#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/76/2227681.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2227681_Fobs loop_ _publ_author_name 'Nagasawa, Atsushi' 'Mitsui, Ryosuke' 'Kato, Yuichi' 'Okamoto, Akiko' 'Yonezawa, Noriyuki' _publ_section_title ; (2-Hydroxy-7-methoxynaphthalen-1-yl)(phenyl)methanone ; _journal_coeditor_code IS2606 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2677 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 93.167 _cell_angle_gamma 90.000 _cell_length_a 9.8101 _cell_length_b 6.2789 _cell_length_c 22.0737 _exptl_crystal_F_000 584.00 _reflns_d_resolution_high 0.8302 _[local]_cod_data_source_file is2606Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' yonezawaLab_090420_1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 183.96 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 5533.28 5540.57 132.33 o 2 0 0 4013.18 3728.77 61.00 o 3 0 0 401.10 378.93 3.21 o 4 0 0 2051.47 1898.73 19.33 o 5 0 0 2934.46 2903.13 33.28 o 6 0 0 343.36 376.83 4.36 o 7 0 0 896.89 977.37 14.70 o 8 0 0 11.70 15.45 0.85 o 9 0 0 6.99 9.69 0.87 o 10 0 0 48.94 38.41 1.17 o 11 0 0 1.75 1.30 0.50 o 1 1 0 322.53 274.89 2.09 o 2 1 0 240.01 227.53 2.50 o 3 1 0 35.44 38.26 0.43 o 4 1 0 125.51 147.42 1.18 o 5 1 0 82.81 91.17 0.79 o 6 1 0 7.04 9.36 0.30 o 7 1 0 272.01 277.35 3.14 o 8 1 0 32.97 31.23 1.26 o 9 1 0 16.61 19.39 0.69 o 10 1 0 5.88 4.67 0.64 o 11 1 0 0.02 0.01 0.40 o 0 2 0 5.25 8.18 0.41 o 1 2 0 478.36 459.46 3.53 o 2 2 0 219.39 204.94 1.75 o 3 2 0 1313.94 1256.23 11.02 o 4 2 0 0.10 1.60 0.39 o 5 2 0 14.87 18.70 0.35 o 6 2 0 0.01 0.43 0.25 o 7 2 0 617.36 614.54 8.37 o 8 2 0 79.68 70.81 1.74 o 9 2 0 106.20 100.53 1.87 o 10 2 0 50.65 49.82 1.02 o 11 2 0 0.50 0.15 0.49 o 1 3 0 51.35 55.44 0.77 o 2 3 0 1042.89 1110.82 10.69 o 3 3 0 2.32 4.05 0.59 o 4 3 0 19.51 15.66 0.67 o 5 3 0 22.30 33.57 3.14 o 6 3 0 306.45 297.55 4.94 o 7 3 0 121.28 118.64 2.10 o 8 3 0 106.88 100.18 1.80 o 9 3 0 6.27 5.07 0.61 o 10 3 0 0.00 0.40 0.47 o 0 4 0 8.63 26.74 6.00 o 1 4 0 42.56 55.66 7.03 o 2 4 0 65.32 63.80 1.21 o 3 4 0 43.28 41.05 1.08 o 4 4 0 34.99 38.18 0.94 o 5 4 0 44.30 45.92 1.11 o 6 4 0 119.05 122.11 1.99 o 7 4 0 149.45 161.81 5.28 o 