#------------------------------------------------------------------------------ #$Date: 2010-12-22 21:36:50 +0200 (Wed, 22 Dec 2010) $ #$Revision: 5269 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2227683.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2227683_Fobs loop_ _publ_author_name 'Loh, Wan-Sin' 'Hemamalini, Madhukar' 'Fun, Hoong-Kun' _publ_section_title ; 8-Hydroxyquinolin-1-ium nitrate ; _journal_coeditor_code IS2609 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2907 _journal_page_last o2908 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 128.882 _cell_angle_gamma 90.000 _cell_length_a 11.3186 _cell_length_b 6.7568 _cell_length_c 14.5006 _exptl_crystal_F_000 432.00 _reflns_d_resolution_high 0.7696 _[local]_cod_data_source_file is2609Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' jac16m in P21/c (100K)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 173.40 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 4.51 -0.26 0.65 o 3 0 0 572.47 565.95 13.52 o 4 0 0 1624.66 1890.10 23.82 o 5 0 0 407.98 368.92 4.42 o 6 0 0 844.44 869.45 9.41 o 7 0 0 44.84 36.30 1.34 o 8 0 0 34.73 28.36 1.30 o 9 0 0 2.91 6.02 0.81 o 10 0 0 74.76 81.70 3.67 o 11 0 0 47.75 68.71 2.43 o 1 1 0 0.08 0.89 0.30 o 3 1 0 48.53 54.13 0.97 o 4 1 0 1187.49 1223.72 11.33 o 5 1 0 76.15 58.22 0.97 o 6 1 0 12.01 9.34 0.53 o 7 1 0 71.47 66.74 1.86 o 8 1 0 16.43 16.53 0.75 o 9 1 0 126.20 123.06 1.99 o 10 1 0 7.16 7.19 0.82 o 11 1 0 23.49 32.78 1.61 o 0 2 0 9375.22 8866.16 120.45 o 1 2 0 1299.43 1319.34 15.52 o 2 2 0 186.17 185.29 2.57 o 3 2 0 459.86 466.17 6.47 o 4 2 0 215.10 225.04 4.44 o 5 2 0 53.82 51.04 1.06 o 6 2 0 92.29 99.93 1.58 o 7 2 0 9.24 10.89 0.78 o 8 2 0 106.10 101.15 1.99 o 9 2 0 1.83 1.10 0.53 o 10 2 0 16.45 15.64 1.00 o 11 2 0 2.21 3.07 0.76 o 1 3 0 258.93 239.26 3.24 o 2 3 0 562.36 534.89 6.55 o 3 3 0 122.76 129.47 2.01 o 4 3 0 2019.87 2024.66 21.43 o 5 3 0 202.57 192.02 3.27 o 6 3 0 49.74 44.32 1.38 o 7 3 0 137.14 132.66 3.02 o 8 3 0 19.81 20.43 1.48 o 9 3 0 331.50 323.92 5.78 o 10 3 0 7.28 8.58 0.95 o 0 4 0 9831.47 10075.80 163.98 o 1 4 0 2688.10 2918.22 25.76 o 2 4 0 250.47 252.74 3.02 o 3 4 0 48.75 50.97 1.25 o 4 4 0 29.30 33.87 1.26 o 5 4 0 46.35 45.78 