#------------------------------------------------------------------------------ #$Date: 2009-11-11 20:41:08 +0200 (Wed, 11 Nov 2009) $ #$Revision: 840 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2223599.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2223599_Fobs loop_ _publ_author_name 'Harcourt, Emily M.' 'Lynch, Daniel E.' 'Hamilton, Darren G.' _publ_section_title ; Bis(2-thienyl)acetylene ; _journal_coeditor_code ZS2008 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2484 _journal_volume 65 _journal_year 2009 _space_group_IT_number 60 _symmetry_space_group_name_Hall '-P 2n 2ab' _symmetry_space_group_name_H-M 'P b c n' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 10.6325 _cell_length_b 10.8713 _cell_length_c 7.5600 _exptl_crystal_F_000 392.00 _reflns_d_resolution_high 0.8109 _[local]_cod_data_source_file zs2008Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 2006src1206 in Pbcn' _shelx_refln_list_code 4 _shelx_f_calc_maximum 139.12 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y+1/2, z+1/2' '-x, y, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y-1/2, -z-1/2' 'x, -y, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 11528.39 11931.83 346.61 o 4 0 0 3089.35 2828.93 74.25 o 6 0 0 7068.14 7353.92 213.82 o 8 0 0 3022.39 3054.08 144.02 o 10 0 0 1.88 7.43 25.05 o 12 0 0 100.22 85.24 31.58 o 1 1 0 562.41 -2.94 1.96 o 3 1 0 585.43 558.64 14.60 o 5 1 0 21.41 26.62 5.57 o 7 1 0 241.50 273.71 15.01 o 9 1 0 1685.34 1794.41 64.07 o 11 1 0 6.78 -5.25 22.58 o 13 1 0 61.45 66.87 25.86 o 0 2 0 442.44 332.53 19.33 o 2 2 0 1672.86 1670.70 83.88 o 4 2 0 2666.04 2986.49 90.48 o 6 2 0 2632.82 2746.23 62.69 o 8 2 0 59.18 39.73 7.94 o 10 2 0 40.03 31.73 20.18 o 12 2 0 1059.58 1018.79 72.29 o 1 3 0 440.93 518.51 35.41 o 3 3 0 4013.58 3819.64 285.22 o 5 3 0 2693.29 2768.79 84.75 o 7 3 0 75.25 92.11 10.82 o 9 3 0 51.20 51.40 12.81 o 11 3 0 363.18 369.68 31.09 o 0 4 0 5653.35 5454.64 177.62 o 2 4 0 1341.02 1347.85 68.91 o 4 4 0 217.83 365.35 28.50 o 6 4 0 1000.16 980.32 36.38 o 8 4 0 1841.35 2033.06 87.11 o 10 4 0 10.34 16.81 19.44 o 12 4 0 43.56 42.42 43.84 o 1 5 0 1195.63 1120.92 158.06 o 3 5 0 75.34 250.25 102.02 o 5 5 0 3.89 -3.61 7.81 o 7 5 0 46.45 -264.44 179.44 o 9 5 0 244.30 255.67 26.49 o 11 5 0 10.25 -18.33 28.10 o 0 6 