#------------------------------------------------------------------------------ #$Date: 2016-04-03 04:15:26 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181154 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/33/2223367.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2223367_Fobs loop_ _publ_author_name 'Rivera, Augusto' 'Maldonado, Mauricio' 'R\'ios-Motta, Jaime' 'Gonz\'alez-Salas, Diego' 'Dacunha-Marinho, Bruno' _publ_section_title ; 2,9-Dimethyl-6H,13H-5:12,7:14-dimethanodibenzo[d,i][1,3,6,8]tetraazecine ; _journal_coeditor_code FB2167 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2553 _journal_volume 65 _journal_year 2009 _space_group_IT_number 41 _symmetry_space_group_name_Hall 'A 2 -2ab' _symmetry_space_group_name_H-M 'A b a 2' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 9.9777 _cell_length_b 18.8351 _cell_length_c 7.6963 _exptl_crystal_F_000 624.00 _reflns_d_resolution_high 0.8003 _cod_data_source_file fb2167Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' jg06zd1n in A b a 2' _shelx_refln_list_code 4 _shelx_f_calc_maximum 155.74 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z' '-x+1/2, y+1/2, z' 'x+1/2, -y+1/2, z' 'x, y+1/2, z+1/2' '-x, -y+1/2, z+1/2' '-x+1/2, y+1, z+1/2' 'x+1/2, -y+1, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 11041.38 9958.75 117.08 o 4 0 0 5.77 2.03 3.23 o 6 0 0 100.78 111.53 7.26 o 8 0 0 121.28 139.53 9.04 o 10 0 0 2413.34 2497.76 106.18 o 12 0 0 119.55 119.23 17.57 o 0 2 0 2358.62 2143.49 26.16 o 1 2 0 3027.27 2750.60 19.21 o 2 2 0 1050.73 1021.55 8.57 o 3 2 0 999.39 842.99 8.21 o 4 2 0 587.37 614.10 7.48 o 5 2 0 164.68 161.79 4.80 o 6 2 0 513.43 534.14 9.90 o 7 2 0 6.05 -1.21 3.55 o 8 2 0 521.41 550.03 12.74 o 9 2 0 159.94 158.16 11.02 o 10 2 0 251.25 286.42 18.20 o 11 2 0 1706.93 1782.79 45.46 o 12 2 0 1.57 0.62 10.53 o 0 4 0 6671.05 6067.90 58.81 o 1 4 0 1821.06 1612.10 11.06 o 2 4 0 127.64 95.07 2.76 o 3 4 0 2290.42 2020.27 15.71 o 4 4 0 1561.61 1514.15 14.12 o 5 4 0 98.13 114.67 3.79 o 6 4 0 28.85 42.05 4.12 o 7 4 0 1119.87 1326.90 16.60 o 8 4 0 4.16 6.52 4.86 o 9 4 0 413.31 378.58 13.31 o 10 4 0 2.24 10.62 7.58 o 11 4 0 60.51 65.28 11.74 o 12 4 0 215.16 254.53 24.91 o 0 6 0 3367.27 2996.71 29.94 o 1 6 0 1199.04 1118.70 9.05 o 2 6 0 350.77 289.41 4.20 o 3 6 0 563.02 478.53 6.12 o 4 6 0 1667.83 1699.55 15.54 o 5 6 0 947.99 991.17 10.85 o 6 6 0 1681.88 1788.64 17.21 o 7 6 0 468.88 413.99 8.67 o 8 6 0 134.87 134.01 6.84 o 9 6 0 20.39 25.81 7.27 o 10 6 0 55.33 36.71 9.08 o 11 6 0 216.25 239.59 21.00 o 12 6 0 42.08 53.33 13.41 o 0 8 0 0.68 6.27 2.34 o 1 8 0 1491.74 1349.41 10.65 o 2 8 0 658.65 664.32 6.71 o 3 8 0 469.92 589.78 6.78 o 4 8 0 199.05 215.32 4.86 o 5 8 0 18.54 16.78 3.74 o 6 8 0 545.77 530.43 10.11 o 7 8 0 193.24 211.24 8.07 o 8 8 0 844.29 873.12 16.66 o 9 8 0 34.36 38.98 9.34 o 10 8 0 108.72 94.64 11.67 o 11 8 0 0.44 3.91 10.91 o 0 10 0 1540.76 1583.87 21.30 o 1 10 0 2040.83 