1.53 o 6 4 0 91.92 86.31 2.36 o 7 4 0 18.41 18.93 1.38 o 8 4 0 24.26 24.02 1.65 o 9 4 0 26.11 26.59 1.83 o 10 4 0 6.19 4.81 1.54 o 1 5 0 457.99 459.77 5.47 o 2 5 0 246.55 248.23 3.85 o 3 5 0 0.31 0.82 0.43 o 4 5 0 26.05 24.58 1.22 o 5 5 0 107.01 109.11 2.40 o 6 5 0 17.60 21.23 1.93 o 7 5 0 0.02 -0.73 0.71 o 8 5 0 11.44 6.74 2.27 o 9 5 0 32.04 36.20 2.21 o 0 6 0 912.71 893.58 13.80 o 1 6 0 22.22 26.07 1.26 o 2 6 0 22.29 23.47 0.95 o 3 6 0 9.86 10.46 0.78 o 4 6 0 0.04 -0.25 0.50 o 5 6 0 20.95 21.73 1.32 o 6 6 0 43.01 41.91 1.92 o 7 6 0 62.98 63.52 2.61 o 8 6 0 82.30 76.86 2.95 o 1 7 0 101.82 101.52 5.02 o 2 7 0 3.20 3.77 1.39 o 3 7 0 87.90 85.41 2.90 o 4 7 0 179.44 180.66 3.33 o 5 7 0 36.48 39.32 1.70 o 6 7 0 0.24 0.38 0.72 o 0 8 0 738.41 737.46 21.77 o 1 8 0 350.68 359.31 7.47 o 2 8 0 7.66 6.52 1.42 o 3 8 0 5.57 4.81 0.78 o 4 8 0 21.49 18.66 1.37 o -11 1 1 212.47 233.69 3.98 o -10 1 1 430.98 426.51 5.34 o -9 1 1 48.81 47.90 1.15 o -8 1 1 325.26 309.78 3.59 o -7 1 1 296.77 280.76 2.94 o -6 1 1 1396.92 1405.71 10.63 o -5 1 1 818.69 913.54 7.40 o -4 1 1 0.54 0.50 0.21 o -3 1 1 508.36 481.11 7.96 o -2 1 1 353.06 330.63 9.04 o -1 1 1 111.44 123.35 2.06 o 0 1 1 1148.44 1142.03 25.43 o 1 1 1 2289.52 2375.55 39.73 o 2 1 1 1168.41 1160.93 18.02 o 3 1 1 4496.24 4505.97 43.25 o 4 1 1 13.64 22.26 0.59 o 5 1 1 826.78 858.25 7.23 o 6 1 1 3.66 2.75 0.37 o 7 1 1 0.91 0.82 0.36 o 8 1 1 260.49 239.36 3.01 o 9 1 1 36.68 32.41 1.36 o 10 1 1 3.42 2.27 0.67 o -11 2 1 12.93 16.07 1.05 o -10 2 1 37.66 44.49 1.70 o -9 2 1 196.94 198.81 3.06 o -8 2 1 15.47 15.36 0.90 o -7 2 1 0.63 0.85 0.43 o -6 2 1 266.31 254.49 2.54 o -5 2 1 2.46 0.68 0.25 o -4 2 1 558.73 500.47 32.97 o -3 2 1 432.85 442.49 6.47 o -2 2 1 2519.96 2297.13 55.23 o -1 2 1 30067.73 27953.95 377.88 o 0 2 1 12917.57 13220.14 137.32 o 1 2 1 701.19 695.49 9.75 o 2 2 1 104.28 102.06 2.03 o 3 2 1 1283.93 1367.56 13.40 o 4 2 1 230.62 239.19 2.86 o 5 2 1 354.60 366.92 3.82 o 6 2 1 13.60 14.54 0.75 o 7 2 1 11.16 13.73 0.87 o 8 2 1 0.21 0.10 0.50 o 9 2 1 52.56 53.30 1.61 o 10 2 1 75.75 81.31 2.03 o -11 3 1 17.18 25.28 1.66 o -10 3 1 8.44 9.46 1.05 o -9 3 1 2.02 1.71 0.83 o -8 3 1 285.31 275.87 4.28 o -7 3 1 73.51 66.80 1.69 o -6 3 1 52.91 49.82 1.43 o -5 3 1 217.87 211.07 2.84 o -4 3 1 133.18 126.85 2.75 o -3 3 1 122.65 119.08 1.84 o -2 3 1 336.21 341.06 3.73 o -1 3 1 240.82 248.83 3.34 o 0 3 1 1773.99 1845.22 19.57 o 1 3 1 152.07 143.91 2.88 o 2 3 1 1.72 1.93 0.35 o 3 3 1 92.52 108.77 1.83 o 4 3 1 862.20 920.28 8.39 o 5 3 1 31.44 30.66 1.47 o 6 3 1 18.16 19.11 1.30 o 7 3 1 15.01 12.54 1.18 o 8 3 1 1.20 1.63 0.81 o 9 3 1 36.12 37.87 1.84 o 10 3 1 16.51 15.09 1.44 o -10 4 1 0.94 1.04 0.87 o -9 4 1 182.39 191.22 4.17 o -8 4 1 25.01 27.07 1.83 o -7 4 1 2.20 0.74 0.59 o -6 4 1 2.68 2.69 0.67 o -5 4 1 33.34 36.42 1.48 o -4 4 1 342.65 312.17 4.64 o -3 4 1 2.78 3.03 0.39 o -2 4 1 480.96 461.55 4.96 o -1 4 1 2731.72 2733.45 26.26 o 0 4 1 27.62 22.23 1.00 o 1 4 1 50.78 51.53 1.27 o 2 4 1 8.38 6.87 0.65 o 3 4 1 37.33 35.48 1.03 o 4 4 1 0.02 0.31 0.50 o 5 4 1 261.97 264.59 4.61 o 6 4 1 77.27 73.06 2.04 o 7 4 1 63.66 60.50 2.42 o 8 4 1 0.98 1.07 0.68 o 9 4 1 23.11 21.29 1.76 o -9 5 1 3.21 3.51 1.09 o -8 5 1 245.09 242.58 4.34 o -7 5 1 31.97 31.36 1.79 o -6 5 1 72.99 75.99 2.79 o -5 5 1 0.20 0.92 0.57 o -4 5 1 181.07 181.13 2.98 o -3 5 1 0.55 1.13 0.42 o -2 5 1 117.56 122.72 1.83 o -1 5 1 12.39 12.01 0.79 o 0 5 1 29.41 24.62 1.05 o 1 5 1 0.46 0.50 0.44 o 2 5 1 32.49 34.38 1.01 o 3 5 1 568.18 590.17 7.39 o 4 5 1 399.35 407.45 5.49 o 5 5 1 59.89 60.11 1.81 o 6 5 1 15.84 12.68 1.33 o 7 5 1 0.21 0.63 0.85 o 8 5 1 6.80 8.83 2.10 o -8 6 1 24.21 27.04 2.21 o -7 6 1 78.84 81.03 2.35 o -6 6 1 92.42 93.41 2.41 o -5 6 1 30.29 29.93 1.55 o -4 6 1 65.29 64.59 1.95 o -3 6 1 67.64 67.63 2.32 o -2 6 1 0.01 0.17 0.44 o -1 6 1 518.42 544.36 6.51 o 0 6 1 2731.84 2857.58 27.65 o 1 6 1 38.50 42.10 1.57 o 2 6 1 1.17 2.03 0.56 o 3 6 1 76.97 76.15 2.25 o 4 6 1 26.55 30.19 1.40 o 5 6 1 13.58 14.30 1.46 o 6 6 1 31.09 31.31 2.58 o 7 6 1 59.49 61.89 2.69 o -7 7 1 111.12 108.81 3.17 o -6 7 1 13.49 14.38 2.37 o -5 7 1 13.20 13.17 1.40 o -4 7 1 4.92 5.44 0.99 o -3 7 1 3.99 4.05 0.69 o -2 7 1 3.36 2.90 1.03 o -1 7 1 56.57 55.84 1.56 o 0 7 1 598.65 594.44 7.90 o 1 7 1 5.13 6.79 1.54 o 2 7 1 1.76 1.60 1.04 o 3 7 1 0.00 0.16 0.58 o 4 7 1 69.45 72.10 2.04 o 5 7 1 18.92 20.92 1.95 o 6 7 1 79.78 80.71 3.01 o -5 8 1 4.02 5.81 0.99 o -4 8 1 4.10 4.89 0.93 o -3 8 1 13.09 12.86 1.23 