#------------------------------------------------------------------------------ #$Date: 2016-04-03 04:50:20 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181197 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/76/2227691.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2227691_Fobs loop_ _publ_author_name 'Venter, Gertruida J. S.' 'Steyl, Gideon' 'Roodt, Andreas' _publ_section_title ; 4-[(4-Methylphenyl)amino]pent-3-en-2-one ; _journal_coeditor_code IS2620 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3011 _journal_page_last o3012 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 110.291 _cell_angle_gamma 90.000 _cell_length_a 10.0736 _cell_length_b 10.8800 _cell_length_c 10.0723 _exptl_crystal_F_000 408.00 _reflns_d_resolution_high 0.7828 _cod_data_source_file is2620Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 10Ltv3_0ma in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 163.44 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 17.27 19.10 0.59 o 3 0 0 65.45 56.85 0.75 o 4 0 0 776.99 800.12 6.17 o 5 0 0 200.80 179.43 2.01 o 6 0 0 1707.73 1734.94 16.04 o 7 0 0 68.11 81.71 1.35 o 8 0 0 20.36 18.57 0.84 o 9 0 0 27.56 25.91 1.58 o 10 0 0 24.14 24.75 1.73 o 11 0 0 279.35 282.03 5.80 o 12 0 0 30.22 31.93 2.21 o 2 1 0 372.77 398.82 2.17 o 3 1 0 0.18 0.88 0.11 o 4 1 0 0.12 0.13 0.10 o 5 1 0 385.59 416.05 2.78 o 6 1 0 1822.68 1844.39 10.85 o 7 1 0 186.22 185.27 2.32 o 8 1 0 92.98 90.24 1.28 o 9 1 0 24.72 23.31 0.93 o 10 1 0 23.38 25.59 1.82 o 11 1 0 0.22 0.47 0.55 o 12 1 0 14.75 14.89 1.34 o 0 2 0 1552.67 1375.22 19.12 o 1 2 0 6300.17 5993.69 30.49 o 2 2 0 1829.60 1803.48 10.62 o 3 2 0 0.01 0.32 0.09 o 4 2 0 102.03 103.99 0.96 o 5 2 0 31.23 32.90 0.63 o 6 2 0 101.74 97.69 1.18 o 7 2 0 97.22 90.66 1.28 o 8 2 0 0.13 0.08 0.30 o 9 2 0 17.52 14.67 0.82 o 10 2 0 14.34 15.64 1.13 o 11 2 0 26.63 29.66 1.45 o 1 3 0 675.27 651.19 3.32 o 2 3 0 233.80 269.89 1.71 o 3 3 0 257.20 250.59 1.78 o 4 3 0 46.82 58.58 0.68 o 5 3 0 1.37 1.57 0.19 o 6 3 0 92.04 88.10 1.08 o 7 3 0 51.83 48.45 0.81 o 8 3 0 440.31 429.04 4.25 o 9 3 0 0.88 0.31 0.43 o 10 3 0 46.69 46.82 1.49 o 11 