#------------------------------------------------------------------------------ #$Date: 2009-05-03 21:56:13 +0300 (Sun, 03 May 2009) $ #$Revision: 691 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2218170.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2218170_Fobs loop_ _publ_author_name 'Nakaema, Kosuke' 'Watanabe, Shoji' 'Okamoto, Akiko' 'Noguchi, Keiichi' 'Yonezawa, Noriyuki' _publ_section_title ; 1,8-Dibenzoyl-2,7-dimethoxynaphthalene ; _journal_coeditor_code IS2282 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o807 _journal_volume 64 _journal_year 2008 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 109.711 _cell_angle_gamma 90.000 _cell_length_a 13.9677 _cell_length_b 10.2145 _cell_length_c 14.6966 _exptl_crystal_F_000 832.00 _reflns_d_resolution_high 0.8302 _[local]_cod_data_source_file is2282Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 071029-2' _shelx_refln_list_code 4 _shelx_F_calc_maximum 300.50 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 46.44 81.76 2.72 o 4 0 0 90300.20 98006.07 1037.37 o 6 0 0 4708.37 4874.04 39.05 o 8 0 0 16445.25 17211.83 170.34 o 10 0 0 3777.69 3969.81 50.40 o 12 0 0 507.91 508.91 12.98 o 14 0 0 730.56 752.70 14.55 o 1 1 0 11896.28 11224.77 55.42 o 3 1 0 814.59 845.14 7.67 o 5 1 0 12443.10 12433.61 69.14 o 7 1 0 99.34 109.13 2.20 o 9 1 0 1623.22 1715.16 13.02 o 11 1 0 1069.30 1108.08 15.72 o 13 1 0 1013.38 1062.65 15.25 o 15 1 0 144.16 144.52 6.03 o 0 2 0 8038.72 7267.85 63.61 o 2 2 0 595.79 557.63 6.50 o 4 2 0 528.25 517.21 4.61 o 6 2 0 6581.92 7188.50 38.34 o 8 2 0 117.53 117.92 2.07 o 10 2 0 269.39 285.29 5.61 o 12 2 0 95.99 96.20 5.12 o 14 2 0 152.33 142.81 8.06 o 1 3 0 2846.54 2569.07 14.00 o 3 3 0 2825.12 2696.25 13.01 o 5 3 0 473.98 503.70 4.27 o 7 3 0 403.45 399.64 3.28 o 9 3 0 78.09 76.27 2.94 o 11 3 0 376.87 343.04 9.60 o 13 3 0 20.60 16.46 4.27 o 15 3 0 13.50 6.36 3.16 o 0 4 0 18683.84 18693.64 154.39 o 2 4 0 81.06 66.06 1.89 o 4 4 0 532.68 549.83 4.33 o 6 4 0 2395.25 2619.44 14.32 o 8 4 0 413.35 436.97 7.60 o 10 4 0 364.16 347.35 7.72 o 12 4 0 66.93 61.49 3.96 o 14 4 0 90.37 102.47 8.03 o 1 5 0 6408.72 6951.55 35.86 o 3 5 0 2376.68 2452.00 12.76 o 5 5 0 4636.57 5069.52 27.82 o 7 5 0 1508.20 1515.20 20.84 o 9 5 0 573.46 