#------------------------------------------------------------------------------ #$Date: 2010-12-22 21:36:50 +0200 (Wed, 22 Dec 2010) $ #$Revision: 5269 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2227686.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2227686_Fobs loop_ _publ_author_name 'Kumar, Raju Suresh' 'Osman, Hasnah' 'Ali, Mohamed Ashraf' 'Hemamalini, Madhukar' 'Fun, Hoong-Kun' _publ_section_title ; 11-[(E)-4-Bromobenzylidene]-8-(4-bromophenyl)-14-hydroxy-3,13-diazaheptacyclo[13.7.1.1^9,13^.0^2,9^.0^2,14^.0^3,7^.0^19,23^]tetracosa-1(22),15,17,19(23),20-pentaen-10-one ; _journal_coeditor_code IS2614 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2926 _journal_page_last o2927 _journal_volume 66 _journal_year 2010 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 79.868 _cell_angle_beta 80.705 _cell_angle_gamma 77.359 _cell_length_a 8.4833 _cell_length_b 11.8334 _cell_length_c 14.8942 _exptl_crystal_F_000 676.00 _reflns_d_resolution_high 0.7697 _[local]_cod_data_source_file is2614Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' mo_pbracp_0m in P-1 (100K)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 137.62 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 347.49 369.56 13.69 o 2 0 0 668.68 616.42 18.18 o 3 0 0 218.85 248.71 9.88 o 4 0 0 3725.76 3838.49 104.44 o 5 0 0 344.40 308.12 14.03 o 6 0 0 2273.40 2433.50 56.68 o 7 0 0 2025.11 2074.39 49.69 o 8 0 0 1131.20 1101.91 30.34 o 9 0 0 958.68 1017.73 54.22 o 10 0 0 27.14 32.87 18.58 o -9 1 0 10.87 7.02 11.95 o -8 1 0 1614.03 1616.52 42.68 o -7 1 0 1300.09 1325.92 34.32 o -6 1 0 1289.87 1339.34 33.44 o -5 1 0 979.36 1040.08 32.27 o -4 1 0 405.84 406.53 14.98 o -3 1 0 237.13 221.63 9.21 o -2 1 0 3581.34 3781.72 187.96 o 1 1 0 199.93 216.49 6.71 o 2 1 0 592.36 682.59 19.84 o 3 1 0 380.96 359.89 12.66 o 4 1 0 2094.08 2202.07 68.16 o 5 1 0 3036.39 3177.81 71.69 o 6 1 0 472.52 473.25 19.17 o 7 1 0 3419.98 3394.16 77.75 o 8 1 0 1054.64 1019.19 36.53 o 9 1 0 175.64 164.16 22.41 o 10 1 0 36.61 61.00 19.92 o -9 2 0 33.06 49.14 11.32 o -8 2 0 1102.58 1112.73 38.76 o -7 2 0 137.70 140.23 9.85 o -6 2 0 3627.90 3685.87 83.85 o -5 2 0 188.35 231.25 12.27 o -4 2 0 8995.95 9261.60 247.34 o -3 2 0 290.37 306.22 16.59 o -2 2 0 7634.27 7603.57 283.40 o -1 2 0 9.33 15.06 2.68 o 1 2 0 1027.14 1100.80 30.04 o 2 2 0 219.17 213.15 7.43 o 3 2 0 13088.49 13981.41 513.06 o 4 2 0 242.17 234.74 9.05 o 5 2 0 340.42 320.60 10.72 o 6 2 0 607.69 626.40 17.73 o 7 2 0 839.84 847.99 30.41 o 8 2 0 163.42 155.48 20.55 o 9 2 0 863.49 949.09 52.26 o 10 2 0 25.80 43.70 19.85 o -10 3 0 