#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/81/2218134.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2218134_Fobs loop_ _publ_author_name 'Yamada, Kazuhiko' 'Sato, Akira' 'Shimizu, Tadashi' 'Yamazaki, Toshio' 'Yokoyama, Shigeyuki' _publ_section_title ; L-Alanine hydrochloride monohydrate ; _journal_coeditor_code HG2382 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o806 _journal_volume 64 _journal_year 2008 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 6.1925 _cell_length_b 9.9289 _cell_length_c 11.7590 _exptl_crystal_F_000 304.00 _reflns_d_resolution_high 0.7827 _[local]_cod_data_source_file hg2382Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' L-Alanine hydrochloride monohydrate' _shelx_refln_list_code 4 _shelx_F_calc_maximum 82.45 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 883.09 997.94 17.34 o 4 0 0 490.49 530.19 9.28 o 6 0 0 79.82 82.26 1.70 o 1 1 0 746.47 679.08 8.79 o 2 1 0 392.04 421.94 6.07 o 3 1 0 2441.58 2514.01 30.88 o 4 1 0 0.10 0.76 0.14 o 5 1 0 14.55 14.10 0.36 o 6 1 0 211.95 208.78 2.74 o 7 1 0 53.02 51.96 0.87 o 0 2 0 5220.24 3601.05 103.92 o 1 2 0 98.45 66.53 0.80 o 2 2 0 1010.22 1058.82 12.98 o 3 2 0 1459.51 1502.45 18.38 o 4 2 0 56.07 48.09 1.05 o 5 2 0 376.05 382.55 4.81 o 6 2 0 52.09 49.85 0.81 o 7 2 0 86.99 84.55 1.27 o 1 3 0 182.63 198.16 2.26 o 2 3 0 1200.06 1200.25 14.72 o 3 3 0 0.01 0.38 0.13 o 4 3 0 170.19 157.09 2.21 o 5 3 0 113.40 112.38 1.53 o 6 3 0 200.63 192.98 2.55 o 7 3 0 10.31 10.81 0.35 o 0 4 0 701.46 720.24 18.68 o 1 4 0 338.21 348.74 3.96 o 2 4 0 609.60 704.83 9.01 o 3 4 0 1545.44 1543.59 52.00 o 4 4 0 34.76 31.04 0.52 o 5 4 0 529.56 536.62 6.69 o 6 4 0 84.25 83.96 1.36 o 7 4 0 89.24 89.55 1.64 o 1 5 0 94.28 88.35 1.06 o 2 5 0 17.85 14.91 0.28 o 3 5 0 728.15 803.92 9.87 o 4 5 0 462.72 431.70 9.95 o 5 5 0 30.38 29.01 0.59 o 6 5 0 320.66 319.08 4.99 o 7 5 0 16.71 17.26 0.93 o 0 6 0 1674.84 1691.69 25.05 o 1 6 0 171.96 160.58 2.40 o 2 6 0 38.77 29.37 0.60 o 3 6 0 30.86 28.17 0.53 o 4 6 0 5.38 4.94 0.26 o 5 6 0 253.55 265.03 4.17 o 6 6 0 0.65 0.65 0.24 o 1 7 0 1477.15 1526.80 18.59 o 2 7 0 57.64 58.52 1.04 o 3 7 0 6.48 7.17 0.44 o 4 7 0 305.98 301.53 4.69 o 5 7 0 52.72 51.82 1.03 o 6 7 0 26.41 25.01 0.67 o 