#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:44:07 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181088 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/68/2216820.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2216820_Fobs loop_ _publ_author_name 'Strasser, Christoph E.' 'Cronje, Stephanie' 'Raubenheimer, Helgard G.' _publ_section_title ; The low-temperature phase of diethylammonium tetrachloridocuprate(II) ; _journal_coeditor_code WM2156 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2915 _journal_page_last m2916 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 90.258 _cell_angle_gamma 90.000 _cell_length_a 7.3150 _cell_length_b 14.8426 _cell_length_c 45.2425 _exptl_crystal_F_000 2196.00 _reflns_d_resolution_high 0.7944 _cod_data_source_file wm2156Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' xm in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 636.03 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 404539.59 426088.00 15776.79 o 4 0 0 904.60 728.42 55.43 o 6 0 0 22775.40 22901.96 1263.54 o 8 0 0 5721.24 5801.36 538.36 o 1 1 0 52.37 -11.40 11.40 o 2 1 0 124837.60 143136.42 6327.45 o 3 1 0 90.25 82.71 16.60 o 4 1 0 89142.39 97274.18 2764.61 o 5 1 0 2.60 4.94 17.30 o 6 1 0 4300.62 4823.86 245.50 o 7 1 0 18.93 20.16 52.19 o 8 1 0 1141.31 1088.35 134.47 o 9 1 0 3.21 123.85 76.15 o 0 2 0 94355.39 90256.65 6974.39 o 1 2 0 832.64 792.57 43.38 o 2 2 0 128924.04 136713.22 4671.58 o 3 2 0 3343.53 3457.01 179.91 o 5 2 0 387.37 453.86 31.94 o 6 2 0 5172.08 4902.15 214.19 o 7 2 0 21.07 129.63 60.10 o 8 2 0 3.86 73.53 110.62 o 9 2 0 0.62 24.26 72.69 o 1 3 0 2577.24 2541.47 106.71 o 2 3 0 6479.74 6955.73 322.33 o 3 3 0 58.40 54.41 18.14 o 4 3 0 3551.07 4035.83 208.15 o 5 3 0 114.65 107.35 22.69 o 6 3 0 15445.42 15195.26 608.83 o 7 3 0 38.16 70.56 43.96 o 8 3 0 7821.74 8649.08 536.81 o 9 3 0 4.41 21.77 92.18 o 0 4 0 26300.21 27793.87 2163.85 o 1 4 0 6093.41 6690.35 267.59 o 2 4 0 133.50 313.57 22.35 o 3 4 0 6041.11 5768.31 402.36 o 4 4 0 23506.77 23860.01 803.79 o 5 4 0 1434.99 1491.68 83.58 o 6 4 0 13922.08 13818.35 557.13 o 7 4 0 62.70 15.06 40.98 o 8 4 0 311.32 405.38 88.77 o 1 5 0 270.47 287.85 25.47 o 2 5 0 839.15 701.35 40.57 o 3 5 0 104.56 57.51 23.88 o 4 5 0 989.51 996.67 68.00 o 5 5 0 61.32 61.94 23.06 o 6 5 0 