#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/77/2227703.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2227703_Fobs loop_ _publ_author_name 'Nakanishi, Waka' 'Hitosugi, Shunpei' 'Piskareva, Anna' 'Isobe, Hiroyuki' _publ_section_title ; 1,8-Diiodoanthracene ; _journal_coeditor_code JH2197 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2515 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 101.829 _cell_angle_gamma 90.000 _cell_length_a 10.1167 _cell_length_b 10.8680 _cell_length_c 11.3930 _exptl_crystal_F_000 792.00 _reflns_d_resolution_high 0.7597 _[local]_cod_data_source_file jh2197Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ap09' _shelx_refln_list_code 4 _shelx_f_calc_maximum 406.29 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 509.21 368.48 10.44 o 2 0 0 165067.64 135059.03 2556.99 o 3 0 0 6153.79 6066.25 55.04 o 4 0 0 89228.23 83437.52 1158.56 o 5 0 0 6823.69 6676.80 60.93 o 6 0 0 54814.81 54255.98 570.11 o 7 0 0 8696.97 8852.70 94.18 o 8 0 0 17456.92 17459.38 222.11 o 9 0 0 10275.43 10174.95 172.20 o 10 0 0 13931.93 13823.83 165.51 o 11 0 0 4984.37 4786.75 77.40 o 12 0 0 8572.98 8506.55 124.02 o 1 1 0 118.71 30.50 1.87 o 2 1 0 594.71 566.55 5.89 o 3 1 0 706.16 677.05 6.86 o 4 1 0 394.82 442.90 5.97 o 5 1 0 1.77 0.64 1.87 o 6 1 0 2.92 5.20 1.84 o 7 1 0 0.12 8.72 3.31 o 8 1 0 6.59 11.43 3.07 o 9 1 0 124.11 122.67 5.70 o 10 1 0 3.97 7.48 3.20 o 11 1 0 3.05 3.80 2.98 o 12 1 0 178.16 195.52 9.88 o 0 2 0 62122.53 58422.54 1339.34 o 1 2 0 509.96 563.96 6.74 o 2 2 0 79934.02 73414.66 649.56 o 3 2 0 2946.12 3010.46 20.08 o 4 2 0 67853.55 67447.34 650.89 o 5 2 0 2319.90 2233.27 18.11 o 6 2 0 35454.21 34797.76 254.98 o 7 2 0 4898.36 4808.61 39.34 o 8 2 0 23789.14 23711.08 183.57 o 9 2 0 4005.50 3932.50 44.57 o 10 2 0 8743.20 8632.96 75.81 o 11 2 0 3283.82 3255.32 36.41 o 12 2 0 3390.06 3222.87 37.31 o 1 3 0 96.74 97.62 2.61 o 2 3 0 6.11 15.28 2.54 o 3 3 0 12.32 16.87 1.87 o 4 3 0 378.46 491.84 5.43 o 5 3 0 32.54 43.26 3.37 o 6 3 0 173.27 182.70 4.63 o 7 3 0 47.72 43.70 2.96 o 8 3 0 2837.24 2679.67 28.94 o 9 3 0 298.22 292.66 8.36 o 10 3 0 321.93 326.86 9.36 o 11 3 0 60.37 56.18 4.81 o 12 3 0 232.70 269.01 9.67 o 0 4 0 4651.43 4699.51 42.97 o 1 4 0 19.28 -2.08 2.08 o 2 4 0 7199.95 7382.33 49.48 o 3 4 0 183.63 167.62 3.58 o 4 4 0 5220.71 5261.92 37.10 o 5 4 0 790.27 785.33 10.91 o 6 4 0 2450.61 2495.26 24.33 o 7 4 0 348.68 353.97 7.91 o 8 4 0 2428.70 2547.82 31.34 o 9 4 0 325.11 300.72 8.63 o 10 4 0 1236.59 1180.98 18.53 o 11 4 0 623.67 606.18 15.88 o 12 4 0 348.22 352.91 12.16 o 1 5 0 28.05 -1.70 1.70 o 2 5 0 163.57 168.79 5.05 o 3 5 0 39.71 21.11 2.64 o 4 5 0 3940.77 4375.37 32.05 o 5 5 0 187.38 222.68 5.22 o 6 5 0 