8 4 0 1.60 2.39 0.48 o 9 4 0 44.04 51.16 1.07 o 10 4 0 66.67 71.04 4.59 o 1 5 0 178.55 171.13 3.64 o 2 5 0 481.02 471.98 8.88 o 3 5 0 8.40 8.34 1.16 o 4 5 0 0.82 2.17 0.79 o 5 5 0 28.03 24.65 0.88 o 6 5 0 0.01 0.99 0.50 o 7 5 0 28.18 29.50 0.82 o 8 5 0 16.82 20.17 0.94 o 0 6 0 157.91 155.35 7.18 o 1 6 0 43.13 38.28 10.50 o 2 6 0 0.54 0.20 0.65 o 3 6 0 35.71 27.80 1.22 o 4 6 0 142.39 151.11 2.99 o 5 6 0 79.40 79.37 2.13 o 6 6 0 15.62 16.40 0.91 o 7 6 0 13.98 16.61 1.73 o 1 7 0 0.05 0.06 1.29 o 2 7 0 26.90 25.70 1.11 o 3 7 0 109.30 97.77 2.40 o 4 7 0 163.24 180.90 4.87 o -11 1 1 8.31 4.50 0.78 o -10 1 1 23.63 26.61 0.65 o -9 1 1 16.01 16.56 0.58 o -8 1 1 324.51 314.42 3.72 o -7 1 1 7.32 9.41 1.31 o -6 1 1 311.71 360.48 2.66 o -5 1 1 49.48 47.78 0.50 o -4 1 1 22.03 27.61 0.48 o -3 1 1 64.59 74.14 1.23 o -2 1 1 734.75 627.55 4.79 o -1 1 1 50.82 53.64 0.95 o 0 1 1 2.14 3.97 0.21 o 1 1 1 9078.30 8861.22 90.36 o 2 1 1 967.82 829.93 5.83 o 3 1 1 539.15 517.52 3.25 o 4 1 1 490.50 508.41 3.77 o 5 1 1 63.39 71.16 0.68 o 6 1 1 106.89 96.32 0.81 o 7 1 1 60.18 62.18 1.46 o 8 1 1 3.08 2.00 0.40 o 9 1 1 1.82 1.36 0.36 o 10 1 1 95.12 83.37 1.31 o 11 1 1 21.52 19.58 1.00 o -11 2 1 4.34 5.64 2.01 o -10 2 1 36.75 34.71 0.87 o -9 2 1 7.35 6.93 0.66 o -8 2 1 215.52 218.32 3.05 o -7 2 1 41.52 41.31 1.03 o -6 2 1 61.17 60.14 0.78 o -5 2 1 3.18 6.41 0.75 o -4 2 1 522.46 556.01 4.59 o -3 2 1 192.26 178.52 1.60 o -2 2 1 248.33 249.07 3.11 o -1 2 1 28.57 24.84 0.56 o 0 2 1 852.79 757.36 5.84 o 1 2 1 27.98 25.27 0.63 o 2 2 1 4818.74 4604.54 44.93 o 3 2 1 155.04 199.70 2.29 o 4 2 1 321.82 345.39 2.85 o 5 2 1 35.43 33.91 0.44 o 6 2 1 202.55 194.08 1.80 o 7 2 1 510.20 522.72 12.59 o 8 2 1 56.33 60.99 4.14 o 9 2 1 73.12 75.43 1.46 o 10 2 1 15.92 16.23 0.95 o 11 2 1 14.35 18.98 1.11 o -10 3 1 41.40 46.78 1.91 o -9 3 1 2.04 2.52 1.03 o -8 3 1 0.21 0.44 0.49 o -7 3 1 341.86 332.09 4.50 o -6 3 1 57.20 60.57 1.79 o -5 3 1 461.44 461.72 5.17 o -4 3 1 3.24 4.51 0.38 o -3 3 1 86.25 91.79 1.29 o -2 3 1 1624.92 1731.84 16.14 o -1 3 1 591.71 627.74 5.90 o 0 3 1 822.98 813.05 7.19 o 1 3 1 973.61 1013.51 8.92 o 2 3 1 36.51 37.82 0.85 o 3 3 1 82.82 97.27 1.03 o 4 3 1 280.25 307.98 2.74 o 5 3 1 207.67 