#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2216673.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2216673_Fobs loop_ _publ_author_name 'Chen, Juan' 'Cao, Ke-Ning' 'Guo, Jianping' _publ_section_title ; Bis{N-[(dimethylamino)dimethylsilyl]-2,6-dimethylanilido-\k^2^N,N'}zinc(II) ; _journal_coeditor_code NG2346 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m3112 _journal_volume 63 _journal_year 2007 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 88.654 _cell_angle_beta 86.151 _cell_angle_gamma 89.858 _cell_length_a 9.6000 _cell_length_b 10.4470 _cell_length_c 27.3380 _exptl_crystal_F_000 1088.00 _reflns_d_resolution_high 0.8405 _[local]_cod_data_source_file ng2346Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' s080p in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 420.15 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 108.57 179.72 22.37 o 2 0 0 918.18 936.65 63.76 o 3 0 0 73.00 147.66 45.86 o 4 0 0 125.71 28.34 39.15 o 5 0 0 132.57 262.87 68.24 o 6 0 0 1169.41 1107.42 123.79 o 7 0 0 5.59 11.56 67.86 o 8 0 0 1938.03 2051.90 195.01 o 9 0 0 656.63 466.83 131.25 o 10 0 0 3.14 -9.32 92.10 o 11 0 0 80.25 16.41 100.67 o -11 1 0 47.59 9.69 94.34 o -10 1 0 0.52 79.42 102.17 o -9 1 0 517.68 527.24 130.88 o -8 1 0 369.81 305.38 107.39 o -7 1 0 1132.58 943.36 137.22 o -5 1 0 2067.25 2366.23 57.05 o -4 1 0 314.30 299.41 30.95 o -3 1 0 5273.35 5395.43 87.25 o -2 1 0 1908.28 2011.63 54.44 o -1 1 0 17740.42 18611.05 138.71 o 0 1 0 0.54 -2.63 6.19 o 1 1 0 93.09 97.55 12.63 o 2 1 0 6953.10 7299.36 87.25 o 3 1 0 24100.62 26687.97 355.35 o 4 1 0 180.80 190.53 24.98 o 5 1 0 778.23 1069.76 111.49 o 6 1 0 8105.57 8819.12 297.92 o 7 1 0 1842.77 1863.98 166.67 o 8 1 0 241.31 235.28 96.95 o 9 1 0 929.92 791.98 140.94 o 10 1 0 630.14 674.52 146.54 o 11 1 0 57.48 0.00 92.84 o -11 2 0 325.05 149.52 121.56 o -10 2 0 357.58 434.77 146.17 o -9 2 0 16.23 -43.63 75.32 o -8 2 0 6.98 -13.42 71.22 o -7 2 0 24.80 10.81 73.83 o -6 2 0 2366.35 1999.70 167.79 o -5 2 0 416.41 568.63 51.83 o -4 2 0 1511.15 1322.94 64.51 o -3 2 0 21.04 71.22 29.08 o -2 2 0 21991.13 23674.26 208.43 o -1 2 0 6031.28 5951.38 93.59 o 0 2 0 136.46 167.73 16.01 o 1 2 0 4018.66 3888.60 80.05 o 2 2 0 29216.28 31318.08 187.71 o 3 2 0 2029.22 2112.32 57.59 o 4 2 0 5181.83 5258.86 138.33 o 5 2 0 603.43 538.92 46.75 o 6 2 0 1825.81 1594.76 140.94 o 7 2 0 0.68 49.22 67.86 o 8 2 0 325.47 288.60 96.95 o 9 2 0 0.09 -43.63 64.88 o 10 2 0 18.67 27.97 86.51 o 11 2 0 221.16 220.74 124.17 o -11 3 0 62.75 67.12 103.66 o -10 3 0 237.47 187.93 124.54 o -9 3 0 126.30 199.49 111.49 o -8 3 0 184.82 98.44 98.06 o -7 3 0 3047.46 3314.44 237.15 o -6 3 0 2928.28 2740.97 200.98 o -5 3 0 833.87 810.99 67.12 o -4 3 0 102.60 133.86 35.05 o -3 3 0 4438.11 4094.48 110.74 o -2 3 0 1288.85 1502.29 67.49 o -1 3 0 1189.21 1403.86 59.66 o 0 3 0 1.73 34.64 49.96 o 1 3 0 247.90 456.04 43.87 o 2 3 0 317.98 349.60 26.90 o 3 3 0 210.78 150.71 27.63 o 4 3 0 275.55 298.52 33.42 o 5 3 0 4306.64 3853.07 109.81 o 6 3 0 100.75 151.39 51.08 o 7 3 0 1664.36 1758.83 114.47 o 8 3 0 1.40 16.41 52.57 o 9 3 0 108.52 107.01 65.25 o 10 3 0 11.43 4.85 87.25 o 11 3 0 169.95 253.92 134.61 o -10 4 0 223.14 284.50 141.69 o -9 4 0 312.07 272.94 121.56 o -8 4 0 2053.16 2024.68 215.15 o -7 4 0 1240.27 