0 214.05 -0.38 24.78 o 2 6 0 525.08 599.71 36.31 o 4 6 0 207.28 229.83 60.42 o 6 6 0 570.63 621.87 52.95 o 8 6 0 35.77 163.46 342.26 o 10 6 0 4.83 19.45 23.90 o 1 7 0 628.44 659.65 37.07 o 3 7 0 2896.10 2888.52 124.51 o 5 7 0 242.07 261.58 20.60 o 7 7 0 246.88 304.50 120.48 o 9 7 0 209.77 304.76 83.75 o 11 7 0 276.15 341.18 56.34 o 0 8 0 39.28 45.97 30.09 o 2 8 0 374.79 381.06 31.96 o 4 8 0 1.39 -28.97 105.54 o 6 8 0 282.02 222.83 200.66 o 10 8 0 4.97 71.32 52.36 o 1 9 0 90.05 60.10 142.56 o 3 9 0 321.52 263.80 69.11 o 5 9 0 368.90 384.66 20.53 o 7 9 0 25.17 80.47 45.06 o 9 9 0 96.47 105.87 44.36 o 0 10 0 292.30 140.49 96.26 o 2 10 0 33.90 31.20 5.82 o 4 10 0 139.76 92.64 145.43 o 6 10 0 456.47 381.70 97.08 o 8 10 0 86.68 69.75 78.91 o 1 11 0 54.12 63.28 51.04 o 3 11 0 115.10 400.99 106.79 o 5 11 0 20.95 -369.01 246.01 o 7 11 0 12.07 12.87 23.90 o 0 12 0 1157.64 1227.52 126.78 o 2 12 0 250.92 275.35 69.34 o 4 12 0 39.66 25.24 95.84 o 1 13 0 12.65 119.55 74.35 o 3 13 0 128.38 -187.06 126.71 o 1 1 1 207.27 186.26 11.78 o 2 1 1 13.10 7.73 1.75 o 3 1 1 1692.82 1515.27 28.23 o 4 1 1 517.91 492.85 10.95 o 5 1 1 992.78 951.26 17.12 o 6 1 1 138.75 142.27 7.11 o 7 1 1 22.60 17.54 4.49 o 8 1 1 366.65 361.04 11.57 o 9 1 1 650.95 654.71 20.53 o 10 1 1 428.04 395.95 16.29 o 11 1 1 220.13 205.21 24.66 o 12 1 1 0.04 8.28 15.43 o 13 1 1 5.58 10.92 19.44 o 0 2 1 5461.98 5019.18 127.81 o 1 2 1 9232.44 9995.17 225.21 o 2 2 1 631.25 669.15 32.10 o 3 2 1 252.76 236.23 8.00 o 4 2 1 535.78 547.21 12.62 o 5 2 1 671.44 744.27 16.17 o 6 2 1 761.10 767.26 16.32 o 7 2 1 313.88 312.54 10.56 o 8 2 1 124.97 113.38 7.37 o 9 2 1 10.85 8.82 6.41 o 10 2 1 8.43 3.23 11.58 o 11 2 1 4.32 -3.31 13.00 o 12 2 1 84.83 91.04 19.42 o 1 3 1 169.27 145.03 8.41 o 2 3 1 95.69 155.37 23.23 o 3 3 1 457.77 408.70 23.62 o 4 3 1 236.92 223.71 10.10 o 5 3 1 84.26 68.46 6.01 o 6 3 1 9.30 5.22 4.67 o 7 3 1 23.27 20.30 5.59 o 8 3 1 286.94 264.71 13.35 o 9 3 1 84.49 79.53 10.15 o 10 3 1 80.45 57.64 11.90 o 11 3 1 59.39 70.86 20.20 o 12 3 1 50.11 46.68 20.74 o 0 4 1 3154.17 3009.60 170.67 o 1 4 1 275.82 384.33 9.40 o 2 4 1 1045.42 1091.36 40.77 o 3 4 1 22.91 -14.78 57.23 o 4 4 1 232.28 236.82 26.21 o 5 4 1 427.60 486.24 20.73 o 6 4 1 1209.73 1325.64 34.88 o 7 4 1 3.92 6.07 8.08 o 8 4 1 423.41 464.52 19.75 o 9 