#------------------------------------------------------------------------------ #$Date: 2010-12-22 21:36:50 +0200 (Wed, 22 Dec 2010) $ #$Revision: 5269 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2227684.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2227684_Fobs loop_ _publ_author_name 'Kessler, Monty' 'Spannenberg, Anke' 'Rosenthal, Uwe' _publ_section_title ; Iodidobis(\h^5^-pentamethylcyclopentadienyl)titanium(III) ; _journal_coeditor_code IS2610 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1400 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 103.158 _cell_angle_gamma 90.000 _cell_length_a 8.5513 _cell_length_b 14.1353 _cell_length_c 16.9547 _exptl_crystal_F_000 900.00 _reflns_d_resolution_high 0.7286 _[local]_cod_data_source_file is2610Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ks1157m in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 246.01 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1069.38 1302.83 48.34 o 4 0 0 23144.22 22779.30 266.36 o 6 0 0 6451.03 6092.32 118.36 o 8 0 0 4214.11 4032.24 77.39 o 10 0 0 3074.85 3152.36 68.85 o 1 1 0 274.24 339.20 47.59 o 2 1 0 9291.85 9527.23 55.24 o 3 1 0 5218.20 5276.56 39.54 o 4 1 0 9057.74 8781.93 69.37 o 5 1 0 81.84 90.90 27.09 o 6 1 0 465.12 502.63 29.18 o 7 1 0 593.19 597.50 34.27 o 8 1 0 3194.56 3045.54 70.65 o 9 1 0 86.72 85.72 37.32 o 10 1 0 517.09 532.98 46.03 o 11 1 0 122.53 151.08 52.16 o 0 2 0 60519.57 67364.02 1121.63 o 1 2 0 22418.52 24720.51 132.73 o 2 2 0 935.72 1057.30 39.51 o 3 2 0 362.48 369.01 32.08 o 4 2 0 18207.92 18677.27 96.11 o 5 2 0 5269.91 4895.23 36.73 o 6 2 0 8787.27 8800.88 109.71 o 7 2 0 1213.82 1177.56 32.70 o 8 2 0 1242.38 1254.06 38.82 o 9 2 0 2470.09 2391.54 42.30 o 10 2 0 2350.93 2358.40 46.09 o 11 2 0 471.64 478.01 54.73 o 1 3 0 2561.78 2741.10 54.20 o 2 3 0 2607.24 2777.39 43.49 o 3 3 0 7764.99 7665.94 48.95 o 4 3 0 1933.23 1848.91 33.28 o 5 3 0 885.03 899.23 30.53 o 6 3 0 734.42 754.39 31.70 o 7 3 0 1581.83 1488.46 33.52 o 8 3 0 786.05 825.71 37.35 o 9 3 0 1393.58 1393.57 41.48 o 10 3 0 472.12 525.33 48.21 o 11 3 0 128.44 154.96 55.43 o 0 4 0 4369.32 4518.10 84.19 o 1 4 0 34763.07 36219.33 415.19 o 2 4 0 46.52 93.33 38.02 o 3 4 0 11468.96 11968.13 89.91 o 4 4 0 4821.79 4884.67 40.18 o 5 4 0 21370.25 21142.79 77.74 o 6 4 0 2572.79 2680.96 36.73 o 7 4 0 1.58 0.37 33.39 o 8 4 0 151.60 145.58 40.53 o 9 4 0 