#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:43:21 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181086 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/66/2216648.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2216648_Fobs loop_ _publ_author_name 'Fitchett, Christopher M.' 'Steel, Peter J.' _publ_section_title ; (5R)-5,9,9-Trimethyl-5,6,7,8-tetrahydro-5,8-methanoquinoxaline: a chiral Mills--Nixon pyrazine ; _journal_coeditor_code LW2042 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o4899 _journal_volume 63 _journal_year 2007 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 6.7201 _cell_length_b 12.0685 _cell_length_c 12.8803 _exptl_crystal_F_000 408.00 _reflns_d_resolution_high 0.8020 _cod_data_source_file lw2042Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 3cf2o in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 86.70 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 127.43 129.17 1.84 o 4 0 0 479.68 482.64 7.01 o 6 0 0 42.84 49.56 1.34 o 8 0 0 519.56 528.70 12.82 o 1 1 0 2866.97 2569.12 24.34 o 2 1 0 136.70 118.90 1.05 o 3 1 0 20.51 13.95 0.26 o 4 1 0 5.62 5.41 0.34 o 5 1 0 159.84 143.00 1.89 o 6 1 0 8.57 9.00 0.60 o 7 1 0 32.44 31.36 0.97 o 8 1 0 15.72 15.56 1.22 o 0 2 0 2593.33 2359.48 74.51 o 1 2 0 7516.34 6073.74 87.13 o 2 2 0 25.58 32.52 0.55 o 3 2 0 378.62 393.73 3.17 o 4 2 0 43.21 41.72 0.56 o 5 2 0 98.24 98.59 2.26 o 6 2 0 13.58 14.64 0.78 o 7 2 0 54.55 57.27 1.27 o 8 2 0 4.25 3.76 1.14 o 1 3 0 27.35 35.51 0.45 o 2 3 0 5.25 4.35 0.31 o 3 3 0 104.74 112.85 1.04 o 4 3 0 39.31 39.37 0.76 o 5 3 0 20.31 21.93 0.58 o 6 3 0 16.25 15.97 0.87 o 7 3 0 18.27 18.54 0.95 o 8 3 0 6.07 4.34 1.00 o 0 4 0 514.20 519.11 7.08 o 1 4 0 107.11 108.99 1.01 o 2 4 0 936.80 969.00 8.02 o 3 4 0 13.27 9.22 0.43 o 4 4 0 19.22 18.04 0.49 o 5 4 0 6.13 5.95 0.52 o 6 4 0 415.13 387.24 5.53 o 7 4 0 3.29 3.35 0.83 o 8 4 0 0.98 -1.09 1.74 o 1 5 0 17.57 26.35 0.38 o 2 5 0 226.81 271.39 2.63 o 3 5 0 156.36 163.05 1.67 o 4 5 0 27.53 30.43 0.70 o 5 5 0 199.92 184.18 2.08 o 6 5 0 1.50 -0.43 0.69 o 7 5 0 7.77 8.52 0.89 o 0 6 0 10.49 11.99 0.61 o 1 6 0 99.45 89.36 0.84 o 2 6 0 174.64 180.97 1.63 o 3 6 0 60.97 74.10 1.05 o 4 6 0 1.80 2.95 0.45 o 5 6 0 82.09 72.51 1.83 o 6 6 0 2.45 2.24 0.75 o 7 6 0 59.33 55.03 1.71 o 1 7 0 116.53 104.28 0.97 o 2 7 0 85.84 95.68 1.03 o 3 7 0 67.71 62.08 0.83 o 4 7 0 173.26 166.64 2.06 o 5 7 0 71.05 64.98 1.09 o 6 7 0 5.33 4.04 0.78 o 7 7 0 2.72 3.22 0.92 o 0 8 0 0.90 0.11 0.44 o 1 8 0 23.25 20.82 0.49 o 2 8 0 95.51 91.75 1.11 o 3 8 0 65.85 60.33 0.98 o 4 8 0 40.43 37.98 0.84 o 5 8 0 11.81 14.43 0.73 o 6 8 0 1.79 0.44 0.71 o 7 8 0 0.43 -2.09 2.19 o 1 9 0 13.40 12.05 0.51 o 2 9 0 232.79 214.10 2.41 o 3 9 0 83.57 83.98 1.28 o 4 9 0 34.55 44.96 0.91 o 5 9 0 12.27 12.23 0.99 o 6 9 0 12.88 15.94 1.01 o 0 10 0 55.64 54.27 1.32 o 1 10 0 32.41 29.99 0.68 o 2 10 0 