2 4 369.15 466.34 7.99 o 2 2 4 33.17 41.25 1.78 o 4 2 4 835.37 852.94 14.50 o 6 2 4 70.66 68.69 3.65 o 8 2 4 32.40 25.09 3.89 o 10 2 4 11.54 10.21 2.86 o 12 2 4 24.89 30.16 4.64 o 14 2 4 25.67 29.33 6.52 o 1 3 4 925.75 920.95 12.72 o 3 3 4 171.97 158.96 3.07 o 5 3 4 312.92 327.25 7.06 o 7 3 4 30.09 27.72 3.07 o 9 3 4 106.65 118.41 6.97 o 11 3 4 4.08 7.14 2.95 o 13 3 4 15.09 18.57 4.98 o 0 4 4 1037.13 1098.32 17.42 o 2 4 4 724.77 694.81 9.63 o 4 4 4 964.63 1059.19 15.20 o 6 4 4 419.20 406.55 10.58 o 8 4 4 16.02 21.95 3.44 o 10 4 4 178.53 175.60 15.03 o 12 4 4 40.64 35.37 5.58 o 1 5 4 1353.11 1352.65 17.15 o 3 5 4 501.94 497.45 9.88 o 5 5 4 542.78 560.05 10.09 o 7 5 4 197.04 242.13 7.04 o 9 5 4 263.81 256.59 10.36 o 11 5 4 15.50 15.73 4.25 o 13 5 4 74.83 94.38 9.26 o 0 6 4 370.13 361.09 11.26 o 2 6 4 102.13 117.61 5.36 o 4 6 4 255.09 261.45 6.49 o 6 6 4 41.16 42.20 4.28 o 8 6 4 31.32 23.60 3.93 o 10 6 4 102.86 95.54 9.06 o 12 6 4 0.08 11.42 3.49 o 1 7 4 280.68 289.00 9.28 o 3 7 4 674.06 669.42 16.24 o 5 7 4 200.52 180.83 7.53 o 7 7 4 19.46 19.07 3.94 o 9 7 4 137.40 145.91 6.83 o 11 7 4 10.73 24.41 4.67 o 0 8 4 356.83 326.85 11.53 o 2 8 4 891.47 895.43 19.50 o 4 8 4 1141.37 1157.81 28.13 o 6 8 4 364.72 410.26 8.89 o 8 8 4 15.78 19.51 3.88 o 10 8 4 5.03 3.37 2.79 o 1 9 4 82.66 80.21 7.94 o 3 9 4 81.02 83.76 8.39 o 5 9 4 49.46 44.86 6.69 o 7 9 4 7.98 10.40 3.04 o 9 9 4 13.23 19.07 6.05 o 0 10 4 111.64 85.65 17.34 o 2 10 4 260.76 270.67 12.62 o 4 10 4 272.23 263.69 9.73 o 6 10 4 191.74 203.16 10.90 o 8 10 4 45.43 52.00 11.70 o 1 11 4 44.92 52.74 7.97 o 3 11 4 91.51 79.60 11.75 o 5 11 4 69.51 60.04 10.26 o 7 11 4 18.57 21.41 4.80 o 0 12 4 24.28 32.80 9.14 o 2 12 4 52.35 45.30 9.24 o 4 12 4 12.71 18.64 5.87 o 6 12 4 6.62 13.91 5.32 o 1 13 4 2.50 7.60 3.48 o 1 1 5 190.97 175.97 3.17 o 3 1 5 59.48 56.83 2.43 o 5 1 5 195.00 188.08 6.10 o 7 1 5 203.44 225.07 8.06 o 9 1 5 32.92 34.94 4.10 o 11 1 5 20.92 15.20 3.00 o 13 1 5 1.82 4.89 3.19 o 0 2 5 2595.80 2659.72 51.73 o 2 2 5 1616.93 1732.74 26.50 o 4 2 5 288.41 284.38 6.30 o 6 2 5 10.45 10.82 2.08 o 8 2 5 235.33 196.55 7.64 o 10 2 5 31.71 19.65 3.58 o 12 2 5 5.80 9.19 2.75 o 1 3 5 1677.08 1770.19 21.47 o 3 3 5 74.41 71.64 2.86 o 5 3 5 80.91 78.30 3.72 o 7 3 5 53.77 54.45 4.50 o 9 3 5 154.06 138.30 