3 0 35.26 36.54 1.85 o 0 4 0 670.55 652.98 4.58 o 1 4 0 1023.12 1042.91 5.12 o 2 4 0 402.46 410.04 2.60 o 3 4 0 12.14 7.91 0.38 o 4 4 0 266.68 265.44 2.04 o 5 4 0 150.82 134.49 1.27 o 6 4 0 5.57 3.29 0.28 o 7 4 0 5.37 4.95 0.43 o 8 4 0 25.74 26.96 1.09 o 9 4 0 116.16 109.99 2.01 o 10 4 0 245.90 245.11 3.92 o 11 4 0 0.79 0.20 0.58 o 1 5 0 117.64 141.77 1.14 o 2 5 0 337.63 293.03 1.89 o 3 5 0 409.22 454.77 3.54 o 4 5 0 372.49 403.65 3.17 o 5 5 0 196.35 194.33 1.90 o 6 5 0 37.79 42.73 0.92 o 7 5 0 1021.91 999.52 8.28 o 8 5 0 146.54 146.75 2.64 o 9 5 0 147.79 152.61 2.60 o 10 5 0 1.01 0.48 0.63 o 11 5 0 1.44 0.72 0.70 o 0 6 0 16.86 23.49 0.74 o 1 6 0 39.40 50.35 0.84 o 2 6 0 353.81 377.52 2.94 o 3 6 0 271.09 304.51 3.02 o 4 6 0 63.30 51.15 0.93 o 5 6 0 84.36 76.17 1.09 o 6 6 0 296.23 300.12 3.01 o 7 6 0 449.04 438.07 5.25 o 8 6 0 52.31 54.32 1.61 o 9 6 0 13.44 15.25 1.02 o 10 6 0 16.77 15.44 1.18 o 1 7 0 949.20 1029.85 6.48 o 2 7 0 114.58 98.07 1.24 o 3 7 0 0.49 -0.14 0.19 o 4 7 0 72.32 62.24 1.07 o 5 7 0 198.70 209.66 2.28 o 6 7 0 63.59 61.70 1.42 o 7 7 0 2.31 1.47 0.53 o 8 7 0 78.66 79.23 2.03 o 9 7 0 85.85 88.63 2.95 o 10 7 0 1.02 0.92 0.72 o 0 8 0 264.73 296.93 5.64 o 1 8 0 9.47 10.05 0.48 o 2 8 0 73.70 71.14 1.08 o 3 8 0 160.27 153.68 3.70 o 4 8 0 80.69 78.91 1.31 o 5 8 0 10.37 7.72 0.74 o 6 8 0 53.08 47.65 1.53 o 7 8 0 56.12 48.84 1.54 o 8 8 0 150.10 145.21 2.91 o 9 8 0 0.61 -0.23 0.65 o 1 9 0 532.01 541.84 4.31 o 2 9 0 262.40 261.23 2.63 o 3 9 0 427.39 396.56 4.33 o 4 9 0 18.67 15.01 1.12 o 5 9 0 87.55 81.85 1.88 o 6 9 0 153.57 154.14 3.38 o 7 9 0 0.13 -0.75 0.57 o 8 9 0 2.80 5.76 0.93 o 9 9 0 3.60 2.88 0.82 o 0 10 0 82.39 85.11 6.23 o 1 10 0 10.51 8.81 0.77 o 2 10 0 54.41 51.31 1.89 o 3 10 0 73.69 71.11 1.82 o 4 10 0 1.01 0.46 0.54 o 5 10 0 17.13 16.72 1.08 o 6 10 0 1.75 1.86 0.65 o 7 10 0 49.75 57.84 1.98 o 8 10 0 1.24 0.04 0.81 o 1 11 0 18.23 15.82 1.53 o 2 11 0 19.54 19.98 1.67 o 3 11 0 8.12 4.68 0.89 o 4 11 0 88.21 91.87 2.74 o 5 11 0 38.29 41.18 1.85 o 6 11 0 53.61 66.27 2.76 o 7 11 0 6.76 6.45 1.05 o 0 12 0 88.14 95.38 4.31 o 1 12 0 1.38 1.38 1.18 o 2 12 0 0.39 -1.58 2.34 o 3 12 