#------------------------------------------------------------------------------ #$Date: 2009-11-11 20:41:08 +0200 (Wed, 11 Nov 2009) $ #$Revision: 840 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2223352.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2223352_Fobs loop_ _publ_author_name 'Gao, Zhi-Hua' 'Wang, Hao' 'He, Jing-Yu' 'Wang, Rui-Fen' _publ_section_title ; Tetrakis(\m-4-methoxybenzoato)bis[(4-methoxybenzoato)(1,10-phenanthroline)terbium(III)] ; _journal_coeditor_code CV2614 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1240 _journal_page_last m1241 _journal_volume 65 _journal_year 2009 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 109.070 _cell_angle_gamma 90.000 _cell_length_a 18.0547 _cell_length_b 15.1404 _cell_length_c 25.9539 _exptl_crystal_F_000 3168.00 _reflns_d_resolution_high 0.8406 _[local]_cod_data_source_file cv2614Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 080307b in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 702.60 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 6417.09 3153.11 126.97 o 2 0 0 11.74 -7.26 43.51 o 3 0 0 6493.43 6882.23 205.89 o 4 0 0 24070.50 24350.17 500.44 o 5 0 0 7805.67 7432.46 262.99 o 6 0 0 17640.32 19754.12 478.65 o 7 0 0 7647.25 6009.13 261.93 o 8 0 0 3115.68 3136.43 286.34 o 9 0 0 120477.48 124633.71 2119.13 o 10 0 0 248.39 -11.69 125.55 o 11 0 0 18592.93 19813.61 585.95 o 12 0 0 31396.75 33431.32 837.91 o 13 0 0 20071.46 21708.90 1046.03 o 14 0 0 68.69 -219.94 264.03 o 15 0 0 239.63 -129.62 293.78 o 16 0 0 31133.88 31981.09 1402.49 o 17 0 0 2032.87 2383.28 557.86 o 18 0 0 278.47 -46.75 328.86 o 19 0 0 84.11 -502.83 335.22 o 20 0 0 8273.45 9191.64 852.12 o 1 1 0 55466.95 59248.39 937.93 o 2 1 0 245.01 179.06 34.31 o 3 1 0 4885.17 5636.28 158.23 o 4 1 0 16221.73 15852.63 257.53 o 5 1 0 4912.11 4392.21 145.33 o 6 1 0 216.62 28.15 63.88 o 7 1 0 1805.95 1692.54 171.39 o 8 1 0 10365.15 10300.98 262.91 o 9 1 0 632.53 257.14 102.61 o 10 1 0 338.97 376.53 105.89 o 11 1 0 4463.18 4263.07 205.64 o 12 1 0 7246.58 6924.68 261.91 o 13 1 0 1405.51 1343.42 216.08 o 14 1 0 2195.92 1750.51 364.46 o 15 1 0 2169.21 2503.21 361.40 o 16 1 0 0.41 -61.60 247.59 o 17 1 0 2364.88 2169.19 546.18 o 18 1 0 82.16 -224.91 246.23 o 19 1 0 1021.92 542.17 316.99 o 20 1 0 850.72 1178.72 380.94 o 0 2 0 78881.34 82778.43 1825.90 o 1 2 0 7095.84 7930.01 162.36 o 2 2 0 2054.03 2194.18 92.18 o 3 2 