#------------------------------------------------------------------------------ #$Date: 2016-04-03 04:17:27 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181157 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/36/2223600.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2223600_Fobs loop_ _publ_author_name 'Liu, Jian-Feng' 'Liu, Jia-Lu' 'Zhao, Guo-Liang' _publ_section_title ; Tris{2-methoxy-6-[(4-methylphenyl)iminiomethyl]phenolato-\k^2^O,O'}tris(thiocyanato-\kN)praseodymium(III) monohydrate ; _journal_coeditor_code AT2866 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1269 _journal_page_last m1270 _journal_volume 65 _journal_year 2009 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 105.810 _cell_angle_gamma 90.000 _cell_length_a 16.6770 _cell_length_b 14.2420 _cell_length_c 22.2021 _exptl_crystal_F_000 2160.00 _reflns_d_resolution_high 0.8409 _cod_data_source_file at2866Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' J in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 537.00 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 1800.98 1596.73 93.87 o 4 0 0 46843.00 48180.52 1754.04 o 5 0 0 2258.46 1682.57 85.63 o 6 0 0 6655.94 6828.38 321.96 o 7 0 0 40419.29 38967.36 1003.75 o 8 0 0 148.19 0.00 44.15 o 9 0 0 6526.06 5774.19 174.35 o 10 0 0 4625.88 4561.49 135.70 o 11 0 0 7673.93 7441.62 220.30 o 12 0 0 11113.39 11060.61 299.80 o 13 0 0 11.60 142.30 82.68 o 14 0 0 2141.90 2312.80 311.91 o 15 0 0 344.99 400.84 106.97 o 16 0 0 3364.32 3354.04 218.67 o 17 0 0 826.68 876.41 144.99 o 18 0 0 162.93 180.57 111.25 o 19 0 0 1204.71 1119.03 278.75 o 1 1 0 144926.22 153964.77 3170.52 o 2 1 0 14014.03 14797.58 393.06 o 3 1 0 24097.07 23371.59 613.84 o 4 1 0 6898.64 6127.54 190.37 o 5 1 0 325.70 286.79 31.48 o 6 1 0 13618.83 13002.14 229.51 o 7 1 0 342.57 247.85 39.91 o 8 1 0 20958.91 20724.45 324.51 o 9 1 0 9990.70 9597.55 173.52 o 10 1 0 4941.51 4900.99 110.38 o 11 1 0 11850.20 11358.11 232.35 o 12 1 0 62.90 8.82 48.04 o 13 1 0 12277.35 11874.36 452.94 o 14 1 0 21.36 51.28 68.95 o 15 1 0 6014.64 5942.80 225.38 o 16 1 0 431.30 536.60 96.16 o 17 1 0 1503.25 1544.94 138.98 o 18 1 0 1239.75 1329.58 141.20 o 19 1 0 13.27 86.27 97.69 o 0 2 0 43438.31 48386.64 1763.80 o 1 2 0 8290.60 8467.98 201.52 o 2 2 0 15325.83 16141.61 358.53 o 3 2 0 5990.87 6691.48 283.35 o 4 2 0 14739.99 15614.98 433.86 o 5 2 0 2103.58 2140.86 64.97 o 6 2 0 3470.02 3401.81 76.11 o 7 2 0 25468.39 25099.29 382.68 o 8 2 0 5089.58 5201.14 110.38 o 9 2 0 2760.45 2438.65 74.39 o 10 2 0 7347.35 7107.32 154.77 o 11 2 0 1515.30 1409.85 79.63 o 12 2 0 5173.54 5014.80 148.68 o 13 2 0 40.74 0.00 58.83 o 14 2 0 6096.37 6157.54 223.02 o 15 2 0 1465.96 1443.04 208.99 o 16 2 0 1637.81 2004.86 149.88 