556.89 16.83 o 11 5 0 20.81 18.05 4.50 o 13 5 0 436.57 505.51 13.80 o 0 6 0 682.86 653.97 6.45 o 2 6 0 0.57 1.71 0.76 o 4 6 0 850.52 860.06 6.73 o 6 6 0 3511.69 3550.82 33.80 o 8 6 0 611.41 611.50 11.60 o 10 6 0 91.08 107.22 5.53 o 12 6 0 104.65 79.46 5.31 o 1 7 0 3.93 5.55 1.41 o 3 7 0 0.01 0.92 0.91 o 5 7 0 647.64 651.09 9.86 o 7 7 0 17.84 14.10 3.15 o 9 7 0 0.08 1.27 1.92 o 11 7 0 10.07 7.73 2.75 o 13 7 0 0.57 -0.55 2.97 o 0 8 0 15.87 10.54 3.80 o 2 8 0 23.38 21.16 2.77 o 4 8 0 336.24 288.22 7.10 o 6 8 0 1354.31 1427.84 21.16 o 8 8 0 260.73 281.77 9.27 o 10 8 0 0.04 0.14 1.48 o 12 8 0 55.95 56.30 17.33 o 1 9 0 0.37 -0.55 1.36 o 3 9 0 39.15 31.66 3.88 o 5 9 0 234.92 245.59 8.18 o 7 9 0 121.07 138.19 6.77 o 9 9 0 16.76 15.14 3.58 o 0 10 0 58.15 54.63 5.59 o 2 10 0 40.76 37.70 4.30 o 4 10 0 275.43 238.78 12.67 o 6 10 0 19.78 24.27 4.03 o 8 10 0 92.44 104.47 7.41 o 1 11 0 1.55 2.65 2.29 o 3 11 0 18.23 9.70 2.43 o 5 11 0 13.75 9.73 2.43 o 7 11 0 4.56 1.63 3.32 o 0 12 0 6.23 0.97 4.15 o 2 12 0 33.45 29.98 6.64 o -15 1 1 191.50 167.53 6.94 o -13 1 1 344.11 323.49 6.92 o -11 1 1 70.21 75.92 3.66 o -9 1 1 2300.07 2463.44 16.17 o -7 1 1 1758.55 1822.53 9.68 o -5 1 1 15947.07 15659.68 88.43 o -3 1 1 7221.56 6622.97 38.94 o -1 1 1 140.06 135.38 2.09 o 1 1 1 2779.12 2500.90 12.59 o 3 1 1 19335.92 18547.09 114.88 o 5 1 1 155.10 189.55 3.46 o 7 1 1 3514.80 3485.09 19.57 o 9 1 1 0.20 2.80 1.53 o 11 1 1 3659.81 3876.95 36.51 o 13 1 1 21.14 21.56 2.83 o 15 1 1 78.07 45.70 6.43 o -14 2 1 93.21 90.35 4.71 o -12 2 1 13.08 10.25 2.55 o -10 2 1 1866.28 1956.13 18.37 o -8 2 1 532.44 577.46 4.35 o -6 2 1 1286.57 1330.30 8.33 o -4 2 1 3373.89 3314.55 17.16 o -2 2 1 15739.64 14642.57 85.93 o 0 2 1 587.45 601.32 7.02 o 2 2 1 806.45 766.40 6.45 o 4 2 1 5564.82 5496.70 30.09 o 6 2 1 0.05 3.84 1.27 o 8 2 1 1342.24 1415.83 10.33 o 10 2 1 0.34 1.75 2.03 o 12 2 1 119.99 122.01 4.79 o 14 2 1 193.23 186.24 6.28 o -15 3 1 109.87 108.35 5.07 o -13 3 1 0.32 -0.40 2.80 o -11 3 1 2.64 8.48 2.83 o -9 3 1 146.54 129.77 3.05 o -7 3 1 212.48 236.72 3.03 o -5 3 1 78.45 58.88 1.46 o -3 3 1 7.95 8.67 1.22 o -1 3 1 5.66 8.44 1.35 o 1 3 1 2475.15 2373.07 12.95 o 3 3 1 2945.09 2923.87 15.26 o 5 3 1 823.14 964.71 6.58 o 7 3 1 46.62 52.65 1.76 o 9 3 1 1545.27 