#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/74/2217441.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2217441_Fobs loop_ _publ_author_name 'Gzella, Andrzej' 'Melzer, Ewa' 'Kaczmarek, Micha\/l S.' 'Wo\'zniak, Zenon' _publ_section_title ; 1-Methyl-2-(4-methylphenyl)-4-morpholinopyridazine-3,6(1H,2H)-dione ; _journal_coeditor_code CF2177 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o435 _journal_volume 64 _journal_year 2008 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _cell_angle_alpha 90.000 _cell_angle_beta 99.530 _cell_angle_gamma 90.000 _cell_length_a 5.6246 _cell_length_b 8.8923 _cell_length_c 15.0842 _exptl_crystal_F_000 320.00 _reflns_d_resolution_high 0.8199 _[local]_cod_data_source_file cf2177Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' melz1007 in P2(1); Gzella et al.' _shelx_refln_list_code 4 _shelx_f_calc_maximum 107.68 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 -10 0 24.76 27.52 0.67 o 1 -10 0 10.72 11.41 0.21 o 2 -10 0 7.79 8.08 0.21 o 1 -9 0 21.90 24.08 0.43 o 2 -9 0 34.32 34.35 0.62 o 3 -9 0 9.51 9.65 0.17 o 0 -8 0 302.77 295.23 4.01 o 1 -8 0 51.56 51.22 2.50 o 2 -8 0 5.21 5.09 0.14 o 3 -8 0 14.88 14.29 0.26 o 4 -8 0 0.17 0.05 0.23 o 1 -7 0 355.07 357.69 4.79 o 2 -7 0 201.60 199.88 2.33 o 3 -7 0 2.51 2.59 0.12 o 4 -7 0 3.63 3.15 0.18 o 5 -7 0 2.59 2.26 0.08 o 0 -6 0 376.93 373.06 3.80 o 1 -6 0 29.16 33.48 0.79 o 2 -6 0 50.31 55.05 0.98 o 3 -6 0 4.34 4.50 0.14 o 4 -6 0 9.40 9.02 0.18 o 5 -6 0 5.07 5.85 0.12 o 1 -5 0 47.29 53.78 0.98 o 2 -5 0 321.57 338.23 5.93 o 3 -5 0 81.04 77.40 1.36 o 4 -5 0 21.75 21.11 0.38 o 5 -5 0 17.33 16.56 0.76 o 6 -5 0 2.83 2.27 0.10 o 0 -4 0 248.53 228.02 2.18 o 1 -4 0 65.38 60.51 1.75 o 2 -4 0 156.91 168.72 2.45 o 3 -4 0 84.44 86.33 1.34 o 4 -4 0 4.08 3.39 0.13 o 5 -4 0 1.66 1.34 0.14 o 1 -3 0 58.25 69.53 0.78 o 2 -3 0 679.26 712.27 25.99 o 3 -3 0 144.48 157.28 9.06 o 4 -3 0 12.10 13.86 0.24 o 5 -3 0 1.92 2.15 0.31 o 0 -2 0 72.94 73.92 0.82 o 1 -2 0 1823.73 1751.39 33.64 o 2 -2 0 3.08 4.23 0.12 o 3 -2 0 233.25 217.83 7.33 o 4 -2 0 91.14 98.87 3.47 o 5 -2 0 5.01 7.41 2.45 o 6 -2 0 23.54 22.76 0.55 o 1 -1 0 2349.34 2346.89 49.15 o 2 -1 0 92.97 84.13 2.46 o 3 -1 0 297.44 286.04 15.55 o 4 -1 0 48.78 50.88 1.03 o 5 -1 0 10.31 10.10 1.24 o 6 -1 0 20.66 16.30 0.41 o 1 0 0 882.84 913.71 