o 17 2 0 808.33 665.39 108.05 o 18 2 0 277.61 252.77 108.70 o 1 3 0 34685.82 33509.68 627.00 o 2 3 0 494.76 335.85 37.95 o 3 3 0 8596.22 8104.83 206.93 o 4 3 0 6266.24 6108.03 166.55 o 5 3 0 20732.56 20439.98 346.90 o 6 3 0 45984.80 46695.22 683.19 o 7 3 0 1926.40 2046.75 58.39 o 8 3 0 317.06 229.61 33.54 o 9 3 0 2316.14 2205.98 74.65 o 10 3 0 1763.87 1904.87 74.33 o 11 3 0 5241.53 5168.29 137.66 o 12 3 0 21.61 0.00 47.69 o 13 3 0 1232.55 1330.88 140.30 o 14 3 0 192.99 136.16 77.79 o 15 3 0 4146.09 3829.95 184.28 o 16 3 0 1923.61 1836.13 144.55 o 17 3 0 127.27 93.89 83.95 o 18 3 0 1320.19 1158.45 162.51 o 0 4 0 45720.01 48211.15 1301.04 o 1 4 0 15770.48 17483.75 408.80 o 2 4 0 77445.74 75124.52 1207.34 o 3 4 0 3418.42 3558.79 103.12 o 4 4 0 5022.71 4749.25 146.92 o 5 4 0 52165.24 53513.41 962.51 o 6 4 0 3450.08 4160.30 104.54 o 7 4 0 6477.32 6423.95 132.50 o 8 4 0 1702.68 1846.97 79.42 o 9 4 0 5086.88 4993.50 110.16 o 10 4 0 4708.47 4763.90 108.81 o 11 4 0 350.11 335.41 67.36 o 12 4 0 5108.50 5311.67 208.21 o 13 4 0 17.18 0.00 58.67 o 14 4 0 6429.03 6693.43 195.62 o 15 4 0 46.53 115.62 90.14 o 16 4 0 1043.21 1076.63 137.81 o 17 4 0 1483.10 1351.03 160.67 o 18 4 0 284.18 175.64 261.38 o 1 5 0 8868.63 7662.71 158.62 o 2 5 0 5222.85 4518.03 111.65 o 3 5 0 18268.92 19820.29 357.22 o 4 5 0 13317.68 14695.68 310.83 o 5 5 0 10356.93 10252.51 198.07 o 6 5 0 9354.37 9285.66 187.85 o 7 5 0 340.27 335.28 45.81 o 8 5 0 14455.03 15011.37 261.41 o 9 5 0 1964.63 1965.94 79.07 o 10 5 0 2074.02 2089.54 93.04 o 11 5 0 2138.14 2089.01 96.45 o 12 5 0 945.90 952.54 86.90 o 13 5 0 2493.51 2635.21 131.88 o 14 5 0 45.54 81.43 62.96 o 15 5 0 853.09 747.31 92.93 o 16 5 0 982.39 934.74 131.51 o 17 5 0 353.33 124.61 95.57 o 18 5 0 777.08 992.70 221.48 o 0 6 0 3325.41 3036.37 154.86 o 1 6 0 549.57 509.52 40.82 o 2 6 0 5100.84 4934.94 124.60 o 3 6 0 1992.46 2008.27 79.11 o 4 6 0 10314.44 11697.95 239.21 o 5 6 0 12352.30 12287.94 275.59 o 6 6 0 1444.56 1317.25 105.74 o 7 6 0 1266.46 1090.66 60.57 o 8 6 0 263.92 225.84 42.48 o 9 6 0 4236.03 4374.27 127.84 o 10 6 0 1668.39 1724.39 75.63 o 11 6 0 218.48 173.09 52.00 o 12 6 0 1916.03 1813.53 124.89 o 13 6 0 45.97 22.21 75.29 o 14 6 0 499.45 485.94 94.75 o 15 6 0 219.35 243.49 103.61 o 16 6 0 353.68 320.60 83.99 o 17 6 0 1213.59 1078.19 147.78 o 1 7 0 957.32 902.32 58.29 o 2 7 0 36.90 0.00 27.63 o 3 7 0 1318.16 1644.39 102.83 o 4 7 0 2925.67 3273.81 194.23 o 5 7 0 51.40 15.68 29.81 o 6 7 0 15.55 53.27 39.72 o 7 7 0 2240.15 2405.25 117.80 o 8 7 0 4098.68 3977.07 118.81 o 9 7 0 1174.43 1364.15 77.07 o 10 7 0 1658.12 1637.51 97.41 o 11 7 0 1576.21 1729.14 82.10 o 12 7 0 15.94 0.00 44.65 o 13 7 0 963.39 1101.47 93.31 o 14 7 0 20.97 0.00 81.02 o 15 7 0 372.33 316.29 81.48 