1618.92 15.66 o 11 3 1 173.42 146.72 6.18 o 13 3 1 288.04 280.78 11.53 o 15 3 1 1.83 -0.35 2.60 o -14 4 1 116.51 111.10 5.05 o -12 4 1 10.66 15.39 4.03 o -10 4 1 747.18 778.65 12.77 o -8 4 1 0.53 0.67 1.08 o -6 4 1 377.07 361.68 3.67 o -4 4 1 2803.83 2903.26 14.57 o -2 4 1 3694.09 3782.82 18.69 o 0 4 1 1701.00 1592.85 9.20 o 2 4 1 431.01 447.58 3.88 o 4 4 1 3454.02 3467.30 23.38 o 6 4 1 144.89 144.77 2.35 o 8 4 1 1048.56 1083.53 13.26 o 10 4 1 32.94 24.06 3.63 o 12 4 1 141.93 130.27 5.53 o 14 4 1 12.48 2.94 2.97 o -13 5 1 18.78 16.31 2.86 o -11 5 1 524.84 467.80 12.54 o -9 5 1 293.39 308.75 7.01 o -7 5 1 81.61 81.12 2.25 o -5 5 1 432.47 501.84 4.62 o -3 5 1 3.92 4.14 0.81 o -1 5 1 6875.70 7180.86 41.29 o 1 5 1 224.07 236.95 2.81 o 3 5 1 931.80 910.42 6.14 o 5 5 1 50.60 36.88 1.53 o 7 5 1 52.94 68.44 3.65 o 9 5 1 96.85 81.83 3.51 o 11 5 1 156.00 117.38 6.73 o 13 5 1 34.05 19.67 3.54 o -14 6 1 8.36 2.32 2.86 o -12 6 1 45.62 34.01 4.14 o -10 6 1 119.90 122.98 5.33 o -8 6 1 64.88 63.82 4.24 o -6 6 1 165.33 171.17 3.52 o -4 6 1 272.39 264.55 3.03 o -2 6 1 857.01 930.14 6.33 o 0 6 1 217.12 212.69 2.81 o 2 6 1 219.00 246.40 2.84 o 4 6 1 285.44 275.24 3.16 o 6 6 1 198.24 199.92 5.22 o 8 6 1 3.66 5.54 2.41 o 10 6 1 377.51 348.56 8.59 o 12 6 1 0.00 3.34 2.55 o -13 7 1 45.06 45.80 8.59 o -11 7 1 16.82 16.52 2.83 o -9 7 1 44.81 41.91 5.10 o -7 7 1 545.23 548.69 9.85 o -5 7 1 129.11 118.39 5.77 o -3 7 1 6.58 2.32 1.07 o -1 7 1 276.75 294.61 3.85 o 1 7 1 72.67 63.81 2.24 o 3 7 1 465.45 502.37 5.86 o 5 7 1 3462.27 3556.50 39.51 o 7 7 1 4.59 2.87 2.13 o 9 7 1 8.83 7.43 2.57 o 11 7 1 25.56 16.37 2.56 o -12 8 1 97.25 110.32 6.49 o -10 8 1 0.18 2.04 2.61 o -8 8 1 2.31 1.70 3.06 o -6 8 1 1185.28 1238.53 18.82 o -4 8 1 230.66 228.29 7.24 o -2 8 1 3.04 2.67 1.79 o 0 8 1 15.81 18.59 2.48 o 2 8 1 320.48 327.14 7.13 o 4 8 1 18.89 11.78 2.95 o 6 8 1 0.01 1.52 2.10 o 8 8 1 12.39 17.28 2.96 o 10 8 1 12.97 9.39 2.62 o -11 9 1 210.36 260.10 10.28 o -9 9 1 0.56 -1.58 2.97 o -7 9 1 0.06 1.13 2.91 o -5 9 1 1.01 1.14 2.79 o -3 9 1 18.18 13.13 3.34 o -1 9 1 706.62 522.38 9.71 o 1 9 1 135.67 141.24 5.22 o 3 9 1 76.81 57.55 3.69 o 5 9 1 252.08 279.15 7.30 o 7 9 1 150.57 171.69 6.05 o 9 9 1 3.41 3.31 2.01 o -8 10 1 0.92 0.78 2.21 o -6 10 1 44.03 