2061.20 17.35 o 2 10 0 1796.61 1758.42 16.66 o 3 10 0 1203.75 1290.40 14.84 o 4 10 0 175.05 188.95 6.51 o 5 10 0 311.72 305.86 7.39 o 6 10 0 510.17 507.54 11.51 o 7 10 0 210.01 177.98 8.58 o 8 10 0 1138.82 1059.01 34.92 o 9 10 0 244.67 236.85 15.45 o 10 10 0 293.56 303.32 17.71 o 11 10 0 197.57 196.89 20.78 o 0 12 0 34.71 35.42 5.03 o 1 12 0 269.64 215.60 5.44 o 2 12 0 761.93 760.64 9.96 o 3 12 0 800.00 828.94 11.31 o 4 12 0 39.87 35.37 4.58 o 5 12 0 2.95 9.31 4.59 o 6 12 0 3.80 -2.04 6.16 o 7 12 0 63.80 74.89 8.88 o 8 12 0 1253.23 1200.36 25.99 o 9 12 0 919.71 883.54 28.40 o 10 12 0 69.00 89.85 13.77 o 0 14 0 125.71 136.06 7.23 o 1 14 0 1073.04 1002.28 12.71 o 2 14 0 1005.87 1008.69 12.99 o 3 14 0 4037.09 3903.05 37.61 o 4 14 0 96.98 97.51 6.19 o 5 14 0 30.41 37.83 5.86 o 6 14 0 67.89 70.35 6.61 o 7 14 0 1209.39 1230.59 27.38 o 8 14 0 286.47 277.79 15.80 o 9 14 0 164.02 160.83 21.60 o 10 14 0 119.95 111.79 17.39 o 0 16 0 2.07 2.58 5.47 o 1 16 0 402.70 392.35 9.57 o 2 16 0 1909.88 1788.17 22.75 o 3 16 0 80.55 91.93 6.54 o 4 16 0 1154.68 1071.96 17.03 o 5 16 0 104.80 100.79 7.59 o 6 16 0 73.50 72.57 7.92 o 7 16 0 0.34 -5.77 9.87 o 8 16 0 5.70 19.89 12.80 o 9 16 0 72.48 96.65 17.20 o 0 18 0 5.09 -6.86 6.86 o 1 18 0 36.93 44.40 6.85 o 2 18 0 983.59 937.38 17.57 o 3 18 0 144.07 159.05 8.84 o 4 18 0 894.90 892.76 18.80 o 5 18 0 14.50 8.39 6.80 o 6 18 0 63.18 66.65 8.97 o 7 18 0 32.79 57.94 12.57 o 8 18 0 20.80 12.23 18.87 o 0 20 0 15.90 2.52 7.86 o 1 20 0 5.71 9.58 5.61 o 2 20 0 69.13 83.93 7.35 o 3 20 0 31.78 11.26 6.87 o 4 20 0 212.30 231.45 11.80 o 5 20 0 37.51 38.24 9.78 o 6 20 0 42.56 34.71 12.16 o 0 22 0 204.09 281.81 13.94 o 1 22 0 13.70 12.68 6.79 o 2 22 0 193.81 199.73 9.65 o 3 22 0 50.60 65.09 8.23 o 4 22 0 41.43 50.19 10.38 o 1 1 1 20720.38 19871.30 94.15 o 2 1 1 10752.86 10242.58 47.54 o 3 1 1 5137.86 5006.93 25.00 o 4 1 1 1066.45 1050.14 7.20 o 5 1 1 185.20 183.53 3.45 o 6 1 1 189.84 198.16 4.38 o 7 1 1 221.00 244.37 4.84 o 8 1 1 411.90 435.23 6.69 o 9 1 1 360.22 370.80 10.81 o 10 1 1 71.23 87.80 8.05 o 11 1 1 96.28 81.11 8.37 o 12 1 1 427.22 431.87 17.84 o 1 3 1 210.68 198.44 2.33 o 2 3 1 4705.39 4583.31 22.96 o 3 3 1 1716.19 1716.66 9.97 o 4 3 1 860.13 889.92 6.92 o 5 3 1 2420.19 2546.88 16.31 o 6 3 1 473.03 494.72 6.10 o 7 3 1 1451.23 1451.12 11.82 o 8 3 1 407.51 394.23 6.64 o 9 3 1 627.76 605.02 12.93 o 10 3 1 1092.70 1068.26 20.42 o 11 3 1 18.57 14.14 7.02 o 12 3 1 38.52 35.41 8.12 o 1 5 1 584.64 539.60 4.22 o 2 5 1 1082.29 1044.40 6.82 o 3 5 1 1408.40 1470.53 8.55 o 4 5 1 941.97 969.07 8.38 o 5 5 1 649.96 681.85 6.37 o 6 5 1 1372.27 1421.09 11.61 o 7 5 1 85.25 86.07 3.71 o 8 5 1 167.80 204.20 6.04 o 9 5 1 13.92 7.73 5.60 o 10 5 1 145.77 154.70 9.30 o 11 5 1 41.87 36.18 7.49 o 12 5 1 53.08 60.15 9.60 o 1 7 1 957.75 1056.78 7.27 o 2 7 1 1299.53 1421.50 8.73 o 3 7 1 93.39 114.18 2.71 o 4 7 1 8.57 28.03 2.23 o 5 7 1 238.29 283.19 4.50 o 6 7 1 24.62 22.17 3.03 