o 16 7 0 540.71 551.49 94.68 o 17 7 0 122.45 46.31 79.10 o 0 8 0 2368.67 2020.19 154.51 o 1 8 0 873.28 770.67 54.17 o 2 8 0 304.45 244.06 42.74 o 3 8 0 3443.73 3409.37 115.97 o 4 8 0 1442.14 1397.35 108.30 o 5 8 0 193.16 253.83 43.19 o 6 8 0 593.33 604.23 60.18 o 7 8 0 3113.94 3047.89 115.52 o 8 8 0 176.02 157.12 50.33 o 9 8 0 4.07 6.29 37.79 o 10 8 0 393.42 281.90 59.93 o 11 8 0 772.50 656.10 77.92 o 12 8 0 634.09 659.55 66.33 o 13 8 0 17.91 0.00 62.13 o 14 8 0 1.53 0.00 80.56 o 15 8 0 120.95 3.86 69.99 o 16 8 0 30.86 57.16 76.97 o 1 9 0 435.50 506.99 51.27 o 2 9 0 835.53 979.47 68.81 o 3 9 0 57.95 78.52 41.53 o 4 9 0 1014.07 1062.87 109.36 o 5 9 0 161.28 127.97 47.15 o 6 9 0 210.68 255.44 52.50 o 7 9 0 2.13 0.00 40.80 o 8 9 0 808.95 668.48 73.05 o 9 9 0 498.87 430.75 66.93 o 10 9 0 496.80 435.11 127.44 o 11 9 0 555.23 472.82 96.23 o 12 9 0 804.62 688.77 124.64 o 13 9 0 91.22 13.01 69.60 o 14 9 0 18.63 0.00 63.23 o 15 9 0 51.12 54.87 71.18 o 16 9 0 57.86 80.46 77.89 o 0 10 0 513.20 461.52 55.13 o 1 10 0 350.86 318.06 50.24 o 2 10 0 743.13 938.73 108.20 o 3 10 0 20.68 6.84 42.58 o 4 10 0 502.70 557.79 65.65 o 5 10 0 118.75 37.44 44.94 o 6 10 0 683.68 560.71 79.18 o 7 10 0 43.29 5.03 48.54 o 8 10 0 500.84 650.44 81.32 o 9 10 0 62.47 50.83 50.18 o 10 10 0 15.40 0.00 79.66 o 11 10 0 0.18 0.00 79.38 o 12 10 0 142.10 246.00 128.56 o 13 10 0 2.44 71.58 71.32 o 14 10 0 10.56 0.00 109.38 o 15 10 0 12.32 28.09 88.25 o 1 11 0 419.51 357.63 56.96 o 2 11 0 61.02 0.12 59.75 o 3 11 0 1076.08 1224.60 156.48 o 4 11 0 2.83 64.36 48.88 o 5 11 0 455.62 482.61 68.59 o 6 11 0 355.01 396.04 76.63 o 7 11 0 467.95 554.02 92.78 o 8 11 0 1.02 4.64 58.14 o 9 11 0 13.75 0.00 63.91 o 10 11 0 57.57 92.49 79.18 o 11 11 0 2.49 51.86 84.50 o 12 11 0 1.65 0.00 85.55 o 13 11 0 140.61 290.52 164.50 o 14 11 0 13.77 0.00 81.72 o 0 12 0 484.54 383.69 117.23 o 1 12 0 64.77 1.11 48.20 o 2 12 0 194.11 305.41 59.09 o 3 12 0 1314.47 1267.89 104.31 o 4 12 0 18.61 0.00 50.68 o 5 12 0 15.17 0.00 49.56 o 6 12 0 136.09 91.70 79.19 o 7 12 0 935.08 968.72 191.51 o 8 12 0 4.81 18.20 66.79 o 9 12 0 54.04 1.42 78.18 o 10 12 0 1.02 87.23 83.01 o 11 12 0 23.54 62.72 88.14 o 12 12 0 283.27 46.58 95.36 o 13 12 0 18.45 30.14 167.37 o 1 13 0 1237.17 1111.95 93.51 o 2 13 0 543.39 409.95 73.09 o 3 13 0 296.55 149.66 85.28 o 4 13 0 212.11 144.56 61.79 o 5 13 0 402.13 371.20 72.79 o 6 13 0 472.29 558.98 103.55 o 7 13 0 201.39 200.54 78.67 o 8 13 0 340.31 636.28 114.87 o 9 13 0 119.47 57.86 85.33 o 10 13 0 118.23 119.57 101.80 o 11 13 0 109.87 0.00 89.93 o 12 13 0 1.75 12.01 102.84 o 0 14 0 1102.15 1145.84 110.27 o 1 14 0 694.57 703.83 66.15 o 2 14 0 388.11 344.94 75.60 o 3 14 0 111.34 73.37 59.06 o 4 14 0 436.97 384.91 79.08 o 5 14 0 649.94 