4 1 12.29 18.53 8.23 o 10 4 1 2.76 7.41 10.16 o 11 4 1 67.17 50.66 20.17 o 12 4 1 180.56 206.58 41.52 o 1 5 1 164.13 161.49 21.94 o 2 5 1 508.90 486.61 16.74 o 3 5 1 198.09 140.12 24.20 o 4 5 1 462.63 605.12 37.91 o 5 5 1 9.72 4.72 5.33 o 6 5 1 277.70 327.17 31.75 o 7 5 1 12.59 2.02 12.31 o 8 5 1 378.41 348.54 18.58 o 9 5 1 18.74 16.96 15.68 o 10 5 1 20.88 13.21 16.60 o 11 5 1 6.14 18.07 20.24 o 12 5 1 1.21 -22.86 28.19 o 0 6 1 2580.84 2533.78 240.52 o 1 6 1 2232.16 2324.09 85.55 o 2 6 1 953.41 959.77 33.30 o 3 6 1 392.16 430.17 19.83 o 4 6 1 161.92 158.93 31.24 o 5 6 1 2.78 2.26 7.81 o 6 6 1 1673.49 1848.39 47.04 o 7 6 1 1580.48 1706.89 43.24 o 8 6 1 728.63 784.92 33.21 o 9 6 1 260.31 246.77 21.17 o 10 6 1 50.54 59.68 85.11 o 11 6 1 35.10 1079.44 575.27 o 1 7 1 33.30 28.02 20.13 o 2 7 1 1.73 26.44 30.41 o 3 7 1 40.07 34.28 5.90 o 4 7 1 856.95 870.09 34.79 o 5 7 1 14.23 18.20 11.12 o 6 7 1 104.88 109.13 9.38 o 7 7 1 1.49 -5.66 46.73 o 8 7 1 130.29 1244.78 371.02 o 9 7 1 1.45 6.79 16.65 o 10 7 1 0.14 445.55 459.23 o 0 8 1 1952.35 2234.37 81.87 o 1 8 1 57.57 88.87 34.97 o 2 8 1 734.91 751.76 36.24 o 3 8 1 4.63 101.83 78.62 o 4 8 1 178.61 159.10 26.64 o 5 8 1 1098.59 1159.35 55.23 o 6 8 1 1212.14 1295.53 79.83 o 7 8 1 149.95 107.92 91.38 o 8 8 1 449.62 437.28 137.14 o 10 8 1 11.42 29.36 22.64 o 1 9 1 97.18 103.45 20.98 o 2 9 1 536.92 510.51 44.09 o 3 9 1 373.38 423.49 86.79 o 4 9 1 1159.22 1090.23 76.71 o 5 9 1 66.66 13.24 100.29 o 6 9 1 0.38 11.37 18.34 o 7 9 1 21.43 -14.52 97.38 o 8 9 1 20.35 -37.27 109.65 o 9 9 1 62.82 581.15 327.37 o 0 10 1 627.86 772.22 206.68 o 1 10 1 562.51 480.63 37.76 o 2 10 1 114.72 133.36 37.63 o 3 10 1 20.21 13.33 38.47 o 4 10 1 81.58 125.99 63.45 o 5 10 1 10.99 9.09 88.20 o 7 10 1 92.76 82.28 20.92 o 8 10 1 87.06 99.07 73.48 o 1 11 1 46.35 67.60 34.18 o 2 11 1 0.15 -9.29 9.89 o 3 11 1 183.22 219.79 33.65 o 4 11 1 98.30 73.79 53.04 o 5 11 1 120.27 -6.04 106.08 o 6 11 1 29.43 643.94 361.00 o 0 12 1 124.62 202.86 87.17 o 1 12 1 1.21 -43.64 58.08 o 2 12 1 46.76 38.41 23.08 o 3 12 1 7.50 -211.62 237.13 o 4 12 1 14.88 23.92 64.95 o 5 12 1 144.46 1147.17 332.04 o 1 13 1 9.75 -73.53 53.03 o 2 13 1 10.96 -15.02 32.63 o 0 0 2 5510.19 6136.34 504.97 o 1 0 2 14520.81 15050.60 382.24 o 2 0 2 140.66 120.04 4.25 o 3 0 2 315.91 329.24 10.55 