50.21 o 2 0 0 8.86 10.12 0.18 o 3 0 0 127.06 127.70 2.79 o 4 0 0 82.49 76.55 3.78 o 5 0 0 0.22 0.76 0.10 o 1 1 0 2348.31 2260.48 82.25 o 2 1 0 91.64 83.74 0.84 o 3 1 0 295.92 298.49 6.97 o 4 1 0 48.31 50.74 1.01 o 5 1 0 10.24 10.20 0.21 o 6 1 0 20.79 21.42 0.53 o 0 2 0 74.90 73.30 0.82 o 1 2 0 1821.19 1687.21 52.84 o 2 2 0 3.07 4.17 0.08 o 3 2 0 231.48 220.21 1.85 o 4 2 0 91.76 102.69 2.40 o 5 2 0 5.13 5.41 0.15 o 6 2 0 23.64 20.68 0.53 o 1 3 0 59.34 69.47 1.05 o 2 3 0 679.39 708.49 2.95 o 3 3 0 145.22 151.63 1.65 o 4 3 0 12.26 13.55 0.51 o 5 3 0 1.97 2.53 0.12 o 0 4 0 250.56 233.66 2.22 o 1 4 0 64.85 61.33 0.85 o 2 4 0 157.72 169.41 1.61 o 3 4 0 84.57 90.57 2.52 o 4 4 0 3.97 3.13 0.18 o 5 4 0 1.62 1.31 0.14 o 1 5 0 47.05 53.40 0.92 o 2 5 0 321.02 340.13 4.00 o 3 5 0 81.17 77.37 1.37 o 4 5 0 21.88 21.11 0.82 o 5 5 0 17.14 16.70 0.33 o 6 5 0 2.79 2.29 0.10 o 0 6 0 376.56 377.83 3.82 o 1 6 0 29.06 32.35 0.63 o 2 6 0 50.19 54.02 1.56 o 3 6 0 4.56 4.57 0.14 o 4 6 0 9.55 8.97 0.17 o 5 6 0 4.98 5.84 0.31 o 1 7 0 355.03 351.44 2.99 o 2 7 0 202.41 201.34 2.33 o 3 7 0 2.36 2.59 0.12 o 4 7 0 3.78 3.30 0.12 o 5 7 0 2.61 2.45 0.19 o 0 8 0 302.97 300.24 4.06 o 1 8 0 51.36 50.45 0.87 o 2 8 0 5.06 6.94 1.71 o 3 8 0 14.98 14.54 0.27 o 4 8 0 0.14 0.11 0.22 o 1 9 0 21.50 23.27 0.41 o 2 9 0 34.20 34.12 0.75 o 3 9 0 9.66 9.07 0.23 o 0 10 0 24.89 27.79 0.69 o 1 10 0 10.66 11.15 0.27 o 2 10 0 7.85 8.05 0.15 o -2 -10 1 10.89 11.54 0.29 o -1 -10 1 0.23 0.19 0.33 o 0 -10 1 36.67 37.65 0.98 o 1 -10 1 2.99 2.82 0.14 o 2 -10 1 2.69 2.41 0.12 o -3 -9 1 12.65 11.49 0.31 o -2 -9 1 51.33 46.64 1.22 o -1 -9 1 0.78 0.93 0.12 o 0 -9 1 15.05 15.34 0.43 o 1 -9 1 80.60 88.78 2.11 o 2 -9 1 13.76 13.47 0.36 o 3 -9 1 19.96 20.46 0.48 o -4 -8 1 3.64 3.20 0.14 o -3 -8 1 12.44 12.83 0.33 o -2 -8 1 11.53 12.09 0.29 o -1 -8 1 19.49 19.26 0.45 o 0 -8 1 103.07 105.64 2.43 o 1 -8 1 120.38 121.12 2.60 o 2 -8 1 30.32 33.74 0.86 o 3 -8 1 5.83 5.87 0.19 o 4 -8 1 0.06 0.21 0.10 o -5 -7 1 7.73 7.24 0.17 o -4 -7 1 2.66 2.05 0.14 o -3 -7 1 0.86 0.43 0.50 o -2 -7 1 27.07 27.57 0.69 o -1 -7 1 328.74 329.31 4.07 o 0 -7 1 262.33 252.47 3.52 o 1 -7 1 154.84 149.66 2.75 o 2 -7 1 196.50 189.34 3.21 o 3 -7 1 1.37 1.24 0.14 o 4 -7 1 21.78 23.83 0.57 o 5 -7 1 4.52 4.27 0.12 o -5 -6 1 15.02 15.72 0.43 o -4 -6 1 33.15 30.16 0.77 o -3 -6 1 