230.14 2.78 o 6 3 1 564.96 582.10 10.55 o 7 3 1 21.53 26.57 1.91 o 8 3 1 400.28 409.59 5.27 o 9 3 1 0.34 0.01 0.30 o 10 3 1 0.44 0.51 0.46 o -10 4 1 76.95 84.37 3.03 o -9 4 1 93.89 100.06 1.57 o -8 4 1 0.16 0.58 0.38 o -7 4 1 82.32 80.57 1.48 o -6 4 1 66.77 60.77 1.33 o -5 4 1 10.64 10.32 0.72 o -4 4 1 6.41 13.92 2.98 o -3 4 1 27.91 29.55 0.67 o -2 4 1 7.41 4.84 0.35 o -1 4 1 434.06 454.88 5.90 o 0 4 1 152.97 139.72 2.44 o 1 4 1 17.15 14.98 0.56 o 2 4 1 4.00 6.74 1.22 o 3 4 1 60.27 67.98 1.36 o 4 4 1 353.08 355.94 4.76 o 5 4 1 122.65 132.62 2.12 o 6 4 1 756.76 780.90 9.88 o 7 4 1 0.17 1.97 0.84 o 8 4 1 6.91 6.76 0.55 o 9 4 1 59.74 66.49 1.27 o -8 5 1 7.20 8.44 0.49 o -7 5 1 0.23 0.19 0.35 o -6 5 1 12.81 9.15 0.67 o -5 5 1 16.15 12.81 0.85 o -4 5 1 4.76 14.31 4.73 o -3 5 1 208.09 193.77 3.78 o -2 5 1 233.99 231.69 4.36 o -1 5 1 1.27 2.03 1.17 o 0 5 1 1.55 2.15 0.54 o 1 5 1 91.96 91.07 2.26 o 2 5 1 33.58 29.55 1.38 o 3 5 1 2.59 2.54 1.07 o 4 5 1 76.29 68.65 1.35 o 5 5 1 0.82 1.07 0.47 o 6 5 1 1.45 1.20 0.51 o 7 5 1 1.98 0.79 0.44 o 8 5 1 1.77 0.97 0.61 o -7 6 1 1.45 1.13 0.82 o -6 6 1 15.17 12.95 0.83 o -5 6 1 11.76 10.15 1.04 o -4 6 1 36.31 41.40 1.46 o -3 6 1 683.14 685.08 10.65 o -2 6 1 237.38 245.74 4.37 o -1 6 1 156.14 163.14 8.82 o 0 6 1 0.03 -0.67 1.97 o 1 6 1 8.07 7.91 1.53 o 2 6 1 72.04 76.50 1.92 o 3 6 1 9.69 6.60 0.84 o 4 6 1 55.36 46.14 1.62 o 5 6 1 69.94 75.35 1.90 o 6 6 1 2.39 3.60 0.71 o 7 6 1 13.90 14.83 0.96 o -4 7 1 31.85 34.30 1.56 o -3 7 1 101.40 113.28 2.64 o -2 7 1 11.84 13.78 0.93 o -1 7 1 6.74 5.53 1.88 o 0 7 1 34.68 41.58 3.00 o 1 7 1 8.88 7.93 1.42 o 2 7 1 1.71 1.16 0.85 o 3 7 1 13.40 13.27 1.23 o 4 7 1 60.28 68.92 1.92 o -11 0 2 154.32 162.78 3.79 o -10 0 2 6.13 6.19 0.86 o -9 0 2 104.74 81.60 1.89 o -8 0 2 96.47 88.95 1.76 o -7 0 2 3.53 3.09 0.55 o -6 0 2 475.36 475.45 4.82 o -5 0 2 4485.49 4500.02 58.02 o -4 0 2 4049.04 3907.29 48.31 o -3 0 2 46.49 48.91 0.61 o -2 0 2 3276.81 2964.79 39.05 o -1 0 2 2503.74 2351.34 26.36 o 0 0 2 235.57 228.95 1.58 o 1 0 2 3995.26 3822.91 60.56 o 2 0 2 3133.59 2907.39 37.99 o 3 0 2 694.09 661.09 5.75 o 4 0 2 217.54 259.47 2.23 o 5 0 2 1103.98 1179.85 11.48 o 6 0 2 325.03 365.37 3.68 o 7 0 2 358.43 