o 4 0 2 326.73 369.68 11.62 o 5 0 2 3838.72 4252.09 86.12 o 6 0 2 520.73 496.48 15.47 o 7 0 2 1967.09 1987.27 73.27 o 8 0 2 0.06 -2.16 6.91 o 9 0 2 26.08 22.05 13.39 o 10 0 2 40.64 13.19 13.52 o 11 0 2 280.03 286.39 28.38 o 12 0 2 684.20 583.60 52.48 o 1 1 2 91.19 115.74 3.51 o 2 1 2 286.07 282.49 6.35 o 3 1 2 1541.75 1603.76 32.56 o 4 1 2 606.66 611.69 12.45 o 5 1 2 308.77 347.90 8.66 o 6 1 2 256.76 249.77 9.23 o 7 1 2 118.69 123.35 6.96 o 8 1 2 100.81 87.20 6.36 o 9 1 2 657.26 591.76 17.12 o 10 1 2 156.71 146.64 14.22 o 11 1 2 19.80 20.89 10.78 o 12 1 2 0.16 14.98 17.61 o 0 2 2 19353.39 19143.44 501.01 o 1 2 2 5907.66 5543.36 116.91 o 2 2 2 1749.22 1855.61 46.83 o 3 2 2 166.59 188.22 7.54 o 4 2 2 4.65 2.08 2.99 o 5 2 2 1746.74 1734.01 33.89 o 6 2 2 1100.64 1053.13 21.99 o 7 2 2 1318.86 1320.60 29.03 o 8 2 2 1355.26 1349.74 40.82 o 9 2 2 178.68 153.85 10.76 o 10 2 2 0.45 14.27 9.38 o 11 2 2 87.21 80.55 14.57 o 12 2 2 0.05 -9.82 16.49 o 1 3 2 1475.83 1573.81 38.49 o 2 3 2 0.09 -2.07 4.59 o 3 3 2 30.25 39.43 13.02 o 4 3 2 440.68 466.78 14.53 o 5 3 2 268.92 296.97 11.13 o 6 3 2 41.52 40.06 5.40 o 7 3 2 206.03 234.21 9.86 o 8 3 2 115.24 132.70 10.25 o 9 3 2 350.48 323.65 15.55 o 10 3 2 233.47 226.50 14.99 o 11 3 2 1.93 7.51 12.72 o 12 3 2 5.18 -5.32 19.78 o 0 4 2 262.81 250.58 21.14 o 1 4 2 487.91 518.88 21.88 o 2 4 2 163.57 178.26 12.54 o 3 4 2 116.22 108.33 16.33 o 4 4 2 1112.23 1267.56 22.78 o 5 4 2 207.41 196.47 11.74 o 6 4 2 430.42 496.89 46.42 o 7 4 2 837.11 849.89 26.31 o 8 4 2 67.44 72.49 12.37 o 9 4 2 51.99 36.72 17.51 o 10 4 2 1.51 -0.66 13.36 o 11 4 2 178.24 161.74 46.77 o 12 4 2 206.80 201.64 31.46 o 1 5 2 1.82 6.84 14.53 o 2 5 2 720.64 648.58 34.33 o 3 5 2 2134.94 2254.78 73.39 o 4 5 2 287.04 295.80 13.96 o 5 5 2 838.72 867.87 25.09 o 6 5 2 28.94 32.87 7.02 o 7 5 2 11.88 8.16 8.30 o 8 5 2 30.74 41.41 9.50 o 9 5 2 131.46 145.94 30.06 o 0 6 2 136.18 97.23 14.08 o 1 6 2 415.73 422.22 21.78 o 2 6 2 45.16 58.43 6.28 o 3 6 2 34.85 19.46 22.39 o 4 6 2 39.85 37.71 10.47 o 5 6 2 204.89 216.82 42.17 o 6 6 2 33.97 36.71 31.93 o 7 6 2 211.72 216.69 13.44 o 8 6 2 26.15 27.63 14.44 o 9 6 2 20.41 26.52 12.29 o 10 6 2 1.41 -12.69 98.03 o 11 6 2 33.94 99.61 153.68 o 1 7 2 28.71 3.33 30.24 o 2 7 2 1048.37 983.19 57.10 o 3 7 2 1.62 1.81 16.82 o 4 7 2 607.24 618.09 