4.67 5.63 0.19 o -2 -6 1 6.48 5.33 0.17 o -1 -6 1 4.04 4.68 0.17 o 0 -6 1 386.48 402.96 3.97 o 1 -6 1 61.41 71.60 1.73 o 2 -6 1 84.33 94.09 2.14 o 3 -6 1 35.77 36.36 0.86 o 4 -6 1 10.21 8.79 0.24 o 5 -6 1 28.69 28.13 0.74 o -6 -5 1 10.72 8.05 0.22 o -5 -5 1 9.92 8.12 0.21 o -4 -5 1 1.07 1.15 0.14 o -3 -5 1 9.72 9.05 0.21 o -2 -5 1 199.59 246.74 3.05 o -1 -5 1 424.24 421.78 3.65 o 0 -5 1 7.33 8.14 0.19 o 1 -5 1 4.35 5.90 0.14 o 2 -5 1 100.02 114.11 2.12 o 3 -5 1 14.84 13.83 0.36 o 4 -5 1 39.23 39.70 0.96 o 5 -5 1 2.23 2.29 0.17 o -5 -4 1 7.73 7.71 0.21 o -4 -4 1 11.35 10.41 0.26 o -3 -4 1 33.85 32.04 0.77 o -2 -4 1 42.76 46.82 1.13 o -1 -4 1 405.79 419.69 3.14 o 0 -4 1 406.29 409.44 2.97 o 1 -4 1 723.88 722.14 4.21 o 2 -4 1 438.48 441.52 3.73 o 3 -4 1 22.83 22.54 0.55 o 4 -4 1 25.71 25.82 0.67 o -5 -3 1 1.84 1.89 0.17 o -4 -3 1 1.31 1.34 0.14 o -3 -3 1 97.12 98.04 1.85 o -2 -3 1 337.90 305.33 2.70 o -1 -3 1 389.46 408.91 2.64 o 0 -3 1 112.31 94.28 1.19 o 1 -3 1 1817.83 1832.56 17.98 o 2 -3 1 354.39 383.19 3.10 o 3 -3 1 134.56 143.58 2.29 o 4 -3 1 42.16 47.44 1.17 o 5 -3 1 9.27 8.93 0.24 o -5 -2 1 24.61 22.54 0.55 o -4 -2 1 56.35 52.35 1.34 o -3 -2 1 454.62 489.33 3.88 o -2 -2 1 1515.70 1563.81 5.77 o -1 -2 1 100.17 115.48 1.19 o 0 -2 1 4034.40 3525.32 21.04 o 1 -2 1 599.21 566.01 2.73 o 2 -2 1 208.79 198.89 2.00 o 3 -2 1 283.97 309.83 3.17 o 4 -2 1 154.73 155.91 2.75 o 5 -2 1 5.27 5.52 0.21 o 6 -2 1 15.74 14.58 0.36 o -5 -1 1 12.14 11.16 0.26 o -4 -1 1 15.40 15.51 0.33 o -3 -1 1 108.60 105.00 1.71 o -2 -1 1 1147.12 1129.60 4.48 o -1 -1 1 2006.60 2059.14 14.15 o 0 -1 1 2846.66 2340.73 13.00 o 1 -1 1 2511.86 2743.91 17.33 o 2 -1 1 659.94 676.87 3.52 o 3 -1 1 195.97 211.25 2.50 o 4 -1 1 82.05 84.67 1.99 o 5 -1 1 41.09 39.58 1.01 o 6 -1 1 5.46 5.06 0.19 o -5 0 1 0.77 0.81 0.14 o -4 0 1 9.51 8.12 0.21 o -3 0 1 41.36 51.26 1.20 o -2 0 1 6.14 5.02 0.12 o -1 0 1 203.96 201.36 1.22 o 0 0 1 217.36 206.35 2.28 o 1 0 1 3947.37 4096.23 21.32 o 2 0 1 1002.33 1060.25 4.34 o 3 0 1 171.91 163.12 2.18 o 4 0 1 1.86 -0.10 0.43 o 5 0 1 5.60 5.54 0.21 o -5 1 1 12.13 12.25 0.33 o -4 1 1 15.73 16.75 0.41 o -3 1 1 108.10 109.48 1.76 o -2 1 1 1150.68 1214.59 4.64 o -1 1 1 2012.88 2046.34 14.09 o 0 1 1 2847.08 2543.59 13.56 o 1 1 1 2512.90 2457.51 16.41 o 2 1 1 662.50 656.60 3.47 o 3 1 1 195.84 210.38 