4399.02 4312.37 49.15 o 10 4 0 191.56 201.65 55.38 o 11 4 0 149.73 143.65 57.86 o 1 5 0 5577.29 5764.40 54.83 o 2 5 0 468.61 579.34 36.95 o 3 5 0 9843.59 9496.46 65.13 o 4 5 0 160.92 152.02 31.14 o 5 5 0 580.96 558.08 32.52 o 6 5 0 944.01 910.99 34.16 o 7 5 0 2263.42 2253.07 37.62 o 8 5 0 14.22 54.93 37.24 o 9 5 0 1823.75 1896.48 46.55 o 10 5 0 94.84 105.66 51.93 o 11 5 0 28.24 28.79 74.92 o 0 6 0 3974.33 4091.45 67.53 o 1 6 0 20327.94 20108.87 284.89 o 2 6 0 8.27 33.17 35.14 o 3 6 0 5148.71 5388.39 67.56 o 4 6 0 4018.37 3974.34 45.98 o 5 6 0 13628.00 13667.87 67.22 o 6 6 0 29.18 42.35 33.45 o 7 6 0 17.77 59.30 34.57 o 8 6 0 152.29 181.42 36.88 o 9 6 0 2851.55 2861.43 52.77 o 10 6 0 285.00 253.55 51.02 o 1 7 0 433.46 492.53 35.08 o 2 7 0 1546.65 1503.21 39.45 o 3 7 0 4321.89 4107.69 40.42 o 4 7 0 1664.11 1724.99 35.77 o 5 7 0 55.87 74.86 32.17 o 6 7 0 848.54 841.42 36.50 o 7 7 0 580.09 636.44 37.81 o 8 7 0 1348.05 1340.47 42.08 o 9 7 0 1499.94 1554.72 48.71 o 10 7 0 2.41 30.08 54.95 o 0 8 0 29240.02 29174.03 779.09 o 1 8 0 5415.66 5382.47 95.96 o 2 8 0 2110.20 2160.00 42.42 o 3 8 0 148.21 157.23 34.40 o 4 8 0 7802.10 7806.44 120.63 o 5 8 0 4072.52 4002.18 41.05 o 6 8 0 3235.60 3228.48 41.30 o 7 8 0 725.59 711.58 37.70 o 8 8 0 1124.84 1104.02 41.05 o 9 8 0 943.51 1047.09 49.30 o 10 8 0 1400.11 1368.91 55.73 o 1 9 0 0.21 50.95 38.64 o 2 9 0 5447.21 5506.82 83.16 o 3 9 0 703.82 679.50 34.88 o 4 9 0 4005.06 3971.86 42.00 o 5 9 0 97.62 92.06 34.90 o 6 9 0 234.01 240.97 37.87 o 7 9 0 11.83 25.18 39.52 o 8 9 0 1703.52 1768.86 44.99 o 9 9 0 327.49 377.13 60.51 o 10 9 0 216.09 208.12 55.49 o 0 10 0 17000.47 16876.96 535.65 o 1 10 0 129.31 188.25 40.88 o 2 10 0 1284.71 1217.59 41.75 o 3 10 0 2.09 43.71 34.33 o 4 10 0 8631.86 8300.72 81.64 o 5 10 0 10.49 29.05 36.86 o 6 10 0 4337.85 4249.52 46.48 o 7 10 0 602.10 639.30 43.95 o 8 10 0 1169.39 1230.30 52.32 o 9 10 0 236.72 246.97 59.95 o 1 11 0 1012.85 986.19 43.32 o 2 11 0 3075.52 2948.74 47.93 o 3 11 0 271.96 310.30 37.53 o 4 11 0 1905.61 1885.07 42.14 o 5 11 0 238.08 199.61 38.14 o 6 11 0 49.82 24.61 39.31 o 7 11 0 5.96 28.22 44.46 o 8 11 0 1822.33 1974.05 52.44 o 9 11 0 1.81 -17.69 50.54 o 0 12 0 5572.91 5595.75 175.61 o 1 12 0 2161.41 2073.93 45.17 o 2 12 0 345.79 344.82 37.86 o 3 12 0 761.13 760.20 40.19 o 4 12 0 3286.19 3280.07 44.98 o 5 12 0 2491.00 2484.05 44.91 o 6 12 0 1079.90 1142.39 46.27 o 7 