55.18 54.00 1.09 o 3 10 0 139.61 136.29 1.82 o 4 10 0 10.86 14.36 1.05 o 5 10 0 2.16 6.41 0.83 o 6 10 0 0.24 0.97 2.21 o 1 11 0 195.69 184.70 2.39 o 2 11 0 13.57 13.21 0.77 o 3 11 0 0.37 -0.07 0.56 o 4 11 0 9.35 10.01 0.77 o 5 11 0 70.57 79.48 1.74 o 0 12 0 79.26 86.60 6.77 o 1 12 0 11.46 11.51 0.73 o 2 12 0 3.52 2.98 0.65 o 3 12 0 9.69 8.33 0.75 o 4 12 0 3.33 2.43 0.76 o 1 13 0 49.95 50.65 1.28 o 2 13 0 322.39 314.69 4.29 o 3 13 0 5.43 5.42 0.84 o 4 13 0 12.65 16.07 1.46 o 0 14 0 5.41 6.09 1.27 o 1 14 0 63.21 65.04 1.70 o 2 14 0 13.97 12.98 1.23 o 3 14 0 10.63 7.66 1.71 o 1 0 1 7302.45 6010.89 110.93 o 2 0 1 177.84 184.76 1.78 o 3 0 1 1.86 2.72 0.34 o 4 0 1 23.55 21.47 0.39 o 5 0 1 10.99 10.29 0.55 o 6 0 1 25.57 21.36 0.69 o 7 0 1 1.02 0.82 0.75 o 8 0 1 38.32 37.55 1.40 o 0 1 1 248.19 235.22 5.76 o 1 1 1 1275.27 1184.51 8.90 o 2 1 1 438.18 410.34 2.57 o 3 1 1 164.05 165.32 1.08 o 4 1 1 4.92 5.35 0.23 o 5 1 1 47.01 49.21 0.62 o 6 1 1 174.72 158.28 1.60 o 7 1 1 112.14 111.96 1.47 o 8 1 1 75.84 79.13 1.39 o 0 2 1 7158.87 5820.16 94.94 o 1 2 1 1111.40 1055.86 6.72 o 2 2 1 3625.74 3457.10 22.88 o 3 2 1 107.80 130.46 0.88 o 4 2 1 357.92 340.67 2.32 o 5 2 1 243.96 244.12 2.21 o 6 2 1 72.02 73.34 0.91 o 7 2 1 15.03 17.55 0.62 o 8 2 1 87.51 85.22 1.33 o 0 3 1 30.52 33.43 0.44 o 1 3 1 789.24 736.02 4.19 o 2 3 1 695.79 729.84 4.28 o 3 3 1 103.34 114.20 0.76 o 4 3 1 27.66 33.19 0.38 o 5 3 1 56.79 54.54 0.68 o 6 3 1 103.45 95.10 1.16 o 7 3 1 68.98 67.51 1.00 o 8 3 1 3.36 2.36 0.85 o 0 4 1 103.56 88.62 0.83 o 1 4 1 1763.56 1758.61 10.27 o 2 4 1 385.19 417.37 2.48 o 3 4 1 1066.04 1128.28 6.99 o 4 4 1 6.41 7.62 0.46 o 5 4 1 239.12 231.78 1.96 o 6 4 1 28.17 28.19 0.62 o 7 4 1 21.24 23.73 0.69 o 8 4 1 5.36 5.02 1.41 o 0 5 1 7.80 7.70 0.32 o 1 5 1 295.24 311.31 1.86 o 2 5 1 283.12 292.58 2.19 o 3 5 1 319.98 314.44 2.10 o 4 5 1 27.90 28.06 0.42 o 5 5 1 141.32 128.81 1.19 o 6 5 1 10.07 9.37 0.51 o 7 5 1 2.97 2.64 0.62 o 0 6 1 216.23 207.87 1.77 o 1 6 1 88.34 97.27 0.66 o 2 6 1 316.98 369.12 2.30 o 3 6 1 21.62 19.63 0.40 o 4 6 1 173.77 157.72 1.32 o 5 6 1 22.04 20.37 0.57 o 6 6 1 136.33 122.79 1.47 o 7 6 1 52.24 54.46 0.95 o 0 7 1 17.71 18.28 0.42 o 1 7 1 174.98 182.15 1.30 o 2 7 1 78.86 83.38 0.73 o 3 7 1 46.79 50.04 0.52 o 4 7 1 112.80 107.80 1.00 o 5 7 1 30.62 27.11 0.50 o 6 7 1 13.82 15.09 0.57 o 7 7 1 27.47 29.19 0.79 o 0 8 1 178.96 177.80 1.72 o 1 8 1 54.66 49.90 0.52 o 2 8 1 59.32 53.68 0.58 o 3 8 1 17.17 16.79 0.40 o 4 8 1 8.02 7.40 0.43 o 5 8 1 35.61 25.68 0.56 o 6 8 1 4.10 3.46 0.56 o 7 8 1 3.52 3.39 2.13 o 0 9 1 23.09 23.59 0.65 o 1 9 1 263.07 246.66 1.72 o 2 9 1 31.18 28.94 0.47 o 3 9 1 268.40 257.22 2.20 o 4 9 1 61.25 60.30 0.79 o 5 9 1 54.86 51.61 0.80 o 6 9 1 18.30 18.98 0.72 o 0 10 1 343.14 338.52 3.64 o 1 10 1 24.48 23.30 0.42 o 2 10 1 237.52 214.39 1.73 o 3 10 1 5.05 3.20 0.41 o 4 10 1 61.53 54.60 0.76 o 5 10 1 