#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/38/2223860.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2223860_Fobs loop_ _publ_author_name 'Deng, Ji-Hua' 'Guo, Meng-Ping' 'Zhang, Qiao-Chu' 'Yuan, Lin' 'Guo, Hui-Rui' 'Mei, Guang-Quan' _publ_section_title ; Naphthalene-1,4,5,8-tetracarboxylic acid 1,8-anhydride--4,4'-bipyridine (1/1) ; _journal_coeditor_code IM2151 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2912 _journal_volume 65 _journal_year 2009 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 81.384 _cell_angle_beta 85.615 _cell_angle_gamma 83.947 _cell_length_a 9.6193 _cell_length_b 9.6964 _cell_length_c 10.1916 _exptl_crystal_F_000 456.00 _reflns_d_resolution_high 0.8409 _[local]_cod_data_source_file im2151Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 1011 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 182.69 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1623.08 1406.78 71.90 o 2 0 0 16.11 12.50 0.38 o 3 0 0 7.84 14.98 0.66 o 4 0 0 160.90 154.82 2.45 o 5 0 0 628.00 707.79 9.96 o 6 0 0 274.34 268.18 4.86 o 7 0 0 95.95 99.64 1.98 o 8 0 0 31.48 42.09 1.24 o 9 0 0 417.00 364.16 10.20 o 10 0 0 4.80 9.77 1.91 o 11 0 0 1.87 0.00 1.54 o -11 1 0 68.18 67.62 3.58 o -10 1 0 0.35 0.00 1.27 o -9 1 0 9.56 8.12 1.62 o -8 1 0 0.37 0.70 1.10 o -7 1 0 258.69 262.29 4.20 o -6 1 0 82.73 97.41 1.87 o -5 1 0 57.57 72.29 1.44 o -4 1 0 62.35 72.59 1.35 o -3 1 0 40.36 52.95 1.02 o -2 1 0 1451.21 1489.08 25.25 o -1 1 0 794.61 751.57 12.45 o 0 1 0 2.17 4.09 0.15 o 1 1 0 5.59 5.80 0.34 o 2 1 0 373.39 336.59 4.78 o 3 1 0 370.56 348.84 4.98 o 4 1 0 39.36 57.14 1.12 o 5 1 0 677.40 763.81 10.70 o 6 1 0 365.63 394.00 5.86 o 7 1 0 43.65 44.77 1.50 o 9 1 0 91.60 78.67 2.38 o 11 1 0 0.02 0.13 1.30 o -10 2 0 7.04 7.02 1.77 o -9 2 0 172.49 163.53 3.87 o -8 2 0 10.10 11.27 1.17 o -7 2 0 6.05 6.20 0.90 o -6 2 0 1043.01 1152.92 18.22 o -5 2 0 0.04 0.21 0.34 o -4 2 0 17.78 17.09 0.82 o -3 2 0 471.76 480.89 6.79 o -2 2 0 523.57 447.47 7.62 o -1 2 0 10.38 11.93 0.53 o 0 2 0 113.87 116.63 2.10 o 1 2 0 1517.53 1521.62 20.72 o 2 2 0 123.34 129.72 2.98 o 3 2 0 4.37 5.31 0.48 o 4 2 0 1467.51 1400.57 19.18 o 5 2 0 272.27 238.46 3.63 o 6 2 0 560.49 553.83 7.94 o 7 2 0 13.93 11.20 1.00 o 8 2 0 29.30 31.26 1.40 o 9 2 0 33.27 