12 0 127.48 125.66 44.09 o 8 12 0 64.75 24.39 49.42 o 1 13 0 5.07 37.97 42.27 o 2 13 0 543.15 590.94 43.16 o 3 13 0 573.60 617.02 43.00 o 4 13 0 821.33 808.83 42.86 o 5 13 0 283.26 298.65 40.44 o 6 13 0 28.69 24.20 44.57 o 7 13 0 584.07 598.05 52.87 o 8 13 0 696.50 760.57 66.70 o 0 14 0 407.66 355.57 79.69 o 1 14 0 4463.28 4437.40 51.86 o 2 14 0 178.01 159.00 42.23 o 3 14 0 597.01 590.18 41.30 o 4 14 0 367.59 418.67 44.10 o 5 14 0 2998.45 3098.52 52.79 o 6 14 0 182.58 224.20 48.06 o 7 14 0 0.98 11.99 68.66 o 1 15 0 164.64 167.91 46.17 o 2 15 0 1.55 27.91 45.00 o 3 15 0 432.92 478.15 45.54 o 4 15 0 87.64 87.70 49.50 o 5 15 0 40.58 81.32 50.85 o 6 15 0 159.92 180.07 52.92 o 7 15 0 525.04 501.18 75.55 o 0 16 0 979.57 1005.14 81.43 o 1 16 0 2093.90 2119.16 60.22 o 2 16 0 172.41 179.95 48.06 o 3 16 0 550.14 544.08 51.94 o 4 16 0 520.85 518.37 51.82 o 5 16 0 1874.08 1837.79 58.98 o 6 16 0 1.59 18.54 58.18 o 1 17 0 92.78 103.06 60.83 o 2 17 0 78.25 86.42 63.14 o 3 17 0 342.57 375.16 50.06 o 4 17 0 134.55 197.58 56.37 o 5 17 0 199.60 191.24 60.91 o 0 18 0 2368.12 2413.96 115.32 o 1 18 0 743.90 783.34 72.66 o 2 18 0 0.83 0.37 68.51 o 3 18 0 334.93 301.63 69.48 o 4 18 0 1113.91 980.12 73.30 o 1 19 0 17.51 47.85 86.71 o 2 19 0 45.96 30.61 76.59 o -11 0 1 1654.51 1569.48 67.13 o -9 0 1 580.09 544.65 54.21 o -7 0 1 14891.17 14246.62 263.70 o -5 0 1 11876.39 11626.98 100.56 o -3 0 1 11104.11 10862.53 137.54 o -1 0 1 315.65 362.22 60.17 o 1 0 1 1853.41 2436.59 98.16 o 3 0 1 21.79 48.86 46.23 o 5 0 1 6898.12 7114.66 115.03 o 7 0 1 1266.27 1119.39 52.34 o 9 0 1 534.53 571.95 56.02 o 11 0 1 817.30 733.34 76.89 o -11 1 1 372.82 341.16 51.70 o -10 1 1 12.22 15.31 42.86 o -9 1 1 362.15 392.90 44.65 o -8 1 1 112.58 164.14 33.82 o -7 1 1 5315.79 5307.01 47.92 o -6 1 1 55.93 66.69 25.53 o -5 1 1 532.56 554.06 27.08 o -4 1 1 276.18 257.98 27.21 o -3 1 1 39217.60 40294.06 211.03 o -2 1 1 4382.32 4756.27 46.25 o -1 1 1 56966.52 64828.76 386.94 o 0 1 1 347.30 409.77 116.53 o 1 1 1 4226.70 4876.41 77.25 o 2 1 1 3142.44 3453.48 43.51 o 3 1 1 26472.78 25970.89 194.82 o 4 1 1 174.15 308.03 28.45 o 5 1 1 42.81 87.96 28.50 o 6 1 1 1259.86 1291.02 34.16 o 7 1 1 13302.44 12768.35 122.76 o 8 1 1 948.04 939.44 37.78 o 9 1 1 794.73 804.68 41.64 o 10 1 1 6.97 68.70 41.22 o 11 1 1 1180.11 1083.68 51.33 o -11 2 1 1795.33 1772.98 54.83 o -10 2 1 796.34 809.66 46.56 o -9 2 1 509.84 