13.16 11.60 0.56 o 6 10 1 1.33 3.72 1.28 o 0 11 1 306.34 302.47 3.68 o 1 11 1 37.13 35.14 0.59 o 2 11 1 14.23 14.94 0.44 o 3 11 1 11.82 11.95 0.48 o 4 11 1 64.66 66.31 0.90 o 5 11 1 23.34 24.03 0.69 o 0 12 1 27.08 27.99 1.15 o 1 12 1 23.10 23.93 0.63 o 2 12 1 25.32 25.14 0.56 o 3 12 1 25.87 26.20 0.62 o 4 12 1 13.91 13.26 0.60 o 0 13 1 6.07 6.61 0.85 o 1 13 1 86.19 84.48 1.51 o 2 13 1 44.58 44.43 0.83 o 3 13 1 16.56 14.93 0.61 o 4 13 1 5.75 5.27 0.73 o 0 14 1 3.33 2.96 0.96 o 1 14 1 29.76 31.37 1.03 o 2 14 1 50.99 52.44 1.04 o 3 14 1 29.90 36.20 1.94 o 0 15 1 1.20 0.74 2.68 o 0 0 2 3239.97 2789.26 96.72 o 1 0 2 1441.10 1345.25 15.93 o 2 0 2 78.02 75.27 0.82 o 3 0 2 42.15 39.93 0.47 o 4 0 2 167.19 186.33 1.84 o 5 0 2 21.55 19.61 0.61 o 6 0 2 73.49 72.85 1.35 o 7 0 2 73.96 71.33 1.44 o 8 0 2 39.48 39.93 1.45 o 0 1 2 142.80 129.22 1.25 o 1 1 2 2856.16 2619.35 18.07 o 2 1 2 3.80 2.93 0.23 o 3 1 2 242.98 250.03 1.60 o 4 1 2 126.62 134.62 0.98 o 5 1 2 15.49 14.86 0.41 o 6 1 2 144.33 138.63 1.44 o 7 1 2 251.35 251.74 2.66 o 8 1 2 34.05 35.58 0.90 o 0 2 2 1213.12 1128.98 9.32 o 1 2 2 2150.71 2081.33 14.22 o 2 2 2 1394.85 1401.22 9.62 o 3 2 2 834.42 881.83 6.05 o 4 2 2 415.30 466.12 3.77 o 5 2 2 37.63 37.99 0.60 o 6 2 2 58.10 58.00 0.79 o 7 2 2 29.09 33.49 0.80 o 8 2 2 41.46 43.50 0.98 o 0 3 2 5.18 5.44 0.39 o 1 3 2 434.29 457.38 2.55 o 2 3 2 118.04 129.70 0.84 o 3 3 2 72.60 75.32 0.65 o 4 3 2 1.79 1.09 0.36 o 5 3 2 23.91 21.37 0.56 o 6 3 2 67.95 66.39 0.86 o 7 3 2 23.78 22.26 0.67 o 8 3 2 6.32 4.19 1.32 o 0 4 2 101.77 93.40 0.87 o 1 4 2 199.30 198.07 1.12 o 2 4 2 2508.02 2501.58 14.47 o 3 4 2 941.21 1005.30 6.42 o 4 4 2 87.51 94.03 0.90 o 5 4 2 138.06 133.67 1.27 o 6 4 2 174.15 174.95 1.92 o 7 4 2 6.73 6.42 0.81 o 8 4 2 1.39 -1.56 1.67 o 0 5 2 419.88 432.07 3.44 o 1 5 2 948.76 971.77 5.25 o 2 5 2 1199.29 1240.66 7.22 o 3 5 2 216.91 214.36 1.52 o 4 5 2 13.29 12.46 0.37 o 5 5 2 6.72 8.08 0.37 o 6 5 2 14.47 14.36 0.49 o 7 5 2 61.23 61.40 0.98 o 0 6 2 15.60 20.30 0.39 o 1 6 2 609.28 603.33 3.21 o 2 6 2 27.62 26.58 0.41 o 3 6 2 219.71 228.07 1.63 o 4 6 2 52.70 51.39 0.59 o 5 6 2 1.81 1.12 0.36 o 6 6 2 3.57 3.56 0.46 o 7 6 2 20.08 19.74 0.72 o 0 7 2 44.72 44.17 0.58 o 1 7 2 171.16 194.40 1.24 o 2 7 2 260.47 264.69 1.94 o 3 7 2 150.75 152.78 1.19 o 4 7 2 46.32 48.14 0.65 o 5 7 2 26.40 23.69 0.51 o 6 7 2 25.86 25.73 0.63 o 7 7 2 5.90 4.89 0.75 o 0 8 2 166.12 174.83 1.62 o 1 8 2 29.41 26.00 0.39 o 2 8 2 16.75 17.30 0.39 o 3 8 2 1.85 1.52 0.35 o 4 8 2 116.46 102.69 1.03 o 5 8 2 19.02 22.66 0.60 o 6 8 2 20.15 20.59 0.67 o 7 8 2 0.85 -0.45 2.03 o 0 9 2 35.89 33.73 0.63 o 1 9 2 200.50 187.29 1.41 o 2 9 2 46.44 43.05 0.59 o 3 9 2 50.23 48.66 0.65 o 4 9 2 148.45 143.45 1.50 o 5 9 2 46.14 47.14 1.02 o 6 9 2 18.71 23.04 0.73 o 0 10 2 232.33 236.34 3.93 o 1 10 2 40.09 34.33 0.61 o 2 10 2 23.52 22.39 0.46 o 3 10 2 28.49 23.86 0.52 o 4 