36.45 o 5 7 2 103.39 120.81 12.25 o 6 7 2 2.67 195.06 73.72 o 7 7 2 20.48 30.51 11.57 o 8 7 2 128.83 152.88 17.86 o 9 7 2 108.65 73.14 40.54 o 10 7 2 129.86 175.23 42.40 o 0 8 2 82.16 41.90 16.54 o 1 8 2 35.89 -0.03 15.69 o 2 8 2 67.99 16.40 26.18 o 3 8 2 38.39 81.47 59.91 o 4 8 2 39.72 56.88 36.99 o 5 8 2 45.79 56.53 12.16 o 6 8 2 1.45 1.23 86.51 o 7 8 2 133.12 114.65 41.78 o 8 8 2 8.32 -4.76 23.02 o 9 8 2 4.45 8.34 22.05 o 10 8 2 5.58 38.37 309.29 o 1 9 2 19.75 35.28 42.97 o 2 9 2 67.83 77.70 39.83 o 3 9 2 104.23 -178.68 119.12 o 4 9 2 126.38 137.53 33.98 o 5 9 2 4.84 -3.93 12.55 o 6 9 2 23.51 42.06 134.33 o 7 9 2 96.02 45.73 60.11 o 8 9 2 35.54 43.97 21.50 o 9 9 2 34.53 315.36 859.85 o 1 10 2 315.84 264.33 27.53 o 2 10 2 167.87 120.71 15.13 o 3 10 2 9.24 10.25 89.60 o 4 10 2 1.61 124.55 135.64 o 5 10 2 178.27 127.34 14.24 o 6 10 2 47.48 203.39 175.16 o 7 10 2 237.58 218.54 109.16 o 8 10 2 37.70 745.40 294.71 o 1 11 2 88.73 81.82 34.68 o 2 11 2 7.89 -10.23 12.66 o 3 11 2 269.18 277.08 34.06 o 4 11 2 4.47 9.66 14.38 o 5 11 2 82.79 -261.48 251.42 o 6 11 2 19.81 1144.18 349.64 o 0 12 2 13.24 -69.07 94.62 o 1 12 2 218.94 153.41 45.97 o 2 12 2 8.89 -10.57 24.56 o 4 12 2 58.00 -31.02 53.23 o 5 12 2 126.50 305.19 244.18 o 1 13 2 20.88 31.06 31.67 o 1 1 3 139.99 129.30 4.90 o 2 1 3 1167.09 1095.86 27.63 o 3 1 3 35.89 29.32 3.15 o 4 1 3 1240.44 1160.70 21.17 o 5 1 3 74.09 89.28 5.08 o 6 1 3 62.25 64.43 5.06 o 7 1 3 21.58 18.44 4.86 o 8 1 3 88.07 100.37 8.93 o 9 1 3 28.37 21.52 8.45 o 10 1 3 180.64 187.26 12.96 o 11 1 3 1.08 13.96 10.00 o 12 1 3 61.94 50.77 17.99 o 0 2 3 1760.44 1807.15 64.38 o 1 2 3 0.29 25.51 8.64 o 2 2 3 0.00 3.87 7.71 o 3 2 3 39.11 45.89 3.27 o 4 2 3 464.36 543.93 13.38 o 5 2 3 313.27 322.78 9.06 o 6 2 3 26.17 38.69 5.44 o 7 2 3 174.36 177.25 10.36 o 8 2 3 41.91 44.13 6.12 o 9 2 3 6.24 12.74 11.56 o 10 2 3 1.71 5.50 8.29 o 11 2 3 126.04 82.44 14.99 o 12 2 3 0.69 27.20 19.45 o 1 3 3 15.78 17.92 11.00 o 2 3 3 441.19 436.01 12.73 o 3 3 3 238.99 286.02 9.27 o 4 3 3 147.04 131.00 12.24 o 5 3 3 302.23 317.12 10.66 o 6 3 3 1.10 -0.56 5.21 o 7 3 3 0.56 -3.43 6.11 o 8 3 3 698.42 710.53 28.10 o 9 3 3 244.00 240.01 14.96 o 10 3 3 480.42 468.88 25.91 o 11 3 3 24.82 22.16 13.13 o 12 3 3 1.53 8.06 18.86 o 0 4 3 150.59 178.37 13.85 o 1 4 3 6512.20 