527.96 38.95 o -8 2 1 831.16 829.06 34.61 o -7 2 1 3559.62 3464.68 37.40 o -6 2 1 6051.56 5945.96 63.62 o -5 2 1 2928.66 2719.39 31.52 o -4 2 1 4213.92 4577.88 35.90 o -3 2 1 735.40 682.25 30.71 o -2 2 1 2965.56 3087.45 42.77 o -1 2 1 9658.52 10419.86 82.69 o 0 2 1 245.67 316.42 61.85 o 1 2 1 3526.50 3662.82 68.65 o 2 2 1 151.37 192.62 40.07 o 3 2 1 4411.43 4646.95 43.12 o 4 2 1 2894.23 3081.91 34.66 o 5 2 1 2935.38 2810.81 40.56 o 6 2 1 1940.88 1876.84 44.80 o 7 2 1 10.30 16.23 34.15 o 8 2 1 19.16 45.54 36.81 o 9 2 1 355.67 361.42 38.41 o 10 2 1 666.91 693.46 43.68 o 11 2 1 955.28 944.53 58.27 o -11 3 1 156.38 186.83 58.19 o -10 3 1 142.18 160.66 49.69 o -9 3 1 336.22 352.28 41.90 o -8 3 1 1823.02 1789.36 36.02 o -7 3 1 2554.11 2545.68 33.82 o -6 3 1 2642.96 2595.31 34.67 o -5 3 1 661.67 760.34 30.74 o -4 3 1 4819.06 4827.67 39.25 o -3 3 1 4552.49 4409.74 43.72 o -2 3 1 38641.09 40670.92 312.21 o -1 3 1 1897.63 1997.12 46.47 o 0 3 1 1463.40 1588.67 60.94 o 1 3 1 6404.53 6501.42 73.01 o 2 3 1 33351.46 34294.22 283.09 o 3 3 1 10077.02 9932.67 82.69 o 4 3 1 2460.74 2330.24 35.28 o 5 3 1 12.26 44.10 28.78 o 6 3 1 7457.31 7578.23 59.70 o 7 3 1 3834.92 3650.82 41.85 o 8 3 1 5551.90 5422.25 58.63 o 9 3 1 980.33 977.69 44.85 o 10 3 1 99.15 93.48 45.52 o 11 3 1 606.54 630.26 56.95 o -11 4 1 620.09 627.48 57.48 o -10 4 1 2152.94 2225.41 53.76 o -9 4 1 23.62 60.62 43.33 o -8 4 1 1019.01 982.79 35.85 o -7 4 1 467.35 436.17 34.09 o -6 4 1 10644.02 10395.46 121.33 o -5 4 1 2.83 38.96 31.01 o -4 4 1 649.77 577.57 31.93 o -3 4 1 92.72 108.27 32.54 o -2 4 1 23821.89 23832.99 90.60 o -1 4 1 5904.77 6297.66 53.72 o 0 4 1 9294.40 9544.75 75.03 o 1 4 1 126.21 170.88 39.79 o 2 4 1 359.05 410.22 38.87 o 3 4 1 299.47 339.34 30.63 o 4 4 1 1756.47 1623.83 33.94 o 5 4 1 426.64 452.58 31.85 o 6 4 1 2435.72 2356.81 36.34 o 7 4 1 52.93 60.03 37.42 o 8 4 1 66.86 112.72 38.75 o 9 4 1 0.39 23.33 44.06 o 10 4 1 804.11 855.07 53.09 o 11 4 1 294.44 314.61 56.41 o -11 5 1 96.84 119.01 61.76 o -10 5 1 26.83 38.81 51.16 o -9 5 1 4.85 7.61 40.06 o -8 5 1 3428.75 3415.39 41.95 o -7 5 1 180.56 139.63 34.27 o -6 5 1 1719.58 1737.83 36.18 o -5 5 1 0.59 4.72 32.11 o -4 5 1 3883.39 3839.20 40.28 o -3 5 1 174.88 265.84 31.93 o -2 5 1 22340.13 21777.12 202.94 o -1 5 1 1730.77 1918.42 41.38 o 0 5 1 539.63 576.02 39.91 o 1 5 1 4.85 21.31 40.19 o 2 5 1 43729.84 44215.22 184.18 o 3 5 1 1061.10 