0 8 0 108.89 100.90 3.30 o 1 8 0 230.30 235.20 4.25 o 2 8 0 407.33 400.99 7.11 o 3 8 0 41.12 36.73 0.76 o 4 8 0 259.18 249.73 3.94 o 5 8 0 23.73 21.16 0.58 o 6 8 0 5.87 6.43 0.70 o 1 9 0 1063.11 1071.96 22.06 o 2 9 0 204.70 199.11 3.69 o 3 9 0 3.28 4.14 0.41 o 4 9 0 15.51 14.04 0.54 o 5 9 0 3.53 3.57 0.36 o 0 10 0 13.81 14.05 0.89 o 1 10 0 9.14 7.93 0.49 o 2 10 0 131.29 127.91 2.99 o 3 10 0 2.74 3.04 0.60 o 4 10 0 26.47 23.48 0.74 o 1 11 0 291.65 304.72 6.63 o 2 11 0 129.88 135.00 3.19 o 3 11 0 3.92 4.15 0.63 o 1 0 1 67.71 57.61 1.13 o 2 0 1 852.68 916.28 11.23 o 3 0 1 908.16 912.61 11.18 o 4 0 1 0.05 0.17 0.12 o 5 0 1 603.00 621.13 7.70 o 6 0 1 93.66 94.08 1.34 o 7 0 1 76.03 74.86 1.45 o -7 1 1 32.52 32.97 0.64 o -6 1 1 300.94 292.20 3.80 o -5 1 1 46.90 43.49 0.76 o -4 1 1 794.01 802.58 10.96 o -3 1 1 647.28 665.62 8.91 o -2 1 1 3942.12 3905.34 54.35 o -1 1 1 132.21 137.61 2.00 o 0 1 1 794.35 764.24 11.62 o 1 1 1 137.79 141.69 1.70 o 2 1 1 3963.49 4114.57 42.19 o 3 1 1 642.45 649.52 7.43 o 4 1 1 803.36 812.59 9.14 o 5 1 1 46.93 43.03 0.69 o 6 1 1 301.90 299.15 3.79 o 7 1 1 33.23 33.04 0.63 o -7 2 1 143.66 147.89 2.03 o -6 2 1 43.91 41.17 0.69 o -5 2 1 429.81 428.52 5.44 o -4 2 1 88.20 85.23 1.45 o -3 2 1 128.10 127.21 1.87 o -2 2 1 245.05 279.31 3.58 o -1 2 1 375.93 368.93 5.83 o 0 2 1 881.11 909.94 11.23 o 1 2 1 369.73 361.85 4.13 o 2 2 1 229.16 267.31 3.11 o 3 2 1 117.48 113.90 1.56 o 4 2 1 89.63 85.22 2.16 o 5 2 1 437.28 439.64 5.43 o 6 2 1 41.84 39.75 0.69 o 7 2 1 141.67 144.89 2.24 o -7 3 1 71.66 71.60 1.38 o -6 3 1 100.75 98.73 1.41 o -5 3 1 228.06 226.75 2.94 o -4 3 1 320.86 331.12 4.09 o -3 3 1 297.74 310.04 3.89 o -2 3 1 221.75 237.85 3.03 o -1 3 1 4057.08 3980.17 97.54 o 0 3 1 231.62 245.66 3.05 o 1 3 1 4057.15 3977.12 44.68 o 2 3 1 229.20 248.09 2.79 o 3 3 1 300.47 313.98 3.89 o 4 3 1 313.44 320.27 5.57 o 5 3 1 228.28 229.53 2.94 o 6 3 1 100.02 99.70 1.41 o 7 3 1 73.43 73.52 1.25 o -7 4 1 2.21 2.62 0.30 o -6 4 1 180.70 179.79 2.91 o -5 4 1 31.73 29.31 0.59 o -4 4 1 106.33 105.73 1.45 o -3 4 1 134.55 129.96 1.90 o -2 4 1 643.78 643.67 7.89 o -1 4 1 1171.44 1241.12 16.82 o 0 4 1 2759.90 2619.14 68.60 o 1 4 1 1171.39 1250.36 14.00 o 2 4 1 632.74 642.84 7.26 o 3 4 1 134.92 129.51 