333.76 372.00 7.39 o 7 5 0 44.16 43.16 3.16 o 8 5 0 309.14 310.46 13.13 o 9 5 0 2.21 7.92 3.16 o 10 5 0 219.27 231.39 8.43 o 11 5 0 51.94 59.96 5.38 o 12 5 0 95.25 93.38 8.32 o 0 6 0 18697.48 19470.55 176.10 o 1 6 0 32.62 30.40 1.87 o 2 6 0 10417.41 10761.19 66.90 o 3 6 0 327.97 321.35 5.31 o 4 6 0 5851.29 5774.08 41.22 o 5 6 0 606.31 626.48 9.26 o 6 6 0 4091.74 4107.40 38.37 o 7 6 0 383.98 371.38 7.88 o 8 6 0 2835.41 2855.49 28.19 o 9 6 0 564.85 550.30 13.81 o 10 6 0 1311.44 1294.67 20.16 o 11 6 0 257.60 268.39 9.62 o 1 7 0 35.10 32.35 1.80 o 2 7 0 7.24 13.95 1.62 o 3 7 0 43.98 47.30 2.62 o 4 7 0 5.26 17.02 2.84 o 5 7 0 13.41 13.87 2.22 o 6 7 0 134.14 148.34 6.40 o 7 7 0 1.67 4.76 2.33 o 8 7 0 4.86 13.38 2.87 o 9 7 0 22.84 15.10 3.57 o 10 7 0 40.25 55.20 5.09 o 11 7 0 5.84 -0.37 9.54 o 0 8 0 47881.45 46882.04 722.22 o 1 8 0 32.65 40.67 2.96 o 2 8 0 34862.43 35254.86 328.43 o 3 8 0 1087.15 1087.89 11.82 o 4 8 0 33636.77 33483.99 232.34 o 5 8 0 1114.00 1078.34 13.62 o 6 8 0 19056.10 19051.87 160.83 o 7 8 0 2565.22 2523.88 25.88 o 8 8 0 9204.68 9304.47 74.53 o 9 8 0 2773.34 2745.29 36.75 o 10 8 0 5805.51 5690.67 64.02 o 1 9 0 119.88 114.10 3.77 o 2 9 0 0.16 8.76 2.95 o 3 9 0 202.60 201.41 5.01 o 4 9 0 348.55 354.71 7.31 o 5 9 0 127.69 122.67 4.95 o 6 9 0 17.72 21.51 3.45 o 7 9 0 69.15 66.79 5.16 o 8 9 0 5.84 14.74 3.59 o 9 9 0 16.55 17.02 4.60 o 0 10 0 21216.77 21911.80 219.15 o 1 10 0 134.39 141.97 5.83 o 2 10 0 29073.84 29624.61 207.54 o 3 10 0 827.72 866.73 11.18 o 4 10 0 27025.48 26950.50 209.04 o 5 10 0 1645.34 1619.18 20.97 o 6 10 0 16463.73 16255.55 131.92 o 7 10 0 2290.88 2298.85 40.53 o 8 10 0 13569.02 13486.51 127.76 o 9 10 0 1858.75 1869.91 54.10 o 1 11 0 150.81 149.60 5.90 o 2 11 0 0.57 6.25 5.11 o 3 11 0 121.94 122.96 5.53 o 4 11 0 410.17 411.21 9.68 o 5 11 0 0.51 -2.47 2.47 o 6 11 0 21.21 20.34 4.14 o 7 11 0 158.22 160.95 9.47 o 8 11 0 21.35 27.94 5.12 o 0 12 0 10139.91 10261.97 221.35 o 1 12 0 31.39 29.13 4.59 o 2 12 0 9672.09 9877.49 95.73 o 3 12 0 261.66 271.73 13.69 o 4 12 0 6646.53 6715.97 79.86 o 5 12 0 857.67 838.86 19.72 o 6 12 0 5364.78 5370.95 59.31 o 7 12 0 838.10 884.68 25.98 o 1 13 0 16.73 20.99 4.94 o 2 13 0 21.04 34.64 7.25 o 3 13 0 74.97 69.86 8.70 o 4 13 0 1175.22 1145.68 41.50 o 5 13 0 10.07 8.22 7.66 o 0 14 0 703.54 728.18 35.51 o 1 14 0 27.01 21.15 7.21 o -13 1 1 108.00 129.37 16.15 o -12 1 1 2153.35 2065.86 31.65 o -11 1 1 0.25 6.14 2.96 o -10 1 1 4901.27 4804.65 70.91 o -9 1 1 84.71 96.37 4.56 o -8 1 1 5790.68 5787.59 46.78 o -7 1 1 516.79 545.67 8.59 o -6 1 1 9727.54 9600.78 65.02 o -5 1 1 1049.89 1079.01 18.77 o -4 1 1 14224.46 14163.12 110.23 o -3 1 1 5754.95 5873.56 40.09 o -2 1 1 9340.38 9410.76 76.47 o -1 1 1 8.78 1.45 