8.16 o 11 3 5 5.25 7.73 3.13 o 13 3 5 30.08 36.57 6.63 o 0 4 5 92.68 100.53 7.59 o 2 4 5 270.46 280.51 6.16 o 4 4 5 151.07 149.27 5.74 o 6 4 5 69.58 74.85 5.45 o 8 4 5 30.19 16.30 3.01 o 10 4 5 0.07 7.14 3.27 o 12 4 5 26.00 45.39 5.76 o 1 5 5 208.35 222.00 5.70 o 3 5 5 78.06 80.29 5.40 o 5 5 5 205.22 179.69 5.93 o 7 5 5 190.57 197.64 6.89 o 9 5 5 65.16 56.93 6.63 o 11 5 5 16.79 18.66 4.23 o 0 6 5 159.61 167.00 10.22 o 2 6 5 497.86 545.45 13.03 o 4 6 5 1085.77 1061.44 23.39 o 6 6 5 272.16 280.16 9.59 o 8 6 5 30.75 36.56 5.38 o 10 6 5 7.38 9.95 4.18 o 12 6 5 125.02 144.35 13.86 o 1 7 5 664.56 627.22 13.69 o 3 7 5 126.83 129.38 8.26 o 5 7 5 91.38 83.70 10.29 o 7 7 5 170.89 210.16 9.41 o 9 7 5 33.75 32.54 6.12 o 11 7 5 2.99 11.25 4.09 o 0 8 5 127.04 130.61 9.83 o 2 8 5 193.60 195.15 6.96 o 4 8 5 276.42 284.28 7.84 o 6 8 5 25.07 25.62 4.45 o 8 8 5 3.41 5.91 3.24 o 10 8 5 3.58 9.70 3.46 o 1 9 5 561.97 598.51 12.22 o 3 9 5 138.40 158.34 11.81 o 5 9 5 240.80 249.73 7.91 o 7 9 5 140.35 137.93 9.77 o 9 9 5 100.14 96.84 7.40 o 0 10 5 131.58 128.16 25.88 o 2 10 5 65.54 61.62 9.41 o 4 10 5 125.98 135.40 9.55 o 6 10 5 70.04 59.60 9.62 o 8 10 5 17.06 11.47 3.29 o 1 11 5 30.40 37.15 7.33 o 3 11 5 15.67 16.15 4.05 o 5 11 5 7.33 9.03 3.71 o 7 11 5 59.73 81.33 10.05 o 0 12 5 14.42 10.71 4.92 o 2 12 5 74.09 91.08 9.97 o 4 12 5 51.05 57.72 12.95 o 0 0 6 47.64 53.16 5.79 o 2 0 6 63.68 71.59 4.65 o 4 0 6 1175.03 1154.63 29.62 o 6 0 6 242.78 231.54 9.86 o 8 0 6 63.70 53.31 7.42 o 10 0 6 78.74 83.77 9.43 o 12 0 6 28.18 34.84 7.13 o 1 1 6 31.14 27.59 1.83 o 3 1 6 92.43 97.32 3.61 o 5 1 6 430.20 400.03 11.29 o 7 1 6 20.11 18.06 2.90 o 9 1 6 9.25 10.20 2.57 o 11 1 6 13.24 12.16 3.72 o 13 1 6 9.34 10.82 3.67 o 0 2 6 279.81 269.19 11.40 o 2 2 6 659.89 704.83 12.10 o 4 2 6 1435.90 1499.29 24.13 o 6 2 6 329.99 373.20 11.05 o 8 2 6 12.94 9.68 3.29 o 10 2 6 28.75 23.50 4.36 o 12 2 6 39.43 25.74 6.30 o 1 3 6 308.01 323.95 13.02 o 3 3 6 312.98 305.29 6.38 o 5 3 6 1052.86 1058.10 23.12 o 7 3 6 89.39 78.68 7.83 o 9 3 6 6.36 13.08 4.23 o 11 3 6 25.90 33.89 4.93 o 13 3 6 36.02 34.79 6.57 o 0 4 6 171.73 160.05 5.25 o 2 4 6 220.73 239.99 5.93 o 4 4 6 132.22 156.83 5.93 o 6 4 6 156.83 143.92 6.28 o 8 4 6 15.47 15.50 3.24 o 10 4 6 17.66 16.03 4.12 o 12 4 6 35.70 39.78 6.16 o 1 5 