1.83 o 4 4 1 111.64 110.19 1.46 o 5 4 1 31.83 29.88 0.53 o 6 4 1 174.82 177.45 2.38 o 7 4 1 2.16 2.80 0.46 o -7 5 1 106.16 116.79 3.96 o -6 5 1 53.16 50.74 1.04 o -5 5 1 374.40 374.10 5.76 o -4 5 1 4.90 4.10 0.24 o -3 5 1 514.68 515.06 7.19 o -2 5 1 261.86 260.41 3.32 o -1 5 1 726.22 755.22 10.48 o 0 5 1 92.67 98.96 1.29 o 1 5 1 742.69 766.55 8.57 o 2 5 1 264.36 270.40 3.06 o 3 5 1 523.17 538.63 6.53 o 4 5 1 4.95 4.21 0.19 o 5 5 1 374.55 373.97 5.21 o 6 5 1 52.69 51.56 1.06 o 7 5 1 108.88 114.80 3.96 o -6 6 1 120.01 119.16 2.07 o -5 6 1 139.21 134.06 2.26 o -4 6 1 106.97 102.05 1.77 o -3 6 1 430.03 425.84 6.37 o -2 6 1 508.74 512.20 6.92 o -1 6 1 74.64 74.52 1.12 o 0 6 1 290.90 281.38 4.50 o 1 6 1 77.42 76.03 0.93 o 2 6 1 498.25 504.22 5.77 o 3 6 1 419.15 415.49 5.83 o 4 6 1 109.49 107.67 1.60 o 5 6 1 139.44 137.23 2.26 o 6 6 1 116.52 119.11 2.06 o -6 7 1 100.08 100.67 1.80 o -5 7 1 5.40 4.41 0.30 o -4 7 1 280.56 279.59 4.38 o -3 7 1 52.29 52.64 0.97 o -2 7 1 278.51 277.30 4.25 o -1 7 1 246.57 241.96 4.32 o 0 7 1 104.89 113.27 2.17 o 1 7 1 244.30 240.07 3.03 o 2 7 1 286.81 275.56 5.63 o 3 7 1 49.18 50.85 0.86 o 4 7 1 284.58 282.73 4.38 o 5 7 1 5.53 4.52 0.28 o 6 7 1 99.51 98.27 2.10 o -5 8 1 232.50 233.80 3.79 o -4 8 1 9.43 9.18 0.36 o -3 8 1 317.97 302.48 4.70 o -2 8 1 113.23 111.66 2.20 o -1 8 1 206.26 202.89 3.70 o 0 8 1 30.01 28.82 0.71 o 1 8 1 203.26 202.68 3.26 o 2 8 1 114.26 115.56 1.66 o 3 8 1 314.91 305.79 4.71 o 4 8 1 9.46 9.49 0.36 o 5 8 1 235.45 238.99 3.79 o -5 9 1 15.57 13.83 0.71 o -4 9 1 195.14 196.94 3.77 o -3 9 1 29.32 26.96 0.75 o -2 9 1 10.11 8.42 0.49 o -1 9 1 33.05 31.59 1.27 o 0 9 1 43.29 40.37 1.14 o 1 9 1 32.96 34.88 2.17 o 2 9 1 11.18 9.09 0.39 o 3 9 1 30.11 27.63 0.75 o 4 9 1 195.75 201.79 3.24 o 5 9 1 15.45 14.82 0.50 o -4 10 1 4.49 4.86 0.53 o -3 10 1 230.32 223.55 5.03 o -2 10 1 95.23 92.52 2.29 o -1 10 1 144.88 144.82 3.34 o 0 10 1 275.94 276.16 5.99 o 1 10 1 145.28 146.04 3.34 o 2 10 1 94.12 93.03 2.27 o 3 10 1 230.09 229.64 4.23 o 4 10 1 4.57 4.53 0.38 o -3 11 1 33.32 32.96 1.55 o -2 11 1 49.08 47.78 1.48 o -1 11 1 85.09 84.60 2.19 o 0 11 1 0.01 0.07 0.57 o 1 11 1 87.08 89.36 2.20 o 2 11 1 47.26 49.04 1.42 o 3 11 1 34.46 32.62 1.54 o 0 12 1 103.59 101.53 3.61 