10 2 27.35 27.28 0.63 o 5 10 2 18.32 21.60 0.74 o 6 10 2 0.92 2.15 2.33 o 0 11 2 90.43 81.43 1.33 o 1 11 2 185.84 179.58 1.53 o 2 11 2 72.79 67.84 0.77 o 3 11 2 17.60 15.89 0.48 o 4 11 2 40.90 42.03 0.85 o 5 11 2 32.83 32.09 0.93 o 0 12 2 1.01 0.91 0.77 o 1 12 2 132.88 132.84 1.92 o 2 12 2 85.87 83.80 0.98 o 3 12 2 29.76 28.05 0.70 o 4 12 2 7.05 7.77 0.53 o 0 13 2 154.91 151.28 2.46 o 1 13 2 33.21 33.48 0.79 o 2 13 2 19.81 17.50 0.72 o 3 13 2 6.17 5.03 0.64 o 4 13 2 0.49 0.53 0.90 o 0 14 2 61.51 61.95 1.56 o 1 14 2 46.05 48.74 1.06 o 2 14 2 16.63 19.36 0.82 o 1 0 3 2882.00 2649.67 26.47 o 2 0 3 2670.81 2540.29 25.13 o 3 0 3 1083.21 1160.12 9.60 o 4 0 3 135.58 128.94 1.39 o 5 0 3 426.90 426.27 5.37 o 6 0 3 511.74 499.07 7.02 o 7 0 3 107.91 109.17 3.72 o 8 0 3 2.62 1.86 1.06 o 0 1 3 1014.68 930.70 7.73 o 1 1 3 168.45 166.21 1.04 o 2 1 3 88.50 104.27 0.83 o 3 1 3 273.19 289.24 1.85 o 4 1 3 88.73 99.65 0.89 o 5 1 3 2.34 3.74 0.37 o 6 1 3 2.08 0.92 0.48 o 7 1 3 123.69 121.78 1.48 o 8 1 3 0.37 -0.74 0.74 o 0 2 3 2010.57 1840.61 18.50 o 1 2 3 719.77 700.13 3.99 o 2 2 3 768.59 804.14 5.36 o 3 2 3 607.32 633.94 4.61 o 4 2 3 119.09 130.57 1.14 o 5 2 3 273.53 268.68 2.50 o 6 2 3 4.56 4.36 0.44 o 7 2 3 11.54 12.49 0.64 o 8 2 3 14.39 11.28 0.94 o 0 3 3 963.60 905.70 7.09 o 1 3 3 443.55 420.53 2.85 o 2 3 3 156.47 174.54 1.14 o 3 3 3 98.92 88.65 0.75 o 4 3 3 54.89 55.19 0.68 o 5 3 3 217.04 217.90 2.08 o 6 3 3 182.95 177.12 1.79 o 7 3 3 49.40 46.09 0.86 o 8 3 3 22.47 23.06 1.06 o 0 4 3 0.04 0.47 0.24 o 1 4 3 41.69 43.06 0.35 o 2 4 3 517.23 565.51 3.25 o 3 4 3 796.77 837.98 5.38 o 4 4 3 27.55 32.44 0.56 o 5 4 3 14.54 16.28 0.51 o 6 4 3 13.17 13.38 0.55 o 7 4 3 18.17 15.49 0.63 o 0 5 3 534.42 550.67 4.38 o 1 5 3 381.29 448.86 2.53 o 2 5 3 76.83 73.19 0.55 o 3 5 3 487.91 479.50 3.99 o 4 5 3 244.70 255.78 2.14 o 5 5 3 182.33 182.72 1.68 o 6 5 3 60.42 58.62 0.79 o 7 5 3 11.59 11.09 0.60 o 0 6 3 698.71 753.32 5.95 o 1 6 3 3.34 3.94 0.27 o 2 6 3 38.74 44.02 0.44 o 3 6 3 169.85 185.66 1.41 o 4 6 3 100.21 94.09 0.94 o 5 6 3 55.70 46.93 0.63 o 6 6 3 2.48 2.23 0.44 o 7 6 3 0.78 -0.57 0.57 o 0 7 3 700.38 708.45 5.96 o 1 7 3 13.17 10.11 0.29 o 2 7 3 339.10 362.11 2.61 o 3 7 3 66.29 63.61 0.64 o 4 7 3 38.02 39.96 0.62 o 5 7 3 28.56 31.14 0.60 o 6 7 3 65.59 65.03 0.89 o 7 7 3 30.45 33.24 0.85 o 0 8 3 212.18 200.65 1.96 o 1 8 3 89.28 97.07 0.77 o 2 8 3 36.17 36.40 0.52 o 3 8 3 65.69 54.75 0.65 o 4 8 3 3.42 3.21 0.41 o 5 8 3 10.55 8.09 0.45 o 6 8 3 11.52 12.41 0.56 o 0 9 3 125.00 128.39 1.52 o 1 9 3 442.47 414.72 2.82 o 2 9 3 253.11 221.02 1.77 o 3 9 3 48.35 46.35 0.62 o 4 9 3 1.55 1.84 0.42 o 5 9 3 47.62 49.61 0.80 o 6 9 3 15.42 20.34 0.78 o 0 10 3 57.79 55.03 0.90 o 1 10 3 68.35 69.66 0.83 o 2 10 3 68.02 61.54 0.91 o 3 10 3 61.41 51.71 0.74 o 4 10 3 12.30 12.30 0.51 o 5 10 3 2.14 2.24 0.56 o 6 10 3 65.67 73.25 2.08 o 0 11 3 6.07 3.72 0.67 o 