6745.46 174.09 o 2 4 3 11.05 4.41 8.85 o 3 4 3 137.60 177.42 10.95 o 4 4 3 13.82 19.96 10.27 o 5 4 3 805.12 782.73 22.39 o 6 4 3 101.79 87.24 8.89 o 7 4 3 2254.64 2322.88 97.74 o 8 4 3 32.07 25.69 8.08 o 9 4 3 236.14 208.85 22.43 o 10 4 3 41.10 18.73 25.25 o 11 4 3 84.86 78.88 19.88 o 1 5 3 273.15 262.56 9.38 o 2 5 3 10.82 7.10 6.70 o 3 5 3 132.63 144.64 22.42 o 4 5 3 820.08 838.73 22.87 o 5 5 3 4.07 10.61 8.32 o 6 5 3 132.74 145.62 9.78 o 7 5 3 2.10 10.36 15.99 o 8 5 3 106.85 111.87 52.65 o 9 5 3 5.44 848.04 364.42 o 10 5 3 0.27 2.48 14.67 o 11 5 3 0.77 -10.61 24.86 o 0 6 3 164.50 149.22 14.67 o 1 6 3 796.84 726.47 16.28 o 2 6 3 15.66 -10.68 30.45 o 3 6 3 6.34 -0.09 8.42 o 4 6 3 63.44 99.43 21.08 o 5 6 3 2111.68 2228.23 59.96 o 6 6 3 0.02 12.52 11.76 o 7 6 3 499.95 550.80 57.05 o 8 6 3 25.96 14.36 11.93 o 9 6 3 0.32 -5.25 10.95 o 10 6 3 41.09 28.47 17.53 o 1 7 3 31.66 20.61 10.62 o 2 7 3 69.11 36.75 27.28 o 3 7 3 2.98 83.66 62.76 o 4 7 3 1022.09 1013.49 39.96 o 5 7 3 7.69 7.66 25.97 o 6 7 3 122.03 105.87 28.14 o 7 7 3 12.17 -0.34 20.68 o 8 7 3 76.28 76.00 39.29 o 9 7 3 28.58 476.44 345.44 o 10 7 3 11.75 -7.05 28.81 o 0 8 3 31.75 3.35 18.35 o 1 8 3 2604.38 2538.63 72.58 o 2 8 3 74.01 -55.18 74.83 o 3 8 3 44.51 171.19 69.92 o 4 8 3 1.45 -0.16 11.01 o 5 8 3 171.95 163.35 58.98 o 6 8 3 52.23 29.61 53.22 o 7 8 3 1257.02 1308.74 64.43 o 8 8 3 13.39 677.19 414.77 o 9 8 3 172.76 164.66 120.56 o 1 9 3 18.22 8.56 66.33 o 2 9 3 15.69 100.50 107.53 o 3 9 3 53.38 33.39 52.74 o 4 9 3 70.01 27.67 78.70 o 5 9 3 31.87 13.56 16.57 o 6 9 3 9.25 122.73 62.45 o 7 9 3 52.66 13.09 63.48 o 8 9 3 153.38 749.54 186.62 o 0 10 3 0.01 17.29 26.94 o 1 10 3 177.88 280.59 24.74 o 2 10 3 62.81 68.33 12.26 o 3 10 3 33.35 37.58 32.85 o 4 10 3 7.65 -0.54 137.94 o 5 10 3 717.99 733.33 86.54 o 6 10 3 52.40 16.74 20.82 o 7 10 3 217.16 101.16 122.21 o 1 11 3 5.96 -11.50 35.43 o 2 11 3 247.54 331.25 77.09 o 3 11 3 56.48 62.26 42.99 o 4 11 3 782.45 782.86 273.69 o 5 11 3 0.09 683.50 429.81 o 6 11 3 6.22 147.28 58.34 o 0 12 3 13.19 48.60 65.88 o 1 12 3 204.35 212.86 18.07 o 2 12 3 13.43 32.58 60.16 o 3 12 3 1.83 -19.91 19.58 o 4 12 3 5.88 -26.61 78.86 o 0 0 4 264.25 343.61 28.96 o 1 0 4 1462.37 1287.95 66.33 o 2 0 4 94.20 97.47 8.48 o 3 0 4 848.13 964.58 31.96 o 4 0 4 498.53 565.56 16.83 o 5 0 4 