311.00 303.41 32.32 o -9 3 0 15.44 6.78 12.59 o -8 3 0 1705.52 1729.69 68.66 o -7 3 0 124.04 129.34 10.39 o -6 3 0 2806.60 2830.34 65.73 o -5 3 0 457.81 427.40 24.92 o -4 3 0 669.79 664.34 21.39 o -3 3 0 1391.81 1336.89 38.02 o -2 3 0 116.15 144.01 6.62 o -1 3 0 4145.29 4305.77 165.46 o 0 3 0 1706.81 1762.73 38.18 o 2 3 0 86.28 120.79 8.61 o 3 3 0 8148.35 8194.50 213.54 o 4 3 0 4636.96 5207.16 140.78 o 5 3 0 6058.83 6198.76 167.88 o 6 3 0 764.19 817.47 21.48 o 7 3 0 2164.90 2127.34 91.59 o 8 3 0 315.50 277.95 26.12 o 9 3 0 110.27 97.75 21.34 o 10 3 0 787.26 831.77 51.21 o -9 4 0 61.88 61.99 14.65 o -8 4 0 343.34 362.10 21.37 o -7 4 0 324.04 335.06 20.95 o -6 4 0 1510.58 1535.02 38.42 o -5 4 0 421.90 417.97 16.63 o -4 4 0 1542.05 1541.27 45.57 o -3 4 0 93.23 78.55 12.32 o -2 4 0 2572.99 2662.69 72.11 o -1 4 0 2323.61 2451.89 95.45 o 0 4 0 2460.98 2582.51 69.22 o 1 4 0 1396.70 1425.83 41.66 o 2 4 0 7.90 10.14 2.54 o 3 4 0 2309.03 2384.02 90.32 o 4 4 0 71.08 60.55 6.07 o 5 4 0 998.81 950.24 30.47 o 6 4 0 521.45 543.16 21.66 o 7 4 0 15.18 17.61 13.22 o 8 4 0 362.16 375.08 30.51 o 9 4 0 300.79 294.83 28.57 o 10 4 0 144.00 126.42 25.53 o -9 5 0 152.91 148.60 17.99 o -8 5 0 223.90 240.81 19.16 o -7 5 0 374.36 380.18 38.67 o -6 5 0 1070.88 1052.58 52.23 o -5 5 0 991.85 961.34 30.22 o -4 5 0 251.60 233.28 11.55 o -3 5 0 6756.07 6709.09 179.46 o -2 5 0 2.01 0.60 2.05 o 0 5 0 129.83 99.60 3.85 o 2 5 0 24.51 30.09 3.28 o 3 5 0 9806.88 10148.22 220.75 o 4 5 0 242.45 227.35 12.40 o 5 5 0 500.99 405.55 21.72 o 6 5 0 827.81 760.53 41.50 o 7 5 0 1532.53 1459.10 68.87 o 8 5 0 492.34 492.20 37.62 o 9 5 0 128.44 120.70 23.39 o 10 5 0 503.74 523.42 43.79 o -8 6 0 12.02 15.88 13.09 o -7 6 0 232.62 224.13 17.80 o -6 6 0 1227.03 1240.12 41.71 o -5 6 0 1577.08 1535.58 49.01 o -4 6 0 118.44 145.50 12.82 o -3 6 0 1898.76 1925.60 76.89 o -2 6 0 1.82 0.46 3.76 o -1 6 0 51.05 59.48 7.99 o 0 6 0 28.60 70.90 5.60 o 1 6 0 139.11 152.36 12.99 o 2 6 0 2090.88 2159.08 48.68 o 3 6 0 535.48 563.91 15.11 o 4 6 0 2378.59 2275.17 64.40 o 5 6 0 81.61 82.95 10.00 o 6 6 0 1545.10 1517.36 69.25 o 7 6 0 620.63 627.99 38.72 o 8 6 0 556.14 594.44 42.20 o 9 6 0 64.07 55.45 21.24 o 10 6 0 230.25 253.59 32.56 o -8 7 0 85.16 99.51 16.92 o -7 7 0 497.19 508.51 30.70 o -6 7 0 31.11 29.19 11.90 o -5 7 0 1859.69 1862.33 56.62 o -4 7 0 216.39 201.94 12.62 o -3 7 0 2790.04 2856.14 112.50 o -2 7 0 21.58 15.69 7.27 o -1 7 0 4126.15 4351.55 116.90 o 0 7 0 31.55 37.59 3.79 o 1 7 0 1763.59 1612.30 44.65 o 2 7 0 103.99 119.87 8.40 o 3 7 0 1320.26 1410.06 33.16 o 4 7 0 7.42 15.67 3.88 o 5 7 0 135.67 