1 11 3 485.06 461.65 4.24 o 2 11 3 13.75 12.62 0.50 o 3 11 3 25.63 26.16 0.60 o 4 11 3 21.00 21.95 0.63 o 5 11 3 3.67 4.70 0.61 o 0 12 3 39.47 42.55 1.20 o 1 12 3 6.71 7.67 0.69 o 2 12 3 57.06 53.63 0.77 o 3 12 3 21.33 20.13 0.59 o 4 12 3 7.93 7.45 0.62 o 0 13 3 130.18 127.71 2.21 o 1 13 3 34.13 33.18 0.97 o 2 13 3 2.77 1.99 0.59 o 3 13 3 16.91 20.51 0.70 o 0 14 3 36.39 37.60 1.67 o 1 14 3 24.60 26.10 1.11 o 2 14 3 5.16 5.09 0.92 o 0 0 4 71.78 64.32 1.09 o 1 0 4 442.08 467.96 4.40 o 2 0 4 112.93 116.95 2.13 o 3 0 4 154.57 181.24 1.59 o 4 0 4 815.15 822.85 8.40 o 5 0 4 294.69 293.24 3.85 o 6 0 4 35.86 37.46 1.03 o 7 0 4 6.66 5.27 0.92 o 8 0 4 34.57 35.64 2.37 o 0 1 4 784.28 814.10 7.11 o 1 1 4 1765.47 1759.21 10.57 o 2 1 4 84.63 106.78 0.71 o 3 1 4 134.35 139.61 1.02 o 4 1 4 17.18 16.87 0.41 o 5 1 4 79.72 81.98 0.84 o 6 1 4 10.64 11.36 0.56 o 7 1 4 8.91 8.56 0.62 o 8 1 4 11.95 11.74 1.03 o 0 2 4 1448.26 1440.80 11.26 o 1 2 4 402.40 398.39 2.23 o 2 2 4 523.05 530.84 3.05 o 3 2 4 32.14 36.35 0.41 o 4 2 4 98.89 87.38 0.94 o 5 2 4 263.39 266.73 2.38 o 6 2 4 110.62 106.99 1.31 o 7 2 4 31.06 30.21 0.72 o 8 2 4 29.29 28.95 1.15 o 0 3 4 2.08 2.84 0.25 o 1 3 4 684.54 701.32 4.12 o 2 3 4 36.31 43.59 0.52 o 3 3 4 279.97 288.41 2.08 o 4 3 4 224.29 233.36 2.00 o 5 3 4 186.03 186.56 1.71 o 6 3 4 54.10 57.55 0.79 o 7 3 4 11.35 9.81 0.61 o 0 4 4 67.46 76.37 0.73 o 1 4 4 111.91 124.26 0.79 o 2 4 4 506.96 526.12 2.95 o 3 4 4 636.60 644.80 4.31 o 4 4 4 79.63 82.34 0.87 o 5 4 4 170.04 156.20 1.49 o 6 4 4 17.80 17.06 0.56 o 7 4 4 15.68 16.48 0.65 o 0 5 4 101.54 125.31 1.41 o 1 5 4 374.96 408.43 2.32 o 2 5 4 391.58 417.98 2.50 o 3 5 4 213.84 204.61 1.53 o 4 5 4 94.46 94.14 0.89 o 5 5 4 173.27 170.14 1.62 o 6 5 4 70.44 65.73 1.46 o 7 5 4 20.08 19.35 0.75 o 0 6 4 3.26 1.00 0.36 o 1 6 4 166.35 179.78 1.20 o 2 6 4 142.12 144.10 0.99 o 3 6 4 255.87 270.41 1.99 o 4 6 4 62.68 69.06 0.73 o 5 6 4 58.56 63.80 0.75 o 6 6 4 9.82 6.46 0.54 o 7 6 4 11.33 10.54 0.63 o 0 7 4 15.35 16.02 0.46 o 1 7 4 239.38 255.30 1.78 o 2 7 4 208.89 197.30 1.46 o 3 7 4 267.03 280.34 2.17 o 4 7 4 148.03 142.73 1.40 o 5 7 4 5.29 5.25 0.43 o 6 7 4 20.49 21.28 0.54 o 7 7 4 16.54 21.73 0.96 o 0 8 4 8.10 10.09 0.52 o 1 8 4 23.84 26.12 0.41 o 2 8 4 37.12 36.55 0.55 o 3 8 4 32.17 28.92 0.50 o 4 8 4 19.20 19.91 0.56 o 5 8 4 2.00 2.35 0.46 o 6 8 4 34.03 35.84 0.72 o 0 9 4 331.26 339.49 3.68 o 1 9 4 623.98 613.94 4.25 o 2 9 4 246.72 246.16 1.96 o 3 9 4 59.85 60.91 0.77 o 4 9 4 7.12 9.93 0.54 o 5 9 4 45.09 51.07 0.79 o 6 9 4 45.05 46.25 0.92 o 0 10 4 15.26 14.83 0.71 o 1 10 4 16.68 16.32 0.53 o 2 10 4 99.29 97.45 0.96 o 3 10 4 19.94 15.99 0.54 o 4 10 4 17.26 19.45 0.64 o 5 10 4 4.45 3.44 0.59 o 0 11 4 99.67 102.14 1.47 o 1 11 4 59.91 63.87 0.84 o 2 11 4 185.73 177.29 1.61 o 3 11 4 33.47 38.26 0.95 o 4 11 4 3.01 2.16 0.60 o 5 11 4 1.17 1.42 1.00 o 0 12 4 28.35 29.09 1.58 o 1 12 