40.70 4.18 o -4 10 1 39.29 31.25 3.98 o -2 10 1 117.34 89.38 4.67 o 0 10 1 230.52 161.33 7.84 o 2 10 1 13.99 9.17 2.87 o 4 10 1 86.02 88.87 5.58 o 6 10 1 2.96 2.86 2.18 o 8 10 1 39.28 20.55 4.87 o -7 11 1 96.02 107.66 5.08 o -5 11 1 56.90 59.55 8.20 o -3 11 1 11.12 3.40 2.45 o -1 11 1 218.58 188.96 13.47 o 1 11 1 9.07 4.42 2.83 o 3 11 1 30.68 22.24 4.32 o 5 11 1 67.84 85.31 9.10 o -2 12 1 0.54 0.90 1.98 o 0 12 1 2.33 2.40 2.22 o 2 12 1 44.43 16.18 4.45 o -16 0 2 201.93 190.96 9.53 o -14 0 2 347.18 333.74 29.97 o -12 0 2 5488.20 5872.00 91.26 o -10 0 2 234.58 215.52 5.69 o -8 0 2 1530.59 1497.16 12.27 o -6 0 2 1364.79 1364.75 11.41 o -4 0 2 5515.20 5050.08 37.30 o -2 0 2 27582.93 27016.54 232.12 o 0 0 2 1912.88 1962.00 13.76 o 2 0 2 2300.25 2096.90 17.19 o 4 0 2 2174.98 2082.63 15.01 o 6 0 2 118.00 143.73 3.65 o 8 0 2 443.94 476.37 8.22 o 10 0 2 3003.53 3171.47 50.68 o 12 0 2 44.88 43.79 4.20 o 14 0 2 0.92 0.00 1.24 o -15 1 2 12.46 8.84 2.82 o -13 1 2 6.59 5.74 2.49 o -11 1 2 25.09 40.27 3.16 o -9 1 2 316.73 330.88 3.66 o -7 1 2 331.69 424.17 3.86 o -5 1 2 25.28 27.62 1.91 o -3 1 2 1043.32 1039.41 8.67 o -1 1 2 12391.77 11521.99 61.64 o 1 1 2 1349.63 1272.82 10.00 o 3 1 2 503.29 523.70 4.57 o 5 1 2 879.70 968.36 6.50 o 7 1 2 1503.92 1647.71 11.02 o 9 1 2 33.58 48.01 3.56 o 11 1 2 64.43 51.37 3.37 o 13 1 2 35.76 33.66 2.95 o 15 1 2 11.20 1.95 4.07 o -16 2 2 0.55 -0.21 1.87 o -14 2 2 4.19 2.04 2.17 o -12 2 2 230.62 229.34 6.52 o -10 2 2 2.96 0.98 1.58 o -8 2 2 503.53 466.12 3.95 o -6 2 2 3323.36 3687.47 18.94 o -4 2 2 1296.08 1249.49 8.26 o -2 2 2 81.46 99.01 3.11 o 0 2 2 1936.16 1750.27 13.41 o 2 2 2 0.02 2.96 1.00 o 4 2 2 11498.35 11711.23 67.78 o 6 2 2 4.64 1.26 0.82 o 8 2 2 694.80 761.69 8.31 o 10 2 2 53.35 54.20 3.34 o 12 2 2 196.86 196.11 5.74 o 14 2 2 12.50 4.48 2.14 o -15 3 2 75.20 71.10 11.02 o -13 3 2 2.70 3.71 2.43 o -11 3 2 299.45 316.48 6.99 o -9 3 2 149.49 151.19 3.94 o -7 3 2 702.45 722.76 6.39 o -5 3 2 91.68 96.56 2.33 o -3 3 2 2304.14 2164.39 11.85 o -1 3 2 1701.04 1647.19 9.33 o 1 3 2 94.45 94.28 2.23 o 3 3 2 81.56 77.45 1.66 o 5 3 2 27.46 18.08 1.41 o 7 3 2 241.95 243.74 3.29 o 9 3 2 32.14 35.40 3.61 o 11 3 2 29.58 33.98 3.88 o 13 3 2 16.33 11.24 3.45 o -14 4 2 2.70 1.52 1.91 o -12 4 2 377.47 