o 7 7 1 206.36 200.63 5.80 o 8 7 1 62.67 63.47 5.04 o 9 7 1 7.55 2.79 5.30 o 10 7 1 32.81 33.46 6.51 o 11 7 1 47.30 41.41 8.47 o 1 9 1 1274.10 1392.85 8.88 o 2 9 1 734.81 710.27 6.03 o 3 9 1 143.11 144.29 3.46 o 4 9 1 11.69 15.71 2.39 o 5 9 1 49.54 65.65 3.25 o 6 9 1 7.78 3.87 3.28 o 7 9 1 60.94 61.94 4.50 o 8 9 1 135.11 140.71 6.29 o 9 9 1 302.36 294.48 10.30 o 10 9 1 138.19 141.61 9.20 o 11 9 1 32.38 29.04 8.56 o 1 11 1 261.16 253.73 3.61 o 2 11 1 465.62 491.37 5.52 o 3 11 1 956.85 916.58 8.20 o 4 11 1 632.47 650.27 7.08 o 5 11 1 1499.75 1447.15 12.58 o 6 11 1 320.22 341.33 7.43 o 7 11 1 1404.72 1248.89 15.15 o 8 11 1 29.25 19.93 5.29 o 9 11 1 341.24 340.17 13.49 o 10 11 1 200.41 187.02 15.91 o 1 13 1 7.31 6.37 2.33 o 2 13 1 427.31 403.55 5.43 o 3 13 1 202.15 201.58 4.39 o 4 13 1 1776.29 1769.58 15.22 o 5 13 1 1252.69 1194.30 12.59 o 6 13 1 1374.55 1322.77 14.15 o 7 13 1 692.15 658.50 13.28 o 8 13 1 18.55 18.85 6.20 o 9 13 1 111.09 109.19 9.92 o 10 13 1 296.60 249.37 13.75 o 1 15 1 734.85 740.92 7.44 o 2 15 1 921.74 926.04 8.52 o 3 15 1 75.08 67.59 4.05 o 4 15 1 217.32 210.15 6.44 o 5 15 1 419.91 419.27 7.95 o 6 15 1 35.43 40.92 5.03 o 7 15 1 210.11 209.29 10.58 o 8 15 1 306.02 308.17 13.00 o 9 15 1 40.83 27.56 9.38 o 1 17 1 949.93 866.29 9.37 o 2 17 1 33.02 21.50 3.82 o 3 17 1 1910.37 1809.26 17.69 o 4 17 1 75.59 79.19 5.27 o 5 17 1 40.41 35.79 5.02 o 6 17 1 54.33 59.44 6.63 o 7 17 1 20.98 26.16 7.39 o 8 17 1 24.09 30.13 11.53 o 1 19 1 68.44 73.56 4.72 o 2 19 1 18.45 13.88 4.48 o 3 19 1 136.95 155.28 7.76 o 4 19 1 94.36 110.26 6.34 o 5 19 1 224.77 239.13 8.64 o 6 19 1 23.26 17.90 7.52 o 7 19 1 202.12 197.96 19.18 o 1 21 1 1.23 -1.16 4.69 o 2 21 1 78.06 83.89 5.97 o 3 21 1 38.67 41.95 5.78 o 4 21 1 234.95 237.51 8.93 o 5 21 1 71.38 67.47 8.41 o 1 23 1 14.82 19.25 6.20 o 2 23 1 280.30 341.07 11.02 o 0 0 2 13307.19 12997.08 138.04 o 2 0 2 24255.63 24509.90 171.94 o 4 0 2 3054.40 3177.28 25.43 o 6 0 2 200.37 227.33 7.87 o 8 0 2 168.11 165.41 7.26 o 10 0 2 127.89 118.82 11.96 o 12 0 2 1575.15 1708.14 46.04 o 0 2 2 5247.45 5178.33 43.50 o 1 2 2 7625.27 7403.85 40.99 o 2 2 2 4020.75 3912.01 20.41 o 3 2 2 1434.25 1534.85 10.84 o 4 2 2 2668.16 2683.42 15.28 o 5 2 2 68.59 69.58 2.61 o 6 2 2 42.70 39.12 2.93 o 7 2 2 179.26 183.05 4.98 o 8 2 2 1043.44 1063.01 10.44 o 9 2 2 669.70 669.76 19.33 o 10 2 2 557.99 599.19 15.55 o 11 2 2 268.45 263.75 11.42 o 12 2 2 3.46 -3.48 7.38 o 0 4 2 201.78 224.51 14.20 o 1 4 2 1132.10 1089.06 8.43 o 2 4 2 5717.51 5549.56 31.23 o 3 4 2 2797.69 3083.63 17.21 o 4 4 2 1237.74 1247.03 9.02 o 5 4 2 87.44 103.16 3.24 o 6 4 2 813.73 808.86 7.96 o 7 4 2 540.55 554.89 8.13 o 8 4 2 990.54 962.77 11.68 o 9 4 2 273.25 314.21 9.96 o 10 4 2 79.30 88.94 8.26 o 11 4 2 26.72 24.54 8.70 o 12 4 2 5.97 1.32 9.65 o 0 6 2 3648.62 3866.38 40.08 o 1 6 2 735.75 713.01 7.36 o 2 6 2 1540.87 1634.01 12.69 o 3 6 2 2817.71 2892.95 17.87 o 4 6 2 361.79 428.78 6.04 o 5 6 2 357.18 