0 2217.66 2562.03 95.19 o 4 2 0 58285.36 58974.86 790.87 o 5 2 0 46721.18 46450.07 599.24 o 6 2 0 3085.06 2685.75 121.36 o 7 2 0 6557.19 6180.88 187.78 o 8 2 0 2363.69 2802.67 166.72 o 9 2 0 37621.32 34081.25 855.74 o 10 2 0 7368.33 6729.45 230.16 o 11 2 0 26503.29 24978.26 481.92 o 12 2 0 2172.04 1762.10 225.07 o 13 2 0 13.76 -28.04 139.34 o 14 2 0 2760.56 2688.04 455.57 o 15 2 0 2931.60 3447.38 510.29 o 16 2 0 5532.92 6255.24 465.42 o 17 2 0 881.66 1213.39 340.82 o 18 2 0 8.75 -320.50 213.67 o 19 2 0 103.98 -61.10 271.88 o 20 2 0 3830.94 4852.91 1102.52 o 1 3 0 286505.09 291352.94 3543.27 o 2 3 0 8504.21 8691.61 203.52 o 3 3 0 5703.05 6199.09 152.59 o 4 3 0 10120.63 9296.72 238.47 o 5 3 0 59953.71 61812.83 768.42 o 6 3 0 3712.39 4307.19 149.42 o 7 3 0 5917.20 6253.14 188.46 o 8 3 0 190251.30 194502.61 3092.46 o 9 3 0 472.44 568.86 108.66 o 10 3 0 253.42 209.11 103.44 o 11 3 0 13791.98 13040.30 373.28 o 12 3 0 7337.79 6549.60 323.81 o 13 3 0 3324.49 3428.30 289.43 o 14 3 0 1100.46 947.96 213.20 o 15 3 0 11005.21 10309.74 741.36 o 16 3 0 126.51 173.14 260.32 o 17 3 0 14413.81 14960.68 910.56 o 18 3 0 80.70 -144.43 250.82 o 19 3 0 1343.41 1254.02 372.96 o 20 3 0 2821.64 2799.13 482.17 o 0 4 0 67458.55 65187.77 1569.84 o 1 4 0 47428.35 47655.11 859.46 o 2 4 0 404.44 190.04 76.67 o 3 4 0 106027.87 111121.65 2261.52 o 4 4 0 3105.32 3270.37 132.95 o 5 4 0 2935.40 3264.75 137.60 o 6 4 0 55026.14 57520.05 932.26 o 7 4 0 6683.69 6384.71 199.56 o 8 4 0 467.24 569.15 127.30 o 9 4 0 3504.15 3840.43 176.67 o 10 4 0 12470.13 12335.18 381.71 o 11 4 0 421.18 221.57 151.79 o 12 4 0 5841.26 5421.52 307.91 o 13 4 0 6212.70 6151.21 335.44 o 14 4 0 2426.42 2259.09 272.59 o 15 4 0 4360.57 3922.74 707.38 o 16 4 0 603.43 202.89 285.66 o 17 4 0 2590.29 2676.75 427.64 o 18 4 0 671.22 673.50 338.12 o 19 4 0 2994.21 3475.67 497.17 o 1 5 0 26335.30 26709.00 843.09 o 2 5 0 60897.02 64619.61 1421.89 o 3 5 0 38211.46 39279.68 1209.41 o 4 5 0 9885.62 9286.08 260.55 o 5 5 0 89.42 26.95 87.65 o 6 5 0 3068.36 2842.21 154.85 o 7 5 0 21994.00 23457.42 455.40 o 8 5 0 4558.44 4142.47 180.03 o 9 5 0 8791.67 9250.32 335.39 o 10 5 0 907.28 997.38 137.19 o 11 5 0 1228.29 1422.74 281.75 o 12 5 0 13405.96 12697.81 449.06 o 13 5 0 4601.70 4480.60 434.87 o 14 5 0 5857.24 5799.50 357.15 o 15 5 0 1291.57 1231.97 330.99 o 16 5 0 340.09 -195.00 282.10 o 17 5 0 2429.03 2610.33 435.04 o 18 5 0 3657.94 4372.27 