336.31 8.69 o -10 4 2 42.64 41.29 2.91 o -8 4 2 66.10 56.56 3.02 o -6 4 2 374.44 394.33 3.71 o -4 4 2 111.37 84.91 1.81 o -2 4 2 191.70 217.30 2.79 o 0 4 2 2507.81 2593.79 14.12 o 2 4 2 411.64 368.00 3.27 o 4 4 2 1107.58 1153.39 7.57 o 6 4 2 141.24 118.05 2.18 o 8 4 2 7.48 9.57 2.27 o 10 4 2 801.00 740.15 12.29 o 12 4 2 24.66 21.83 4.21 o 14 4 2 0.78 1.70 3.03 o -13 5 2 10.78 8.50 2.64 o -11 5 2 194.18 178.50 6.36 o -9 5 2 43.44 41.14 3.50 o -7 5 2 758.57 770.47 7.91 o -5 5 2 554.65 567.16 4.12 o -3 5 2 195.84 139.10 2.18 o -1 5 2 1143.81 1217.21 7.41 o 1 5 2 566.06 612.46 4.31 o 3 5 2 1092.62 1044.91 7.42 o 5 5 2 407.85 366.88 4.19 o 7 5 2 10.19 9.56 2.26 o 9 5 2 3.47 -0.32 2.25 o 11 5 2 48.60 53.56 5.43 o 13 5 2 1.98 0.58 2.47 o -14 6 2 17.08 6.60 2.27 o -12 6 2 54.95 32.54 5.31 o -10 6 2 10.44 12.57 3.17 o -8 6 2 125.23 120.71 4.47 o -6 6 2 2925.61 2886.83 50.78 o -4 6 2 33.18 30.19 2.04 o -2 6 2 4.11 3.63 1.09 o 0 6 2 41.01 19.68 1.26 o 2 6 2 0.59 0.40 0.74 o 4 6 2 3416.23 3352.64 28.22 o 6 6 2 40.59 45.75 3.87 o 8 6 2 37.46 41.02 3.58 o 10 6 2 91.12 70.06 4.52 o 12 6 2 46.17 17.44 4.85 o -13 7 2 2.43 0.56 3.53 o -11 7 2 3.35 0.55 1.92 o -9 7 2 24.64 28.67 4.83 o -7 7 2 127.85 143.03 6.89 o -5 7 2 333.85 327.76 6.68 o -3 7 2 68.30 57.89 2.41 o -1 7 2 181.98 173.50 3.25 o 1 7 2 36.36 42.74 1.95 o 3 7 2 267.33 273.54 5.16 o 5 7 2 666.69 705.68 9.43 o 7 7 2 31.36 33.07 3.10 o 9 7 2 23.95 23.78 2.86 o 11 7 2 0.34 0.70 2.41 o -12 8 2 11.91 6.35 2.87 o -10 8 2 15.58 17.41 4.38 o -8 8 2 22.50 22.88 3.63 o -6 8 2 1169.58 1208.06 17.59 o -4 8 2 0.90 1.01 3.07 o -2 8 2 0.72 2.54 2.10 o 0 8 2 0.82 2.22 2.01 o 2 8 2 5.81 6.91 1.79 o 4 8 2 1078.77 1099.69 15.43 o 6 8 2 19.53 22.12 3.29 o 8 8 2 1.97 2.17 2.62 o 10 8 2 73.04 55.58 7.64 o -11 9 2 0.00 0.07 1.70 o -9 9 2 68.36 70.86 5.50 o -7 9 2 193.92 186.02 6.40 o -5 9 2 5.56 1.25 2.50 o -3 9 2 94.03 92.64 4.79 o -1 9 2 9.39 6.49 2.47 o 1 9 2 24.77 27.95 3.69 o 3 9 2 31.04 37.65 3.92 o 5 9 2 283.28 278.15 6.41 o 7 9 2 0.89 0.21 1.84 o 9 9 2 8.75 4.98 1.95 o -8 10 2 154.58 172.70 6.41 o -6 10 2 12.31 10.68 3.15 o -4 10 2 242.50 235.99 7.36 o -2 10 2 1.58 2.05 1.76 o 0 10 2 631.64 584.70 12.05 o 2 10 2 81.16 85.24 6.26 o 4 10 2 240.32 265.58 6.84 o 6 10 2 69.67 73.05 