0 3.17 3.20 0.91 o 4 12 0 8.32 9.72 1.25 o 5 12 0 87.35 89.84 2.95 o 6 12 0 37.51 56.21 3.89 o 1 13 0 0.61 0.52 1.13 o 2 13 0 44.36 43.23 3.58 o 3 13 0 0.76 1.72 1.43 o 4 13 0 3.17 3.73 1.36 o -12 1 1 8.96 8.81 0.94 o -11 1 1 29.16 27.06 1.27 o -10 1 1 37.25 38.59 1.82 o -9 1 1 0.24 0.29 0.41 o -8 1 1 4.88 5.08 0.36 o -7 1 1 195.20 205.90 1.83 o -6 1 1 493.96 484.04 3.72 o -5 1 1 57.88 61.32 0.78 o -4 1 1 15.63 12.95 0.37 o -3 1 1 219.76 189.66 1.73 o -2 1 1 220.19 205.37 1.89 o -1 1 1 1007.35 649.47 91.53 o 1 1 1 1288.42 1270.47 6.19 o 2 1 1 2892.79 2884.12 13.86 o 3 1 1 370.75 384.96 2.18 o 4 1 1 163.57 179.97 1.31 o 5 1 1 49.52 47.82 0.69 o 6 1 1 167.29 163.30 1.61 o 7 1 1 67.97 65.55 0.95 o 8 1 1 278.39 271.81 2.69 o 9 1 1 37.40 36.56 1.21 o 10 1 1 6.99 5.98 0.95 o 11 1 1 19.09 19.34 1.22 o -12 2 1 2.49 2.88 0.77 o -11 2 1 26.84 27.09 1.29 o -10 2 1 323.60 321.94 6.81 o -9 2 1 24.11 26.17 1.09 o -8 2 1 0.17 0.02 0.26 o -7 2 1 6.97 4.61 0.40 o -6 2 1 4.40 4.24 0.36 o -5 2 1 1102.89 1138.10 8.64 o -4 2 1 18.86 18.08 0.37 o -3 2 1 869.69 868.41 5.88 o -2 2 1 1404.46 1436.92 9.90 o -1 2 1 1625.18 1593.39 8.40 o 0 2 1 2472.47 2457.64 11.68 o 1 2 1 1691.27 1649.57 8.46 o 2 2 1 372.20 371.98 2.19 o 3 2 1 198.46 181.73 1.25 o 4 2 1 39.99 39.32 0.59 o 5 2 1 24.89 19.84 0.51 o 6 2 1 46.06 45.53 0.86 o 7 2 1 2.36 0.99 0.30 o 8 2 1 19.24 15.71 0.84 o 9 2 1 74.68 76.73 1.67 o 10 2 1 78.19 84.48 2.03 o 11 2 1 45.63 47.73 1.78 o -12 3 1 13.17 17.73 1.62 o -11 3 1 43.95 44.37 1.53 o -10 3 1 132.58 131.92 2.41 o -9 3 1 392.18 391.08 5.58 o -8 3 1 342.74 344.39 3.48 o -7 3 1 15.46 14.57 0.67 o -6 3 1 0.78 0.41 0.20 o -5 3 1 323.69 343.86 2.73 o -4 3 1 181.74 178.40 1.85 o -3 3 1 2113.66 2185.51 15.04 o -2 3 1 29.56 36.62 0.39 o -1 3 1 182.55 205.57 1.28 o 0 3 1 160.01 163.13 1.05 o 1 3 1 1908.00 1889.56 9.73 o 2 3 1 695.01 710.60 3.82 o 3 3 1 521.93 561.38 3.25 o 4 3 1 213.43 214.75 1.79 o 5 3 1 0.23 -0.09 0.18 o 6 3 1 0.61 0.97 0.24 o 7 3 1 138.75 138.98 1.65 o 8 3 1 666.63 668.37 6.55 o 9 3 1 42.50 45.21 1.39 o 10 3 1 4.35 4.85 0.77 o 11 3 1 105.76 111.70 2.47 o -11 4 1 2.49 2.32 0.65 o -10 4 1 6.45 