o -2 8 1 5.12 3.51 0.72 o -1 8 1 79.08 74.16 2.10 o 0 8 1 258.78 270.35 7.66 o 1 8 1 6.87 7.52 1.40 o 2 8 1 4.05 2.47 1.31 o 3 8 1 0.06 1.11 0.90 o 4 8 1 1.35 1.75 0.97 o -12 0 2 11.76 12.72 1.34 o -11 0 2 9.18 13.26 1.58 o -10 0 2 327.11 313.06 7.11 o -9 0 2 76.37 82.32 2.40 o -8 0 2 1275.76 1187.15 14.09 o -7 0 2 464.81 463.42 6.12 o -6 0 2 3.05 7.53 0.59 o -5 0 2 2344.41 2354.91 29.44 o -4 0 2 370.14 368.18 8.08 o -3 0 2 8064.67 7669.58 169.88 o -2 0 2 3364.05 3217.57 66.58 o 0 0 2 3775.04 3739.33 84.91 o 1 0 2 233.83 231.38 6.24 o 2 0 2 765.90 830.33 10.81 o 3 0 2 582.77 537.39 7.48 o 4 0 2 59.13 75.65 1.64 o 5 0 2 699.78 726.76 9.00 o 6 0 2 143.38 122.61 2.53 o 7 0 2 1.41 -0.51 0.47 o 8 0 2 13.35 9.69 1.45 o 9 0 2 42.95 39.44 1.94 o 10 0 2 104.88 103.69 2.95 o -12 1 2 176.72 195.63 3.64 o -11 1 2 0.84 0.00 0.61 o -10 1 2 9.47 8.92 0.68 o -9 1 2 308.69 301.25 3.53 o -8 1 2 625.32 597.29 5.87 o -7 1 2 2.49 2.15 0.33 o -6 1 2 34.50 30.97 0.66 o -5 1 2 12.76 8.86 0.38 o -4 1 2 108.63 110.65 1.42 o -3 1 2 0.36 2.28 0.54 o -2 1 2 0.15 0.12 0.20 o -1 1 2 115.83 108.83 2.46 o 0 1 2 1707.14 1756.35 27.56 o 1 1 2 1606.44 1550.24 19.69 o 2 1 2 128.37 116.94 2.07 o 3 1 2 1082.12 1216.08 11.05 o 4 1 2 836.21 910.87 7.17 o 5 1 2 14.96 15.37 0.62 o 6 1 2 104.69 94.36 1.50 o 7 1 2 30.34 23.58 0.83 o 8 1 2 0.04 0.44 0.54 o 9 1 2 5.51 4.79 0.75 o 10 1 2 11.21 13.17 1.49 o -12 2 2 1.18 2.33 0.75 o -11 2 2 0.29 0.20 0.57 o -10 2 2 52.95 49.40 1.52 o -9 2 2 1.17 1.14 0.51 o -8 2 2 8.47 5.57 0.61 o -7 2 2 45.99 50.93 1.21 o -6 2 2 62.90 61.50 1.08 o -5 2 2 518.36 519.99 5.26 o -4 2 2 140.57 114.32 16.05 o -3 2 2 761.88 703.49 8.62 o -2 2 2 1860.74 1839.64 23.16 o -1 2 2 1154.56 1171.24 13.84 o 0 2 2 529.22 548.25 7.86 o 1 2 2 22.00 21.55 1.21 o 2 2 2 74.53 80.40 1.54 o 3 2 2 3.23 6.05 0.43 o 4 2 2 35.32 37.71 1.88 o 5 2 2 79.27 82.66 1.59 o 6 2 2 41.71 36.21 1.13 o 7 2 2 32.84 32.80 1.29 o 8 2 2 1.03 0.77 0.54 o 9 2 2 0.18 -0.02 0.51 o 10 2 2 1.48 1.41 0.93 o -11 3 2 11.68 7.43 1.03 o -10 3 2 5.21 3.92 0.93 o -9 3 2 345.79 343.71 5.10 o -8 3 2 358.28 358.96 4.65 o -7 3 2 38.43 36.73 1.27 o -6 3 2 9.50 9.18 0.75 o -5 3 2 44.62 36.97 2.25 o -4 3 2 274.51 260.35 4.87 o -3 3 2 37.85 28.81 0.76 o -2 3 