127.75 12.39 o 6 7 0 605.89 617.71 38.80 o 7 7 0 12.52 27.91 16.27 o 8 7 0 341.82 337.69 32.65 o 9 7 0 35.80 35.20 22.41 o 10 7 0 206.77 248.78 32.44 o -7 8 0 350.45 343.42 28.69 o -6 8 0 34.70 10.25 11.74 o -5 8 0 241.06 221.64 15.95 o -4 8 0 27.00 21.92 9.13 o -3 8 0 584.37 593.93 20.45 o -2 8 0 1471.87 1456.98 41.68 o -1 8 0 109.31 126.15 7.75 o 0 8 0 3098.19 3026.94 137.37 o 1 8 0 18.67 27.38 5.12 o 2 8 0 2282.57 2237.10 50.97 o 3 8 0 943.18 1024.74 66.85 o 4 8 0 4314.67 4417.61 122.39 o 5 8 0 110.24 93.93 16.68 o 6 8 0 671.43 682.23 40.92 o 7 8 0 495.17 485.84 38.70 o 8 8 0 569.46 525.50 41.98 o 9 8 0 28.50 51.47 23.12 o 10 8 0 19.57 4.94 22.57 o -7 9 0 326.03 338.27 32.92 o -6 9 0 23.23 18.87 12.83 o -5 9 0 812.07 822.31 31.75 o -4 9 0 565.78 574.59 30.96 o -3 9 0 106.57 125.24 11.27 o -2 9 0 796.51 872.75 27.13 o -1 9 0 8.81 6.85 4.96 o 0 9 0 86.93 66.36 10.06 o 1 9 0 1634.41 1590.88 43.22 o 2 9 0 0.90 -1.49 3.64 o 3 9 0 436.58 437.79 15.56 o 4 9 0 32.70 34.10 7.41 o 5 9 0 1114.94 1147.52 57.62 o 6 9 0 43.84 56.70 17.85 o 7 9 0 359.63 391.62 34.68 o 8 9 0 397.40 355.18 33.98 o 9 9 0 6.30 -17.60 22.16 o -6 10 0 116.62 108.52 16.14 o -5 10 0 300.59 289.10 19.44 o -4 10 0 421.40 414.90 20.97 o -3 10 0 48.56 27.87 10.29 o -2 10 0 554.14 570.35 36.20 o -1 10 0 69.03 53.60 5.88 o 0 10 0 5428.97 5375.83 119.15 o 1 10 0 101.20 99.57 10.56 o 2 10 0 2428.39 2418.07 55.47 o 3 10 0 46.88 40.10 5.41 o 4 10 0 104.44 116.80 19.10 o 5 10 0 69.46 99.88 19.71 o 6 10 0 328.11 346.78 31.64 o 7 10 0 568.96 516.62 41.90 o 8 10 0 280.02 322.11 35.64 o 9 10 0 138.47 207.27 32.74 o -5 11 0 150.84 165.55 15.96 o -4 11 0 58.47 52.30 11.94 o -3 11 0 4.42 8.24 9.37 o -2 11 0 214.18 239.76 14.63 o -1 11 0 1119.77 1086.83 50.93 o 0 11 0 148.51 147.04 12.58 o 1 11 0 14.26 6.07 13.52 o 2 11 0 94.32 112.80 11.80 o 3 11 0 599.09 584.11 17.45 o 4 11 0 54.74 59.75 7.90 o 5 11 0 728.96 759.61 45.69 o 6 11 0 20.75 35.80 19.27 o 7 11 0 619.83 666.45 47.45 o 8 11 0 0.14 -3.41 21.52 o -4 12 0 187.86 194.50 16.34 o -3 12 0 117.27 124.10 12.85 o -2 12 0 158.42 173.26 17.45 o -1 12 0 215.58 213.32 12.45 o 0 12 0 884.85 847.27 25.41 o 1 12 0 73.84 41.96 11.03 o 2 12 0 1228.74 1199.00 43.97 o 3 12 0 39.22 43.44 5.79 o 4 12 0 150.45 153.03 10.57 o 5 12 0 111.42 119.71 22.54 o 6 12 0 2.62 -7.91 19.71 o 7 12 0 14.16 14.84 22.73 o 8 12 0 4.09 -8.31 24.08 o -3 13 0 409.14 440.43 21.52 o -2 13 0 6.12 2.37 10.33 o -1 13 0 93.10 90.07 8.59 o 0 13 0 250.12 271.18 29.66 o 1 13 0 397.01 412.74 22.02 o 2 13 0 72.95 87.42 13.27 o 3 13 0 1101.04 1126.49 39.36 o 4 13 0 40.80 31.34 7.45 