544.56 o 19 5 0 1648.07 1878.49 436.94 o 0 6 0 120664.67 117283.48 2770.46 o 1 6 0 3762.12 3689.29 223.49 o 2 6 0 21535.86 20222.57 696.98 o 3 6 0 27538.15 28753.68 540.79 o 4 6 0 914.13 769.88 121.73 o 5 6 0 978.03 1009.88 120.13 o 6 6 0 6505.01 6100.90 212.64 o 7 6 0 17403.91 19547.64 394.65 o 8 6 0 1441.73 1678.26 338.55 o 9 6 0 16057.40 15703.51 533.38 o 10 6 0 4703.42 5344.33 244.77 o 11 6 0 749.15 380.82 167.06 o 12 6 0 2453.99 2027.92 255.83 o 13 6 0 8177.14 8723.62 403.48 o 14 6 0 483.85 608.40 208.58 o 15 6 0 503.56 277.54 221.01 o 16 6 0 6977.49 6953.19 562.63 o 17 6 0 8.33 -248.01 259.43 o 18 6 0 7.46 -240.43 269.80 o 19 6 0 2371.73 1966.42 448.05 o 1 7 0 5371.38 5132.48 313.06 o 2 7 0 156507.84 155327.69 4476.29 o 3 7 0 65818.21 70822.23 2322.77 o 4 7 0 12222.25 11289.70 334.12 o 5 7 0 35141.55 34979.20 919.53 o 6 7 0 17182.39 19461.56 404.68 o 7 7 0 44799.51 44453.25 1658.49 o 8 7 0 6192.90 6413.41 248.21 o 9 7 0 15671.97 15197.27 572.41 o 10 7 0 3325.13 2627.45 261.31 o 11 7 0 15018.07 14927.01 492.15 o 12 7 0 9.71 -184.59 154.11 o 13 7 0 4276.02 4914.21 373.78 o 14 7 0 22180.19 23315.19 685.49 o 15 7 0 870.82 685.00 258.10 o 16 7 0 628.38 109.16 276.32 o 17 7 0 2.53 -448.89 328.84 o 18 7 0 9268.03 10297.14 1132.09 o 0 8 0 47244.98 56447.70 1637.30 o 1 8 0 7015.49 6625.30 335.41 o 2 8 0 2857.82 3130.94 256.59 o 3 8 0 17122.91 17792.68 693.01 o 4 8 0 4210.79 3752.63 221.18 o 5 8 0 18596.20 17481.64 575.09 o 6 8 0 11942.82 12417.43 355.71 o 7 8 0 281.59 200.63 115.04 o 8 8 0 365.64 -146.44 103.74 o 9 8 0 5.07 -89.13 108.12 o 10 8 0 4432.22 4329.55 363.15 o 11 8 0 2854.49 2404.44 277.80 o 12 8 0 558.15 371.11 202.26 o 13 8 0 810.22 666.01 227.90 o 14 8 0 2219.45 3099.51 438.17 o 15 8 0 3460.36 3355.65 502.80 o 16 8 0 591.13 308.63 301.51 o 17 8 0 711.12 814.45 354.13 o 18 8 0 315.13 434.17 342.65 o 1 9 0 4527.27 3736.76 287.14 o 2 9 0 43842.13 44379.88 1391.87 o 3 9 0 5247.99 4936.76 312.96 o 4 9 0 1889.97 1135.61 174.99 o 5 9 0 5605.76 5327.85 271.11 o 6 9 0 8126.47 8847.75 457.12 o 7 9 0 12665.74 12090.33 782.43 o 8 9 0 613.64 114.05 125.35 o 9 9 0 6951.14 6697.29 348.54 o 10 9 0 1411.31 1359.11 284.34 o 11 9 0 5790.42 5895.56 367.92 o 12 9 0 1808.21 1865.16 289.80 o 13 9 0 1555.54 1438.28 281.16 o 14 9 0 6550.28 6924.73 431.33 o 15 9 0 2006.21 1851.55 321.78 o 16 9 0 34.10 -330.37 220.25 o 17 9 0 27.38 26.41 318.45 o 0 10 0 65.16 -12.22 218.35 o 1 