4616.95 4670.78 181.77 o 7 5 0 229.22 305.93 59.32 o 8 5 0 1534.19 1424.52 122.52 o 0 6 0 24476.15 19386.60 1517.91 o 1 6 0 1077.81 1130.59 101.95 o 2 6 0 50668.24 52889.16 2048.78 o 3 6 0 3825.53 4416.87 219.03 o 4 6 0 19457.40 18020.53 1141.48 o 5 6 0 1869.03 1873.65 100.50 o 6 6 0 764.56 788.35 57.31 o 7 6 0 316.82 379.83 53.82 o 8 6 0 577.63 589.09 80.77 o 1 7 0 120.00 38.03 23.77 o 2 7 0 81458.79 87373.44 3377.97 o 3 7 0 1524.46 1563.85 149.81 o 4 7 0 24197.00 22904.17 903.35 o 5 7 0 453.69 447.23 47.95 o 6 7 0 3658.84 3513.19 144.98 o 7 7 0 109.53 103.36 41.26 o 8 7 0 919.77 1006.89 122.30 o 0 8 0 40167.56 47833.79 3725.57 o 1 8 0 23.13 0.70 19.59 o 2 8 0 27081.16 27180.13 1224.80 o 3 8 0 2.16 -13.32 30.65 o 4 8 0 5150.88 4965.06 209.84 o 5 8 0 74.85 156.64 35.21 o 6 8 0 1667.45 1575.48 87.69 o 7 8 0 74.54 210.13 58.97 o 8 8 0 107.29 53.01 61.06 o 1 9 0 15.86 14.84 27.98 o 2 9 0 6964.01 6136.36 289.44 o 3 9 0 1819.14 1934.02 144.18 o 4 9 0 14946.38 15390.58 598.40 o 5 9 0 144.82 105.45 34.25 o 6 9 0 28.58 42.37 30.50 o 7 9 0 112.80 101.13 37.59 o 8 9 0 460.69 621.27 88.25 o 0 10 0 281.89 431.21 75.05 o 1 10 0 0.82 -19.67 20.69 o 2 10 0 1986.50 1754.12 100.57 o 3 10 0 737.44 609.07 104.11 o 4 10 0 16258.80 15086.49 587.95 o 5 10 0 334.60 281.80 116.03 o 6 10 0 11064.00 9683.51 460.59 o 7 10 0 1.31 22.01 35.50 o 1 11 0 1.26 -23.86 23.86 o 2 11 0 3834.35 3974.42 251.53 o 3 11 0 247.67 303.67 84.59 o 4 11 0 230.31 140.05 44.60 o 5 11 0 476.02 445.30 54.03 o 6 11 0 969.21 948.59 82.79 o 7 11 0 77.30 105.95 44.80 o 0 12 0 6158.11 5728.05 486.74 o 1 12 0 231.95 319.19 50.87 o 2 12 0 1959.84 1925.69 209.53 o 3 12 0 245.56 259.16 45.91 o 4 12 0 5707.21 5299.55 263.78 o 5 12 0 47.00 1.61 49.46 o 6 12 0 1403.00 1428.92 100.28 o 7 12 0 84.38 134.36 48.89 o 2 13 0 1938.68 1881.01 215.17 o 3 13 0 93.70 137.38 49.83 o 4 13 0 2793.32 2738.36 228.46 o 5 13 0 60.00 112.68 41.91 o 6 13 0 3467.78 2986.64 185.18 o 1 14 0 250.96 193.91 91.97 o 2 14 0 38032.75 36863.05 1600.02 o 3 14 0 98.82 95.95 46.64 o 4 14 0 63.64 81.04 61.02 o 5 14 0 164.81 186.64 56.79 o 6 14 0 5997.04 5812.85 298.87 o 1 15 0 337.61 430.24 65.94 o 2 15 0 13650.09 13799.23 635.31 o 3 15 0 1.00 23.51 55.64 o 4 15 0 13178.63 12889.02 719.45 o 5 15 0 10.25 -24.57 47.57 o 0 16 0 51059.87 53775.98 2771.12 o 1 16 0 