7.04 0.79 o -9 4 1 147.87 145.60 2.25 o -8 4 1 100.93 106.03 1.74 o -7 4 1 901.29 879.49 6.46 o -6 4 1 7.47 6.04 0.35 o -5 4 1 21.42 18.72 0.49 o -4 4 1 120.93 130.17 1.32 o -3 4 1 2.32 1.77 0.20 o -2 4 1 1.67 2.33 0.16 o -1 4 1 684.21 712.07 3.72 o 0 4 1 110.63 106.33 0.84 o 1 4 1 1050.47 1069.24 5.74 o 2 4 1 1508.82 1701.26 8.67 o 3 4 1 396.47 450.12 2.96 o 4 4 1 355.59 337.16 2.88 o 5 4 1 251.96 260.03 2.48 o 6 4 1 48.96 44.59 0.93 o 7 4 1 365.06 354.68 3.14 o 8 4 1 9.10 8.48 0.71 o 9 4 1 393.49 396.28 4.66 o 10 4 1 138.94 141.77 2.99 o 11 4 1 18.75 18.09 1.24 o -11 5 1 0.52 1.83 0.68 o -10 5 1 158.90 162.21 4.06 o -9 5 1 0.01 0.26 0.44 o -8 5 1 148.84 140.86 2.20 o -7 5 1 44.64 44.70 1.25 o -6 5 1 81.21 79.09 1.15 o -5 5 1 354.31 344.66 3.07 o -4 5 1 679.17 749.48 5.72 o -3 5 1 136.75 137.84 1.39 o -2 5 1 160.13 192.93 1.54 o -1 5 1 929.95 1047.06 5.49 o 0 5 1 189.24 219.01 1.67 o 1 5 1 464.54 522.40 3.59 o 2 5 1 340.52 354.62 2.85 o 3 5 1 0.60 0.68 0.21 o 4 5 1 34.76 35.83 0.82 o 5 5 1 10.65 12.29 0.57 o 6 5 1 243.85 235.04 2.36 o 7 5 1 256.88 259.34 3.33 o 8 5 1 530.15 516.54 5.57 o 9 5 1 96.46 106.26 2.15 o 10 5 1 50.82 51.07 1.88 o -11 6 1 28.03 26.16 1.43 o -10 6 1 200.54 195.13 3.40 o -9 6 1 1.42 1.38 0.66 o -8 6 1 20.47 18.58 1.00 o -7 6 1 329.72 343.64 3.78 o -6 6 1 505.16 479.49 4.40 o -5 6 1 110.19 91.83 1.36 o -4 6 1 129.12 141.33 1.74 o -3 6 1 75.59 89.95 1.17 o -2 6 1 24.05 29.94 0.73 o -1 6 1 0.04 0.24 0.17 o 0 6 1 853.77 903.45 6.22 o 1 6 1 994.00 1068.42 7.18 o 2 6 1 274.96 307.93 2.43 o 3 6 1 14.10 18.21 0.58 o 4 6 1 15.26 15.14 0.68 o 5 6 1 9.22 10.92 0.58 o 6 6 1 0.04 0.55 0.41 o 7 6 1 37.97 35.85 1.34 o 8 6 1 0.03 0.07 0.48 o 9 6 1 0.00 -0.37 0.51 o 10 6 1 3.56 2.13 0.78 o -10 7 1 144.19 146.63 2.90 o -9 7 1 36.98 37.43 1.43 o -8 7 1 136.48 128.73 2.48 o -7 7 1 6.09 6.78 0.59 o -6 7 1 81.84 88.59 1.62 o -5 7 1 369.81 377.46 3.68 o -4 7 1 65.38 63.99 1.02 o -3 7 1 32.50 32.63 0.73 o -2 7 1 93.42 96.30 1.15 o -1 7 1 35.62 50.28 0.79 o 0 7 1 66.55 66.42 1.03 o 1 7 1 68.51 76.25 1.11 o 2 7 1 0.00 -0.33 0.19 o 3 7 1 0.01 0.18 0.22 o 4 7 1 0.99 0.28 0.29 o 5 7 1 283.55 