#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/45/2224584.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2224584_Fobs loop_ _publ_author_name 'Han, Shuang' 'Li, Wan-Cheng' 'Xia, Dao-Cheng' _publ_section_title ; Bis(2-phenyl-1H-imidazole-\kN^3^)silver(I) nitrate ; _journal_coeditor_code CI2975 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m3 _journal_volume 66 _journal_year 2010 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 88.307 _cell_angle_beta 80.976 _cell_angle_gamma 72.369 _cell_length_a 9.2090 _cell_length_b 9.2740 _cell_length_c 23.1370 _exptl_crystal_F_000 920.00 _reflns_d_resolution_high 0.7302 _[local]_cod_data_source_file ci2975Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 01 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 223.91 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 250.57 270.58 12.13 o 2 0 0 1940.87 1798.40 33.69 o 3 0 0 228.73 220.59 9.34 o 4 0 0 19647.98 18934.42 543.53 o 5 0 0 80.24 86.83 41.10 o 6 0 0 1786.89 1858.84 44.93 o 7 0 0 61.06 63.99 45.96 o 8 0 0 1844.10 1896.97 78.00 o 9 0 0 130.72 220.76 55.23 o 10 0 0 159.19 151.23 52.93 o -10 1 0 39.91 64.29 52.54 o -9 1 0 487.84 505.68 59.92 o -8 1 0 9.13 13.08 9.47 o -7 1 0 19.78 17.36 11.79 o -6 1 0 198.59 208.35 15.72 o -5 1 0 2578.05 2558.01 30.04 o -4 1 0 969.59 955.81 42.63 o -3 1 0 1170.26 1204.04 40.24 o -2 1 0 1138.35 1240.01 39.49 o -1 1 0 40699.29 39199.49 509.75 o 0 1 0 208.06 231.56 11.77 o 1 1 0 1169.87 1343.47 21.86 o 2 1 0 187.75 186.94 17.52 o 3 1 0 26289.75 25503.89 536.36 o 4 1 0 49.99 397.60 32.80 o 5 1 0 375.78 405.58 32.58 o 6 1 0 9.88 22.94 23.72 o 7 1 0 3176.20 3142.30 84.98 o 8 1 0 77.32 123.25 48.74 o 9 1 0 652.95 651.80 61.21 o 10 1 0 11.78 21.76 44.84 o 11 1 0 335.86 289.36 58.90 o -10 2 0 126.97 75.29 54.95 o -9 2 0 5.12 11.69 43.81 o -8 2 0 195.83 211.89 50.38 o -7 2 0 238.60 213.66 21.49 o -6 2 0 1707.33 1718.57 36.96 o -5 2 0 79.08 73.90 17.14 o -4 2 0 98.40 159.44 18.14 o -3 2 0 5089.69 5461.05 134.62 o -2 2 0 8857.02 9517.06 172.32 o -1 2 0 2860.41 2860.41 46.62 o 0 2 0 9672.35 10204.60 73.95 o 1 2 0 397.91 418.99 23.17 o 2 2 0 15495.73 15020.70 262.92 o 3 2 0 386.22 544.84 29.43 o 4 2 0 473.66 526.07 11.84 o 5 2 0 128.47 139.21 25.35 o 6 2 0 8330.64 8528.22 287.87 o 7 2 0 0.02 58.59 41.95 o 8 2 0 660.38 723.46 57.21 o 9 2 0 1.66 -7.99 41.78 o 10 2 0 305.65 306.26 54.45 o 11 2 0 7.09 -5.26 55.75 o -9 3 0 196.86 204.54 49.46 o -8 3 0 20.91 42.40 46.79 o -7 3 0 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599.20 560.77 21.37 o 8 4 0 1145.93 1108.28 65.47 o 9 4 0 26.65 33.98 43.07 o 10 4 0 0.12 23.77 47.51 o 11 4 0 38.28 53.97 55.87 o -8 5 0 0.10 24.06 46.52 o -7 5 0 138.13 132.47 53.80 o -6 5 0 34.76 49.31 48.10 o -5 5 0 572.67 530.97 34.11 o -4 5 0 393.04 389.54 32.26 o -3 5 0 627.60 607.46 34.65 o -2 5 0 1203.82 1248.52 31.16 o -1 5 0 303.51 271.16 19.63 o 0 5 0 1173.41 1208.12 43.23 o 1 5 0 3554.28 3873.54 52.29 o 2 5 0 615.45 618.77 28.40 o 3 5 0 221.66 224.74 21.96 o 4 5 0 2724.54 2763.06 37.42 o 5 5 0 351.03 342.42 19.62 o 6 5 0 1965.05 1970.00 38.74 o 7 5 0 857.79 869.90 60.26 o 8 5 0 149.50 147.18 12.36 o 9 5 0 66.32 28.45 41.13 o 10 5 0 26.68 41.61 52.06 o 11 5 0 146.22 155.37 57.48 o -7 6 0 5.67 18.56 47.04 o -6 6 0 155.88 151.42 46.34 o -5 6 0 