32.25 1.50 o 10 2 0 140.26 147.82 4.13 o 11 2 0 88.78 101.97 4.25 o -10 3 0 41.99 42.27 1.90 o -9 3 0 33.94 35.58 1.69 o -8 3 0 45.69 45.20 1.76 o -7 3 0 3.81 5.58 0.95 o -6 3 0 35.36 33.41 1.38 o -5 3 0 365.33 367.82 6.79 o -4 3 0 19.64 17.34 0.87 o -3 3 0 118.23 127.06 2.66 o -2 3 0 1780.27 1811.44 29.76 o -1 3 0 142.36 145.34 2.20 o 0 3 0 513.37 469.89 7.98 o 1 3 0 389.38 408.43 5.72 o 2 3 0 1071.05 1083.43 18.16 o 3 3 0 72.83 77.04 1.76 o 4 3 0 2324.70 2478.98 41.26 o 5 3 0 435.13 426.82 7.73 o 6 3 0 530.34 528.66 9.92 o 7 3 0 12.58 10.86 1.06 o 8 3 0 6.68 6.05 1.67 o 9 3 0 121.68 121.36 3.16 o 10 3 0 34.44 43.77 1.87 o 11 3 0 8.14 6.97 1.26 o -10 4 0 0.97 0.55 1.25 o -9 4 0 306.34 330.36 6.83 o -8 4 0 12.48 12.40 1.47 o -7 4 0 9.33 8.17 1.06 o -6 4 0 19.36 19.50 1.61 o -5 4 0 47.57 40.86 2.02 o -4 4 0 3.49 1.90 0.69 o -3 4 0 48.11 51.28 1.46 o -2 4 0 170.31 152.43 2.39 o -1 4 0 1985.00 2141.90 29.01 o 0 4 0 34.31 28.69 0.87 o 1 4 0 860.09 868.07 15.71 o 2 4 0 0.78 0.00 0.24 o 3 4 0 46.19 48.92 1.32 o 4 4 0 95.43 92.13 2.13 o 5 4 0 126.91 134.42 2.96 o 6 4 0 193.17 203.30 4.23 o 7 4 0 185.94 186.81 4.05 o 8 4 0 44.44 49.31 1.80 o 9 4 0 67.96 65.46 2.21 o 10 4 0 12.63 14.29 1.43 o 11 4 0 15.99 16.74 1.38 o -9 5 0 20.60 24.60 1.58 o -8 5 0 11.97 12.92 1.42 o -7 5 0 86.12 86.90 2.60 o -6 5 0 19.43 19.19 1.26 o -5 5 0 555.16 579.76 18.78 o -4 5 0 149.27 139.48 3.13 o -3 5 0 57.70 49.73 1.53 o -2 5 0 860.28 979.16 13.55 o -1 5 0 0.31 3.12 0.58 o 0 5 0 6.09 5.59 0.53 o 1 5 0 1053.52 1012.37 13.93 o 2 5 0 1459.78 1491.80 20.36 o 3 5 0 130.10 127.29 2.67 o 4 5 0 51.18 45.07 1.39 o 5 5 0 57.08 48.51 1.55 o 6 5 0 150.08 156.29 3.49 o 7 5 0 593.55 600.45 16.64 o 8 5 0 230.01 240.83 5.53 o 9 5 0 3.46 2.81 0.98 o 10 5 0 12.28 13.38 1.41 o -9 6 0 15.97 18.03 1.50 o -8 6 0 70.89 75.61 4.20 o -7 6 0 46.37 47.72 1.97 o -6 6 0 833.95 832.17 14.78 o -5 6 0 28.25 25.97 1.31 o -4 6 0 26.94 27.20 1.31 o -3 6 0 112.36 106.72 2.63 o -2 6 0 109.62 103.45 2.42 o -1 6 0 1164.87 1291.69 17.78 o 0 6 0 225.32 217.12 13.53 o 1 6 0 215.09 217.79 4.04 o 2 6 0 121.28 127.77 2.17 o 3 6 0 1588.57 1563.71 26.35 o 4 6 0 18.39 16.37 0.93 o 5 6 0 270.12 258.50 5.13 o 6 6 0 798.89 786.02 13.89 o 7 6 0 935.66 980.37 17.21 o 8 6 0 546.57 549.22 12.61 o 9 6 0 18.30 