557.52 113.42 o 6 14 0 73.57 80.52 74.18 o 7 14 0 626.67 766.44 112.79 o 8 14 0 204.65 212.94 103.64 o 9 14 0 195.34 125.58 123.18 o 10 14 0 200.59 299.37 109.75 o 1 15 0 968.70 1214.08 87.59 o 2 15 0 322.55 204.47 55.87 o 3 15 0 800.11 964.57 115.58 o 4 15 0 319.27 346.12 108.50 o 5 15 0 147.10 135.52 95.92 o 6 15 0 565.91 660.35 119.46 o 7 15 0 3.73 0.00 79.68 o 8 15 0 304.01 249.01 135.53 o 0 16 0 668.60 468.77 106.68 o 1 16 0 18.30 2.68 58.30 o 2 16 0 819.38 815.06 81.63 o 3 16 0 228.13 207.90 79.20 o 4 16 0 278.53 46.09 92.90 o 5 16 0 222.00 123.36 99.46 o 6 16 0 13.99 106.12 105.19 o -19 1 1 0.69 0.00 91.00 o -18 1 1 6.19 67.14 86.92 o -17 1 1 16.55 65.74 81.10 o -16 1 1 325.96 281.86 84.74 o -15 1 1 316.49 350.13 86.23 o -14 1 1 257.50 42.40 68.77 o -13 1 1 394.94 533.17 85.04 o -12 1 1 6.70 0.00 47.80 o -11 1 1 401.84 365.62 56.67 o -10 1 1 458.69 319.79 36.03 o -9 1 1 857.85 756.32 42.07 o -8 1 1 4679.53 4422.76 95.38 o -7 1 1 542.77 657.54 51.31 o -6 1 1 11037.18 11283.06 225.57 o -5 1 1 14038.24 14509.01 274.86 o -4 1 1 33201.29 34087.39 879.63 o -3 1 1 6352.85 6497.53 149.16 o -2 1 1 7954.33 8319.60 159.26 o -1 1 1 4450.53 5142.06 115.02 o 0 1 1 4377.22 4664.72 192.63 o 2 1 1 752.53 1017.95 53.74 o 3 1 1 5098.82 5362.50 174.66 o 4 1 1 7728.10 7907.99 246.33 o 5 1 1 274.75 309.55 34.85 o 6 1 1 639.17 696.65 52.56 o 7 1 1 12442.12 13659.45 208.06 o 8 1 1 2049.54 2190.67 62.87 o 9 1 1 346.79 375.24 39.49 o 10 1 1 735.68 803.85 45.29 o 11 1 1 0.10 23.69 42.63 o 12 1 1 214.65 231.44 57.92 o 13 1 1 32.29 0.00 61.54 o 14 1 1 5.22 0.00 65.36 o 15 1 1 134.29 88.69 76.58 o 16 1 1 13.88 6.05 73.78 o 17 1 1 27.71 0.00 79.14 o 18 1 1 63.61 0.00 85.70 o -19 2 1 313.51 252.89 108.71 o -18 2 1 159.49 119.46 88.66 o -17 2 1 657.29 433.04 97.37 o -16 2 1 107.56 0.00 72.11 o -15 2 1 1802.61 1734.90 135.77 o -14 2 1 15.83 99.10 107.98 o -13 2 1 1278.49 1161.59 145.56 o -12 2 1 724.23 661.78 116.27 o -11 2 1 314.69 295.41 68.55 o -10 2 1 5.58 0.00 27.91 o -9 2 1 1253.16 1338.19 71.19 o -8 2 1 13418.12 13699.80 227.01 o -7 2 1 14614.75 15302.71 244.27 o -6 2 1 938.06 897.96 36.77 o -5 2 1 2268.72 2360.87 101.05 o -4 2 1 1268.56 1561.64 74.77 o -3 2 1 17824.84 18602.15 408.96 o -2 2 1 362.33 295.93 32.86 o -1 2 1 16.80 15.15 18.42 o 0 2 1 1273.06 1513.88 66.93 o 1 2 1 39.31 60.98 21.38 o 2 2 1 3615.67 3886.41 137.17 o 3 2 1 1892.25 1650.95 147.13 o 4 2 1 22796.29 23449.99 640.19 o 5 2 1 1800.42 2032.56 60.06 o 6 2 1 4496.74 4251.89 94.09 o 7 2 1 4367.80 3835.30 88.97 o 8 2 1 6002.65 7222.55 141.19 o 9 2 1 938.43 911.51 51.54 o 10 2 1 461.81 468.75 45.00 o 11 2 1 4011.21 4148.10 127.93 o 12 2 1 0.64 0.00 45.64 o 13 2 1 56.69 17.03 111.35 o 14 2 1 1426.71 1465.97 122.96 o 15 2 1 66.99 27.56 