10 0 37978.46 40894.91 1006.49 o 2 10 0 8218.46 8427.15 477.59 o 3 10 0 33932.90 31871.82 947.21 o 4 10 0 60.23 -217.88 150.67 o 5 10 0 9955.42 10455.04 512.16 o 6 10 0 24629.96 24364.50 594.51 o 7 10 0 2640.30 2700.39 217.93 o 8 10 0 148.33 -179.68 119.79 o 9 10 0 5.11 -214.31 165.12 o 10 10 0 29962.39 30770.41 1580.99 o 11 10 0 8955.00 7909.61 413.53 o 12 10 0 793.45 161.48 212.90 o 13 10 0 13722.66 13043.50 1129.15 o 14 10 0 5285.62 5888.32 463.78 o 15 10 0 6818.26 6800.71 432.46 o 16 10 0 32.28 -343.54 229.03 o 1 11 0 3920.60 4046.43 385.99 o 2 11 0 9308.75 10528.45 754.37 o 3 11 0 1421.25 2119.80 295.53 o 4 11 0 2459.32 2797.89 391.56 o 5 11 0 7138.01 7197.79 415.18 o 6 11 0 563.78 483.40 175.53 o 7 11 0 4259.57 4374.66 277.58 o 8 11 0 8767.18 8008.86 327.55 o 9 11 0 20.81 -90.43 185.23 o 10 11 0 2123.24 2039.77 300.15 o 11 11 0 2003.57 2508.54 326.97 o 12 11 0 157.44 -288.38 192.25 o 13 11 0 9.15 -295.97 197.31 o 14 11 0 1483.41 1887.64 320.40 o 15 11 0 372.73 291.45 242.34 o 16 11 0 7.11 -311.53 207.68 o 0 12 0 6086.87 6064.19 602.43 o 1 12 0 7071.48 7058.78 451.36 o 2 12 0 9308.66 9744.89 509.97 o 3 12 0 4072.86 4391.17 738.49 o 4 12 0 5825.90 5675.61 429.53 o 5 12 0 4475.28 5618.47 539.22 o 6 12 0 15235.22 15867.16 616.05 o 7 12 0 910.23 888.10 189.74 o 8 12 0 275.01 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2 1 170881.33 185998.14 5335.05 o 1 2 1 811.76 574.48 60.20 o 2 2 1 1765.42 1831.47 105.16 o 3 2 1 11262.58 10372.70 194.72 o 4 2 1 115878.56 118641.02 1329.37 o 5 2 1 93392.12 93667.15 1094.92 o 6 2 1 56.82 35.02 63.85 o 7 2 1 39098.42 39161.51 576.00 o 8 2 1 22053.11 20234.27 389.78 o 9 2 1 22524.23 23194.37 440.22 o 10 2 1 11293.04 11045.04 302.07 o 11 2 1 150.87 24.25 106.25 o 12 2 1 22884.81 20746.94 554.27 o 13 2 1 5872.43 5940.44 316.04 o 14 2 1 107.36 43.56 203.74 o 15 2 1 910.22 313.18 363.67 o 16 2 1 10422.01 11257.25 590.58 o 17 2 1 135.70 -209.97 238.06 o 18 2 1 161.65 -276.90 239.67 o 19 2 1 4013.11 5100.40 558.48 o -20 3 1 23.20 -109.22 310.91 o -19 3 1 50.91 -250.12 269.85 o -18 3 1 2306.88 2717.05 685.34 o -17 3 1 1635.48 2051.78 532.31 o -16 3 1 1579.33 2028.77 512.15 o -15 3 1 3675.33 4299.32 447.96 o -14 3 1 4824.96 4413.68 843.41 o -13 3 1 3323.17 2920.57 286.54 o -12 3 1 5982.58 5062.41 290.93 o -11 3 1 14173.25 12924.41 411.68 o -10 3 1 1119.61 1366.23 178.61 o -9 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