2.50 o 4 1 1 82.03 88.20 2.02 o 5 1 1 41.43 40.66 0.98 o 6 1 1 5.50 4.82 0.19 o -6 2 1 4.13 3.56 0.17 o -5 2 1 24.49 25.58 0.65 o -4 2 1 56.40 56.30 1.37 o -3 2 1 455.20 510.73 3.95 o -2 2 1 1516.16 1534.03 5.72 o -1 2 1 102.77 118.99 1.21 o 0 2 1 4036.72 3689.99 21.53 o 1 2 1 594.08 554.20 2.71 o 2 2 1 206.69 204.87 2.05 o 3 2 1 283.57 306.78 3.15 o 4 2 1 154.68 152.75 2.70 o 5 2 1 5.18 5.47 0.21 o -5 3 1 1.77 3.20 0.17 o -4 3 1 1.36 1.38 0.14 o -3 3 1 96.87 103.74 1.92 o -2 3 1 339.52 315.38 2.73 o -1 3 1 388.98 391.17 2.59 o 0 3 1 113.06 95.81 1.21 o 1 3 1 1813.70 1829.34 17.94 o 2 3 1 354.00 377.84 3.08 o 3 3 1 134.26 139.04 2.27 o 4 3 1 42.49 45.72 1.12 o 5 3 1 9.09 9.51 0.26 o -4 4 1 11.54 10.89 0.31 o -3 4 1 33.91 32.42 0.77 o -2 4 1 43.08 44.41 1.13 o -1 4 1 406.52 423.03 3.14 o 0 4 1 404.92 399.65 2.92 o 1 4 1 726.35 715.84 4.19 o 2 4 1 440.15 451.45 3.75 o 3 4 1 23.13 22.78 0.55 o 4 4 1 25.72 25.08 0.60 o 5 4 1 22.74 24.45 0.62 o -5 5 1 9.81 8.05 0.21 o -4 5 1 1.05 1.24 0.14 o -3 5 1 9.69 8.55 0.21 o -2 5 1 198.20 242.94 3.03 o -1 5 1 423.95 421.35 3.65 o 0 5 1 7.69 8.24 0.21 o 1 5 1 4.47 7.31 0.19 o 2 5 1 101.15 113.18 2.09 o 3 5 1 14.56 13.38 0.31 o 4 5 1 39.63 40.66 1.01 o 5 5 1 2.19 2.15 0.14 o -5 6 1 15.16 16.46 0.41 o -4 6 1 32.96 32.05 0.79 o -3 6 1 4.44 5.44 0.19 o -2 6 1 6.39 4.90 0.17 o -1 6 1 3.95 4.68 0.17 o 0 6 1 386.29 400.23 3.95 o 1 6 1 61.40 73.59 1.75 o 2 6 1 83.75 90.80 2.11 o 3 6 1 35.79 35.07 0.89 o 4 6 1 10.19 9.10 0.24 o 5 6 1 28.75 30.59 0.77 o -5 7 1 7.77 8.00 0.19 o -4 7 1 2.79 1.98 0.14 o -3 7 1 0.85 1.41 0.14 o -2 7 1 27.52 27.88 0.69 o -1 7 1 327.11 322.69 4.02 o 0 7 1 263.08 251.66 3.50 o 1 7 1 155.03 152.82 2.77 o 2 7 1 195.65 184.40 3.19 o 3 7 1 1.38 1.19 0.14 o 4 7 1 21.61 23.31 0.57 o 5 7 1 4.39 4.23 0.12 o -4 8 1 3.73 3.68 0.14 o -3 8 1 12.31 12.85 0.33 o -2 8 1 11.52 12.42 0.33 o -1 8 1 19.11 17.95 0.43 o 0 8 1 103.04 100.88 2.35 o 1 8 1 121.38 128.61 2.67 o 2 8 1 30.28 34.65 0.81 o 3 8 1 5.90 5.66 0.19 o 4 8 1 0.07 0.24 0.31 o -3 9 1 12.65 12.09 0.31 o -2 9 1 51.43 46.78 1.25 o -1 9 1 0.79 0.91 0.12 o 0 9 1 15.33 16.10 0.41 o 1 9 1 80.28 90.15 2.11 o 2 9 1 13.87 12.85 0.36 o 3 9 1 19.71 20.25 0.50 o -2 10 1 10.94 11.47 0.26 o -1 10 1 0.25 0.43 0.10 o 0 10 1 36.65 37.50 0.96 o 1 10 1 3.01 2.65 0.12 o 2 10 1 2.68 2.20 0.12 o -2 -10 2 11.14 12.14 0.31 o -1 -10 2 16.80 16.59 0.43 o 0 -10 2 3.50 3.58 0.14 o 1 -10 2 20.41 20.34 0.50 o 2 -10 2 0.47 0.64 0.10 o -3 -9 2 6.69 5.56 0.17 o -2 -9 2 5.28 5.56 0.17 o -1 -9 2 15.08 16.06 0.45 o 0 -9 2 62.71 64.49 1.58 o 1 -9 2 7.84 7.64 0.21 o 2 -9 2 46.42 50.84 1.22 o 3 -9 2 13.09 13.36 0.31 o -4 -8 2 22.62 23.67 0.57 o -3 -8 2 8.50 8.02 0.21 o -2 -8 2 120.62 117.69 2.55 o -1 -8 2 60.68 58.73 1.49 o 0 -8 2 103.80 103.09 2.38 o 1 -8 2 265.42 276.86 3.91 o 2 -8 2 45.34 46.51 1.13 o 3 -8 2 5.68 4.44 0.17 o 4 -8 2 5.80 5.37 0.14 o -5 -7 2 5.01 5.47 0.14 o -4 -7 2 5.56 5.40 0.19 o -3 -7 2 0.18 0.07 0.48 o -2 -7 2 1.62 0.17 0.53 o -1 -7 2 236.76 255.87 3.59 o 0 -7 2 70.67 71.75 1.75 o 1 -7 2 7.52 5.99 0.19 o 2 -7 2 208.22 212.20 3.41 o 3 -7 2 76.13 79.87 2.01 o 4 -7 2 1.71 1.29 0.14 o -5 -6 2 69.76 65.71 1.63 o -4 -6 2 0.28 1.05 0.14 o -3 -6 2 5.13 5.97 0.19 o -2 -6 2 6.09 5.54 0.19 o -1 -6 2 128.23 138.53 2.41 o 0 -6 2 31.11 30.72 0.72 o 1 -6 2 165.30 169.60 2.68 o 2 -6 2 485.67 497.45 4.95 o 3 -6 2 51.77 56.85 1.41 o 4 -6 2 5.59 5.01 0.19 o 5 -6 2 0.22 0.19 0.33 o -6 -5 2 9.09 8.48 0.19 o -5 -5 2 4.89 4.70 0.19 o -4 -5 2 12.90 14.17 0.36 o -3 -5 2 7.31 8.00 0.24 o -2 -5 2 16.80 15.34 0.38 o -1 -5 2 524.79 554.16 4.24 o 0 -5 2 22.86 21.55 0.53 o 1 -5 2 326.67 329.41 3.30 o 2 -5 2 55.40 58.87 1.46 o 3 -5 2 126.90 127.79 2.55 o 4 -5 2 16.53 17.35 0.43 o 5 -5 2 45.74 46.33 1.20 o -5 -4 2 41.57 36.40 0.86 o -4 -4 2 51.35 50.63 1.27 o -3 -4 2 33.41 33.71 0.86 o -2 -4 2 93.08 90.10 1.66 o -1 -4 2 371.11 390.65 3.06 o 0 -4 2 347.72 338.96 2.76 o 1 -4 2 66.04 72.00 1.37 o 2 -4 2 224.27 241.04 2.79 o 3 -4 2 42.85 51.37 1.27 o 4 -4 2 22.85 22.45 0.57 o -5 -3 2 39.18 34.39 0.81 o -4 -3 2 1.12 0.93 0.12 o -3 -3 2 136.75 131.40 2.15 o -2 -3 2 381.05 405.16 3.13 o -1 -3 2 242.85 238.73 2.06 o 0 -3 2 66.00 59.61 0.99 o 1 -3 2 690.58 685.79 3.65 o 2 -3 2 249.70 239.38 2.51 o 3 -3 2 73.17 79.28 1.78 o 4 -3 2 25.06 25.56 0.62 o 5 -3 2 8.31 8.62 0.24 o -5 -2 2 12.38 12.66 0.33 o -4 -2 2 116.67 117.90 2.33 o -3 -2 2 56.85 51.41 1.27 o -2 -2 2 66.64 65.87 1.15 o -1 -2 2 791.10 762.46 3.24 o 0 -2 2 946.53 891.39 9.64 o 1 -2 2 697.93 677.28 3.16 o 2 -2 2 382.77 379.36 2.89 o 3 -2 2 1.98 2.58 0.14 o 4 -2 2 74.34 73.49 1.87 o 5 -2 2 78.96 77.03 2.02 o -6 -1 2 27.43 23.44 0.60 o -5 -1 2 