280.20 3.51 o 6 7 1 21.14 21.90 1.14 o 7 7 1 32.21 28.42 1.32 o 8 7 1 18.74 23.05 1.26 o 9 7 1 17.03 17.92 1.18 o 10 7 1 5.51 5.91 0.97 o -10 8 1 0.02 0.81 0.75 o -9 8 1 1.81 1.52 0.65 o -8 8 1 15.88 15.71 1.05 o -7 8 1 2.87 4.81 0.87 o -6 8 1 252.46 255.47 3.53 o -5 8 1 1.49 0.86 0.39 o -4 8 1 192.22 178.83 2.50 o -3 8 1 3.32 1.72 0.39 o -2 8 1 1.15 1.88 0.28 o -1 8 1 121.69 121.92 1.37 o 0 8 1 0.49 0.68 0.27 o 1 8 1 278.83 285.82 2.62 o 2 8 1 23.73 20.65 0.71 o 3 8 1 65.05 64.19 1.12 o 4 8 1 5.44 1.79 0.37 o 5 8 1 62.58 58.25 1.49 o 6 8 1 88.83 84.62 1.96 o 7 8 1 0.08 0.65 0.53 o 8 8 1 8.74 9.34 0.97 o 9 8 1 9.13 6.86 0.92 o -9 9 1 0.05 -0.20 0.66 o -8 9 1 0.04 0.09 0.58 o -7 9 1 2.36 1.26 0.54 o -6 9 1 11.58 8.91 0.83 o -5 9 1 150.03 136.66 2.67 o -4 9 1 781.97 739.69 8.56 o -3 9 1 15.96 9.65 0.79 o -2 9 1 173.04 168.33 1.87 o -1 9 1 313.58 312.82 2.96 o 0 9 1 117.67 110.79 1.72 o 1 9 1 56.04 53.29 1.02 o 2 9 1 392.75 389.81 4.28 o 3 9 1 10.12 7.67 0.66 o 4 9 1 118.36 122.69 2.57 o 5 9 1 0.62 0.30 0.50 o 6 9 1 60.63 61.16 2.13 o 7 9 1 109.14 111.53 2.60 o 8 9 1 8.90 13.38 2.11 o -8 10 1 88.60 90.46 2.36 o -7 10 1 0.05 0.08 0.63 o -6 10 1 4.86 5.22 0.74 o -5 10 1 6.26 5.12 0.85 o -4 10 1 8.48 7.54 0.88 o -3 10 1 6.68 6.45 0.77 o -2 10 1 15.92 16.03 0.96 o -1 10 1 113.42 112.05 2.14 o 0 10 1 216.31 209.77 3.06 o 1 10 1 273.07 262.38 3.91 o 2 10 1 696.53 690.03 7.45 o 3 10 1 1.93 3.39 0.72 o 4 10 1 21.74 17.68 1.20 o 5 10 1 158.49 152.08 3.10 o 6 10 1 187.33 189.30 4.78 o 7 10 1 96.18 92.50 2.92 o -7 11 1 3.75 6.94 1.33 o -6 11 1 1.43 2.95 0.96 o -5 11 1 254.01 249.21 5.47 o -4 11 1 181.75 174.53 4.38 o -3 11 1 35.70 44.36 2.12 o -2 11 1 11.20 13.53 1.28 o -1 11 1 164.67 159.94 3.25 o 0 11 1 78.06 81.80 2.86 o 1 11 1 41.86 36.09 2.22 o 2 11 1 129.44 113.68 2.95 o 3 11 1 77.35 74.29 3.33 o 4 11 1 32.01 30.51 2.38 o 5 11 1 55.66 58.63 2.11 o 6 11 1 25.66 24.18 1.57 o -6 12 1 4.50 3.29 1.14 o -5 12 1 159.28 161.35 6.82 o -4 12 1 340.74 365.97 6.86 o -3 12 1 83.47 79.30 2.60 o -2 12 1 95.19 97.03 2.92 o -1 12 1 21.45 20.06 1.68 o 0 12 1 0.08 0.52 1.29 o 1 12 1 7.52 3.60 1.37 o 2 12 1 2.51 -0.13 