4 12.62 14.72 0.63 o 2 12 4 12.39 11.54 0.63 o 3 12 4 19.09 17.18 0.72 o 4 12 4 8.29 8.99 0.72 o 0 13 4 1.83 -0.19 0.99 o 1 13 4 5.70 5.33 0.62 o 2 13 4 2.26 2.08 0.66 o 3 13 4 21.63 22.42 0.78 o 0 14 4 1.75 1.02 1.18 o 1 14 4 96.24 96.79 1.47 o 2 14 4 20.57 22.59 1.49 o 1 0 5 15.22 18.68 0.34 o 2 0 5 0.22 1.80 0.34 o 3 0 5 4.65 8.96 0.41 o 4 0 5 14.90 21.90 0.61 o 5 0 5 299.44 301.68 4.01 o 6 0 5 158.57 156.46 2.51 o 7 0 5 26.59 25.38 1.05 o 0 1 5 1.67 2.73 0.28 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4.27 3.90 0.82 o 2 13 7 5.08 8.22 1.25 o 0 0 8 0.05 0.15 0.53 o 1 0 8 1.85 1.35 0.38 o 2 0 8 25.93 29.99 0.64 o 3 0 8 221.42 223.86 2.30 o 4 0 8 345.06 303.02 3.30 o 5 0 8 164.77 148.78 3.08 o 6 0 8 64.94 66.02 1.27 o 7 0 8 3.62 4.13 0.77 o 0 1 8 185.17 184.57 1.79 o 1 1 8 32.44 34.59 0.41 o 2 1 8 45.96 50.43 0.57 o 3 1 8 20.06 21.75 0.46 o 4 1 8 64.57 64.35 0.72 o 5 1 8 34.58 33.11 0.59 o 6 1 8 10.80 13.27 0.55 o 7 1 8 12.22 14.49 0.72 o 0 2 8 9.47 9.94 0.39 o 1 2 8 130.19 137.73 0.97 o 2 2 8 494.12 486.63 3.36 o 3 2 8 37.19 35.72 0.47 o 4 2 8 61.47 57.94 0.75 o 5 2 8 44.43 41.24 0.69 o 6 2 8 31.97 31.34 0.71 o 7 2 8 14.33 12.22 2.12 o 0 3 8 75.49 77.96 0.87 o 1 3 8 125.00 124.21 0.96 o 2 3 8 81.97 88.78 0.85 o 3 3 8 4.91 4.59 0.35 o 4 3 8 102.35 101.04 1.09 o 5 3 8 37.72 42.65 0.63 o 6 3 8 68.04 70.81 1.50 o 7 3 8 31.69 35.66 1.25 o 0 4 8 48.42 59.28 0.80 o 1 4 8 0.46 1.39 0.29 o 2 4 8 171.13 163.43 1.42 o 3 4 8 231.69 225.52 1.80 o 4 4 8 120.24 123.96 1.28 o 5 4 8 18.51 20.60 0.53 o 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11 9 0.10 1.58 1.32 o 0 12 9 151.80 155.20 4.13 o 1 12 9 35.21 39.27 1.19 o 0 0 10 563.01 553.85 8.20 o 1 0 10 280.87 286.89 3.18 o 2 0 10 0.36 0.15 0.52 o 3 0 10 3.75 3.01 0.51 o 4 0 10 0.02 0.26 0.58 o 5 0 10 0.35 0.85 0.73 o 6 0 10 2.86 3.70 1.57 o 0 1 10 319.12 302.65 3.29 o 1 1 10 33.27 35.04 0.48 o 2 1 10 22.54 22.46 0.45 o 3 1 10 10.57 8.59 0.40 o 4 1 10 17.32 16.41 0.50 o 5 1 10 8.29 7.32 0.55 o 6 1 10 37.60 36.48 0.83 o 0 2 10 58.56 65.57 0.92 o 1 2 10 652.30 641.34 4.28 o 2 2 10 140.16 128.18 1.14 o 3 2 10 121.52 101.84 1.00 o 4 2 10 129.44 121.47 1.31 o 5 2 10 137.77 134.15 1.45 o 6 2 10 57.82 55.98 0.97 o 0 3 10 75.99 83.86 1.02 o 1 3 10 137.85 130.96 1.11 o 2 3 10 15.44 8.28 0.39 o 3 3 10 49.80 54.03 0.71 o 4 3 10 16.79 16.51 0.53 o 5 3 10 14.55 15.61 0.65 o 6 3 10 56.89 61.21 1.02 o 0 4 10 14.65 14.22 0.56 o 1 4 10 22.11 16.54 0.43 o 2 4 10 216.07 187.78 1.57 o 3 4 10 87.52 80.66 0.92 o 4 4 10 4.89 7.16 0.50 o 5 4 10 71.07 70.49 1.01 o 6 4 10 77.56 78.25 1.58 o 0 5 10 134.79 132.14 1.56 o 1 5 10 25.45 23.89 0.49 o 2 5 10 62.69 60.30 0.74 o 3 5 10 28.21 27.80 0.66 o 4 5 10 1.10 1.47 0.52 o 5 5 10 43.90 48.01 0.86 o 0 6 10 120.08 107.05 1.36 o 1 6 10 1.42 0.94 0.46 o 2 6 10 19.11 18.77 0.51 o 3 6 10 6.59 8.03 0.57 o 4 6 10 39.71 40.22 0.81 o 5 6 10 36.25 