328.83 5.08 o 6 6 2 150.14 159.24 4.95 o 7 6 2 87.10 89.91 4.24 o 8 6 2 476.11 487.14 8.96 o 9 6 2 161.06 170.49 8.03 o 10 6 2 316.68 324.64 12.17 o 11 6 2 65.55 76.26 9.82 o 0 8 2 6060.97 6208.86 98.96 o 1 8 2 3350.67 3543.47 26.34 o 2 8 2 700.24 733.94 9.07 o 3 8 2 665.59 737.79 9.66 o 4 8 2 179.82 197.04 4.30 o 5 8 2 212.11 229.43 4.83 o 6 8 2 428.87 420.28 6.38 o 7 8 2 36.40 41.83 3.96 o 8 8 2 71.63 74.08 5.52 o 9 8 2 26.37 24.38 6.53 o 10 8 2 61.51 51.29 9.28 o 11 8 2 73.74 70.51 9.08 o 0 10 2 11.71 20.95 3.63 o 1 10 2 245.54 262.42 5.03 o 2 10 2 122.54 128.09 4.08 o 3 10 2 640.17 569.99 7.86 o 4 10 2 1091.83 1095.30 9.79 o 5 10 2 440.60 431.52 6.84 o 6 10 2 259.19 254.20 5.61 o 7 10 2 32.36 23.82 4.06 o 8 10 2 6.60 5.48 5.17 o 9 10 2 91.80 88.52 8.45 o 10 10 2 30.11 32.81 7.76 o 0 12 2 424.93 427.21 10.15 o 1 12 2 288.53 279.69 5.05 o 2 12 2 232.30 241.00 4.31 o 3 12 2 963.13 903.52 9.08 o 4 12 2 495.87 512.41 7.31 o 5 12 2 482.49 474.97 7.99 o 6 12 2 949.32 998.36 19.88 o 7 12 2 1100.45 1006.01 17.08 o 8 12 2 31.76 22.91 5.94 o 9 12 2 205.39 187.20 10.52 o 10 12 2 83.62 79.39 10.11 o 0 14 2 2199.43 2095.79 25.65 o 1 14 2 22.39 19.73 2.95 o 2 14 2 582.31 565.11 8.67 o 3 14 2 344.78 318.73 5.95 o 4 14 2 849.14 819.11 9.88 o 5 14 2 630.17 595.61 9.49 o 6 14 2 725.48 707.24 11.89 o 7 14 2 341.23 342.00 10.10 o 8 14 2 210.96 181.33 8.65 o 9 14 2 585.29 580.87 16.52 o 0 16 2 3898.04 3743.84 44.00 o 1 16 2 728.68 729.55 13.91 o 2 16 2 244.34 231.52 6.29 o 3 16 2 190.25 204.40 5.87 o 4 16 2 91.83 92.67 5.16 o 5 16 2 44.18 48.51 5.38 o 6 16 2 332.11 316.82 9.75 o 7 16 2 22.86 23.16 9.91 o 8 16 2 7.68 14.25 7.39 o 0 18 2 1070.21 988.86 16.09 o 1 18 2 85.55 91.27 4.86 o 2 18 2 25.10 17.74 4.40 o 3 18 2 46.96 50.98 5.23 o 4 18 2 14.70 16.86 4.90 o 5 18 2 3.96 3.95 5.29 o 6 18 2 78.17 71.72 7.43 o 7 18 2 19.85 27.75 7.51 o 0 20 2 201.02 201.95 10.65 o 1 20 2 25.68 22.15 5.21 o 2 20 2 55.49 37.11 5.90 o 3 20 2 100.45 112.12 7.21 o 4 20 2 173.35 182.80 8.77 o 5 20 2 3.71 9.22 6.15 o 6 20 2 209.20 206.60 10.66 o 0 22 2 147.63 149.26 11.29 o 1 22 2 103.31 111.21 9.61 o 2 22 2 74.10 110.92 10.46 o 3 22 2 185.13 214.73 10.00 o 1 1 3 513.71 555.68 4.90 o 2 1 3 80.54 109.95 2.42 o 3 1 3 4398.43 4511.74 25.43 o 4 1 3 2355.40 2468.49 15.11 o 5 1 3 528.04 619.00 6.15 o 6 1 3 87.10 94.89 3.54 o 7 1 3 47.15 49.74 3.94 o 8 1 3 37.15 38.39 4.69 o 9 1 3 363.26 332.92 11.05 o 10 1 3 8.38 9.08 6.84 o 11 1 3 71.19 84.02 9.02 o 1 3 3 690.14 705.12 6.36 o 2 3 3 3408.13 3576.98 22.33 o 3 3 3 1299.42 1326.07 9.17 o 4 3 3 2700.69 2926.61 18.79 o 5 3 3 1249.85 1164.02 9.98 o 6 3 3 694.12 663.05 8.25 o 7 3 3 1555.35 1553.12 14.44 o 8 3 3 619.67 583.77 10.87 o 9 3 3 286.39 299.32 12.28 o 10 3 3 15.02 18.15 6.90 o 11 3 3 2.50 4.28 7.90 o 1 5 3 696.87 748.97 7.69 o 2 5 3 454.31 435.22 5.34 o 3 5 3 914.17 900.09 8.51 o 4 5 3 968.15 1087.55 9.47 o 5 5 3 84.66 82.95 3.44 o 6 5 3 282.78 304.75 7.33 o 7 5 3 