68.31 o 16 2 1 110.66 34.33 76.18 o 17 2 1 301.05 111.24 84.65 o 18 2 1 373.91 452.36 106.21 o -18 3 1 163.69 0.00 97.62 o -17 3 1 15.14 11.21 73.86 o -16 3 1 317.27 181.95 83.72 o -15 3 1 153.17 20.59 72.49 o -14 3 1 1693.85 1602.01 122.84 o -13 3 1 860.07 818.41 74.60 o -12 3 1 789.11 865.48 113.45 o -11 3 1 881.83 958.86 65.19 o -10 3 1 67.11 22.71 29.33 o -9 3 1 902.89 778.40 57.67 o -8 3 1 4421.17 4645.09 94.88 o -7 3 1 1269.81 1195.24 50.10 o -6 3 1 4340.55 4715.11 109.19 o -5 3 1 9260.95 9186.86 174.18 o -4 3 1 3482.00 3166.94 108.90 o -3 3 1 4298.03 4591.08 115.13 o -2 3 1 8159.40 8781.00 189.58 o -1 3 1 17206.44 18819.77 367.44 o 0 3 1 1278.90 1220.83 73.85 o 1 3 1 10033.81 10946.36 263.72 o 2 3 1 8.36 11.19 31.76 o 3 3 1 33433.93 34410.94 917.73 o 4 3 1 88.14 84.28 57.61 o 5 3 1 1284.43 1230.69 77.14 o 6 3 1 2709.61 2877.43 66.40 o 7 3 1 18993.52 20054.97 294.36 o 8 3 1 479.76 405.98 36.06 o 9 3 1 481.96 441.43 40.20 o 10 3 1 2581.09 2637.76 85.65 o 11 3 1 2830.19 2749.99 124.61 o 12 3 1 80.94 50.47 55.11 o 13 3 1 308.48 259.15 58.25 o 14 3 1 1669.82 1607.92 141.89 o 15 3 1 1772.12 1815.16 138.69 o 16 3 1 87.13 0.00 75.05 o 17 3 1 362.06 576.33 125.43 o 18 3 1 98.15 24.26 104.33 o -18 4 1 134.79 44.44 96.82 o -17 4 1 396.93 279.18 165.50 o -16 4 1 0.37 52.28 84.84 o -15 4 1 804.11 878.79 121.94 o -14 4 1 229.87 153.59 61.94 o -13 4 1 151.34 276.04 59.28 o -12 4 1 1234.98 1186.62 83.67 o -11 4 1 55.62 26.89 58.86 o -10 4 1 4574.87 4410.70 113.43 o -9 4 1 85.74 39.09 26.90 o -8 4 1 3612.63 3312.42 77.31 o -7 4 1 8475.18 8871.22 205.12 o -6 4 1 233.77 307.69 35.31 o -5 4 1 4539.73 4793.24 115.60 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10698.25 10778.85 205.49 o -8 5 1 234.55 110.05 40.35 o -7 5 1 9193.13 8689.25 181.74 o -6 5 1 1525.79 1906.95 69.75 o -5 5 1 9.44 17.14 21.00 o -4 5 1 670.62 894.32 67.36 o -3 5 1 1865.85 2395.46 216.49 o -2 5 1 15027.91 15314.14 282.99 o -1 5 1 2191.84 2082.50 76.82 o 0 5 1 8380.32 8256.80 199.44 o 1 5 1 21943.75 20870.44 410.30 o 2 5 1 110.79 137.00 31.45 o 3 5 1 5938.08 5727.12 150.20 o 4 5 1 3690.84 3572.34 129.50 o 5 5 1 16230.43 14665.61 268.22 o 6 5 1 1751.22 1724.98 68.78 o 7 5 1 10647.36 10704.78 216.00 o 8 5 1 10664.13 11426.76 212.86 o 9 5 1 1701.56 1361.25 59.10 o 10 5 1 4101.61 4172.68 106.99 o 11 5 1 202.60 191.91 60.70 o 12 5 1 4056.60 4113.69 140.76 o 13 5 1 421.42 457.90 87.83 o 14 5 1 1706.44 1926.68 181.77 o 15 5 1 1250.43 1426.05 114.30 o 16 5 1 437.47 309.99 101.09 o 17 5 1 623.57 522.38 120.17 o 18 5 1 26.42 0.00 86.07 o -18 6 1 188.23 227.09 111.57 o -17 6 1 815.66 625.87 134.78 o -16 6 1 59.90 69.27 69.55 o -15 6 1 1114.28 1032.17 117.56 o -14 6 1 1106.61 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