349.57 5.44 o 8 0 2 108.09 101.38 1.75 o 9 0 2 6.46 7.46 0.87 o 10 0 2 29.46 23.90 1.34 o 11 0 2 3.33 3.43 1.00 o -11 1 2 16.20 16.23 1.02 o -10 1 2 103.78 100.09 1.64 o -9 1 2 11.03 8.79 0.53 o -8 1 2 32.62 27.25 0.73 o -7 1 2 45.63 43.80 0.84 o -6 1 2 370.00 395.84 3.46 o -5 1 2 38.99 36.87 0.45 o -4 1 2 444.21 494.24 3.70 o -3 1 2 524.22 472.74 3.10 o -2 1 2 388.74 346.91 2.48 o -1 1 2 0.19 1.68 0.34 o 0 1 2 942.79 868.41 6.05 o 1 1 2 4166.42 4124.78 33.99 o 2 1 2 1874.42 1713.16 13.13 o 3 1 2 250.75 235.64 1.85 o 4 1 2 620.08 635.31 4.32 o 5 1 2 0.73 1.54 0.20 o 6 1 2 405.95 411.76 2.83 o 7 1 2 13.81 13.91 0.54 o 8 1 2 14.02 14.60 0.68 o 9 1 2 49.03 40.08 0.92 o 10 1 2 38.87 36.88 0.83 o 11 1 2 0.04 0.04 0.32 o -11 2 2 0.02 -0.25 0.75 o -10 2 2 6.41 6.72 0.58 o -9 2 2 6.97 6.73 0.57 o -8 2 2 0.27 0.83 0.45 o -7 2 2 0.63 0.97 0.47 o -6 2 2 3.03 7.15 1.12 o -5 2 2 35.08 43.50 0.62 o -4 2 2 40.29 40.01 1.17 o -3 2 2 239.83 236.49 2.21 o -2 2 2 250.27 246.40 1.83 o -1 2 2 0.82 1.44 0.39 o 0 2 2 17.94 16.55 0.40 o 1 2 2 1052.90 1065.36 9.48 o 2 2 2 2540.87 2417.88 20.77 o 3 2 2 279.51 323.88 2.42 o 4 2 2 55.06 47.39 0.49 o 5 2 2 122.12 125.25 0.99 o 6 2 2 178.44 181.48 1.77 o 7 2 2 45.99 42.92 2.17 o 8 2 2 1636.43 1660.92 23.83 o 9 2 2 287.03 302.48 4.82 o 10 2 2 4.11 6.12 0.86 o 11 2 2 16.12 15.80 0.78 o -10 3 2 1.99 1.49 0.53 o -9 3 2 2.51 2.44 0.61 o -8 3 2 393.82 403.52 5.41 o -7 3 2 655.91 687.59 12.58 o -6 3 2 220.62 221.37 3.30 o -5 3 2 115.80 129.71 2.32 o -4 3 2 506.60 541.06 5.12 o -3 3 2 430.61 483.83 3.92 o -2 3 2 299.47 333.11 2.83 o -1 3 2 926.05 930.73 8.36 o 0 3 2 641.40 629.09 6.25 o 1 3 2 667.98 756.06 6.74 o 2 3 2 438.85 535.58 4.36 o 3 3 2 217.62 262.06 2.26 o 4 3 2 390.29 394.29 3.79 o 5 3 2 22.54 24.44 2.03 o 6 3 2 287.01 280.12 6.73 o 7 3 2 1.26 1.76 0.50 o 8 3 2 191.55 194.06 3.10 o 9 3 2 91.10 97.91 2.05 o 10 3 2 0.28 0.43 0.54 o -10 4 2 64.53 70.10 3.32 o -9 4 2 4.30 4.31 0.51 o -8 4 2 0.00 2.86 1.11 o -7 4 2 1.94 1.61 0.47 o -6 4 2 14.48 17.58 2.49 o -5 4 2 23.56 25.70 0.81 o -4 4 2 425.66 444.91 5.59 o -3 4 2 13.20 15.39 0.46 o -2 4 2 0.09 0.32 0.21 o -1 4 2 56.12 81.29 2.17 o 0 4 2 505.84 528.56 20.80 o 1 4 2 12.01 10.74 0.68 o 2 