914.34 838.35 9.84 o 8 5 3 558.92 508.62 11.72 o 9 5 3 598.16 547.86 13.43 o 10 5 3 21.72 25.84 7.90 o 11 5 3 21.70 18.13 9.25 o 1 7 3 536.90 631.71 10.30 o 2 7 3 1805.83 1926.81 15.75 o 3 7 3 323.94 336.74 4.98 o 4 7 3 149.34 155.07 4.11 o 5 7 3 161.16 155.65 4.39 o 6 7 3 201.97 191.91 5.06 o 7 7 3 45.81 34.83 4.35 o 8 7 3 46.63 38.02 4.77 o 9 7 3 421.52 394.41 12.03 o 10 7 3 49.81 33.62 8.95 o 11 7 3 19.15 24.07 12.45 o 1 9 3 676.67 753.16 9.16 o 2 9 3 971.95 1034.64 10.98 o 3 9 3 188.90 189.06 4.79 o 4 9 3 758.11 715.44 10.57 o 5 9 3 2.66 4.28 3.14 o 6 9 3 105.98 110.48 5.52 o 7 9 3 213.55 208.72 7.43 o 8 9 3 17.58 4.08 5.49 o 9 9 3 3.71 -2.01 6.28 o 10 9 3 12.50 15.50 10.56 o 1 11 3 383.36 394.33 7.27 o 2 11 3 865.98 890.89 14.17 o 3 11 3 142.92 129.46 3.75 o 4 11 3 473.15 484.85 10.43 o 5 11 3 3179.84 3035.98 23.21 o 6 11 3 433.12 441.48 9.22 o 7 11 3 568.74 573.67 12.30 o 8 11 3 35.31 34.83 7.04 o 9 11 3 12.61 1.36 7.77 o 10 11 3 69.22 95.52 12.05 o 1 13 3 121.38 138.91 5.20 o 2 13 3 468.47 442.85 9.45 o 3 13 3 112.59 97.75 4.20 o 4 13 3 42.56 54.91 3.94 o 5 13 3 1282.81 1156.68 15.95 o 6 13 3 1267.19 1145.15 21.72 o 7 13 3 229.50 249.78 10.15 o 8 13 3 17.35 13.53 7.76 o 9 13 3 66.80 79.04 11.78 o 1 15 3 470.34 498.08 8.78 o 2 15 3 840.73 769.09 17.07 o 3 15 3 49.97 47.01 4.52 o 4 15 3 60.60 61.91 5.05 o 5 15 3 182.92 183.30 7.20 o 6 15 3 15.98 12.25 5.40 o 7 15 3 74.40 71.68 6.95 o 8 15 3 17.12 12.67 7.64 o 1 17 3 1890.01 1758.12 20.23 o 2 17 3 345.37 383.93 10.12 o 3 17 3 31.47 29.00 4.84 o 4 17 3 36.64 32.65 5.46 o 5 17 3 83.51 88.53 6.07 o 6 17 3 17.07 14.79 5.62 o 7 17 3 34.75 33.82 7.18 o 1 19 3 91.01 92.28 6.05 o 2 19 3 61.25 58.12 6.00 o 3 19 3 26.45 29.16 5.47 o 4 19 3 24.19 16.88 5.78 o 5 19 3 155.54 183.58 9.41 o 6 19 3 164.70 174.56 10.25 o 1 21 3 0.21 -2.04 5.63 o 2 21 3 76.23 74.06 7.01 o 3 21 3 7.68 -3.81 5.92 o 4 21 3 11.41 23.92 6.71 o 0 0 4 4563.25 4667.17 56.95 o 2 0 4 2092.58 2283.88 21.82 o 4 0 4 422.79 411.51 7.91 o 6 0 4 1219.18 1135.91 17.90 o 8 0 4 149.90 151.18 11.54 o 10 0 4 137.87 157.73 17.14 o 0 2 4 404.30 413.54 7.27 o 1 2 4 396.62 439.91 7.77 o 2 2 4 702.60 772.97 7.83 o 3 2 4 845.02 772.43 7.48 o 4 2 4 1885.24 1969.12 14.91 o 5 2 4 502.11 540.50 7.34 o 6 2 4 1437.35 1402.84 13.51 o 7 2 4 276.39 294.40 7.62 o 8 2 4 77.19 82.02 6.66 o 9 2 4 156.96 152.67 9.82 o 10 2 4 81.76 92.30 9.21 o 11 2 4 213.93 228.67 17.22 o 0 4 4 610.36 585.60 10.33 o 1 4 4 215.91 213.04 4.15 o 2 4 4 29.71 38.42 2.72 o 3 4 4 270.12 291.78 7.52 o 4 4 4 2257.33 2190.61 16.60 o 5 4 4 758.42 774.62 9.01 o 6 4 4 1358.48 1384.10 12.60 o 7 4 4 455.70 453.67 12.57 o 8 4 4 102.45 103.12 6.63 o 9 4 4 53.00 55.72 7.83 o 10 4 4 131.91 143.14 12.85 o 11 4 4 5.18 -1.21 8.71 o 0 6 4 525.78 507.13 11.81 o 1 6 4 49.67 39.73 2.62 o 2 6 4 166.34 182.12 4.05 o 3 6 4 497.22 468.87 7.32 o 4 6 4 223.84 223.50 6.81 o 5 6 4 888.36 820.56 11.24 o 6 6 4 23.47 19.53 3.81 o 7 6 4 355.88 307.75 