41.17 0.94 o 0 7 10 12.00 12.86 1.06 o 1 7 10 42.01 41.49 0.67 o 2 7 10 60.35 61.47 1.04 o 3 7 10 1.55 2.14 0.49 o 4 7 10 25.72 27.68 1.04 o 5 7 10 25.40 32.90 1.34 o 0 8 10 53.66 53.79 1.04 o 1 8 10 67.71 60.93 0.88 o 2 8 10 1.48 2.33 0.53 o 3 8 10 15.58 14.63 0.62 o 4 8 10 59.52 65.80 1.23 o 0 9 10 212.48 225.04 4.47 o 1 9 10 34.58 35.17 0.77 o 2 9 10 5.92 6.93 0.62 o 3 9 10 21.63 24.48 0.76 o 4 9 10 54.75 70.56 4.52 o 0 10 10 134.26 124.34 2.09 o 1 10 10 10.10 9.00 0.69 o 2 10 10 8.86 9.12 0.69 o 3 10 10 18.79 22.21 0.98 o 0 11 10 0.41 1.84 1.66 o 1 11 10 164.82 168.81 1.87 o 2 11 10 7.86 9.43 0.86 o 1 0 11 948.36 889.25 10.20 o 2 0 11 175.02 169.12 2.03 o 3 0 11 94.74 79.36 1.26 o 4 0 11 1.64 1.65 0.59 o 5 0 11 0.52 -0.14 0.77 o 6 0 11 0.03 -1.41 1.41 o 0 1 11 43.88 41.87 0.75 o 1 1 11 46.00 42.68 0.60 o 2 1 11 2.22 3.23 0.38 o 3 1 11 37.97 39.28 0.57 o 4 1 11 3.31 2.69 0.43 o 5 1 11 8.49 7.36 0.59 o 6 1 11 54.94 58.07 1.83 o 0 2 11 654.24 612.27 6.02 o 1 2 11 74.00 72.92 0.86 o 2 2 11 3.78 4.43 0.38 o 3 2 11 113.61 111.95 1.10 o 4 2 11 51.28 40.51 0.70 o 5 2 11 53.46 50.50 0.81 o 6 2 11 10.49 12.35 1.24 o 0 3 11 146.84 141.95 2.01 o 1 3 11 8.68 7.47 0.49 o 2 3 11 109.71 101.58 1.02 o 3 3 11 97.28 91.67 1.01 o 4 3 11 26.19 24.53 0.64 o 5 3 11 63.17 63.27 1.32 o 0 4 11 2.73 2.90 0.56 o 1 4 11 21.79 21.04 0.49 o 2 4 11 63.77 64.29 0.77 o 3 4 11 72.00 66.88 0.84 o 4 4 11 15.95 18.75 0.62 o 5 4 11 69.97 69.59 1.04 o 0 5 11 3.65 3.67 0.58 o 1 5 11 64.10 66.04 0.85 o 2 5 11 81.49 77.99 0.90 o 3 5 11 42.28 41.41 0.92 o 4 5 11 2.95 2.49 0.64 o 5 5 11 20.89 25.48 0.83 o 0 6 11 41.42 34.89 0.83 o 1 6 11 61.90 56.70 0.80 o 2 6 11 81.67 73.77 1.06 o 3 6 11 12.92 11.76 0.53 o 4 6 11 45.98 48.02 0.97 o 5 6 11 2.53 1.36 1.01 o 0 7 11 28.12 25.17 1.13 o 1 7 11 7.42 6.69 0.51 o 2 7 11 46.94 49.04 0.83 o 3 7 11 9.04 9.15 0.61 o 4 7 11 56.92 61.57 1.07 o 0 8 11 52.29 46.47 1.09 o 1 8 11 19.77 20.29 0.62 o 2 8 11 27.44 29.84 0.73 o 3 8 11 3.32 4.10 0.63 o 4 8 11 8.53 7.83 3.87 o 0 9 11 44.69 41.53 1.18 o 1 9 11 17.67 17.59 0.71 o 2 9 11 15.86 14.16 0.69 o 3 9 11 28.08 26.06 1.03 o 0 10 11 30.57 31.67 1.89 o 1 10 11 19.10 21.19 0.86 o 2 10 11 57.31 61.57 1.08 o 0 0 12 1711.40 1656.36 23.88 o 1 0 12 31.13 29.08 0.84 o 2 0 12 36.51 38.03 1.19 o 3 0 12 24.42 25.36 0.75 o 4 0 12 5.20 4.82 0.68 o 5 0 12 11.13 13.93 1.02 o 0 1 12 210.65 197.34 2.37 o 1 1 12 61.03 63.81 0.79 o 2 1 12 22.34 21.90 0.53 o 3 1 12 7.56 7.97 0.44 o 4 1 12 3.88 3.55 0.49 o 5 1 12 65.72 67.32 1.08 o 0 2 12 113.81 112.58 1.53 o 1 2 12 228.78 222.37 1.93 o 2 2 12 11.32 12.93 0.47 o 3 2 12 40.21 34.10 0.64 o 4 2 12 27.18 28.02 0.65 o 5 2 12 18.19 18.30 0.75 o 0 3 12 7.49 6.90 0.62 o 1 3 12 14.05 12.75 0.48 o 2 3 12 58.15 61.47 0.80 o 3 3 12 109.44 111.56 1.19 o 4 3 12 26.92 28.72 0.71 o 5 3 12 1.23 0.79 0.86 o 0 4 12 11.78 12.49 0.64 o 1 4 12 46.93 47.85 0.77 