1243.85 32.77 o 4 5 1 8633.97 8554.77 53.04 o 5 5 1 178.57 211.75 31.87 o 6 5 1 7569.36 7560.57 80.62 o 7 5 1 0.19 -16.51 38.51 o 8 5 1 8585.69 8408.98 77.05 o 9 5 1 191.17 202.09 45.89 o 10 5 1 280.60 271.11 51.27 o -10 6 1 1535.34 1614.22 51.83 o -9 6 1 561.73 557.24 39.56 o -8 6 1 505.79 502.93 39.58 o -7 6 1 0.97 16.36 35.86 o -6 6 1 8801.05 8599.83 67.94 o -5 6 1 575.41 582.88 31.94 o -4 6 1 226.14 170.81 33.43 o -3 6 1 578.59 636.84 34.54 o -2 6 1 7400.03 7315.17 48.86 o -1 6 1 522.80 733.98 38.56 o 0 6 1 6436.99 6478.30 69.24 o 1 6 1 444.51 452.52 41.10 o 2 6 1 54.94 80.55 37.92 o 3 6 1 411.19 374.72 39.02 o 4 6 1 4055.53 3961.72 38.97 o 5 6 1 527.72 543.57 31.96 o 6 6 1 2526.55 2496.31 37.69 o 7 6 1 2.51 -19.52 35.45 o 8 6 1 16.61 52.54 44.31 o 9 6 1 370.90 391.05 47.79 o 10 6 1 1234.01 1323.22 59.62 o -10 7 1 0.24 41.68 54.05 o -9 7 1 206.74 271.60 43.82 o -8 7 1 1694.47 1731.31 42.15 o -7 7 1 1379.20 1380.90 38.00 o -6 7 1 1306.10 1347.91 36.58 o -5 7 1 1124.82 1137.92 34.87 o -4 7 1 3783.60 3769.41 39.91 o -3 7 1 12129.30 12369.70 129.65 o -2 7 1 15564.55 15325.90 111.40 o -1 7 1 3771.11 3942.29 66.43 o 0 7 1 52.59 85.74 33.28 o 1 7 1 2785.70 2569.44 60.78 o 2 7 1 12643.58 12029.53 91.30 o 3 7 1 4847.52 4774.82 56.14 o 4 7 1 3739.19 3847.44 38.59 o 5 7 1 724.35 791.40 33.02 o 6 7 1 5148.94 5173.57 67.98 o 7 7 1 3060.84 2953.75 40.12 o 8 7 1 3926.42 3984.54 54.31 o 9 7 1 1.94 30.28 56.92 o 10 7 1 30.21 60.38 56.19 o -10 8 1 201.14 218.26 64.88 o -9 8 1 454.64 412.62 43.11 o -8 8 1 718.26 778.75 40.14 o -7 8 1 1163.84 1168.64 39.51 o -6 8 1 641.85 656.06 36.75 o -5 8 1 5275.41 5151.17 44.93 o -4 8 1 186.64 225.53 34.14 o -3 8 1 320.08 289.75 35.04 o -2 8 1 2371.65 2395.28 37.49 o -1 8 1 4926.34 4663.11 77.39 o 0 8 1 1855.69 1836.44 39.60 o 1 8 1 1220.67 1167.72 40.05 o 2 8 1 128.87 169.59 35.60 o 3 8 1 2294.42 2271.29 49.65 o 4 8 1 2248.78 2251.84 34.69 o 5 8 1 494.45 534.94 33.19 o 6 8 1 231.89 268.40 34.39 o 7 8 1 163.80 181.96 37.35 o 8 8 1 65.73 98.45 44.19 o 9 8 1 251.36 264.23 51.73 o 10 8 1 474.50 558.03 54.96 o -10 9 1 405.08 426.63 54.72 o -9 9 1 156.68 193.61 51.34 o -8 9 1 125.68 167.09 42.08 o -7 9 1 3496.77 3556.53 43.62 o -6 9 1 53.71 78.96 34.79 o -5 9 1 0.17 30.70 32.77 o -4 9 1 298.96 324.71 35.04 o -3 9 1 10559.14 10295.91 78.18 o -2 9 1 1281.01 1263.05 37.24 o -1 9 1 12093.39 12055.01 189.07 o 0 9 1 29.22 63.03 