6 29.97 38.63 4.11 o 3 5 6 139.38 127.27 6.71 o 5 5 6 271.28 264.42 9.98 o 7 5 6 1.45 6.03 2.66 o 9 5 6 18.44 29.70 4.82 o 11 5 6 6.70 8.01 4.11 o 0 6 6 401.27 347.63 11.63 o 2 6 6 359.85 365.54 10.49 o 4 6 6 653.84 651.33 13.86 o 6 6 6 88.47 76.75 6.88 o 8 6 6 20.04 35.45 5.26 o 10 6 6 95.53 97.19 10.73 o 1 7 6 301.62 305.94 9.99 o 3 7 6 74.64 68.45 8.29 o 5 7 6 264.21 250.38 7.67 o 7 7 6 40.69 51.07 7.19 o 9 7 6 44.75 35.36 5.88 o 11 7 6 15.92 29.00 6.39 o 0 8 6 201.76 212.07 16.49 o 2 8 6 257.21 256.49 7.48 o 4 8 6 375.82 400.37 14.61 o 6 8 6 148.49 128.72 10.97 o 8 8 6 34.49 32.83 5.57 o 10 8 6 53.97 61.14 8.68 o 1 9 6 89.16 84.77 10.89 o 3 9 6 126.80 124.70 10.05 o 5 9 6 13.88 13.93 3.87 o 7 9 6 1.60 4.75 3.42 o 9 9 6 29.06 19.83 5.82 o 0 10 6 201.76 218.78 29.68 o 2 10 6 132.45 132.14 11.21 o 4 10 6 91.58 83.05 11.95 o 6 10 6 124.44 130.39 11.60 o 1 11 6 3.16 8.30 3.85 o 3 11 6 14.42 10.95 2.98 o 5 11 6 76.98 83.20 8.49 o 0 12 6 77.89 68.40 18.15 o 2 12 6 12.65 15.59 4.67 o 1 1 7 732.58 698.15 12.39 o 3 1 7 357.63 368.80 6.71 o 5 1 7 811.84 773.32 18.08 o 7 1 7 78.50 78.10 5.30 o 9 1 7 59.18 66.41 6.56 o 11 1 7 16.74 20.68 3.80 o 0 2 7 155.29 142.01 4.66 o 2 2 7 241.38 256.51 5.28 o 4 2 7 1116.47 1136.88 23.82 o 6 2 7 436.67 461.12 18.91 o 8 2 7 164.04 181.37 6.40 o 10 2 7 20.62 20.18 4.32 o 12 2 7 22.03 22.41 4.98 o 1 3 7 60.86 61.48 3.59 o 3 3 7 27.31 27.80 3.10 o 5 3 7 26.56 33.26 4.07 o 7 3 7 20.73 21.35 4.58 o 9 3 7 9.48 6.15 3.44 o 11 3 7 3.92 8.81 3.16 o 0 4 7 50.98 80.97 7.93 o 2 4 7 26.02 26.75 3.11 o 4 4 7 203.70 175.47 6.96 o 6 4 7 166.78 170.13 8.36 o 8 4 7 33.89 21.86 4.76 o 10 4 7 9.01 12.70 4.03 o 12 4 7 38.41 32.29 6.69 o 1 5 7 97.02 84.23 5.01 o 3 5 7 33.33 31.10 4.27 o 5 5 7 105.52 95.83 11.01 o 7 5 7 9.40 15.60 4.53 o 9 5 7 12.23 17.75 4.29 o 11 5 7 0.13 4.20 2.87 o 0 6 7 102.87 67.20 9.50 o 2 6 7 86.09 104.54 6.68 o 4 6 7 32.37 25.95 4.50 o 6 6 7 16.68 19.04 3.64 o 8 6 7 73.02 84.66 7.34 o 10 6 7 28.35 38.59 9.84 o 1 7 7 168.60 177.65 6.08 o 3 7 7 45.78 45.91 6.26 o 5 7 7 57.56 44.62 6.23 o 7 7 7 43.48 38.28 6.17 o 9 7 7 31.23 42.62 8.98 o 0 8 7 175.15 199.78 27.77 o 2 8 7 94.53 89.74 10.21 o 4 8 7 28.15 31.59 5.40 o 6 8 7 24.88 32.05 5.57 o 8 8 7 61.94 53.60 7.72 o 1 9 7 52.11 57.54 10.01 o 3 9 7 211.80 225.33 