34.00 17.95 45.30 o 2 16 0 20353.29 19757.76 1064.16 o 3 16 0 8.36 -10.16 53.61 o 4 16 0 481.96 311.86 69.75 o 1 17 0 248.79 352.96 78.12 o 2 17 0 4187.90 4530.43 344.23 o 3 17 0 42.84 77.82 74.11 o 1 18 0 29.08 41.97 65.96 o 2 18 0 1968.66 2314.26 202.62 o -9 0 1 680.38 1038.11 200.85 o -7 0 1 1869.46 2030.67 247.27 o -5 0 1 428.38 518.35 47.53 o -3 0 1 99.75 157.90 16.38 o -1 0 1 10629.18 11989.06 661.05 o 1 0 1 5485.01 5793.75 276.23 o 3 0 1 344.11 384.63 46.38 o 5 0 1 19058.94 19781.95 892.55 o 7 0 1 19609.83 20002.18 1615.51 o 9 0 1 5470.25 5488.15 526.65 o -9 1 1 1690.58 2053.94 201.79 o -8 1 1 465.57 593.91 101.53 o -7 1 1 153.03 251.65 69.13 o -6 1 1 0.57 37.82 33.70 o -5 1 1 3861.85 3657.70 142.24 o -4 1 1 1635.94 1724.75 59.57 o -3 1 1 26232.44 27968.57 864.05 o -2 1 1 2378.26 2691.85 98.63 o -1 1 1 28017.73 31468.29 1393.53 o 0 1 1 1.12 3.90 3.04 o 1 1 1 26356.33 30986.76 949.39 o 2 1 1 275.55 306.65 16.43 o 3 1 1 32076.23 35255.36 1002.28 o 4 1 1 8.57 -8.72 14.71 o 5 1 1 10433.58 10559.96 376.28 o 6 1 1 3.69 1.63 29.71 o 7 1 1 1.25 -57.05 57.05 o 8 1 1 9.98 95.89 68.40 o 9 1 1 3748.73 4008.34 309.09 o -9 2 1 34.12 112.12 83.73 o -8 2 1 79.74 37.30 67.13 o -7 2 1 343.13 272.52 98.48 o -6 2 1 108.59 144.54 39.87 o -5 2 1 2821.28 2776.67 100.54 o -4 2 1 146.26 149.67 16.09 o -3 2 1 779.62 796.42 41.51 o -2 2 1 1518.19 1665.96 89.04 o -1 2 1 544.80 592.46 28.48 o 0 2 1 606.22 540.97 35.12 o 1 2 1 41.05 71.33 12.39 o 2 2 1 1134.42 1256.42 50.11 o 3 2 1 453.15 484.19 24.86 o 4 2 1 1072.78 1134.55 43.92 o 5 2 1 13271.66 14401.07 509.51 o 6 2 1 129.26 67.51 53.85 o 7 2 1 12883.39 13043.78 764.11 o 8 2 1 56.70 175.88 95.87 o 9 2 1 4248.66 4666.12 330.50 o -9 3 1 1602.61 1682.26 177.91 o -8 3 1 86.95 81.99 79.39 o -7 3 1 4692.39 4539.13 240.95 o -6 3 1 19.81 81.08 33.06 o -5 3 1 48.59 54.18 20.61 o -4 3 1 1326.29 1307.82 58.96 o -3 3 1 10195.71 10770.19 445.32 o -2 3 1 4133.53 4432.93 210.13 o -1 3 1 2757.36 2533.67 123.29 o 0 3 1 1.66 11.74 9.19 o 1 3 1 3052.75 2938.19 139.66 o 2 3 1 751.32 773.57 39.55 o 3 3 1 10662.39 11197.74 385.27 o 4 3 1 340.82 419.39 25.03 o 5 3 1 1439.59 1587.84 75.34 o 6 3 1 314.09 284.38 42.49 o 7 3 1 541.71 560.99 76.60 o 8 3 1 261.18 282.01 78.75 o 9 3 1 1776.44 1825.40 188.48 o -8 4 1 233.03 321.76 87.98 o -7 4 1 459.00 545.97 71.05 o -6 4 1 40.65 32.73 27.08 o -5 4 1 10468.90 10281.20 400.14 o -4 4 1 2475.71 2446.20 96.87 o -3 4 1 13350.93 12758.33 583.06 o -2 4 1 177.60 149.24 15.90 o -1 4 1 3520.82 3894.78 169.25 o 0 4 1 350.19 422.40 35.74 o 1 4 1 1.10 26.06 9.13 o 2 4 1 474.78 519.71 58.23 o 3 4 1 2664.74 2961.59 124.88 o 4 4 1 2005.96 2082.16 84.15 o 5 4 1 10826.60 11490.76 402.28 o 6 4 1 141.55 169.66 37.92 o 7 4 1 7841.19 7833.84 387.13 o 8 4 1 404.61 477.21 95.56 o -8 5 1 8.74 52.93 67.28 o -7 5 1 2189.52 2036.49 141.05 o -6 5 1 4.71 30.92 26.91 o -5 5 1 380.72 401.32 42.28 o -4 5 1 799.73 859.36 86.01 o -3 5 1 72.30 76.85 24.94 o -2 5 1 211.77 192.89 18.98 o -1 5 1 2829.02 3101.00 148.12 o 0 5 1 12.47 25.32 13.49 o 1 5 1 473.68 453.18 32.93 o 2 5 1 372.52 377.93 27.03 o 3 5 1 798.90 1076.97 89.47 o 4 5 1 64.68 35.48 33.56 o 5 5 1 184.08 225.81 30.78 o 6 5 1 285.77 356.35 41.29 o 7 5 1 366.23 399.04 64.45 o 8 5 1 94.11 73.35 53.46 o -8 6 1 5.20 -46.76 46.76 o -7 6 1 2406.23 2373.34 166.24 o -6 6 1 594.89 558.42 49.03 o -5 6 1 1870.95 1887.19 100.19 o -4 6 1 1520.27 1565.73 244.89 o -3 6 1 18675.67 20148.75 917.85 o -2 6 1 1229.79 1187.59 77.71 o -1 6 1 1448.90 1551.31 100.92 o 0 6 1 102.35 88.10 22.23 o 1 6 1 3421.18 3774.86 220.30 o 2 6 1 762.08 757.09 43.91 o 3 6 1 6278.87 6603.25 303.69 o 4 6 1 195.89 230.18 32.26 o 5 6 1 4469.16 4561.88 175.80 o 6 6 1 0.08 7.12 25.07 o 7 6 1 9745.74 9374.17 396.20 o 8 6 1 62.69 123.81 55.72 o -8 7 1 104.72 157.61 94.65 o -7 7 1 167.43 99.64 56.95 o -6 7 1 402.14 494.05 55.12 o -5 7 1 639.24 627.83 55.17 o -4 7 1 611.15 652.68 106.72 o -3 7 1 5065.16 5026.67 179.32 o -2 7 1 4936.06 5011.96 347.95 o -1 7 1 1528.85 1457.79 131.01 o 0 7 1 0.78 11.09 36.66 o 1 7 1 261.27 212.91 32.67 o 2 7 1 5306.97 5511.73 364.46 o 3 7 1 154.64 271.82 48.44 o 4 7 1 557.40 575.53 59.05 o 5 7 1 165.34 167.40 30.36 o 6 7 1 32.21 65.18 30.17 o 7 7 1 1.51 1.70 34.93 o 8 7 1 42.35 93.35 53.95 o -8 8 1 63.07 60.33 66.06 o -7 8 1 587.41 612.80 57.03 o -6 8 1 0.56 9.98 27.89 o -5 8 1 7826.03 7229.95 297.21 o -4 8 1 59.78 49.94 40.89 o -3 8 1 167.62 110.76 41.48 o -2 8 1 275.11 287.89 44.52 o -1 8 1 72.86 94.33 25.41 o 0 8 1 295.08 217.69 36.13 o 1 8 1 39.51 42.08 31.02 o 2 8 1 137.35 159.83 32.77 o 3 8 1 633.73 635.34 113.01 o 4 8 1 54.02 82.62 28.57 o 5 8 1 9882.26 10066.25 403.45 