35.44 o 1 9 1 5637.60 5335.07 86.42 o 2 9 1 801.68 860.79 42.57 o 3 9 1 7725.21 7579.53 102.08 o 4 9 1 3046.62 3046.06 39.10 o 5 9 1 38.55 54.70 34.66 o 6 9 1 0.24 38.47 37.94 o 7 9 1 8244.93 8147.36 50.79 o 8 9 1 656.67 696.90 50.86 o 9 9 1 189.69 210.07 64.12 o -9 10 1 178.40 190.41 51.87 o -8 10 1 74.87 106.50 42.53 o -7 10 1 1725.98 1807.51 43.94 o -6 10 1 62.87 91.76 40.22 o -5 10 1 2414.26 2385.92 42.99 o -4 10 1 581.00 548.96 38.19 o -3 10 1 158.06 165.52 35.94 o -2 10 1 1.86 44.63 35.52 o -1 10 1 3624.95 3629.06 52.05 o 0 10 1 0.50 63.42 38.54 o 1 10 1 3823.74 3834.16 56.71 o 2 10 1 16.83 32.20 39.99 o 3 10 1 714.85 667.48 41.61 o 4 10 1 98.75 103.70 34.05 o 5 10 1 543.06 578.25 35.86 o 6 10 1 203.21 265.07 40.85 o 7 10 1 315.70 371.77 46.65 o 8 10 1 437.49 465.03 57.94 o 9 10 1 400.21 467.71 66.58 o -9 11 1 352.39 372.67 47.99 o -8 11 1 235.13 265.07 41.41 o -7 11 1 2106.47 2184.33 43.08 o -6 11 1 349.61 363.33 41.62 o -5 11 1 64.18 82.48 37.25 o -4 11 1 721.34 747.21 39.15 o -3 11 1 5073.23 5163.77 46.43 o -2 11 1 665.12 644.91 38.66 o -1 11 1 2672.62 2588.68 41.33 o 0 11 1 8.82 0.14 40.40 o 1 11 1 4591.13 4175.98 51.25 o 2 11 1 327.00 340.98 40.76 o 3 11 1 8603.39 8485.01 97.08 o 4 11 1 53.92 62.99 37.30 o 5 11 1 135.09 132.18 36.47 o 6 11 1 2341.63 2259.27 46.69 o 7 11 1 4698.79 4757.89 73.28 o 8 11 1 352.86 361.67 47.73 o 9 11 1 276.48 274.11 57.21 o -9 12 1 0.50 18.45 64.81 o -8 12 1 0.20 8.97 48.47 o -7 12 1 925.20 945.75 47.15 o -6 12 1 1202.62 1221.58 43.99 o -5 12 1 2241.08 2215.35 45.78 o -4 12 1 450.62 422.18 40.32 o -3 12 1 231.79 287.41 36.91 o -2 12 1 2149.86 2133.00 42.23 o -1 12 1 757.59 719.63 39.53 o 0 12 1 1693.80 1656.07 47.35 o 1 12 1 335.50 353.36 41.89 o 2 12 1 51.44 18.37 42.39 o 3 12 1 21.22 30.21 39.50 o 4 12 1 510.90 507.50 37.82 o 5 12 1 1963.83 2016.16 43.13 o 6 12 1 0.52 -11.20 44.53 o 7 12 1 452.92 484.80 52.36 o 8 12 1 177.94 182.44 60.76 o -8 13 1 594.13 605.82 49.85 o -7 13 1 201.93 257.58 48.47 o -6 13 1 1099.68 1032.90 42.81 o -5 13 1 0.88 -2.27 42.81 o -4 13 1 403.94 389.48 45.06 o -3 13 1 784.29 794.20 41.73 o -2 13 1 7306.27 7011.33 64.63 o -1 13 1 438.74 432.35 39.74 o 0 13 1 9.38 11.99 42.41 o 1 13 1 1410.64 1428.92 46.34 o 2 13 1 8910.74 8491.46 94.25 o 3 13 1 3445.01 3437.42 54.63 o 4 13 1 600.70 615.79 46.05 o 5 13 1 47.27 52.08 42.34 o 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