975.43 161.83 o -6 4 0 549.62 508.22 116.34 o -5 4 0 26.71 53.69 42.51 o -4 4 0 935.16 750.21 66.74 o -3 4 0 85.82 133.11 36.54 o -2 4 0 1149.04 1292.74 69.73 o -1 4 0 861.09 996.31 58.17 o 0 4 0 15358.11 14804.84 473.36 o 1 4 0 60.26 169.25 43.07 o 2 4 0 565.13 607.41 54.83 o 3 4 0 167.37 351.24 33.81 o 4 4 0 664.71 773.44 50.83 o 5 4 0 70.28 -5.77 27.33 o 6 4 0 1111.54 1122.71 92.47 o 7 4 0 1411.66 1318.84 104.78 o 8 4 0 721.22 770.35 143.55 o 9 4 0 487.23 422.46 129.76 o 10 4 0 192.05 268.84 132.00 o -10 5 0 11.55 54.07 113.73 o -9 5 0 235.96 291.58 135.72 o -8 5 0 10.70 20.51 86.13 o -7 5 0 1667.66 1557.85 181.59 o -6 5 0 358.75 418.73 119.32 o -5 5 0 2288.71 2309.93 117.45 o -4 5 0 2129.19 2236.85 110.00 o -3 5 0 809.34 576.08 62.27 o -2 5 0 96.94 60.03 38.78 o -1 5 0 19108.61 20414.63 230.43 o 0 5 0 25.01 5.06 20.62 o 1 5 0 1248.40 1344.84 81.32 o 2 5 0 67.34 59.52 35.26 o 3 5 0 380.00 371.17 55.63 o 4 5 0 246.87 233.30 51.12 o 5 5 0 412.00 412.73 61.56 o 6 5 0 1000.67 1123.46 140.20 o 7 5 0 1715.64 1693.20 180.47 o 8 5 0 116.44 90.98 88.37 o 9 5 0 393.14 317.69 123.79 o 10 5 0 382.42 428.80 151.76 o -9 6 0 4.36 18.64 98.06 o -8 6 0 1.94 -16.41 89.86 o -7 6 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1375.33 1507.51 214.40 o -7 8 0 18.29 7.46 88.00 o -6 8 0 0.82 -15.66 67.12 o -5 8 0 12.44 10.81 51.83 o -4 8 0 159.12 186.43 86.51 o -3 8 0 1192.72 970.95 139.45 o -2 8 0 31.10 59.66 71.96 o -1 8 0 86.98 159.59 86.13 o 0 8 0 9598.14 9628.62 357.58 o 1 8 0 218.46 645.90 82.92 o 2 8 0 174.65 251.25 68.02 o 3 8 0 598.17 660.47 87.51 o 4 8 0 609.67 476.61 87.07 o 5 8 0 84.75 82.85 56.54 o 6 8 0 125.80 94.34 83.52 o 7 8 0 95.20 107.39 90.98 o 8 8 0 257.11 323.65 125.28 o -5 9 0 899.14 1061.93 162.94 o -4 9 0 11.74 6.71 73.46 o -3 9 0 40.23 48.47 75.69 o -2 9 0 548.97 694.66 134.98 o -1 9 0 1142.33 1059.32 155.49 o 0 9 0 21.09 15.29 75.69 o 1 9 0 142.31 223.13 65.39 o 2 9 0 1227.97 1205.42 112.82 o 3 9 0 293.50 393.07 77.73 o 4 9 0 0.11 22.50 54.99 o 5 9 0 464.40 378.88 80.53 o 6 9 0 353.64 283.75 113.35 o 7 9 0 353.79 208.81 111.86 o -5 10 0 637.65 681.98 152.88 o -4 10 0 1.34 -21.25 83.15 o -3 10 0 160.55 227.45 111.86 o -2 10 0 709.61 792.35 148.78 o -1 10 0 0.43 3.73 81.66 o 0 10 0 61.86 88.74 88.74 o 1 10 0 2.53 18.05 51.87 o 2 10 0 773.44 649.68 95.89 o 3 10 0 134.35 266.80 79.47 o 4 10 0 1090.50 1032.67 140.01 o 5 10 0 753.95 715.96 107.03 o 6 10 0 311.97 286.74 114.84 o -5 11 0 31.72 99.93 102.17 o -4 11 0 18.35 45.86 90.98 o -3 11 0 1710.05 1810.28 215.15 o -2 11 0 254.22 144.67 108.13 o -1 11 0 108.46 93.59 99.56 o 0 11 0 2.11 18.64 88.74 o 1 11 0 965.77 951.19 175.62 o 2 11 0 30.34 38.13 62.32 o 3 11 0 421.79 499.65 98.72 o 4 11 0 248.86 259.08 89.62 o 5 11 0 109.03 82.62 68.23 o -2 12 0 67.24 55.56 97.32 o -1 12 0 0.04 70.47 95.83 o 0 12 0 3401.29 3099.29 280.40 o 1 12 0 24.38 35.42 109.25 o 2 12 0 157.07 186.24 86.71 o -2 -12 1 2.10 9.99 66.44 o -1 -12 1 1174.23 1127.19 197.62 o 0 -12 1 5.29 121.56 123.79 o 1 -12 1 221.43 355.35 136.10 o 2 -12 1 2.81 14.54 95.08 o -5 -11 1 950.92 801.49 224.47 o -4 -11 1 538.77 484.57 100.89 o -3 -11 1 83.52 103.19 67.01 o -2 -11 1 877.32 896.77 189.79 o -1 -11 1 33.48 -30.20 82.40 o 0 -11 1 8.58 89.49 101.42 o 1 -11 1 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