61.89 57.10 1.39 o -4 -1 2 79.13 89.23 1.97 o -3 -1 2 41.82 39.02 0.98 o -2 -1 2 90.62 96.81 1.28 o -1 -1 2 379.87 391.91 1.96 o 0 -1 2 31.84 28.26 0.48 o 1 -1 2 4414.65 4988.77 26.77 o 2 -1 2 110.24 102.13 1.40 o 3 -1 2 26.18 27.70 0.72 o 4 -1 2 19.54 19.93 0.50 o 5 -1 2 8.90 10.22 0.26 o 6 -1 2 5.52 5.18 0.17 o -5 0 2 18.98 17.64 0.45 o -4 0 2 11.52 11.78 0.29 o -3 0 2 12.03 12.76 0.33 o -2 0 2 245.82 241.37 1.96 o -1 0 2 13.67 14.19 0.34 o 0 0 2 97.38 91.88 0.71 o 1 0 2 11594.35 12765.22 48.79 o 2 0 2 165.24 160.31 1.72 o 3 0 2 77.89 86.67 1.63 o 4 0 2 55.80 54.60 1.41 o 5 0 2 4.20 5.09 0.19 o 6 0 2 0.62 0.50 0.12 o -5 1 2 62.28 63.53 1.61 o -4 1 2 79.37 89.51 1.97 o -3 1 2 42.23 38.99 0.96 o -2 1 2 91.00 92.14 1.25 o -1 1 2 378.07 390.15 1.96 o 0 1 2 33.06 28.38 0.48 o 1 1 2 4417.90 4524.87 25.49 o 2 1 2 111.71 101.62 1.40 o 3 1 2 26.06 29.25 0.74 o 4 1 2 19.62 20.86 0.50 o 5 1 2 8.83 9.00 0.24 o -5 2 2 12.37 13.11 0.33 o -4 2 2 116.36 125.33 2.38 o -3 2 2 57.17 53.37 1.29 o -2 2 2 66.04 65.24 1.15 o -1 2 2 796.50 697.45 3.09 o 0 2 2 944.38 900.00 9.70 o 1 2 2 701.32 674.21 3.16 o 2 2 2 381.38 375.58 2.87 o 3 2 2 2.10 2.77 0.12 o 4 2 2 73.82 78.98 1.97 o 5 2 2 79.00 83.79 1.99 o -5 3 2 39.07 37.02 0.93 o -4 3 2 1.07 0.76 0.14 o -3 3 2 136.63 130.34 2.15 o -2 3 2 382.01 409.32 3.13 o -1 3 2 242.20 225.10 1.98 o 0 3 2 66.31 60.02 0.99 o 1 3 2 686.55 680.76 3.65 o 2 3 2 251.14 234.31 2.49 o 3 3 2 73.04 75.05 1.70 o 4 3 2 25.02 24.12 0.62 o -4 4 2 51.43 54.39 1.44 o -3 4 2 33.53 36.34 0.91 o -2 4 2 92.14 89.46 1.63 o -1 4 2 372.37 393.45 3.08 o 0 4 2 344.28 331.07 2.71 o 1 4 2 66.27 72.31 1.39 o 2 4 2 224.99 239.52 2.79 o 3 4 2 42.91 48.79 1.29 o 4 4 2 22.67 22.18 0.55 o 5 4 2 11.76 12.66 0.36 o -5 5 2 4.94 5.16 0.19 o -4 5 2 13.13 14.52 0.36 o -3 5 2 7.18 7.83 0.21 o -2 5 2 16.98 15.65 0.36 o -1 5 2 523.98 563.93 4.27 o 0 5 2 22.72 21.28 0.53 o 1 5 2 326.60 320.70 3.25 o 2 5 2 55.08 59.64 1.49 o 3 5 2 125.91 125.03 2.53 o 4 5 2 16.77 16.82 0.41 o 5 5 2 45.75 45.93 1.13 o -5 6 2 69.67 67.91 1.68 o -4 6 2 0.23 0.84 0.14 o -3 6 2 5.36 6.14 0.19 o -2 6 2 6.00 5.37 0.17 o -1 6 2 128.30 137.84 2.38 o 0 6 2 30.73 28.11 0.69 o 1 6 2 165.98 164.37 2.66 o 2 6 2 485.64 492.63 4.92 o 3 6 2 51.61 57.14 1.41 o 4 6 2 5.54 4.94 0.19 o 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