4 2 69.37 72.50 1.24 o 3 4 2 0.68 1.66 0.55 o 4 4 2 1.09 7.27 2.04 o 5 4 2 133.90 151.30 2.19 o 6 4 2 361.03 353.39 4.45 o 7 4 2 0.23 0.44 0.42 o 8 4 2 0.60 0.47 0.34 o 9 4 2 7.74 7.38 0.91 o -8 5 2 5.41 5.97 0.47 o -7 5 2 3.71 3.60 0.44 o -6 5 2 35.42 34.25 1.15 o -5 5 2 38.95 33.10 1.07 o -4 5 2 20.98 15.32 2.32 o -3 5 2 2.90 5.96 0.92 o -2 5 2 7.09 8.32 0.93 o -1 5 2 238.05 231.68 4.47 o 0 5 2 107.09 102.15 2.30 o 1 5 2 78.37 79.05 2.29 o 2 5 2 22.05 23.23 1.34 o 3 5 2 25.80 24.14 0.96 o 4 5 2 12.16 7.46 0.69 o 5 5 2 45.45 42.95 3.44 o 6 5 2 0.87 2.94 0.57 o 7 5 2 2.20 0.98 0.47 o 8 5 2 42.15 48.65 1.24 o -7 6 2 37.61 55.86 2.19 o -6 6 2 51.30 49.99 1.35 o -5 6 2 5.22 4.41 0.83 o -4 6 2 37.74 35.40 1.25 o -3 6 2 164.66 177.26 3.56 o -2 6 2 214.19 211.91 3.69 o -1 6 2 98.65 96.52 3.13 o 0 6 2 7.46 8.82 2.60 o 1 6 2 35.29 37.63 1.25 o 2 6 2 124.37 124.56 2.65 o 3 6 2 0.12 0.78 0.62 o 4 6 2 168.89 159.95 2.80 o 5 6 2 1.78 1.49 0.68 o 6 6 2 11.94 13.16 0.93 o 7 6 2 2.36 2.64 0.70 o -4 7 2 25.76 32.22 1.29 o -3 7 2 3.53 6.66 0.89 o -2 7 2 53.50 55.65 1.58 o -1 7 2 3.34 14.86 6.67 o 0 7 2 8.32 9.62 1.88 o 1 7 2 1.57 0.99 1.07 o 2 7 2 16.01 17.93 2.29 o 3 7 2 50.82 55.35 1.68 o 4 7 2 86.22 81.60 2.80 o -11 1 3 26.05 24.11 0.81 o -10 1 3 7.82 6.94 0.58 o -9 1 3 47.53 41.30 0.94 o -8 1 3 29.51 27.29 0.69 o -7 1 3 74.89 63.48 0.98 o -6 1 3 49.39 55.67 0.90 o -5 1 3 41.48 44.07 0.54 o -4 1 3 19.93 19.23 0.36 o -3 1 3 242.88 224.98 1.46 o -2 1 3 5.42 6.46 0.26 o -1 1 3 1484.46 1315.78 10.36 o 0 1 3 668.21 628.43 4.75 o 1 1 3 14078.38 14867.22 242.41 o 2 1 3 4.55 4.27 0.24 o 3 1 3 80.79 86.33 0.65 o 4 1 3 939.43 894.39 6.22 o 5 1 3 0.60 1.83 0.32 o 6 1 3 552.04 575.27 4.09 o 7 1 3 9.61 12.60 0.50 o 8 1 3 264.73 259.70 3.43 o 9 1 3 100.68 92.83 1.46 o 10 1 3 37.53 39.35 1.21 o 11 1 3 6.14 4.52 0.85 o -11 2 3 3.72 2.07 0.90 o -10 2 3 8.89 9.52 0.74 o -9 2 3 4.51 21.75 10.43 o -8 2 3 288.03 286.44 3.51 o -7 2 3 599.32 597.26 7.13 o -6 2 3 275.49 256.49 2.74 o -5 2 3 31.26 21.17 0.46 o -4 2 3 19.81 18.47 0.36 o -3 2 3 42.83 42.53 0.78 o -2 2 3 510.93 473.26 3.34 o -1 2 3 1424.15 1370.15 10.70 o 0 2 3 29.50 23.79 0.34 o 1 2 3 31.10 37.16 0.55 o 2 2 3 1555.63 1582.40 13.40 