o 5 13 0 303.19 392.27 33.77 o 6 13 0 61.27 69.35 22.08 o 7 13 0 196.78 265.71 33.49 o -2 14 0 138.68 140.86 15.92 o -1 14 0 328.05 345.25 35.93 o 0 14 0 24.04 0.31 21.62 o 1 14 0 25.23 61.59 22.60 o 2 14 0 161.78 210.53 26.82 o 3 14 0 1.36 2.63 16.40 o 4 14 0 325.46 327.28 30.01 o 5 14 0 191.23 198.89 27.16 o 6 14 0 29.69 40.50 23.38 o 1 15 0 331.32 291.27 32.73 o 2 15 0 124.10 131.98 25.29 o 3 15 0 491.01 610.38 41.63 o -5 -14 1 0.94 4.16 19.84 o -4 -14 1 45.01 67.02 19.98 o -3 -14 1 163.53 212.20 24.48 o -2 -14 1 3.40 -0.76 12.53 o -1 -14 1 171.23 170.49 26.27 o 0 -14 1 33.95 33.34 23.63 o 1 -14 1 27.23 27.70 24.48 o -7 -13 1 467.71 473.85 41.22 o -6 -13 1 0.49 -13.30 21.05 o -5 -13 1 191.89 204.10 27.04 o -4 -13 1 338.19 322.42 29.13 o -3 -13 1 705.49 798.23 42.66 o -2 -13 1 6.37 3.50 11.35 o -1 -13 1 390.20 382.56 21.31 o 0 -13 1 66.76 24.22 20.97 o 1 -13 1 331.40 366.52 34.47 o 2 -13 1 80.03 102.55 12.04 o 3 -13 1 4.84 0.59 10.71 o -7 -12 1 6.97 6.69 23.39 o -6 -12 1 60.83 32.56 22.20 o -5 -12 1 7.75 -8.10 16.43 o -4 -12 1 15.90 9.58 16.72 o -3 -12 1 390.14 428.81 18.45 o -2 -12 1 746.32 710.77 20.36 o -1 -12 1 365.05 359.25 27.58 o 0 -12 1 8.72 -2.71 15.97 o 1 -12 1 129.91 177.46 20.55 o 2 -12 1 61.99 56.03 9.87 o 3 -12 1 102.67 114.54 12.49 o 4 -12 1 6.68 10.49 11.72 o -8 -11 1 31.79 36.62 25.37 o -7 -11 1 281.91 353.14 36.06 o -6 -11 1 26.70 44.42 21.47 o -5 -11 1 538.51 546.20 39.39 o -4 -11 1 281.35 306.90 15.59 o -3 -11 1 1161.22 1162.71 29.67 o -2 -11 1 8.23 -0.15 4.78 o -1 -11 1 425.97 439.02 14.35 o 0 -11 1 422.24 518.11 63.61 o 1 -11 1 29.06 32.02 7.28 o 2 -11 1 607.38 593.74 43.53 o 3 -11 1 68.29 77.86 11.39 o 4 -11 1 747.19 755.37 45.78 o 5 -11 1 0.10 15.18 12.05 o -9 -10 1 154.79 94.29 27.78 o -8 -10 1 1.40 8.08 23.22 o -7 -10 1 8.18 19.89 20.39 o -6 -10 1 91.86 106.73 21.95 o -5 -10 1 24.14 14.29 16.95 o -4 -10 1 1216.17 1228.32 30.89 o -3 -10 1 162.30 175.01 11.03 o -2 -10 1 4257.85 4270.68 95.36 o -1 -10 1 140.94 149.38 10.45 o 0 -10 1 14.74 15.12 7.31 o 1 -10 1 206.87 153.11 7.24 o 2 -10 1 93.08 94.74 9.54 o 3 -10 1 42.49 37.08 9.48 o 4 -10 1 193.24 168.39 14.19 o 5 -10 1 40.24 31.17 11.71 o 6 -10 1 0.52 -17.58 12.81 o -9 -9 1 1008.48 1078.36 62.61 o -8 -9 1 26.47 25.55 20.75 o -7 -9 1 149.15 156.05 24.65 o -6 -9 1 17.15 3.28 16.88 o -5 -9 1 301.43 378.71 30.06 o -4 -9 1 224.31 200.70 12.63 o -3 -9 1 216.99 226.63 9.97 o -2 -9 1 553.36 565.57 20.48 o -1 -9 1 31.89 26.32 4.40 o 0 -9 1 1409.55 1507.05 30.79 o 1 -9 1 82.89 72.92 7.96 o 2 -9 1 476.64 426.21 20.53 o 3 -9 1 64.61 61.20 9.34 o 4 -9 1 1077.28 1117.02 37.58 