2 56.15 56.32 1.03 o -1 3 2 827.86 772.11 8.66 o 0 3 2 912.54 960.17 11.84 o 1 3 2 2116.34 2083.94 23.25 o 2 3 2 54.36 56.24 1.26 o 3 3 2 439.98 489.70 5.34 o 4 3 2 980.10 1018.45 10.22 o 5 3 2 99.82 95.89 2.25 o 6 3 2 139.06 143.29 3.20 o 7 3 2 5.60 4.35 1.03 o 8 3 2 8.42 9.80 1.38 o 9 3 2 9.86 8.72 1.24 o -11 4 2 1.75 1.28 1.03 o -10 4 2 38.04 37.30 2.02 o -9 4 2 125.45 131.74 3.06 o -8 4 2 903.93 902.64 9.65 o -7 4 2 70.44 64.15 3.29 o -6 4 2 76.07 79.96 1.98 o -5 4 2 3.29 1.19 0.56 o -4 4 2 4.79 3.87 1.06 o -3 4 2 302.83 312.45 3.64 o -2 4 2 167.50 162.83 2.31 o -1 4 2 2738.07 2975.39 28.46 o 0 4 2 85.89 108.02 2.08 o 1 4 2 71.99 66.16 1.16 o 2 4 2 5.03 5.52 0.76 o 3 4 2 398.10 413.30 5.44 o 4 4 2 1.04 0.61 1.17 o 5 4 2 93.68 87.75 2.39 o 6 4 2 0.03 -0.01 0.87 o 7 4 2 144.45 139.28 3.89 o 8 4 2 2.52 1.34 0.76 o 9 4 2 44.54 38.55 2.31 o -10 5 2 17.79 19.13 1.82 o -9 5 2 49.64 50.19 4.14 o -8 5 2 566.99 575.43 7.73 o -7 5 2 138.74 131.88 2.82 o -6 5 2 119.06 122.61 2.82 o -5 5 2 14.98 15.37 1.11 o -4 5 2 15.58 14.43 0.88 o -3 5 2 92.25 95.43 1.66 o -2 5 2 52.87 54.33 1.17 o -1 5 2 1262.51 1297.46 13.16 o 0 5 2 1.44 -0.06 0.44 o 1 5 2 35.76 36.15 1.63 o 2 5 2 9.72 10.00 0.66 o 3 5 2 475.24 489.09 7.37 o 4 5 2 12.21 14.03 1.31 o 5 5 2 80.46 76.49 2.59 o 6 5 2 0.05 -0.26 0.73 o 7 5 2 53.23 51.66 2.89 o 8 5 2 38.03 37.23 2.26 o -9 6 2 17.50 20.05 2.02 o -8 6 2 127.79 125.40 8.04 o -7 6 2 13.59 15.90 1.99 o -6 6 2 0.00 -0.22 0.58 o -5 6 2 33.68 29.20 1.91 o -4 6 2 3.67 3.23 0.67 o -3 6 2 41.86 38.86 1.32 o -2 6 2 6.36 7.88 0.60 o -1 6 2 128.59 133.49 2.75 o 0 6 2 19.55 21.86 1.30 o 1 6 2 90.30 92.53 2.69 o 2 6 2 29.90 29.47 1.14 o 3 6 2 67.58 66.12 2.08 o 4 6 2 45.71 48.39 3.28 o 5 6 2 76.63 84.19 2.86 o 6 6 2 1.44 1.55 0.99 o 7 6 2 21.70 22.07 2.01 o -7 7 2 5.12 3.83 0.99 o -6 7 2 173.94 187.43 4.17 o -5 7 2 0.03 -1.14 0.67 o -4 7 2 30.53 29.81 1.61 o -3 7 2 30.85 30.80 1.45 o -2 7 2 0.08 0.39 0.49 o -1 7 2 6.65 5.10 0.80 o 0 7 2 41.19 42.52 1.74 o 1 7 2 98.73 104.05 3.02 o 2 7 2 6.55 6.40 1.30 o 3 7 2 326.97 319.03 5.98 o 4 7 2 111.00 108.73 3.31 o 5 7 2 2.09 1.33 1.05 o -5 8 2 41.24 39.05 2.04 o -4 8 2 32.49 31.76 2.36 o -3 8 2 34.03 31.53 3.40 o -2 8 2 6.37 6.46 0.97 o -1 8 2 