o 3 2 3 1157.00 1191.90 9.20 o 4 2 3 392.17 401.31 3.03 o 5 2 3 33.64 26.40 0.39 o 6 2 3 51.17 40.43 0.60 o 7 2 3 758.67 756.46 8.33 o 8 2 3 30.67 35.61 3.70 o 9 2 3 85.23 91.27 2.19 o 10 2 3 32.26 36.38 1.39 o 11 2 3 3.78 2.82 0.59 o -10 3 3 271.12 259.92 18.38 o -9 3 3 41.31 47.79 4.02 o -8 3 3 356.19 359.26 4.84 o -7 3 3 384.65 384.73 4.94 o -6 3 3 1883.72 1781.45 21.76 o -5 3 3 235.63 231.23 2.41 o -4 3 3 1380.72 1382.76 12.04 o -3 3 3 1313.23 1448.13 12.56 o -2 3 3 656.74 696.17 5.90 o -1 3 3 19.72 19.24 0.43 o 0 3 3 538.14 541.85 4.70 o 1 3 3 572.69 579.38 4.84 o 2 3 3 347.42 422.24 3.26 o 3 3 3 83.39 77.85 0.85 o 4 3 3 22.84 17.83 0.82 o 5 3 3 152.43 147.11 2.19 o 6 3 3 358.07 349.07 4.62 o 7 3 3 53.52 54.48 1.24 o 8 3 3 155.39 161.13 2.62 o 9 3 3 0.36 1.37 0.67 o 10 3 3 0.81 0.71 0.51 o -9 4 3 1.47 3.57 0.88 o -8 4 3 11.79 12.60 0.95 o -7 4 3 11.97 12.42 0.67 o -6 4 3 367.48 366.23 5.13 o -5 4 3 131.65 126.34 1.98 o -4 4 3 0.89 2.28 0.73 o -3 4 3 7.29 7.11 0.41 o -2 4 3 60.23 60.52 0.82 o -1 4 3 18.16 11.34 0.46 o 0 4 3 818.05 829.72 22.65 o 1 4 3 0.92 2.13 0.44 o 2 4 3 246.87 266.91 9.10 o 3 4 3 38.00 32.70 0.93 o 4 4 3 16.87 14.13 0.72 o 5 4 3 7.07 8.99 0.79 o 6 4 3 157.42 151.94 2.17 o 7 4 3 225.13 228.33 2.78 o 8 4 3 4.32 6.52 0.54 o 9 4 3 6.05 6.12 0.65 o -8 5 3 0.41 0.29 0.36 o -7 5 3 1.19 1.20 0.36 o -6 5 3 45.37 42.62 1.32 o -5 5 3 32.02 32.58 1.10 o -4 5 3 2.40 1.51 0.79 o -3 5 3 10.76 11.19 1.15 o -2 5 3 198.19 185.87 3.27 o -1 5 3 4.17 3.63 0.62 o 0 5 3 17.06 12.63 0.89 o 1 5 3 170.47 166.71 3.53 o 2 5 3 94.35 90.10 1.83 o 3 5 3 65.94 56.80 1.33 o 4 5 3 33.92 28.95 1.00 o 5 5 3 3.87 4.59 1.03 o 6 5 3 40.08 36.40 1.15 o 7 5 3 54.84 50.22 1.24 o 8 5 3 6.95 7.01 0.75 o -7 6 3 0.01 -0.11 0.46 o -6 6 3 18.88 18.04 0.85 o -5 6 3 2.31 2.49 0.94 o -4 6 3 49.48 44.99 1.53 o -3 6 3 13.43 14.04 1.05 o -2 6 3 25.21 21.70 1.15 o -1 6 3 353.97 360.71 7.91 o 0 6 3 9.38 9.66 2.43 o 1 6 3 96.08 99.26 2.11 o 2 6 3 3.35 4.18 0.74 o 3 6 3 6.81 5.05 0.80 o 4 6 3 8.95 8.92 0.85 o 5 6 3 74.66 81.77 2.61 o 6 6 3 11.83 12.38 1.26 o -4 7 3 0.15 0.23 0.58 o -3 7 3 6.70 5.57 1.06 o -2 7 3 18.55 16.35 0.96 o -1 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