o 6 8 1 279.06 333.69 42.61 o 7 8 1 6566.29 6199.71 277.52 o 8 8 1 65.02 20.92 50.31 o -8 9 1 194.52 170.18 62.62 o -7 9 1 694.97 558.86 56.82 o -6 9 1 182.65 144.14 36.65 o -5 9 1 128.12 144.61 37.19 o -4 9 1 1059.50 1152.84 113.53 o -3 9 1 1440.49 1536.74 102.32 o -2 9 1 255.44 218.74 64.42 o -1 9 1 1092.79 1117.40 87.09 o 0 9 1 119.82 126.78 30.49 o 1 9 1 1791.35 1642.95 115.73 o 2 9 1 1.47 3.65 17.76 o 3 9 1 32.80 97.61 55.09 o 4 9 1 650.20 695.40 58.02 o 5 9 1 1086.28 1164.50 80.43 o 6 9 1 145.73 102.34 33.64 o 7 9 1 72.33 21.53 39.44 o 8 9 1 35.41 105.76 73.96 o -7 10 1 780.12 591.64 59.59 o -6 10 1 125.21 121.65 36.92 o -5 10 1 1356.03 1252.69 86.52 o -4 10 1 594.34 614.59 57.06 o -3 10 1 1158.31 1292.15 114.52 o -2 10 1 416.81 409.76 67.46 o -1 10 1 1443.33 1363.71 102.95 o 0 10 1 16.29 10.75 50.11 o 1 10 1 3345.70 3692.79 228.00 o 2 10 1 25.84 23.82 24.31 o 3 10 1 4273.64 4297.48 284.80 o 4 10 1 1544.52 1605.91 94.73 o 5 10 1 3335.76 3219.15 153.40 o 6 10 1 1608.31 1476.76 98.92 o 7 10 1 3143.79 2866.51 156.78 o -7 11 1 261.43 214.11 45.93 o -6 11 1 880.74 858.35 66.34 o -5 11 1 777.06 794.65 71.15 o -4 11 1 131.23 75.99 38.94 o -3 11 1 823.16 838.56 128.84 o -2 11 1 390.60 396.44 62.54 o -1 11 1 1430.96 1290.16 158.34 o 0 11 1 101.08 46.92 30.82 o 1 11 1 25.24 -9.34 25.57 o 2 11 1 885.21 907.29 132.75 o 3 11 1 797.55 869.18 84.32 o 4 11 1 0.84 -30.27 35.91 o 5 11 1 317.77 348.96 67.34 o 6 11 1 863.43 825.12 66.77 o 7 11 1 35.21 73.42 50.84 o -7 12 1 26.15 60.97 47.37 o -6 12 1 139.03 111.28 44.75 o -5 12 1 1291.60 1238.80 102.97 o -4 12 1 784.70 757.91 102.57 o -3 12 1 538.27 444.22 98.91 o -2 12 1 872.24 838.61 92.95 o -1 12 1 209.72 164.41 60.30 o 0 12 1 549.03 624.25 102.81 o 1 12 1 657.62 606.47 95.44 o 2 12 1 77.80 38.18 54.23 o 3 12 1 1915.11 2137.65 129.63 o 4 12 1 43.72 -32.96 34.46 o 5 12 1 4757.74 4268.34 194.73 o 6 12 1 166.37 190.59 45.35 o 7 12 1 1245.44 1270.40 121.21 o -6 13 1 1229.98 1359.42 116.50 o -5 13 1 3.30 -35.45 38.94 o -4 13 1 516.00 548.87 70.93 o -3 13 1 6316.84 5835.20 513.20 o -2 13 1 18.14 17.79 65.07 o -1 13 1 6859.70 7026.63 420.85 o 0 13 1 4.68 81.99 49.45 o 1 13 1 2497.50 2730.84 257.25 o 2 13 1 13.80 32.71 32.69 o 3 13 1 6946.99 6646.64 320.39 o 4 13 1 246.62 268.01 54.47 o 5 13 1 1220.78 1279.30 107.80 o 6 13 1 313.58 