#------------------------------------------------------------------------------ #$Date: 2009-05-05 17:46:52 +0300 (Tue, 05 May 2009) $ #$Revision: 697 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2218139.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2218139_Fobs loop_ _publ_author_name 'Chan, Isa Y. H.' 'Bishop, Roger' 'Craig, Donald C.' 'Scudder, Marcia L.' 'Yue, Weimin' _publ_section_title ; 8-Methyl-5-methylene-2-oxotricyclo[5.3.1.1^3,9^]dodecan-endo-8-ol ; _journal_coeditor_code HG2391 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o841 _journal_volume 64 _journal_year 2008 _[local]_cod_data_source_file hg2391Isup2.hkl _[local]_cod_data_source_block I loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_meas _refln_F_calc _refln_F_sigma 1 0 0 131.114 -140.794 0.561 2 0 0 16.891 18.578 0.174 3 0 0 3.590 -3.244 0.284 4 0 0 6.720 -6.855 0.234 5 0 0 6.767 -6.659 0.272 6 0 0 11.884 -12.758 0.268 7 0 0 6.865 7.028 0.354 8 0 0 2.767 -2.698 1.482 -8 0 2 6.581 7.428 0.484 -7 0 2 17.401 -18.701 0.280 -6 0 2 13.890 15.204 0.251 -5 0 2 9.231 -8.825 0.235 -4 0 2 31.487 31.934 0.303 -3 0 2 27.326 29.922 0.260 -2 0 2 59.534 -64.847 0.211 -1 0 2 62.101 63.980 0.169 0 0 2 73.905 -75.650 0.133 1 0 2 44.346 -46.411 0.200 2 0 2 14.911 -14.099 0.149 3 0 2 13.165 -12.491 0.171 4 0 2 17.682 16.806 0.191 5 0 2 3.280 3.546 0.539 6 0 2 0.000 0.343 10.057 7 0 2 0.000 0.788 10.062 8 0 2 4.511 4.175 0.742 -8 0 4 7.682 -6.571 0.392 -7 0 4 2.703 2.770 0.754 -6 0 4 9.381 9.504 0.291 -5 0 4 0.000 -1.229 10.041 -4 0 4 2.020 -0.618 0.466 -3 0 4 27.904 -28.593 0.275 -2 0 4 29.564 -30.948 0.246 -1 0 4 108.241 107.831 0.227 0 0 4 59.224 -59.131 0.506 1 0 4 6.714 6.951 0.196 2 0 4 0.308 -0.632 2.873 3 0 4 18.093 19.565 0.188 4 0 4 22.097 -21.800 0.223 5 0 4 9.219 8.031 0.294 6 0 4 0.852 2.803 4.915 7 0 4 1.139 0.044 2.331 -8 0 6 2.199 -2.464 2.008 -7 0 6 3.539 3.165 0.558 -6 0 6 6.812 -6.369 0.347 -5 0 6 9.646 10.178 0.234 -4 0 6 4.232 -4.405 0.337 -3 0 6 18.397 -18.195 0.184 -2 0 6 12.022 10.966 0.172 -1 0 6 0.000 0.312 10.038 0 0 6 29.454 -29.819 0.496 1 0 6 11.044 11.201 0.193 2 0 6 8.642 -8.233 0.230 3 0 6 23.558 24.666 0.233 4 0 6 2.754 -4.538 0.739 5 0 6 0.000 0.664 10.050 6 0 6 1.585 -3.102 1.772 -8 0 8 4.135 -3.790 0.720 -7 0 8 12.948 12.824 0.303 -6 0 8 14.405 -14.821 0.270 -5 0 8 2.534 0.474 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