8.64 o 8 6 4 97.81 93.42 7.14 o 9 6 4 519.79 485.13 21.56 o 10 6 4 123.16 108.23 10.97 o 0 8 4 2399.83 2409.81 35.45 o 1 8 4 1576.86 1635.82 20.86 o 2 8 4 2584.63 2557.34 24.47 o 3 8 4 31.51 34.55 2.80 o 4 8 4 265.35 279.23 5.60 o 5 8 4 454.50 426.77 6.79 o 6 8 4 3.56 0.29 4.04 o 7 8 4 13.14 8.69 4.88 o 8 8 4 6.12 0.28 5.64 o 9 8 4 23.72 21.77 8.23 o 10 8 4 94.43 103.02 12.04 o 0 10 4 331.37 362.73 13.01 o 1 10 4 1046.83 1048.83 15.50 o 2 10 4 232.00 256.96 6.91 o 3 10 4 1005.43 938.79 14.18 o 4 10 4 853.01 874.28 13.77 o 5 10 4 148.59 139.78 6.22 o 6 10 4 78.88 86.78 6.59 o 7 10 4 199.34 187.17 8.06 o 8 10 4 47.09 41.20 7.08 o 9 10 4 57.61 64.43 9.47 o 10 10 4 90.21 114.44 14.56 o 0 12 4 34.92 35.80 6.31 o 1 12 4 156.79 155.37 6.66 o 2 12 4 281.26 296.71 6.66 o 3 12 4 788.39 697.49 11.61 o 4 12 4 70.57 65.70 4.57 o 5 12 4 114.49 133.05 6.95 o 6 12 4 122.47 146.66 8.19 o 7 12 4 455.61 416.43 11.70 o 8 12 4 198.14 201.78 10.51 o 9 12 4 218.00 234.04 13.37 o 0 14 4 587.57 545.03 16.92 o 1 14 4 439.23 415.94 20.15 o 2 14 4 976.43 888.56 14.45 o 3 14 4 645.03 607.38 13.58 o 4 14 4 344.09 310.82 12.20 o 5 14 4 15.96 21.71 5.59 o 6 14 4 159.97 149.21 7.46 o 7 14 4 37.68 27.86 6.06 o 8 14 4 515.65 524.13 14.79 o 0 16 4 789.91 875.60 32.73 o 1 16 4 509.95 512.49 22.15 o 2 16 4 28.20 32.32 5.80 o 3 16 4 140.40 138.17 8.27 o 4 16 4 57.51 47.40 5.46 o 5 16 4 39.91 33.17 5.75 o 6 16 4 35.43 31.51 5.46 o 7 16 4 18.83 20.83 6.77 o 0 18 4 278.55 290.02 21.86 o 1 18 4 295.72 302.84 12.09 o 2 18 4 123.74 145.70 10.44 o 3 18 4 86.99 91.06 6.18 o 4 18 4 31.61 40.95 5.68 o 5 18 4 19.11 31.33 6.29 o 6 18 4 7.70 -0.08 6.06 o 0 20 4 112.82 91.42 15.25 o 1 20 4 57.86 68.33 7.36 o 2 20 4 201.35 202.08 10.48 o 3 20 4 132.46 152.02 9.61 o 4 20 4 127.40 128.97 8.21 o 1 1 5 265.08 313.82 6.61 o 2 1 5 805.05 841.26 10.89 o 3 1 5 0.72 -2.89 3.22 o 4 1 5 337.57 355.13 6.84 o 5 1 5 246.01 252.18 6.77 o 6 1 5 104.51 114.67 5.61 o 7 1 5 247.75 221.54 9.32 o 8 1 5 60.39 78.80 7.60 o 9 1 5 262.04 282.35 12.90 o 10 1 5 4.86 -1.68 8.58 o 1 3 5 134.38 165.33 4.55 o 2 3 5 19.87 20.59 3.16 o 3 3 5 159.98 172.87 6.08 o 4 3 5 467.22 499.07 9.10 o 5 3 5 2761.98 2735.71 21.85 o 6 3 5 967.62 961.15 13.74 o 7 3 5 557.17 491.46 12.30 o 8 3 5 162.08 168.02 11.84 o 9 3 5 111.05 101.10 11.06 o 10 3 5 103.29 105.95 11.97 o 1 5 5 324.41 331.06 5.79 o 2 5 5 405.83 430.74 6.57 o 3 5 5 518.03 533.50 7.18 o 4 5 5 832.57 852.97 9.48 o 5 5 5 2594.55 2449.11 25.21 o 6 5 5 525.11 501.63 9.80 o 7 5 5 19.20 24.28 5.88 o 8 5 5 175.55 147.67 9.59 o 9 5 5 68.17 48.74 9.91 o 10 5 5 59.82 81.24 14.72 o 1 7 5 528.58 529.66 7.85 o 2 7 5 491.29 497.88 6.86 o 3 7 5 601.90 621.95 14.32 o 4 7 5 80.20 75.85 6.43 o 5 7 5 165.89 180.82 8.20 o 6 7 5 256.06 229.24 8.53 o 7 7 5 139.10 153.59 7.96 o 8 7 5 46.23 30.70 6.80 o 9 7 5 26.46 32.02 8.58 o 1 9 5 1173.35 1213.44 16.17 o 2 9 5 1467.61 1481.02 23.45 o 3 9 5 1026.11 997.53 13.73 o 4 9 5 580.44 