252.82 86.73 o -6 14 1 100.48 104.07 52.85 o -5 14 1 1070.29 1236.60 187.19 o -4 14 1 18.80 33.56 46.79 o -3 14 1 1010.22 1093.38 109.76 o -2 14 1 3073.78 3448.37 338.81 o -1 14 1 990.30 1129.70 86.41 o 0 14 1 7368.48 7888.94 442.37 o 1 14 1 13.97 -33.49 33.49 o 2 14 1 1186.70 1581.63 114.53 o 3 14 1 5677.67 5603.38 278.71 o 4 14 1 365.30 338.40 76.62 o 5 14 1 4668.83 4020.08 217.93 o 6 14 1 622.11 620.78 79.88 o -5 15 1 2213.65 1918.70 145.99 o -4 15 1 1527.78 1599.22 156.76 o -3 15 1 11998.03 11290.59 523.95 o -2 15 1 749.91 999.01 92.75 o -1 15 1 1850.14 2572.94 291.09 o 0 15 1 19.14 22.06 80.04 o 1 15 1 513.87 425.79 89.32 o 2 15 1 671.88 651.72 74.45 o 3 15 1 11365.13 11030.87 617.41 o 4 15 1 694.73 816.63 91.06 o 5 15 1 3040.22 2520.44 240.70 o -4 16 1 2.29 8.88 65.10 o -3 16 1 293.63 333.91 85.07 o -2 16 1 2498.40 2919.43 180.42 o -1 16 1 284.19 250.91 57.09 o 0 16 1 6301.27 7029.13 286.69 o 1 16 1 66.98 100.58 48.29 o 2 16 1 2508.20 2510.63 246.84 o 3 16 1 3.31 30.36 60.51 o 4 16 1 64.90 60.65 50.84 o -3 17 1 479.22 495.50 98.54 o -2 17 1 249.08 223.71 115.83 o -1 17 1 510.77 592.91 101.77 o 0 17 1 0.10 34.62 37.20 o 1 17 1 0.14 -60.95 60.95 o 2 17 1 0.80 -38.13 60.43 o 3 17 1 292.77 294.58 66.03 o -2 18 1 627.10 780.37 117.38 o -1 18 1 471.38 377.48 85.31 o 1 18 1 833.11 680.69 120.38 o 2 18 1 811.26 805.47 97.06 o -8 0 2 1712.21 2021.13 265.93 o -6 0 2 1213.62 1389.70 150.97 o -4 0 2 24517.31 26249.69 982.93 o -2 0 2 28539.05 34413.25 1884.52 o 0 0 2 4.26 1.74 1.74 o 2 0 2 19063.62 22257.98 992.68 o 4 0 2 8825.63 9011.31 414.93 o 6 0 2 583.29 655.07 104.77 o 8 0 2 2111.35 2374.68 293.69 o -9 1 2 28.33 -45.54 65.30 o -8 1 2 8031.13 7979.67 499.08 o -7 1 2 218.49 263.39 87.20 o -6 1 2 17722.13 18074.41 825.48 o -5 1 2 0.63 -15.17 16.62 o -4 1 2 9381.85 9421.29 297.54 o -3 1 2 563.81 614.42 38.45 o -2 1 2 271.62 317.60 17.19 o -1 1 2 18.61 -9.25 9.25 o 0 1 2 13.65 11.54 2.98 o 1 1 2 8.33 -4.74 4.74 o 2 1 2 3672.95 4009.62 119.32 o 3 1 2 415.20 470.17 25.01 o 4 1 2 3918.72 3956.10 135.12 o 5 1 2 109.94 96.29 30.62 o 6 1 2 1883.48 1799.89 120.56 o 7 1 2 268.53 389.69 81.43 o 8 1 2 196.52 291.29 82.17 o 9 1 2 16.20 28.61 73.10 o -9 2 2 9.90 -33.12 115.83 o -8 2 2 1990.68 1816.89 176.14 o -7 2 2 622.12 657.87 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