o 1 12 1 3.82 4.20 0.67 o 0 0 2 85.86 53.78 1.20 o 1 0 2 66.51 64.94 0.84 o 2 0 2 2744.87 2818.00 31.77 o 3 0 2 188.14 195.14 2.47 o 4 0 2 198.65 195.75 2.70 o 5 0 2 0.00 0.07 0.14 o 6 0 2 30.65 30.99 0.57 o 7 0 2 27.97 26.75 0.62 o -7 1 2 106.86 108.15 1.58 o -6 1 2 34.96 32.69 0.73 o -5 1 2 15.65 13.85 0.36 o -4 1 2 451.98 464.13 6.41 o -3 1 2 303.11 321.51 7.21 o -2 1 2 44.86 54.61 0.75 o 0 1 2 424.79 456.62 5.66 o 2 1 2 47.76 57.74 0.65 o 3 1 2 323.07 340.64 3.55 o 4 1 2 462.48 469.39 5.34 o 5 1 2 15.62 14.13 0.33 o 6 1 2 33.44 32.67 0.58 o 7 1 2 108.11 109.85 1.97 o -7 2 2 104.16 102.51 1.51 o -6 2 2 3.34 3.15 0.21 o -5 2 2 462.55 459.54 5.67 o -4 2 2 337.53 335.04 8.30 o -3 2 2 160.75 149.41 1.85 o -2 2 2 563.53 580.33 7.11 o -1 2 2 1110.59 1101.58 11.71 o 0 2 2 20.40 13.18 0.35 o 1 2 2 1122.70 1130.15 18.48 o 2 2 2 564.25 578.43 6.53 o 3 2 2 147.61 137.92 1.69 o 4 2 2 334.86 336.15 4.20 o 5 2 2 454.01 445.36 5.65 o 6 2 2 3.94 4.27 0.22 o 7 2 2 104.61 104.99 1.90 o -7 3 2 42.20 40.65 0.91 o -6 3 2 110.52 109.86 1.92 o -5 3 2 76.89 73.55 1.07 o -4 3 2 1033.66 1071.26 13.08 o -3 3 2 150.87 158.11 2.03 o -2 3 2 1116.57 1145.74 13.93 o -1 3 2 781.32 852.40 11.19 o 0 3 2 41.67 50.23 0.74 o 1 3 2 769.37 839.64 11.40 o 2 3 2 1108.56 1135.36 12.79 o 3 3 2 150.92 159.08 1.87 o 4 3 2 1014.49 1063.37 13.07 o 5 3 2 77.00 74.69 1.07 o 6 3 2 116.62 113.21 1.74 o 7 3 2 40.63 40.01 0.92 o -7 4 2 294.99 315.95 6.83 o -6 4 2 21.49 21.11 0.70 o -5 4 2 510.31 505.03 7.80 o -4 4 2 10.96 10.72 0.27 o -3 4 2 1074.46 1085.60 13.54 o -2 4 2 423.08 454.42 5.62 o -1 4 2 259.03 266.35 3.27 o 0 4 2 361.82 352.05 4.71 o 1 4 2 251.03 258.14 3.61 o 2 4 2 421.82 458.92 5.18 o 3 4 2 1112.93 1125.54 12.46 o 4 4 2 10.87 10.26 0.26 o 5 4 2 520.74 517.75 6.41 o 6 4 2 21.17 20.93 0.50 o 7 4 2 283.88 308.17 10.66 o -6 5 2 321.16 334.18 5.33 o -5 5 2 122.46 124.93 2.13 o -4 5 2 529.69 532.82 8.04 o -3 5 2 43.49 44.79 0.83 o -2 5 2 490.83 494.47 6.70 o -1 5 2 221.95 222.68 3.00 o 0 5 2 7.93 6.82 0.20 o 1 5 2 213.37 212.00 3.01 o 2 5 2 479.86 491.43 5.59 o 3 5 2 41.28 45.08 0.77 o 4 5 2 517.36 530.99 6.61 o 5 5 2 122.87 129.26 1.74 o 6 5 2 331.38 348.36 5.47 o -6 6 2 39.19 37.86 0.86 o -5 6 2 202.96 198.90 3.21 o -4 6 2 54.53 