5.49 15.07 47.71 o -4 6 0 1280.37 1274.04 70.01 o -3 6 0 19.35 -0.27 36.50 o -2 6 0 793.31 737.81 35.86 o -1 6 0 84.98 103.47 22.43 o 0 6 0 1657.69 1650.99 35.48 o 1 6 0 1748.56 1786.46 35.09 o 2 6 0 1992.45 2227.50 52.10 o 3 6 0 1969.61 1907.22 35.65 o 4 6 0 3939.84 4209.02 59.84 o 5 6 0 1333.21 1346.92 31.92 o 6 6 0 574.33 545.83 33.73 o 7 6 0 896.91 843.95 66.46 o 8 6 0 597.00 513.75 32.53 o 9 6 0 262.83 314.26 54.90 o 10 6 0 454.94 492.32 64.25 o 11 6 0 15.26 12.14 54.64 o -6 7 0 0.21 -0.11 49.68 o -5 7 0 283.72 248.90 50.35 o -4 7 0 174.03 142.98 53.29 o -3 7 0 100.50 67.44 43.59 o -2 7 0 236.64 203.25 50.17 o -1 7 0 2225.73 2218.85 78.56 o 0 7 0 685.33 716.73 55.48 o 1 7 0 1.72 63.43 40.60 o 2 7 0 167.65 167.54 29.34 o 3 7 0 1534.55 1580.74 45.00 o 4 7 0 778.14 737.81 49.99 o 5 7 0 241.96 238.35 57.56 o 6 7 0 424.15 456.04 85.70 o 7 7 0 1682.73 1562.54 127.83 o 8 7 0 280.63 277.12 25.80 o 9 7 0 224.59 299.33 50.84 o 10 7 0 79.75 80.49 46.98 o -5 8 0 13.04 9.58 50.32 o -4 8 0 44.95 31.33 47.71 o -3 8 0 0.70 22.18 47.39 o -2 8 0 353.99 336.49 53.39 o -1 8 0 406.41 400.08 52.66 o 0 8 0 205.18 218.23 45.44 o 1 8 0 30.33 46.04 46.54 o 2 8 0 315.16 352.20 46.22 o 3 8 0 240.43 235.53 47.62 o 4 8 0 101.43 91.37 29.56 o 5 8 0 40.09 91.75 44.92 o 6 8 0 142.01 186.12 46.29 o 7 8 0 700.60 778.20 64.19 o 8 8 0 0.07 19.93 41.83 o 9 8 0 18.80 40.12 46.21 o 10 8 0 116.29 130.70 50.49 o -4 9 0 0.13 5.38 54.88 o -3 9 0 240.30 207.87 57.36 o -2 9 0 87.52 41.15 44.47 o -1 9 0 33.60 43.92 47.11 o 0 9 0 64.48 63.64 47.14 o 1 9 0 1238.71 1189.56 69.28 o 2 9 0 109.13 133.91 47.58 o 3 9 0 21.11 13.34 43.79 o 4 9 0 14.00 33.09 44.57 o 5 9 0 556.30 540.31 56.44 o 6 9 0 320.88 359.95 55.89 o 7 9 0 18.84 89.21 51.95 o 8 9 0 164.56 165.21 50.19 o 9 9 0 143.49 163.13 51.07 o -2 10 0 0.92 17.64 52.72 o -1 10 0 2.87 9.25 51.12 o 0 10 0 311.79 326.30 53.46 o 1 10 0 124.75 144.45 45.86 o 2 10 0 13.58 -12.93 47.98 o 3 10 0 63.56 88.97 49.57 o 4 10 0 422.59 323.24 51.04 o 5 10 0 21.13 44.60 47.56 o 6 10 0 9.91 17.06 46.04 o 7 10 0 15.41 5.67 50.65 o 8 10 0 159.79 160.19 57.96 o 0 11 0 10.84 18.37 54.69 o 1 11 0 26.80 -0.39 45.18 o 2 11 0 11.48 5.08 44.59 o 3 11 0 169.00 190.27 56.10 o 4 11 0 39.01 55.68 46.50 o 5 11 0 14.65 11.80 51.37 o 6 11 0 34.14 76.53 54.41 o -6 -11 1 222.38 210.14 59.59 o -5 -11 1 8.96 16.16 52.49 o -4 -11 1 77.46 86.10 52.53 o -3 -11 1 26.35 37.64 49.15 o -2 -11 1 185.29 145.60 54.54 o -1 -11 1 13.75 33.75 50.07 o 0 -11 1 6.22 23.60 54.02 o -8 -10 1 20.21 46.26 51.87 o -7 -10 1 97.60 131.97 53.91 o -6 -10 1 0.34 30.04 50.20 o -5 -10 1 14.47 34.10 44.31 o -4 -10 1 118.87 148.47 52.34 o -3 -10 1 114.39 162.05 45.71 o -2 -10 1 35.06 39.49 42.02 o -1 -10 1 0.64 -11.65 46.04 o 0 -10 1 12.69 55.20 43.85 o 1 -10 1 140.57 124.13 54.73 o 2 -10 1 7.84 33.72 53.34 o -9 -9 1 99.77 79.58 51.97 o -8 -9 1 393.30 376.10 55.50 o -7 -9 1 504.73 517.10 60.35 o -6 -9 1 116.81 133.18 45.08 o -5 -9 1 387.03 392.62 52.07 o -4 -9 1 971.65 952.52 62.59 o -3 -9 1 38.53 29.72 43.35 o -2 -9 1 5.94 38.42 39.13 o -1 -9 1 9.15 52.78 48.04 o 0 -9 1 51.76 71.71 47.20 o 1 -9 1 70.00 70.49 48.83 o 2 -9 1 21.67 30.77 41.87 o 3 -9 1 0.05 11.02 51.00 o 4 -9 1 53.25 46.01 55.46 o -10 -8 1 25.05 45.08 54.12 o -9 -8 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