o 2 4 12 249.11 235.25 2.04 o 3 4 12 19.57 22.33 0.60 o 4 4 12 10.21 9.60 0.63 o 5 4 12 3.85 3.19 0.92 o 0 5 12 2.44 3.65 0.62 o 1 5 12 8.16 7.66 0.51 o 2 5 12 3.79 3.55 0.49 o 3 5 12 40.60 44.10 0.78 o 4 5 12 5.23 3.78 0.66 o 0 6 12 31.97 32.48 0.95 o 1 6 12 17.37 15.48 0.59 o 2 6 12 68.85 69.48 1.00 o 3 6 12 25.04 24.72 0.68 o 4 6 12 4.24 4.58 0.81 o 0 7 12 9.13 11.64 0.84 o 1 7 12 6.23 7.67 0.58 o 2 7 12 36.82 37.08 0.77 o 3 7 12 81.27 80.98 1.14 o 0 8 12 2.55 2.70 0.84 o 1 8 12 33.11 36.30 0.80 o 2 8 12 50.40 50.67 0.92 o 3 8 12 7.91 8.36 1.35 o 0 9 12 0.16 -0.25 1.15 o 1 9 12 0.15 0.10 0.71 o 2 9 12 12.19 13.03 0.85 o 1 0 13 67.27 64.82 1.13 o 2 0 13 0.68 0.58 0.59 o 3 0 13 7.35 9.61 0.68 o 4 0 13 2.97 3.32 0.74 o 0 1 13 98.80 100.03 1.66 o 1 1 13 43.56 44.20 0.74 o 2 1 13 39.22 35.84 0.67 o 3 1 13 1.00 0.48 0.43 o 4 1 13 38.92 44.23 0.77 o 0 2 13 27.10 25.34 0.80 o 1 2 13 6.59 6.28 0.47 o 2 2 13 272.22 267.06 2.49 o 3 2 13 123.03 124.12 1.57 o 4 2 13 2.06 3.09 0.54 o 0 3 13 7.58 8.53 0.66 o 1 3 13 36.74 35.61 0.71 o 2 3 13 38.44 40.36 0.68 o 3 3 13 13.72 13.91 0.59 o 4 3 13 42.00 40.33 0.88 o 0 4 13 1.51 1.82 0.67 o 1 4 13 135.21 129.69 1.44 o 2 4 13 37.70 37.51 0.68 o 3 4 13 36.61 36.24 0.75 o 4 4 13 11.95 9.69 0.95 o 0 5 13 26.95 24.97 0.94 o 1 5 13 67.55 71.18 1.01 o 2 5 13 32.67 32.61 0.72 o 3 5 13 30.71 31.32 0.75 o 4 5 13 1.13 1.97 1.90 o 0 6 13 53.09 61.32 1.51 o 1 6 13 6.13 8.82 0.62 o 2 6 13 22.60 22.37 0.73 o 3 6 13 15.51 14.40 0.71 o 0 7 13 35.01 30.20 1.99 o 1 7 13 38.32 40.49 0.85 o 2 7 13 28.26 31.20 0.79 o 0 8 13 6.14 4.56 1.12 o 1 8 13 12.98 11.27 0.95 o 2 8 13 28.98 32.75 1.33 o 0 0 14 92.01 92.34 2.09 o 1 0 14 30.19 28.63 0.84 o 2 0 14 14.88 13.76 0.76 o 3 0 14 6.19 6.53 0.74 o 4 0 14 147.81 158.58 3.59 o 0 1 14 119.76 114.74 1.86 o 1 1 14 104.89 102.79 1.31 o 2 1 14 20.31 22.04 0.60 o 3 1 14 16.25 18.53 0.76 o 4 1 14 30.73 34.21 1.32 o 0 2 14 120.83 114.06 1.85 o 1 2 14 86.11 85.20 1.11 o 2 2 14 27.50 28.39 0.67 o 3 2 14 42.51 48.85 0.82 o 0 3 14 16.27 15.85 1.05 o 1 3 14 1.44 1.77 0.59 o 2 3 14 13.49 15.70 0.62 o 3 3 14 15.26 14.65 0.64 o 0 4 14 8.01 8.52 0.99 o 1 4 14 5.29 6.02 0.62 o 2 4 14 111.85 110.57 1.40 o 3 4 14 42.04 46.33 1.12 o 0 5 14 17.15 18.57 1.07 o 1 5 14 45.24 48.10 0.89 o 2 5 14 4.16 6.77 0.72 o 0 6 14 0.04 0.71 0.99 o 1 6 14 52.61 56.47 0.98 o 2 6 14 4.90 8.08 0.84 o 0 7 14 36.52 34.31 2.27 o 1 7 14 31.94 39.21 1.77 o 1 0 15 114.04 116.92 2.11 o 2 0 15 0.47 0.40 0.77 o 0 1 15 7.49 6.96 0.88 o 1 1 15 14.10 14.79 0.79 o 2 1 15 27.24 26.16 0.68 o 0 2 15 99.24 97.33 1.97 o 1 2 15 2.40 1.95 0.66 o 2 2 15 12.92 13.40 0.65 o 0 3 15 5.21 4.62 1.11 o 1 3 15 46.16 49.50 0.94 o 2 3 15 33.62 35.42 0.97 o 0 4 15 11.07 11.31 1.09 o 1 4 15 2.28 1.72 0.91 o 2 4 15 29.65 27.28 2.08 o 0 5 15 38.19 41.58 4.22 o 1 5 15 5.98 7.60 1.17 o 0 0 16 0.22 -2.95 3.14 o 0 1 16 48.11 53.31 5.54 o