17.87 1.29 o 10 6 0 0.13 0.00 0.92 o -8 7 0 2.53 2.16 1.87 o -7 7 0 202.51 213.47 4.97 o -6 7 0 238.59 233.81 5.15 o -5 7 0 30.69 31.15 1.51 o -4 7 0 236.58 231.67 4.85 o -3 7 0 11.44 12.47 1.12 o -2 7 0 62.56 63.76 1.83 o -1 7 0 83.54 85.77 2.59 o 0 7 0 15.62 14.12 0.81 o 1 7 0 0.13 0.00 0.42 o 2 7 0 4.20 6.03 0.59 o 3 7 0 678.78 719.70 12.59 o 4 7 0 74.51 77.30 2.06 o 5 7 0 599.44 623.42 11.21 o 6 7 0 276.61 286.06 5.73 o 7 7 0 137.08 133.92 3.29 o 8 7 0 1.52 1.86 1.15 o 9 7 0 11.86 11.02 1.29 o -7 8 0 88.83 100.12 3.10 o -6 8 0 86.27 77.73 2.57 o -5 8 0 78.54 81.36 2.54 o -4 8 0 8.00 5.44 1.00 o -3 8 0 53.07 48.34 1.71 o -2 8 0 0.59 0.00 0.62 o -1 8 0 283.66 258.93 5.06 o 0 8 0 20.21 20.76 1.02 o 1 8 0 2.35 2.56 0.76 o 2 8 0 19.64 20.50 1.04 o 3 8 0 1.10 1.45 0.71 o 4 8 0 272.86 273.26 5.42 o 5 8 0 112.86 119.69 3.14 o 6 8 0 75.87 74.61 2.21 o 7 8 0 36.88 38.62 1.61 o 8 8 0 7.92 8.35 1.17 o -6 9 0 2.41 1.65 1.08 o -5 9 0 2.36 1.91 0.99 o -4 9 0 23.96 24.86 1.48 o -3 9 0 59.15 54.38 1.94 o -2 9 0 81.10 69.11 2.12 o -1 9 0 25.95 27.47 1.26 o 0 9 0 2.63 0.00 0.59 o 1 9 0 27.02 27.89 1.54 o 2 9 0 16.58 16.40 1.04 o 3 9 0 644.96 647.87 11.61 o 4 9 0 7.80 8.48 0.99 o 5 9 0 12.99 12.44 1.87 o 6 9 0 19.01 20.65 1.64 o 7 9 0 38.99 46.90 1.83 o -4 10 0 0.00 0.00 2.01 o -3 10 0 3.05 5.34 1.24 o -2 10 0 148.26 136.96 3.44 o -1 10 0 49.39 54.70 1.88 o 0 10 0 36.32 35.45 1.87 o 1 10 0 62.06 60.80 2.44 o 2 10 0 0.05 0.50 0.84 o 3 10 0 45.81 48.27 2.98 o 4 10 0 0.79 0.62 0.80 o 5 10 0 74.38 77.54 2.34 o 6 10 0 0.01 0.00 0.94 o -1 11 0 50.08 58.79 2.74 o 0 11 0 0.11 1.04 1.00 o 1 11 0 40.06 39.06 2.04 o 2 11 0 9.44 11.20 1.24 o 3 11 0 0.06 0.00 0.90 o 4 11 0 26.07 29.80 1.81 o -3 -11 1 3.04 2.34 1.14 o -2 -11 1 3.05 3.85 1.10 o -1 -11 1 50.58 52.71 2.41 o 0 -11 1 112.34 108.42 3.85 o 1 -11 1 27.45 27.46 1.87 o -5 -10 1 26.90 29.97 1.44 o -4 -10 1 11.74 14.15 3.65 o -3 -10 1 1.19 3.18 1.04 o -2 -10 1 24.40 26.39 1.61 o -1 -10 1 72.05 72.57 2.78 o 0 -10 1 94.70 93.34 3.34 o 1 -10 1 55.02 46.62 1.75 o 2 -10 1 1.47 0.12 0.86 o 3 -10 1 47.94 46.40 1.89 o 4 -10 1 0.90 0.47 0.94 o -7 -9 1 1.37 1.26 0.90 o -6 -9 1 94.88 105.78 2.86 o -5 -9 1 21.97 22.35 1.27 o -4 -9 1 21.94 23.37 1.25 o -3 -9 1 10.72 11.19 1.62 o -2 -9 1 5.75 5.03 1.57 o -1 -9 1 0.00 