532.96 17.67 o 5 9 5 212.38 186.14 7.98 o 6 9 5 75.99 80.22 6.39 o 7 9 5 25.29 29.92 5.94 o 8 9 5 274.28 304.88 17.85 o 9 9 5 28.67 11.73 10.39 o 1 11 5 159.28 170.73 19.78 o 2 11 5 732.91 713.44 24.71 o 3 11 5 24.22 29.20 5.70 o 4 11 5 53.06 62.11 5.01 o 5 11 5 60.00 54.65 5.65 o 6 11 5 156.97 164.01 8.21 o 7 11 5 536.50 523.48 17.72 o 8 11 5 198.08 242.88 11.61 o 1 13 5 9.48 13.18 9.50 o 2 13 5 371.91 327.55 14.71 o 3 13 5 776.68 698.95 23.23 o 4 13 5 322.02 305.08 10.58 o 5 13 5 186.90 171.34 7.52 o 6 13 5 131.51 131.37 7.32 o 7 13 5 413.21 427.15 12.61 o 8 13 5 56.41 40.77 8.91 o 1 15 5 280.41 276.00 15.44 o 2 15 5 191.34 173.18 10.50 o 3 15 5 439.12 416.40 12.04 o 4 15 5 110.72 104.34 7.44 o 5 15 5 52.50 50.87 6.18 o 6 15 5 114.69 100.69 7.61 o 7 15 5 91.00 94.35 7.99 o 1 17 5 47.76 51.81 15.27 o 2 17 5 142.02 149.82 9.86 o 3 17 5 51.71 43.10 6.92 o 4 17 5 240.08 230.44 10.58 o 5 17 5 11.16 11.64 5.74 o 1 19 5 113.40 142.52 17.66 o 2 19 5 390.83 396.74 14.81 o 3 19 5 477.99 583.16 34.98 o 0 0 6 1528.45 1613.72 37.38 o 2 0 6 631.54 650.60 15.80 o 4 0 6 259.44 249.36 13.47 o 6 0 6 35.08 26.15 7.10 o 8 0 6 391.09 440.03 27.98 o 0 2 6 697.70 703.12 20.79 o 1 2 6 393.13 418.36 8.98 o 2 2 6 147.68 163.33 6.27 o 3 2 6 107.26 111.22 5.23 o 4 2 6 182.21 181.94 6.42 o 5 2 6 184.00 171.44 6.50 o 6 2 6 385.24 345.85 9.05 o 7 2 6 52.39 40.58 7.18 o 8 2 6 393.90 415.71 18.78 o 9 2 6 93.99 138.00 12.28 o 0 4 6 105.39 111.79 7.30 o 1 4 6 42.69 38.94 4.22 o 2 4 6 50.70 55.05 4.53 o 3 4 6 183.52 207.48 6.19 o 4 4 6 1083.10 963.21 12.87 o 5 4 6 46.17 51.74 5.73 o 6 4 6 310.29 298.62 9.97 o 7 4 6 180.46 176.81 12.10 o 8 4 6 398.29 344.70 19.80 o 9 4 6 26.43 15.54 9.41 o 0 6 6 117.40 136.07 10.87 o 1 6 6 144.69 162.62 4.84 o 2 6 6 483.98 491.70 7.53 o 3 6 6 1430.33 1356.62 16.30 o 4 6 6 663.89 607.48 11.41 o 5 6 6 68.28 82.02 6.47 o 6 6 6 81.58 80.96 6.82 o 7 6 6 809.51 749.39 17.97 o 8 6 6 15.46 4.66 7.70 o 9 6 6 82.45 86.34 11.58 o 0 8 6 3722.34 3595.43 113.53 o 1 8 6 606.39 546.08 11.66 o 2 8 6 483.94 479.84 14.10 o 3 8 6 87.24 92.56 6.05 o 4 8 6 80.68 83.38 6.35 o 5 8 6 169.61 174.02 7.40 o 6 8 6 76.83 83.83 6.68 o 7 8 6 142.41 137.40 8.47 o 8 8 6 28.01 47.51 10.75 o 0 10 6 1105.44 1043.67 24.96 o 1 10 6 272.61 257.09 8.69 o 2 10 6 377.99 349.16 13.45 o 3 10 6 186.35 179.17 7.87 o 4 10 6 47.96 41.80 5.48 o 5 10 6 48.01 53.15 6.27 o 6 10 6 104.78 110.15 7.78 o 7 10 6 254.03 248.26 11.30 o 8 10 6 42.06 36.90 9.82 o 0 12 6 205.34 226.51 33.68 o 1 12 6 59.84 62.84 7.10 o 2 12 6 117.04 117.77 9.59 o 3 12 6 16.08 21.12 5.19 o 4 12 6 37.90 29.01 6.11 o 5 12 6 129.64 122.71 8.20 o 6 12 6 97.34 137.69 8.20 o 7 12 6 66.84 77.14 8.50 o 0 14 6 69.98 62.99 26.22 o 1 14 6 69.83 74.31 15.49 o 2 14 6 195.22 197.43 10.71 o 3 14 6 127.94 135.51 9.47 o 4 14 6 18.11 26.83 5.82 o 5 14 6 144.62 154.00 9.60 o 6 14 6 84.50 92.86 8.45 o 0 16 6 323.45 304.67 41.65 o 1 16 6 5.15 0.94 16.07 o 2 16 6 280.97 