662.46 591.00 18.05 o 6 0 4 433.55 483.57 19.44 o 7 0 4 1416.05 1463.88 56.85 o 8 0 4 11.25 0.71 7.51 o 9 0 4 360.81 361.69 23.65 o 10 0 4 19.32 6.89 15.38 o 11 0 4 112.92 114.93 21.66 o 1 1 4 117.88 126.76 4.30 o 2 1 4 5.53 8.24 3.02 o 3 1 4 515.24 572.05 15.19 o 4 1 4 70.52 75.04 3.94 o 5 1 4 341.53 374.31 9.17 o 6 1 4 246.27 260.29 9.78 o 7 1 4 87.39 82.16 10.12 o 8 1 4 19.87 16.97 7.78 o 9 1 4 227.13 197.30 13.76 o 10 1 4 37.09 29.26 9.55 o 11 1 4 22.99 9.27 13.66 o 0 2 4 5023.93 5299.40 143.86 o 1 2 4 2647.49 2715.21 75.39 o 2 2 4 533.04 598.46 14.35 o 3 2 4 11.80 16.10 5.57 o 4 2 4 5.88 11.19 5.10 o 5 2 4 1126.56 1128.79 24.01 o 6 2 4 405.31 396.75 14.04 o 7 2 4 1455.86 1486.88 41.19 o 8 2 4 716.60 722.31 24.89 o 9 2 4 19.21 -3.83 7.98 o 10 2 4 0.05 -4.42 8.64 o 11 2 4 340.47 332.22 25.38 o 1 3 4 117.08 127.90 13.97 o 2 3 4 1644.95 1724.62 35.83 o 3 3 4 204.20 223.67 7.12 o 4 3 4 394.43 385.17 10.41 o 5 3 4 59.36 59.83 6.68 o 6 3 4 22.10 19.08 9.73 o 7 3 4 27.62 6.31 30.96 o 8 3 4 58.39 60.36 9.03 o 9 3 4 228.40 198.86 16.45 o 10 3 4 38.15 33.37 11.83 o 11 3 4 2.71 11.04 22.38 o 0 4 4 17.13 9.48 8.40 o 1 4 4 2502.47 2438.06 80.44 o 2 4 4 97.48 113.30 8.66 o 3 4 4 1.57 8.64 8.61 o 4 4 4 176.59 170.14 8.64 o 5 4 4 1092.44 1190.10 35.66 o 6 4 4 266.50 261.04 23.08 o 7 4 4 279.04 291.05 19.84 o 8 4 4 1.10 -0.72 11.70 o 9 4 4 43.40 29.03 59.71 o 10 4 4 4.83 285.23 406.69 o 11 4 4 1.49 11.61 20.60 o 1 5 4 11.21 16.17 28.89 o 2 5 4 478.65 482.18 21.92 o 3 5 4 407.08 415.66 22.17 o 4 5 4 1116.49 1145.29 24.04 o 5 5 4 180.64 182.06 11.39 o 6 5 4 19.62 10.48 8.78 o 7 5 4 1.68 -6.83 14.48 o 8 5 4 362.70 415.04 21.74 o 10 5 4 492.11 481.99 50.34 o 0 6 4 167.35 -5.40 55.17 o 1 6 4 5.28 6.53 6.23 o 2 6 4 0.84 0.17 11.02 o 3 6 4 14.18 7.67 22.56 o 4 6 4 13.76 11.26 5.01 o 5 6 4 20.65 21.23 24.76 o 6 6 4 3.02 6.53 18.29 o 7 6 4 2.99 -3.93 58.27 o 8 6 4 63.29 65.47 53.28 o 9 6 4 0.01 926.80 364.31 o 10 6 4 2.63 4.91 20.46 o 1 7 4 45.47 23.33 8.11 o 2 7 4 39.17 40.33 34.10 o 3 7 4 0.71 7.34 21.98 o 4 7 4 198.20 237.62 35.59 o 5 7 4 11.47 1.76 7.51 o 6 7 4 146.25 144.55 54.74 o 7 7 4 13.79 414.09 271.44 o 8 7 4 50.00 39.01 38.62 o 9 7 4 10.37 -10.45 33.78 o 0 8 4 1.30 -21.99 14.66 o 1 8 4 62.17 21.00 18.25 o 2 8 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