1.17 o 3 12 1 54.24 57.41 3.48 o 4 12 1 24.60 26.50 1.65 o 5 12 1 5.91 5.77 1.05 o -4 13 1 40.23 38.70 3.06 o -3 13 1 0.22 -0.32 1.43 o -2 13 1 20.41 21.16 2.09 o -1 13 1 71.61 79.55 3.44 o 0 13 1 19.58 19.53 2.10 o 1 13 1 7.53 5.74 2.34 o 2 13 1 12.14 11.61 2.18 o 3 13 1 3.09 0.92 1.55 o -12 0 2 91.31 91.19 3.03 o -11 0 2 116.81 114.47 3.19 o -10 0 2 137.02 142.68 3.41 o -9 0 2 75.31 63.35 2.03 o -8 0 2 114.93 105.60 1.92 o -7 0 2 151.71 141.30 4.63 o -6 0 2 30.83 27.84 0.99 o -5 0 2 6627.52 6675.80 59.59 o -4 0 2 51.16 43.47 0.71 o -3 0 2 89.15 74.41 0.80 o -2 0 2 623.24 501.57 2.89 o -1 0 2 701.98 717.94 4.57 o 0 0 2 3105.71 2924.22 20.12 o 1 0 2 1729.30 1731.53 11.47 o 2 0 2 1275.94 1281.47 8.70 o 3 0 2 3.79 7.03 0.36 o 4 0 2 11.02 10.86 0.68 o 5 0 2 19.14 19.11 0.77 o 6 0 2 348.15 381.23 4.79 o 7 0 2 476.49 486.79 5.02 o 8 0 2 504.25 516.91 6.31 o 9 0 2 69.39 62.82 2.43 o 10 0 2 123.66 127.89 4.44 o 11 0 2 20.53 16.73 1.67 o -12 1 2 8.43 9.35 0.86 o -11 1 2 111.07 105.24 2.14 o -10 1 2 71.14 62.51 2.10 o -9 1 2 63.28 61.96 1.43 o -8 1 2 12.96 12.65 0.48 o -7 1 2 118.96 105.83 1.12 o -6 1 2 89.38 102.27 1.58 o -5 1 2 885.69 941.12 6.43 o -4 1 2 429.73 414.60 3.03 o -3 1 2 462.37 462.18 2.78 o -2 1 2 21.70 18.13 0.25 o -1 1 2 147.36 142.40 0.77 o 0 1 2 4671.27 4493.38 20.99 o 1 1 2 26711.70 24684.64 142.82 o 2 1 2 3887.26 3897.88 18.33 o 3 1 2 1.17 2.81 0.19 o 4 1 2 45.73 51.26 0.75 o 5 1 2 102.92 93.71 1.11 o 6 1 2 130.22 123.24 1.35 o 7 1 2 61.84 60.04 1.18 o 8 1 2 26.20 28.50 1.29 o 9 1 2 35.84 37.33 1.48 o 10 1 2 32.58 31.30 1.53 o 11 1 2 8.37 8.27 0.95 o -12 2 2 1.11 1.49 0.63 o -11 2 2 8.00 10.47 1.14 o -10 2 2 104.24 102.69 1.97 o -9 2 2 41.76 38.55 0.96 o -8 2 2 10.02 9.25 0.50 o -7 2 2 76.29 72.38 1.09 o -6 2 2 260.93 256.88 2.45 o -5 2 2 348.46 341.45 3.87 o -4 2 2 899.68 936.94 6.82 o -3 2 2 14.86 10.66 0.39 o -2 2 2 163.42 165.14 1.22 o -1 2 2 666.05 643.48 3.31 o 0 2 2 2094.65 2032.20 9.56 o 1 2 2 4993.38 4975.84 23.11 o 2 2 2 1112.41 1105.51 5.51 o 3 2 2 17.11 15.59 0.44 o 4 2 2 5.54 7.03 0.34 o 5 2 2 0.62 0.32 0.20 o 6 2 2 0.87 0.47 0.25 o 7 2 2 722.88 719.41 4.69 o 8 2 