0.00 0.64 o 0 -9 1 31.06 26.94 1.19 o 1 -9 1 8.15 4.72 0.88 o 2 -9 1 133.92 136.88 3.31 o 3 -9 1 24.58 23.77 1.35 o 4 -9 1 51.44 50.61 1.98 o 5 -9 1 0.35 0.41 0.95 o -8 -8 1 220.04 241.65 5.31 o -7 -8 1 256.36 265.48 5.60 o -6 -8 1 566.70 597.95 11.01 o -5 -8 1 777.85 792.10 14.10 o -4 -8 1 0.62 0.00 0.65 o -3 -8 1 87.37 93.96 4.16 o -2 -8 1 238.08 231.69 4.63 o -1 -8 1 3.88 2.94 0.73 o 0 -8 1 279.58 249.83 4.86 o 1 -8 1 5.64 1.51 0.69 o 2 -8 1 8.14 6.48 1.19 o 3 -8 1 33.13 34.66 1.48 o 4 -8 1 52.24 47.57 1.81 o 5 -8 1 1.96 0.45 0.91 o 6 -8 1 156.95 161.27 6.22 o 7 -8 1 34.90 38.20 1.93 o -9 -7 1 1.48 0.28 0.89 o -8 -7 1 158.21 173.83 8.49 o -7 -7 1 519.19 522.54 9.81 o -6 -7 1 18.70 21.36 1.20 o -5 -7 1 52.45 54.17 1.74 o -4 -7 1 9.84 9.41 1.10 o -3 -7 1 95.74 96.32 2.34 o -2 -7 1 106.85 102.19 2.39 o -1 -7 1 58.13 57.47 1.31 o 0 -7 1 7.83 8.68 1.11 o 1 -7 1 7.98 8.54 1.67 o 2 -7 1 86.81 97.55 2.42 o 3 -7 1 10.93 12.21 1.72 o 4 -7 1 22.35 21.41 1.24 o 5 -7 1 282.55 301.70 6.15 o 6 -7 1 439.61 447.80 8.70 o 7 -7 1 93.34 93.12 2.92 o 8 -7 1 248.52 257.24 5.85 o -10 -6 1 14.32 15.55 1.53 o -9 -6 1 37.17 38.17 1.71 o -8 -6 1 149.71 168.31 3.96 o -7 -6 1 38.08 38.42 1.57 o -6 -6 1 19.26 19.18 1.11 o -5 -6 1 84.69 87.09 2.28 o -4 -6 1 33.34 29.28 1.52 o -3 -6 1 174.21 167.53 3.46 o -2 -6 1 0.66 1.15 0.40 o -1 -6 1 453.34 478.77 6.89 o 0 -6 1 23.44 19.85 1.16 o 1 -6 1 133.52 153.18 4.61 o 2 -6 1 19.55 17.58 0.92 o 4 -6 1 10.10 12.80 1.05 o 5 -6 1 1.68 1.25 1.10 o 6 -6 1 1313.13 1358.20 23.79 o 7 -6 1 482.18 469.85 9.08 o 8 -6 1 16.41 15.92 1.62 o 9 -6 1 58.88 61.70 2.46 o -10 -5 1 1.11 0.14 1.05 o -9 -5 1 75.27 72.70 2.37 o -8 -5 1 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22.04 o 2 -2 1 261.24 263.80 4.73 o 3 -2 1 1693.24 1743.60 28.71 o 4 -2 1 55.44 52.13 2.63 o 5 -2 1 658.64 709.66 10.01 o 6 -2 1 136.13 152.84 3.35 o 7 -2 1 12.20 12.60 1.10 o 8 -2 1 2.30 1.66 0.90 o 9 -2 1 21.19 14.17 1.34 o 10 -2 1 28.90 26.04 1.51 o -11 -1 1 24.52 29.33 2.31 o -10 -1 1 5.02 5.59 1.47 o -8 -1 1 13.18 14.41 1.47 o -7 -1 1 93.05 91.57 1.86 o -6 -1 1 285.70 307.75 5.21 o -5 -1 1 1501.96 1700.19 26.43 o -4 -1 1 3092.90 3315.34 79.76 o -3 -1 1 293.84 284.69 4.11 o -2 -1 1 7.13 10.21 0.53 o -1 -1 1 10.91 14.10 0.34 o 0 -1 1 1391.84 1258.95 27.01 