o 5 -9 1 2.88 0.51 10.52 o 6 -9 1 249.11 253.97 20.27 o 7 -9 1 23.63 9.14 14.13 o -10 -8 1 244.23 304.09 37.15 o -9 -8 1 117.21 74.17 24.19 o -8 -8 1 636.16 577.25 42.02 o -7 -8 1 19.46 10.46 18.69 o -6 -8 1 1582.37 1634.32 75.84 o -5 -8 1 33.51 39.15 15.71 o -4 -8 1 4926.88 5085.11 112.84 o -3 -8 1 604.59 679.63 23.70 o -2 -8 1 2339.69 2268.38 59.03 o -1 -8 1 242.39 212.69 8.47 o 0 -8 1 883.74 840.06 20.15 o 1 -8 1 1055.13 968.56 24.36 o 2 -8 1 280.86 303.57 11.20 o 3 -8 1 998.66 964.76 31.76 o 4 -8 1 412.56 389.27 18.96 o 5 -8 1 825.92 813.14 30.79 o 6 -8 1 34.03 29.16 12.22 o 7 -8 1 465.69 455.40 24.40 o -10 -7 1 31.20 28.50 23.39 o -9 -7 1 64.86 107.12 24.67 o -8 -7 1 95.08 91.14 21.49 o -7 -7 1 122.68 124.27 22.52 o -6 -7 1 664.21 710.47 42.44 o -5 -7 1 3.50 -8.28 11.44 o -4 -7 1 14.71 28.78 4.31 o -3 -7 1 121.84 160.56 14.21 o -2 -7 1 92.86 79.26 7.29 o -1 -7 1 1147.42 1173.93 46.75 o 0 -7 1 3856.31 3909.54 184.46 o 1 -7 1 97.05 95.27 5.48 o 2 -7 1 854.38 864.24 27.64 o 3 -7 1 2.18 -2.66 6.14 o 4 -7 1 308.58 305.14 16.17 o 5 -7 1 3.85 2.91 9.65 o 6 -7 1 1.62 4.71 10.88 o 7 -7 1 392.13 362.68 22.16 o 8 -7 1 46.96 41.68 26.80 o -10 -6 1 153.77 154.07 27.65 o -9 -6 1 201.08 207.92 28.42 o -8 -6 1 2736.38 2691.94 118.01 o -7 -6 1 17.25 40.69 17.36 o -6 -6 1 1085.45 1024.66 52.32 o -5 -6 1 14.90 32.28 8.82 o -4 -6 1 4708.15 4929.65 108.92 o -3 -6 1 289.76 299.98 20.52 o -2 -6 1 214.31 203.90 7.81 o -1 -6 1 4965.46 5009.41 110.02 o 0 -6 1 1986.23 2032.95 61.73 o 1 -6 1 3088.04 2889.70 55.41 o 2 -6 1 10.05 7.64 4.60 o 3 -6 1 1994.87 2021.13 79.47 o 4 -6 1 25.04 25.55 4.79 o 5 -6 1 823.91 872.38 30.54 o 6 -6 1 3.31 1.77 9.97 o 7 -6 1 362.34 333.58 32.14 o 8 -6 1 37.24 32.94 17.95 o -10 -5 1 41.78 38.02 22.99 o -9 -5 1 66.79 68.50 20.83 o -8 -5 1 353.82 368.13 32.09 o -7 -5 1 13.61 26.98 16.51 o -6 -5 1 132.62 133.78 17.53 o -4 -5 1 4.29 3.21 4.71 o -3 -5 1 5108.06 5255.14 115.38 o -2 -5 1 60.39 60.09 3.84 o -1 -5 1 1837.49 1831.30 49.79 o 0 -5 1 2558.37 2809.76 53.48 o 1 -5 1 2863.91 2740.77 59.82 o 2 -5 1 1266.52 1193.75 55.60 o 3 -5 1 693.04 849.57 37.45 o 4 -5 1 285.12 275.11 11.99 o 5 -5 1 56.12 54.80 6.09 o 6 -5 1 321.92 317.50 23.42 o 7 -5 1 55.15 45.33 11.99 o 8 -5 1 501.79 509.80 25.99 o 9 -5 1 219.54 208.35 19.35 o -10 -4 1 375.35 419.22 37.26 o -9 -4 1 67.52 72.67 21.31 o -8 -4 1 1394.56 1389.05 68.47 o -7 -4 1 388.00 377.07 29.33 o -6 -4 1 660.83 618.70 23.90 o -5 -4 1 128.78 110.04 9.25 o -4 -4 1 601.76 616.60 28.34 o -3 -4 1 5883.78 6369.65 139.24 o -1 -4 1 644.04 608.44 14.74 o 0 -4 1 8.45 10.60 2.93 o 1 -4 1 126.47 110.62 