410.32 416.45 7.21 o 0 8 2 90.25 83.91 4.03 o 1 8 2 34.59 41.08 2.72 o 2 8 2 41.89 38.11 2.30 o 3 8 2 1.96 0.96 0.95 o -12 1 3 49.02 56.63 1.87 o -11 1 3 1.11 1.06 0.48 o -10 1 3 40.01 38.77 1.14 o -9 1 3 436.02 414.93 4.46 o -8 1 3 300.08 287.54 3.06 o -7 1 3 242.35 262.66 2.45 o -6 1 3 441.22 427.45 3.63 o -5 1 3 512.31 573.39 5.16 o -4 1 3 1113.35 1030.77 10.34 o -3 1 3 56.09 70.97 1.31 o -2 1 3 127.23 114.92 2.89 o -1 1 3 3299.76 3308.02 52.70 o 0 1 3 2973.83 2802.08 43.02 o 1 1 3 938.52 1009.03 12.43 o 2 1 3 178.19 199.83 2.46 o 3 1 3 1219.77 1442.52 11.52 o 4 1 3 220.71 221.87 2.53 o 5 1 3 438.30 424.66 4.11 o 6 1 3 9.95 5.50 0.49 o 7 1 3 25.90 29.81 1.15 o 8 1 3 0.84 0.48 0.57 o 9 1 3 3.37 2.19 0.70 o -12 2 3 13.71 16.42 1.12 o -11 2 3 15.05 14.76 1.46 o -10 2 3 11.29 10.99 0.78 o -9 2 3 1561.37 1555.11 13.76 o -8 2 3 2849.75 2820.05 22.23 o -7 2 3 153.88 142.41 1.86 o -6 2 3 265.59 248.78 2.88 o -5 2 3 732.66 825.62 10.87 o -4 2 3 338.14 376.69 7.99 o -3 2 3 459.99 553.00 6.18 o -2 2 3 739.53 693.45 6.28 o -1 2 3 109.16 115.38 2.79 o 0 2 3 114.16 132.95 3.73 o 1 2 3 667.88 657.52 20.11 o 2 2 3 35.21 28.52 0.82 o 3 2 3 158.03 165.52 2.28 o 4 2 3 481.55 462.43 4.42 o 5 2 3 205.32 201.58 3.31 o 6 2 3 175.20 146.81 2.49 o 7 2 3 555.11 469.09 6.94 o 8 2 3 4.47 2.14 0.62 o 9 2 3 35.82 24.21 1.31 o -12 3 3 53.63 53.54 2.12 o -11 3 3 58.16 53.77 1.94 o -10 3 3 5.07 4.84 0.74 o -9 3 3 422.85 431.41 5.43 o -8 3 3 446.24 442.54 5.34 o -7 3 3 196.57 197.62 2.90 o -6 3 3 89.69 93.48 2.51 o -5 3 3 60.61 50.89 1.72 o -4 3 3 76.76 76.22 1.78 o -3 3 3 114.75 120.02 1.68 o -2 3 3 44.30 48.34 1.03 o -1 3 3 12.05 20.94 0.87 o 0 3 3 2.12 2.83 0.53 o 1 3 3 16.84 16.01 1.11 o 2 3 3 307.67 314.13 4.22 o 3 3 3 175.58 196.58 2.79 o 4 3 3 32.39 32.45 1.41 o 5 3 3 0.67 0.48 0.69 o 6 3 3 25.64 22.66 1.38 o 7 3 3 112.14 96.02 2.54 o 8 3 3 45.80 46.42 2.49 o 9 3 3 19.97 26.28 3.20 o -11 4 3 13.07 13.35 1.49 o -10 4 3 30.45 30.48 1.93 o -9 4 3 51.40 49.21 1.68 o -8 4 3 244.15 246.21 4.08 o -7 4 3 0.23 -0.51 0.36 o -6 4 3 109.23 103.29 2.21 o -5 4 3 45.34 45.44 1.52 o -4 4 3 4.29 4.28 0.54 o -3 4 3 8.06 6.69 0.60 o -2 4 3 227.37 216.23 2.44 o -1 4 3 56.20 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