1.02 o 0 1 1 516.00 495.55 8.54 o 1 1 1 4716.77 4859.71 51.21 o 2 1 1 10615.69 10766.29 82.71 o 3 1 1 7070.69 7221.68 47.05 o 4 1 1 4212.64 4254.99 43.60 o 5 1 1 4241.24 4321.48 31.40 o 6 1 1 2890.01 2809.47 22.56 o 7 1 1 5491.65 5412.39 43.67 o 8 1 1 4941.41 4848.41 40.86 o 9 1 1 2085.96 2068.41 24.93 o 10 1 1 311.53 311.03 9.08 o 11 1 1 1617.74 1585.30 26.28 o 12 1 1 113.31 124.02 9.28 o -13 2 1 1.64 14.34 8.77 o -12 2 1 4084.71 4008.58 43.35 o -11 2 1 6.84 10.06 3.15 o -10 2 1 6704.33 6525.67 59.97 o -9 2 1 402.79 411.55 9.62 o -8 2 1 13800.64 13566.52 109.23 o -7 2 1 975.73 1001.42 12.49 o -6 2 1 14334.94 13910.69 94.93 o -5 2 1 276.29 206.10 4.00 o -4 2 1 15195.82 14641.41 99.65 o -3 2 1 4166.76 4229.87 30.10 o -2 2 1 31799.54 31917.60 253.30 o -1 2 1 5272.57 5312.67 36.04 o 0 2 1 5711.95 5699.63 42.97 o 1 2 1 9538.77 9666.73 79.30 o 2 2 1 27098.52 27007.04 243.71 o 3 2 1 17582.66 17625.23 121.95 o 4 2 1 20861.61 21584.16 150.02 o 5 2 1 15014.97 14683.01 96.84 o 6 2 1 5508.70 5562.21 40.14 o 7 2 1 8928.12 8913.62 67.36 o 8 2 1 3564.69 3500.12 35.22 o 9 2 1 6944.92 6861.16 61.71 o 10 2 1 1214.11 1151.72 18.05 o 11 2 1 4874.74 4654.91 47.54 o 12 2 1 9.83 5.47 3.96 o -12 3 1 1198.67 1204.96 20.09 o -11 3 1 24.21 22.42 3.79 o -10 3 1 1313.21 1284.81 19.19 o -9 3 1 143.28 166.34 6.48 o -8 3 1 980.39 959.05 14.67 o -7 3 1 98.97 104.06 4.13 o -6 3 1 3282.41 3268.95 25.55 o -5 3 1 66.16 56.63 2.60 o -4 3 1 1329.72 1209.14 9.90 o -3 3 1 551.80 553.27 5.32 o -2 3 1 7384.48 7953.70 54.79 o -1 3 1 9474.05 10354.72 66.57 o 0 3 1 21328.04 23014.97 167.37 o 1 3 1 4604.80 4930.63 31.03 o 2 3 1 2004.82 2059.11 14.35 o 3 3 1 2584.85 2620.31 18.02 o 4 3 1 2925.25 3140.60 21.59 o 5 3 1 2219.45 2227.15 18.31 o 6 3 1 319.66 335.43 7.14 o 7 3 1 895.75 941.66 12.35 o 8 3 1 196.40 209.35 6.82 o 9 3 1 726.96 714.71 13.37 o 10 3 1 64.23 63.09 4.69 o 11 3 1 621.29 634.14 15.08 o 12 3 1 9.77 9.15 3.64 o -12 4 1 8623.63 8590.07 78.68 o -11 4 1 36.49 50.59 6.24 o -10 4 1 16032.04 15581.64 127.46 o -9 4 1 1672.60 1539.91 20.73 o -8 4 1 29229.07 28374.04 219.89 o -7 4 1 1253.30 1257.05 15.95 o -6 4 1 37352.12 37235.39 358.55 o -5 4 1 5167.65 5308.96 37.99 o -4 4 1 49807.69 48503.75 326.30 o -3 4 1 13439.54 13481.57 84.53 o -2 4 1 49635.09 49010.27 495.95 o -1 4 1 10267.95 10352.39 67.23 o 0 4 1 38674.97 38303.72 276.21 o 1 4 1 29800.06 29861.50 187.93 o 2 4 1 40053.03 39621.43 276.61 o 3 4 1 25929.20 25125.40 171.15 o 4 4 1 17837.10 17137.71 115.06 o 5 4 1 27713.79 26506.57 298.51 o 6 4 1 13023.27 12978.71 94.22 o 7 4 1 19488.04 19526.30 139.30 o 8 4 1 2988.08 2962.02 31.78 o 9 4 1 15960.87 15656.43 155.44 o 10 4 1 2055.10 2012.31 28.92 o 11 4 1 9543.32 9377.40 88.62 o 12 4 1 1103.61 