9.40 o 5 9 7 30.82 24.79 5.70 o 7 9 7 17.87 24.00 6.01 o 0 10 7 373.93 392.31 15.65 o 2 10 7 44.77 40.09 7.63 o 4 10 7 2.37 5.61 2.32 o 6 10 7 3.35 7.67 3.24 o 1 11 7 186.27 201.59 9.57 o 3 11 7 61.97 59.81 10.82 o 0 0 8 756.42 796.87 32.15 o 2 0 8 1674.24 1850.14 51.71 o 4 0 8 1722.01 1786.01 58.21 o 6 0 8 461.08 498.25 12.52 o 8 0 8 123.56 134.03 7.47 o 10 0 8 18.52 12.77 5.37 o 1 1 8 97.99 99.49 3.75 o 3 1 8 16.26 17.61 2.49 o 5 1 8 47.42 48.96 5.29 o 7 1 8 25.61 23.89 3.97 o 9 1 8 44.52 45.45 6.00 o 11 1 8 28.48 35.36 6.63 o 0 2 8 32.60 32.30 4.00 o 2 2 8 44.94 57.07 5.68 o 4 2 8 150.70 140.89 6.11 o 6 2 8 28.42 24.27 5.64 o 8 2 8 12.15 12.74 3.41 o 10 2 8 0.24 2.88 2.52 o 1 3 8 186.58 186.36 7.42 o 3 3 8 143.21 144.07 6.05 o 5 3 8 211.19 201.04 6.79 o 7 3 8 17.62 13.42 3.67 o 9 3 8 112.71 120.25 14.68 o 11 3 8 81.71 81.60 15.31 o 0 4 8 33.11 13.45 3.24 o 2 4 8 337.55 329.74 14.98 o 4 4 8 319.07 290.43 8.35 o 6 4 8 87.33 92.62 9.02 o 8 4 8 14.65 12.10 4.47 o 10 4 8 4.93 6.79 3.17 o 1 5 8 11.83 15.97 3.02 o 3 5 8 15.19 17.68 3.63 o 5 5 8 63.93 45.34 7.08 o 7 5 8 7.50 8.65 2.66 o 9 5 8 7.57 10.18 3.90 o 0 6 8 10.38 18.14 5.46 o 2 6 8 79.02 73.50 9.52 o 4 6 8 63.81 50.14 7.55 o 6 6 8 5.43 8.11 3.61 o 8 6 8 11.37 12.91 4.27 o 1 7 8 71.65 75.21 9.65 o 3 7 8 70.35 68.26 10.45 o 5 7 8 50.15 56.37 5.93 o 7 7 8 27.80 24.99 5.42 o 9 7 8 3.75 7.00 4.65 o 0 8 8 94.97 118.29 14.55 o 2 8 8 17.34 21.27 4.71 o 4 8 8 8.66 7.55 2.77 o 6 8 8 2.30 5.83 2.93 o 8 8 8 9.04 6.92 8.58 o 1 9 8 172.21 177.68 10.41 o 3 9 8 36.42 26.77 8.70 o 5 9 8 20.24 16.73 4.88 o 0 10 8 45.11 40.38 10.65 o 2 10 8 23.69 19.84 6.92 o 4 10 8 88.20 85.47 10.73 o 1 1 9 1145.93 1168.68 14.57 o 3 1 9 384.81 414.38 18.96 o 5 1 9 220.62 233.10 8.78 o 7 1 9 170.48 191.48 10.67 o 9 1 9 186.18 173.13 12.53 o 0 2 9 467.57 449.48 12.81 o 2 2 9 114.54 113.45 5.83 o 4 2 9 29.70 28.51 3.89 o 6 2 9 146.54 144.37 5.83 o 8 2 9 69.65 64.76 7.99 o 10 2 9 65.05 73.96 8.16 o 1 3 9 132.94 119.95 9.58 o 3 3 9 73.65 57.16 8.99 o 5 3 9 114.86 109.02 7.65 o 7 3 9 8.61 6.77 3.53 o 9 3 9 3.59 6.98 2.76 o 0 4 9 14.29 36.55 7.86 o 2 4 9 35.78 26.42 4.62 o 4 4 9 86.45 98.47 10.68 o 6 4 9 33.58 35.65 6.03 o 8 4 9 11.99 2.60 3.33 o 1 5 9 293.59 300.56 15.19 o 3 5 9 35.38 29.53 5.25 o 5 5 9 18.04 16.93 4.43 