288.96 11.50 o 3 16 6 167.70 166.64 9.08 o 4 16 6 49.51 39.14 5.73 o 0 18 6 200.45 191.80 38.82 o 1 18 6 266.83 299.07 25.19 o 2 18 6 124.63 155.94 49.62 o 1 1 7 2.46 -4.29 4.29 o 2 1 7 337.12 359.39 9.16 o 3 1 7 654.01 594.49 10.73 o 4 1 7 35.41 29.15 5.16 o 5 1 7 122.71 117.06 8.73 o 6 1 7 1.44 -0.40 6.96 o 7 1 7 155.80 170.65 13.13 o 8 1 7 17.60 29.48 11.59 o 1 3 7 164.01 165.74 6.83 o 2 3 7 99.99 108.09 6.14 o 3 3 7 593.69 574.86 11.33 o 4 3 7 157.04 157.14 9.94 o 5 3 7 334.86 338.15 10.53 o 6 3 7 248.01 220.30 16.79 o 7 3 7 469.29 474.57 15.97 o 8 3 7 145.06 124.46 12.73 o 1 5 7 112.10 121.57 6.45 o 2 5 7 560.25 526.86 11.54 o 3 5 7 200.92 204.28 8.44 o 4 5 7 404.00 424.50 10.93 o 5 5 7 1209.06 1111.87 20.68 o 6 5 7 208.25 208.94 10.02 o 7 5 7 385.73 384.25 14.76 o 8 5 7 62.84 59.33 10.47 o 1 7 7 60.05 58.95 7.41 o 2 7 7 112.79 141.27 12.54 o 3 7 7 1190.32 1108.55 19.34 o 4 7 7 236.52 261.33 8.90 o 5 7 7 181.84 203.44 9.71 o 6 7 7 197.82 216.09 9.68 o 7 7 7 104.04 99.71 11.26 o 1 9 7 1725.08 1662.88 27.21 o 2 9 7 724.01 651.70 25.88 o 3 9 7 342.15 340.50 11.14 o 4 9 7 11.80 2.83 5.26 o 5 9 7 180.29 202.38 10.49 o 6 9 7 25.77 26.86 7.23 o 7 9 7 36.37 36.81 8.12 o 1 11 7 296.91 299.29 10.52 o 2 11 7 51.59 59.87 6.95 o 3 11 7 1.25 7.17 5.64 o 4 11 7 341.51 366.79 11.80 o 5 11 7 99.65 115.13 9.41 o 6 11 7 312.23 356.94 17.99 o 1 13 7 178.74 181.82 11.56 o 2 13 7 19.69 14.84 5.68 o 3 13 7 33.23 36.87 6.13 o 4 13 7 38.98 42.79 6.91 o 5 13 7 51.00 47.92 8.94 o 1 15 7 3.83 4.52 7.13 o 2 15 7 28.80 27.67 7.77 o 3 15 7 1.70 10.98 9.01 o 0 0 8 328.05 342.34 19.43 o 2 0 8 42.07 54.30 14.79 o 4 0 8 1.15 0.13 9.81 o 6 0 8 30.11 18.90 16.58 o 0 2 8 744.40 743.31 20.37 o 1 2 8 97.90 97.04 7.05 o 2 2 8 66.57 70.44 7.27 o 3 2 8 507.12 479.67 14.46 o 4 2 8 328.01 314.89 13.52 o 5 2 8 12.19 17.37 8.61 o 6 2 8 6.21 2.16 12.13 o 0 4 8 176.95 184.94 12.74 o 1 4 8 33.33 36.59 6.54 o 2 4 8 288.83 313.05 12.04 o 3 4 8 96.44 99.89 7.56 o 4 4 8 52.79 43.47 7.13 o 5 4 8 18.42 6.67 7.32 o 6 4 8 136.46 140.57 11.07 o 0 6 8 2243.57 2085.84 64.46 o 1 6 8 451.00 443.59 13.89 o 2 6 8 156.59 154.20 8.05 o 3 6 8 18.91 18.90 6.85 o 4 6 8 29.13 30.03 6.27 o 5 6 8 10.83 19.94 7.85 o 6 6 8 71.81 57.10 8.94 o 0 8 8 419.76 460.27 28.07 o 1 8 8 455.22 468.26 17.76 o 2 8 8 681.82 689.88 17.73 o 3 8 8 172.31 180.05 8.91 o 4 8 8 22.85 26.52 7.35 o 5 8 8 0.42 -6.55 6.55 o 0 10 8 588.36 607.28 23.23 o 1 10 8 2.04 3.67 6.80 o 2 10 8 75.40 87.90 9.51 o 3 10 8 55.36 50.54 7.92 o 4 10 8 5.38 -1.45 6.80 o 0 12 8 8.64 2.63 17.98 o 1 12 8 10.09 1.27 7.38 o 2 12 8 22.78 16.99 9.29 o 1 1 9 89.73 99.62 11.03 o 2 1 9 112.73 112.62 12.56 o 3 1 9 28.79 11.55 9.79 o 4 1 9 3.10 -0.83 10.07 o 1 3 9 470.03 473.45 15.95 o 2 3 9 78.46 96.04 9.73 o 3 3 9 31.13 23.58 9.05 o 4 3 9 125.82 108.59 11.63 o 1 5 9 428.92 433.29 12.89 o 2 5 9 467.75 434.81 13.85 o 3 5 9 360.33 357.43 17.27 o 1 7 9 589.87 557.54 17.89 o 2 7 9 294.86 318.34 14.59 o