2 46.87 52.15 1.40 o 9 2 2 202.19 205.72 3.20 o 10 2 2 0.02 0.19 0.57 o 11 2 2 77.65 80.00 3.05 o -12 3 2 35.67 35.80 1.48 o -11 3 2 3.79 3.16 0.67 o -10 3 2 9.03 8.41 0.91 o -9 3 2 359.92 359.61 3.64 o -8 3 2 401.60 366.59 3.59 o -7 3 2 8.08 7.17 0.39 o -6 3 2 56.75 56.56 1.14 o -5 3 2 3.35 2.82 0.40 o -4 3 2 25.57 36.56 0.81 o -3 3 2 1492.03 1599.20 10.75 o -2 3 2 1192.37 1195.28 6.09 o -1 3 2 345.51 317.39 1.78 o 0 3 2 540.88 525.22 3.44 o 1 3 2 157.91 155.93 1.15 o 2 3 2 835.03 837.58 4.66 o 3 3 2 1147.02 1240.08 7.58 o 4 3 2 32.44 34.06 0.65 o 5 3 2 74.24 76.04 1.00 o 6 3 2 129.24 129.41 1.48 o 7 3 2 108.74 107.80 1.61 o 8 3 2 67.58 66.25 1.60 o 9 3 2 63.09 65.70 1.80 o 10 3 2 61.47 59.36 2.74 o -12 4 2 2.41 2.59 0.67 o -11 4 2 5.78 5.94 0.89 o -10 4 2 21.31 25.55 1.33 o -9 4 2 80.03 79.09 2.28 o -8 4 2 58.53 57.43 1.18 o -7 4 2 436.10 416.65 3.65 o -6 4 2 262.97 253.67 2.64 o -5 4 2 41.99 49.84 1.14 o -4 4 2 38.09 44.73 0.74 o -3 4 2 972.98 1072.71 6.76 o -2 4 2 263.17 288.54 1.92 o -1 4 2 165.73 166.17 1.15 o 0 4 2 112.17 112.27 0.97 o 1 4 2 51.08 49.32 0.64 o 2 4 2 361.52 364.72 2.53 o 3 4 2 910.38 854.55 5.66 o 4 4 2 429.72 425.20 3.36 o 5 4 2 84.01 92.59 1.18 o 6 4 2 32.24 30.40 0.80 o 7 4 2 0.12 0.53 0.43 o 8 4 2 127.54 141.40 2.46 o 9 4 2 161.31 160.92 3.37 o 10 4 2 59.58 63.81 2.06 o -11 5 2 118.91 119.79 2.88 o -10 5 2 39.56 42.79 1.47 o -9 5 2 124.66 120.31 2.84 o -8 5 2 3.84 2.52 0.41 o -7 5 2 152.30 148.96 1.55 o -6 5 2 52.09 48.38 1.51 o -5 5 2 182.71 189.57 2.10 o -4 5 2 44.02 44.05 0.69 o -3 5 2 272.97 258.65 2.30 o -2 5 2 210.29 243.52 1.84 o -1 5 2 567.93 639.51 3.69 o 0 5 2 54.89 48.39 0.69 o 1 5 2 24.92 24.71 0.50 o 2 5 2 467.94 532.73 3.81 o 3 5 2 9.81 9.17 0.44 o 4 5 2 57.92 68.01 1.03 o 5 5 2 2.80 3.01 0.42 o 6 5 2 2.14 1.51 0.41 o 7 5 2 52.66 53.20 1.63 o 8 5 2 296.86 286.61 4.01 o 9 5 2 33.45 34.13 1.46 o 10 5 2 45.87 50.96 2.03 o -11 6 2 201.16 212.86 3.55 o -10 6 2 0.88 0.69 0.56 o -9 6 2 0.08 -0.30 0.43 o -8 6 2 227.06 221.11 2.85 o -7 6 2 170.53 166.52 1.82 o -6 6 2 905.37 870.01 7.05 o -5 6 2 18.60 21.16 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