o 7 5 9 43.73 61.82 9.11 o 9 5 9 51.01 43.76 9.23 o 0 6 9 130.00 142.35 38.74 o 2 6 9 131.34 141.41 11.30 o 4 6 9 245.47 272.15 13.29 o 6 6 9 173.17 185.47 20.79 o 8 6 9 10.28 11.90 4.23 o 1 7 9 6.07 9.87 4.42 o 3 7 9 32.22 27.02 5.08 o 5 7 9 114.28 116.22 7.69 o 7 7 9 16.83 9.29 3.59 o 0 8 9 70.94 64.57 24.22 o 2 8 9 38.00 21.04 6.10 o 4 8 9 64.51 83.22 12.14 o 6 8 9 37.25 26.52 6.51 o 1 9 9 0.80 5.64 3.88 o 3 9 9 113.56 102.86 14.61 o 0 0 10 520.08 493.65 18.17 o 2 0 10 75.23 51.08 26.71 o 4 0 10 76.21 55.80 10.26 o 6 0 10 92.67 97.51 11.13 o 8 0 10 96.13 128.54 16.80 o 1 1 10 223.78 214.49 9.72 o 3 1 10 212.64 216.63 8.09 o 5 1 10 40.83 30.32 7.03 o 7 1 10 21.74 23.75 5.07 o 9 1 10 50.21 41.90 10.01 o 0 2 10 316.08 331.62 21.29 o 2 2 10 100.43 114.99 7.53 o 4 2 10 15.14 11.72 4.16 o 6 2 10 28.56 27.62 7.27 o 8 2 10 47.00 46.38 7.11 o 1 3 10 208.62 217.40 16.67 o 3 3 10 285.19 373.28 26.20 o 5 3 10 108.99 105.58 6.42 o 7 3 10 30.18 26.90 9.44 o 0 4 10 37.43 35.27 10.09 o 2 4 10 0.97 2.55 2.80 o 4 4 10 157.88 159.37 13.02 o 6 4 10 46.27 24.33 7.45 o 8 4 10 25.71 20.99 8.83 o 1 5 10 213.29 225.62 17.63 o 3 5 10 62.88 69.41 8.85 o 5 5 10 64.15 75.78 9.92 o 7 5 10 5.09 8.87 3.86 o 0 6 10 166.38 122.93 25.85 o 2 6 10 62.35 79.69 11.41 o 4 6 10 85.12 83.54 9.09 o 6 6 10 65.74 76.45 14.76 o 1 7 10 11.81 12.28 4.20 o 3 7 10 15.68 16.81 5.77 o 5 7 10 75.79 81.06 11.87 o 0 8 10 38.51 20.42 25.97 o 2 8 10 18.78 19.30 5.99 o 1 1 11 53.46 60.05 8.50 o 3 1 11 78.94 69.72 13.17 o 5 1 11 15.04 12.98 6.43 o 7 1 11 47.99 39.48 8.52 o 0 2 11 37.48 35.09 8.96 o 2 2 11 3.53 2.80 3.01 o 4 2 11 3.05 7.12 3.29 o 6 2 11 10.14 5.30 3.43 o 1 3 11 60.76 38.60 12.38 o 3 3 11 71.24 52.28 10.34 o 5 3 11 77.93 63.11 25.90 o 7 3 11 1.76 11.14 18.56 o 0 4 11 31.31 27.99 9.61 o 2 4 11 44.73 37.96 7.97 o 4 4 11 83.85 88.01 19.70 o 6 4 11 5.92 7.41 3.48 o 1 5 11 135.17 122.43 8.19 o 3 5 11 21.39 20.76 7.65 o 5 5 11 30.55 37.45 8.50 o 0 6 11 111.71 77.60 39.67 o 2 6 11 28.63 34.92 7.06 o 4 0 12 44.66 26.26 9.84 o 1 1 12 32.19 23.57 14.05 o 3 1 12 54.51 51.98 19.12 o 5 1 12 28.76 4.72 11.42 o 0 2 12 50.12 70.96 33.86 o 2 2 12 8.33 22.29 18.88 o 4 2 12 1.85 6.58 4.40 o 1 3 12 26.86 21.57 6.61 o 3 3 12 25.98 13.21 5.88 o 0 4 12 187.91 230.84 14.10 o 2 4 12 49.50 21.80 9.24 o