5.18 o 2 -4 1 29.24 38.84 4.43 o 3 -4 1 3483.69 3519.10 78.45 o 4 -4 1 47.97 67.83 5.98 o 5 -4 1 1386.39 1389.74 34.10 o 6 -4 1 127.93 137.24 12.82 o 7 -4 1 107.64 91.25 14.39 o 8 -4 1 246.16 225.46 37.82 o 9 -4 1 53.83 58.26 14.95 o -10 -3 1 12.61 10.98 20.48 o -9 -3 1 666.05 658.48 43.93 o -8 -3 1 102.25 89.46 19.55 o -7 -3 1 2778.46 2773.01 116.14 o -6 -3 1 35.36 37.98 7.07 o -5 -3 1 6059.56 6212.40 168.47 o -4 -3 1 2544.55 2969.87 82.22 o -3 -3 1 1966.04 1835.66 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29.12 o -7 2 12 304.16 280.93 33.11 o -6 2 12 83.30 106.27 13.32 o -5 2 12 236.56 211.13 14.53 o -4 2 12 743.72 722.43 24.83 o -3 2 12 112.10 136.17 11.57 o -2 2 12 1175.36 1198.17 68.41 o -1 2 12 2625.60 2620.32 54.13 o 0 2 12 1743.99 1729.56 37.44 o 1 2 12 1367.06 1417.25 36.21 o 2 2 12 1380.48 1364.87 30.66 o 3 2 12 36.31 39.11 6.70 o 4 2 12 93.22 88.94 11.31 o 5 2 12 1098.86 1015.52 44.33 o 6 2 12 5.43 15.54 8.31 o 7 2 12 233.49 243.28 30.70 o 8 2 12 9.43 13.46 12.97 o 9 2 12 48.89 54.84 22.83 o -7 3 12 167.86 164.03 19.59 o -6 3 12 27.11 25.36 11.97 o -5 3 12 261.51 257.53 15.85 o -4 3 12 2.77 20.36 9.57 o -3 3 12 90.72 77.60 10.26 o -2 3 12 2540.12 2494.01 60.15 o -1 3 12 184.39 175.52 10.69 o 0 3 12 2655.01 2568.34 77.81 o 1 3 12 430.37 437.04 20.14 o 2 3 12 1692.18 1731.74 43.10 o 3 3 12 69.66 64.75 8.53 o 4 3 12 2804.44 2755.92 65.21 o 5 3 12 23.72 43.08 10.14 o 6 3 12 1935.46 1916.82 48.12 o 7 3 12 361.06 350.26 14.06 o 8 3 12 1042.61 982.78 27.18 o 9 3 12 149.00 153.49 22.55 o -6 4 12 427.22 431.36 63.53 o -5 4 12 211.56 175.94 14.10 o -4 4 12 2587.87 2502.92 61.93 o -3 4 12 50.53 54.18 15.95 o -2 4 12 949.26 1047.00 26.07 o -1 4 12 456.85 457.83 34.37 o 0 4 12 2093.54 2101.86 64.86 o 1 4 12 388.61 392.67 13.46 o 2 4 12 17.71 23.00 7.45 o 3 4 12 3382.20 3363.95 78.11 o 4 4 12 29.79 41.79 8.09 o 5 4 12 1886.92 1827.67 71.10 o 6 4 12 0.12 6.51 6.81 o 7 4 12 1254.24 1275.29 30.67 o 8 4 12 113.01 118.77 11.36 o 9 4 12 510.12 519.03 25.95 o -6 5 12 4.95 13.36 17.01 o -5 5 12 35.52 31.43 11.18 o -4 5 12 343.95 330.35 17.38 o -3 5 12 94.13 111.82 11.66 o -2 5 12 1673.64 1654.76 37.04 o -1 5 12 708.52 696.44 19.22 o 0 5 12 3289.36 3259.32 66.09 o 1 5 12 61.81 56.84 8.84 o 2 5 12 74.86 72.50 8.83 o 3 5 12 6.41 3.89 7.04 o 4 5 12 5582.66 5508.17 124.50 o 5 5 12 255.89 200.50 13.98 o 6 5 12 104.45 108.08 8.95 o 7 5 12 102.31 97.11 9.44 o 8 5 12 123.65 139.72 17.18 o 9 5 12 355.96 380.90 23.18 o -6 6 12 355.70 309.49 30.62 o -5 6 12 30.19 13.25 13.95 o -4 6 12 616.14 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