5.47 o 8 10 2 6.03 2.41 2.13 o -7 11 2 6.90 2.79 2.37 o -5 11 2 52.59 45.33 6.22 o -3 11 2 222.67 206.50 10.66 o -1 11 2 199.41 162.72 12.87 o 1 11 2 96.52 85.51 7.28 o 3 11 2 0.54 1.96 2.43 o 5 11 2 281.65 325.39 10.85 o -2 12 2 18.37 6.48 2.78 o 0 12 2 22.92 9.29 5.64 o 2 12 2 8.79 3.08 2.67 o -15 1 3 3.26 3.92 3.38 o -13 1 3 579.94 575.53 11.96 o -11 1 3 1.69 2.85 2.01 o -9 1 3 20.79 32.34 1.48 o -7 1 3 148.71 163.90 2.47 o -5 1 3 74.92 82.79 2.08 o -3 1 3 181.42 218.26 4.51 o -1 1 3 44350.77 44702.40 321.19 o 1 1 3 2361.35 2279.77 12.77 o 3 1 3 261.24 256.94 3.25 o 5 1 3 399.37 387.87 3.76 o 7 1 3 316.79 337.12 4.40 o 9 1 3 658.60 632.33 9.10 o 11 1 3 70.80 70.89 3.82 o 13 1 3 4.68 3.26 2.33 o -16 2 3 1.46 -0.86 1.90 o -14 2 3 5.12 4.04 2.52 o -12 2 3 614.52 636.87 9.47 o -10 2 3 91.51 97.48 3.54 o -8 2 3 1226.84 1245.61 7.54 o -6 2 3 231.13 228.68 2.74 o -4 2 3 4626.42 4330.79 21.74 o -2 2 3 680.64 691.05 6.34 o 0 2 3 15490.37 14240.31 83.37 o 2 2 3 756.11 717.19 4.57 o 4 2 3 439.03 381.73 4.53 o 6 2 3 750.76 765.90 5.39 o 8 2 3 697.22 677.39 8.32 o 10 2 3 265.53 249.59 7.21 o 12 2 3 20.69 19.99 2.87 o 14 2 3 0.44 1.19 2.51 o -15 3 3 3.54 1.13 1.48 o -13 3 3 250.52 258.78 6.59 o -11 3 3 0.29 1.78 1.98 o -9 3 3 4.35 2.89 1.64 o -7 3 3 5689.63 6160.07 33.69 o -5 3 3 841.64 812.02 5.95 o -3 3 3 626.34 618.59 4.77 o -1 3 3 2145.45 2218.69 13.84 o 1 3 3 2484.09 2454.78 14.39 o 3 3 3 558.16 598.16 4.62 o 5 3 3 51.52 85.89 2.10 o 7 3 3 70.95 63.10 2.41 o 9 3 3 3.87 0.51 2.42 o 11 3 3 12.87 14.79 3.08 o 13 3 3 8.72 1.29 1.78 o -14 4 3 0.01 -0.91 2.01 o -12 4 3 7.73 7.91 3.28 o -10 4 3 15.16 12.14 2.74 o -8 4 3 0.07 0.57 1.36 o -6 4 3 5.47 14.67 1.29 o -4 4 3 45.42 40.61 1.69 o -2 4 3 978.32 1013.03 6.03 o 0 4 3 20.82 22.13 1.80 o 2 4 3 170.46 153.46 2.29 o 4 4 3 580.00 633.54 5.99 o 6 4 3 1123.70 1162.25 10.09 o 8 4 3 0.03 -1.51 2.25 o 10 4 3 68.34 79.55 4.82 o 12 4 3 23.96 25.59 3.91 o -15 5 3 0.34 0.00 1.17 o -13 5 3 71.60 47.63 4.45 o -11 5 3 2.17 1.45 1.87 o -9 5 3 33.31 42.23 3.61 o -7 5 3 207.92 185.71 3.81 o -5 5 3 401.24 370.57 3.50 o -3 5 3 63.25 67.25 1.63 o -1 5 3 4404.63 4548.50 30.16 o 1 5 3 33.36 36.82 1.72 o 3 5 3 164.81 170.36 3.11 o 5 5 3 12.22 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