47.48 0.92 o -3 6 2 287.00 281.92 4.49 o -2 6 2 527.47 553.65 8.25 o -1 6 2 95.60 97.83 1.61 o 0 6 2 751.87 801.43 10.84 o 1 6 2 100.00 102.66 1.23 o 2 6 2 521.17 547.61 6.88 o 3 6 2 293.58 298.67 3.40 o 4 6 2 52.05 47.11 0.82 o 5 6 2 198.69 199.33 2.90 o 6 6 2 38.83 38.32 1.01 o -6 7 2 45.60 46.80 1.05 o -5 7 2 6.08 6.09 0.32 o -4 7 2 57.54 58.60 1.09 o -3 7 2 318.56 303.55 4.82 o -2 7 2 254.63 255.33 3.93 o -1 7 2 222.00 211.23 5.71 o 0 7 2 0.22 0.13 0.16 o 1 7 2 228.51 222.46 2.56 o 2 7 2 252.28 255.19 3.23 o 3 7 2 328.45 319.88 3.96 o 4 7 2 56.07 57.45 0.98 o 5 7 2 6.23 6.47 0.32 o 6 7 2 46.41 46.56 1.38 o -5 8 2 6.81 5.40 0.33 o -4 8 2 24.79 22.70 0.57 o -3 8 2 11.61 10.27 0.42 o -2 8 2 227.79 232.45 5.08 o -1 8 2 30.64 28.98 0.88 o 0 8 2 1451.21 1516.26 26.21 o 1 8 2 30.84 29.40 0.50 o 2 8 2 225.62 235.66 3.00 o 3 8 2 11.09 10.86 0.33 o 4 8 2 23.06 21.93 0.57 o 5 8 2 6.56 6.00 0.41 o -5 9 2 0.32 1.00 0.65 o -4 9 2 134.85 131.81 3.12 o -3 9 2 287.53 274.79 6.13 o -2 9 2 7.73 7.36 0.46 o -1 9 2 81.70 76.94 1.96 o 0 9 2 161.57 164.63 3.09 o 1 9 2 85.28 82.47 1.65 o 2 9 2 7.90 7.45 0.43 o 3 9 2 289.29 287.22 3.93 o 4 9 2 131.57 133.25 2.25 o 5 9 2 0.32 0.36 0.30 o -4 10 2 1.99 2.42 0.55 o -3 10 2 255.66 256.98 5.76 o -2 10 2 154.29 155.69 4.07 o -1 10 2 48.19 46.42 1.32 o 0 10 2 600.18 615.39 12.86 o 1 10 2 47.29 46.75 1.32 o 2 10 2 148.08 155.56 2.98 o 3 10 2 258.47 266.10 4.84 o 4 10 2 2.14 2.08 0.33 o -2 11 2 5.23 5.19 0.47 o -1 11 2 43.05 39.45 1.23 o 0 11 2 8.35 7.29 1.04 o 1 11 2 44.48 41.09 1.23 o 2 11 2 4.55 4.81 0.53 o 3 11 2 11.40 9.99 0.85 o 0 12 2 0.40 0.14 0.51 o 1 12 2 16.15 16.26 1.07 o 1 0 3 6798.38 5766.54 198.59 o 2 0 3 1450.98 1529.83 17.24 o 3 0 3 2198.82 2225.92 25.07 o 4 0 3 71.36 66.98 1.79 o 5 0 3 426.97 429.51 5.96 o 6 0 3 120.01 117.49 1.81 o 7 0 3 237.33 244.11 3.56 o -7 1 3 27.08 24.65 0.54 o -6 1 3 259.67 262.62 3.76 o -5 1 3 33.64 31.67 0.61 o -4 1 3 808.44 826.01 12.58 o -3 1 3 10.69 8.09 0.31 o -2 1 3 626.41 695.42 10.23 o -1 1 3 640.67 651.46 11.51 o 0 1 3 20.40 21.70 0.34 o 1 1 3 622.76 615.66 7.13 o 2 1 3 617.98 703.33 7.34 o 3 1 3 12.18 8.79 0.18 o 4 1 3 828.42 818.82 9.29 o 5 1 3 33.83 32.06 0.50 o 6 1 3 261.69 262.31 4.25 o 7 1 3 25.96 24.24 0.67 o -7 2 3 69.89 69.99 1.36 o -6 2 3 35.81 36.06 0.67 o -5 2 3 327.84 320.78 4.08 o -4 2 3 33.96 32.86 0.65 o -3 2 3 1175.47 1256.30 15.32 o -2 2 3 2005.47 2053.97 24.19 o -1 2 3 1372.58 1438.97 17.54 o 0 2 3 1128.73 1214.16 14.95 o 1 2 3 1362.22 1419.61 20.65 o 2 2 3 1997.11 2062.57 23.19 o 3 2 3 1185.42 1250.57 14.08 o 4 2 3 31.82 31.02 0.47 o 5 2 3 324.99 322.56 4.07 o 6 2 3 35.96 35.49 0.80 o 7 2 3 71.46 69.80 1.38 o -7 3 3 84.85 83.32 1.80 o -6 3 3 37.31 36.24 0.80 o -5 3 3 74.12 71.95 1.15 o -4 3 3 43.10 42.37 0.63 o -3 3 3 253.24 250.36 3.10 o -2 3 3 496.24 511.59 6.37 o -1 3 3 643.38 641.12 7.11 o 0 3 3 1921.40 1970.27 24.15 o 1 3 3 635.01 636.31 8.63 o 2 3 3 495.00 523.19 5.86 o 3 3 3 242.08 243.08 2.85 o 4 3 3 38.35 36.94 0.56 o 5 3 3 74.52 73.02 1.17 o 6 3 3 36.69 35.04 0.80 o 7 3 3 82.89 80.94 1.57 o -7 4 3 9.94 9.48 0.87 o -6 4 3 109.75 109.12 1.95 o -5 4 3 126.21 122.71 2.07 o -4 4 3 77.87 74.72 1.35 o -3 4 3 15.19 14.76 0.29 o -2 4 3 1433.38 1510.93 20.06 o -1 4 3 1090.62 1165.80 15.47 o 0 4 3 1227.86 1221.51 14.97 o 1 4 3 1088.70 1176.32 15.74 o 2 4 3 1455.01 1560.76 17.25 o 3 4 3 14.86 14.96 0.28 o 4 4 3 80.87 80.63 1.02 o 5 4 3 125.63 124.55 1.87 o 6 4 3 112.70 115.42 2.00 o 7 4 3 10.11 10.65 0.62 o -6 5 3 14.96 13.32 0.47 o -5 5 3 9.13 9.08 0.36 o -4 5 3 357.40 348.51 5.43 o -3 5 3 176.71 169.33 2.70 o -2 5 3 144.08 149.06 2.37 o -1 5 3 1147.67 1157.43 15.26 o 0 5 3 510.88 529.52 6.52 o 1 5 3 1165.29 1156.02 17.66 o 2 5 3 144.08 152.17 1.79 o 3 5 3 174.46 172.80 2.04 o 4 5 3 353.52 356.83 4.10 o 5 5 3 9.08 9.79 0.33 o 6 5 3 14.52 13.74 0.48 o 7 5 3 26.71 28.32 1.56 o -6 6 3 18.20 18.47 0.56 o -5 6 3 83.71 84.19 1.51 o -4 6 3 43.79 40.98 0.85 o -3 6 3 71.47 63.37 1.16 o -2 6 3 152.99 148.85 2.32 o -1 6 3 173.27 185.62 2.53 o 0 6 3 833.26 850.68 12.67 o 1 6 3 171.25 182.63 2.59 o 2 6 3 145.95 145.80 1.76 o 3 6 3 75.49 67.60 0.88 o 4 6 3 44.53 44.20 0.70 o 5 6 3 81.11 83.05 1.54 o 6 6 3 18.06 19.06 0.57 o -6 7 3 135.80 136.79 3.39 o -5 7 3 20.07 20.53 0.57 o -4 7 3 308.00 302.63 4.80 o -3 7 3 155.73 143.07 2.35 o -2 7 3 383.12 363.86 6.53 o -1 7 3 158.87 153.40 3.36 o 0 7 3 138.71 140.35 2.52 o 1 7 3 154.03 152.29 2.19 o 2 7 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