o 1 -1 1 4370.86 4192.39 71.47 o 2 -1 1 228.25 205.20 4.14 o 3 -1 1 18.94 11.71 0.44 o 4 -1 1 2715.47 2971.21 40.20 o 5 -1 1 1695.87 1928.51 26.31 o 6 -1 1 2.32 2.02 0.46 o 7 -1 1 74.25 78.03 1.68 o 8 -1 1 0.50 0.00 0.69 o 9 -1 1 111.37 95.91 2.65 o 10 -1 1 0.28 1.14 1.37 o 11 -1 1 30.82 31.44 2.54 o -11 0 1 68.51 66.45 3.54 o -10 0 1 179.42 167.65 5.92 o -9 0 1 542.30 463.26 12.44 o -8 0 1 3.90 1.84 0.90 o -7 0 1 117.95 117.72 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4.66 2.67 1.66 o -4 5 9 27.59 32.06 1.59 o -3 5 9 28.21 20.65 1.37 o -2 5 9 12.04 12.25 2.42 o -1 5 9 24.45 23.45 1.37 o 0 5 9 11.70 12.59 1.34 o 1 5 9 148.46 150.95 6.92 o 2 5 9 27.32 26.50 1.45 o 3 5 9 8.75 9.26 1.20 o 4 5 9 3.68 4.14 1.15 o 5 5 9 6.08 5.06 1.09 o 6 5 9 6.18 12.54 2.04 o 7 5 9 0.40 1.27 1.47 o -4 6 9 7.69 6.77 1.23 o -3 6 9 0.14 0.00 0.91 o -2 6 9 0.07 0.00 0.87 o -1 6 9 27.45 26.88 1.47 o 0 6 9 0.97 1.06 1.44 o 1 6 9 17.57 16.91 1.25 o 2 6 9 59.54 61.42 3.85 o 3 6 9 246.38 233.42 5.25 o 4 6 9 6.03 7.32 1.44 o 5 6 9 5.07 2.27 1.44 o 6 6 9 13.04 16.02 2.31 o 7 6 9 166.05 208.75 7.29 o -3 7 9 34.66 40.31 1.86 o -2 7 9 125.16 135.02 3.62 o -1 7 9 0.61 0.35 0.96 o 0 7 9 0.12 0.00 0.88 o 1 7 9 40.97 35.22 1.75 o 2 7 9 237.66 235.57 5.36 o 3 7 9 3.25 2.30 1.61 o 4 7 9 10.36 10.03 1.97 o 5 7 9 1.71 2.24 1.61 o 6 7 9 4.05 4.31 1.67 o -2 8 9 12.70 18.94 1.73 o -1 8 9 81.17 91.63 2.96 o 0 8 9 1.70 1.23 1.06 o 1 8 9 89.98 96.28 4.85 o 2 8 9 56.89 58.17 2.27 o 3 8 9 88.17 101.94 4.48 o 4 8 9 93.42 104.48 4.62 o 0 -5 10 1.57 0.00 1.64 o -3 -4 10 100.44 106.75 4.31 o -2 -4 10 10.30 9.67 1.33 o -1 -4 10 15.69 16.52 1.35 o 0 -4 10 7.23 7.05 1.18 o 1 -4 10 163.06 176.95 6.32 o 2 -4 10 55.63 52.91 3.21 o 3 -4 10 202.49 199.96 6.99 o -4 -3 10 4.56 4.05 1.54 o -3 -3 10 60.73 64.48 2.30 o -2 -3 10 77.03 71.87 2.40 o -1 -3 10 65.42 63.21 2.24 o 0 -3 10 5.63 4.24 1.03 o 1 -3 10 4.08 5.45 1.08 o 2 -3 10 0.12 0.00 0.82 o 3 -3 10 66.15 67.35 3.54 o 4 -3 10 31.81 30.23 2.47 o -5 -2 10 5.75 6.92 1.74 o -4 -2 10 18.40 16.72 1.37 o -3 -2 10 0.05 0.00 0.86 o -2 -2 10 29.84 34.11 1.62 o -1 -2 10 1.22 0.00 0.87 o 0 -2 10 29.18 32.43 1.86 o 1 -2 10 12.78 13.20 1.74 o 2 -2 10 34.58 33.70 1.59 o 3 -2 10 0.02 0.00 0.82 o 4 -2 10 43.01 41.80 2.78 o 5 -2 10 7.10 5.42 1.74 o -5 -1 10 0.30 0.00 0.99 o -4 -1 10 1.33 0.00 0.92 o -3 -1 10 9.43 9.82 1.97 o -2 -1 10 0.14 0.00 0.87 o -1 -1 10 28.91 27.26 2.37 o 0 -1 10 1.25 0.46 0.85 o 1 -1 10 0.06 0.00 0.84 o 2 -1 10 45.30 51.35 1.90 o 3 -1 10 59.18 64.83 2.22 o 4 -1 10 2.82 3.08 0.99 o 5 -1 10 81.46 82.37 3.91 o 6 -1 10 19.39 21.24 2.14 o -5 0 10 87.29 88.06 2.78 o -4 0 10 49.72 43.15 1.88 o -3 0 10 38.10 36.95 1.71 o -2 0 10 52.43 56.43 2.07 o -1 0 10 37.12 35.24 1.63 o 0 0 10 21.48 20.99 1.29 o 1 0 10 96.88 102.18 2.87 o 2 0 10 7.03 6.42 1.08 o 3 0 10 24.75 25.72 1.46 o 4 0 10 8.41 7.46 1.15 o 5 0 10 4.50 5.99 1.13 o 6 0 10 0.86 0.23 1.40 o -5 1 10 5.21 3.87 1.15 o -4 1 10 10.15 11.86 2.22 o -3 1 10 11.47 10.00 1.97 o -2 1 10 5.11 6.22 1.11 o -1 1 10 5.86 5.82 1.08 o 0 1 10 89.36 101.43 2.86 o 1 1 10 49.81 49.24 1.90 o 2 1 10 275.17 289.71 6.11 o 3 1 10 63.60 67.58 2.27 o 4 1 10 15.87 16.74 1.30 o 5 1 10 7.26 5.43 1.66 o 6 1 10 29.04 31.76 2.56 o 7 1 10 1.52 2.17 1.47 o -5 2 10 97.34 89.88 2.80 o -4 2 10 23.89 23.41 1.50 o -3 2 10 25.89 25.11 1.46 o -2 2 10 0.86 1.46 1.62 o -1 2 10 51.37 54.48 2.03 o 0 2 10 46.15 51.40 1.99 o 1 2 10 211.45 220.82 4.97 o 2 2 10 113.15 116.48 3.16 o 3 2 10 625.30 640.63 12.01 o 4 2 10 7.59 8.88 1.52 o 5 2 10 188.52 194.64 4.60 o 6 2 10 3.67 5.29 2.29 o 7 2 10 11.65 14.72 2.74 o -5 3 10 5.68 4.96 1.19 o -4 3 10 9.84 10.39 1.39 o -3 3 10 104.87 98.71 2.94 o -2 3 10 19.49 20.36 1.37 o -1 3 10 3.32 2.52 0.96 o 0 3 10 365.71 364.81 7.42 o 1 3 10 46.00 48.66 1.97 o 2 3 10 1.96 2.14 1.06 o 3 3 10 3.03 4.33 1.07 o 4 3 10 52.35 59.28 2.81 o 5 3 10 105.87 95.12 3.41 o 6 3 10 17.12 11.68 2.49 o 7 3 10 0.98 0.83 1.03 o -4 4 10 43.69 39.13 1.82 o -3 4 10 54.24 47.92 1.99 o -2 4 10 1.73 0.85 0.90 o -1 4 10 101.56 107.98 3.07 o 0 4 10 8.25 9.29 1.24 o 1 4 10 500.35 524.76 11.07 o 2 4 10 8.04 7.70 1.23 o 3 4 10 33.48 34.63 1.69 o 4 4 10 10.17 8.95 1.42 o 5 4 10 10.19 8.54 2.39 o 6 4 10 65.00 69.19 2.47 o -4 5 10 22.08 23.40 1.53 o -3 5 10 10.88 9.54 1.32 o -2 5 10 39.47 34.81 1.86 o -1 5 10 12.52 12.24 1.96 o 0 5 10 95.56 98.48 3.56 o 1 5 10 1.57 0.00 0.90 o 2 5 10 18.18 18.14 2.02 o 3 5 10 4.13 4.91 1.09 o 4 5 10 1.26 1.67 0.96 o 5 5 10 2.94 4.30 1.13 o 6 5 10 17.96 19.36 2.07 o -3 6 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