1098.33 24.58 o -12 5 1 5.77 13.33 4.29 o -11 5 1 7.94 11.73 3.71 o -10 5 1 7.74 23.93 4.20 o -9 5 1 424.81 380.10 9.77 o -8 5 1 345.44 316.49 8.49 o -7 5 1 127.69 130.20 6.41 o -6 5 1 48.61 59.89 3.33 o -5 5 1 4.34 10.62 3.50 o -4 5 1 125.70 117.20 3.35 o -3 5 1 0.17 -1.55 1.55 o -2 5 1 16.98 11.56 1.56 o -1 5 1 7.06 8.11 1.15 o 0 5 1 1045.37 1124.87 9.22 o 1 5 1 1.86 3.13 0.85 o 2 5 1 94.93 93.13 2.21 o 3 5 1 12.45 21.48 1.92 o 4 5 1 38.03 36.11 2.43 o 5 5 1 6.87 14.50 2.71 o 6 5 1 58.99 64.88 4.82 o 7 5 1 3.22 10.05 3.97 o 8 5 1 148.97 145.72 6.11 o 9 5 1 0.49 6.49 3.19 o 10 5 1 63.55 57.23 4.92 o 11 5 1 40.52 40.66 4.93 o -11 6 1 27.40 37.08 4.61 o -10 6 1 10111.62 9803.79 85.89 o -9 6 1 278.14 287.54 8.71 o -8 6 1 14892.71 14826.03 109.60 o -7 6 1 456.72 449.35 9.30 o -6 6 1 27151.49 27121.24 192.74 o -5 6 1 3084.26 3242.26 28.18 o -4 6 1 35095.66 35464.04 249.72 o -3 6 1 6572.21 6762.80 46.90 o -2 6 1 41802.81 42240.66 281.22 o -1 6 1 14938.11 15489.31 96.92 o 0 6 1 36287.85 36389.83 237.16 o 1 6 1 19310.41 19671.12 125.49 o 2 6 1 25995.92 25545.05 172.70 o 3 6 1 15425.64 15295.16 100.64 o 4 6 1 10869.50 10461.35 70.55 o 5 6 1 19738.40 19907.54 140.37 o 6 6 1 9687.17 9658.00 72.59 o 7 6 1 16164.87 16139.11 117.46 o 8 6 1 6333.54 6204.90 56.90 o 9 6 1 11075.61 10959.01 93.60 o 10 6 1 2113.79 2009.43 34.83 o 11 6 1 8312.51 8218.08 86.35 o -11 7 1 13.17 13.13 4.09 o -10 7 1 1110.88 1112.27 18.62 o -9 7 1 1.41 2.85 3.57 o -8 7 1 1586.70 1528.42 18.78 o -7 7 1 41.21 46.00 4.28 o -6 7 1 2366.64 2362.20 23.39 o -5 7 1 58.95 52.04 3.17 o -4 7 1 2196.53 2155.41 18.76 o -3 7 1 358.52 361.79 5.95 o -2 7 1 2439.28 2489.74 20.23 o -1 7 1 18.64 40.58 1.90 o 0 7 1 288.74 236.08 3.97 o 1 7 1 654.63 672.81 7.15 o 2 7 1 2136.73 2140.33 18.04 o 3 7 1 945.99 959.91 10.46 o 4 7 1 2472.59 2532.97 22.29 o 5 7 1 795.03 796.79 11.03 o 6 7 1 1261.36 1255.21 15.21 o 7 7 1 1636.54 1590.29 20.28 o 8 7 1 1943.90 1884.70 26.63 o 9 7 1 384.81 373.92 11.84 o 10 7 1 215.87 217.05 9.88 o 11 7 1 405.74 436.99 29.38 o -10 8 1 2205.87 2198.21 31.93 o -9 8 1 40.10 31.97 4.13 o -8 8 1 3863.62 3950.34 36.82 o -7 8 1 26.65 29.37 3.28 o -6 8 1 6391.66 6386.29 56.60 o -5 8 1 245.31 236.36 6.03 o -4 8 1 5926.75 5940.83 43.45 o -3 8 1 1078.88 1093.83 11.86 o -2 8 1 8586.76 8912.07 61.23 o -1 8 1 2819.32 2932.35 23.45 o 0 8 1 11698.25 12315.22 76.60 o 1 8 1 4304.66 4411.81 32.80 o 2 8 1 6436.96 6642.20 47.12 o 3 8 1 5367.73 5612.84 41.03 o 4 8 1 4884.74 4968.90 40.47 o 5 8 1 4206.88 4223.66 36.06 o 6 8 1 2453.13 2467.00 27.39 o 7 8 1 3748.37 3748.57 38.38 o 8 8 1 763.56 748.53 14.22 o 9 8 1 3127.90 3173.99 47.04 o 10 8 1 273.23 268.62 11.02 o -10 9 1 2023.63 2106.84 68.10 o -9 9 1 10.95 14.30 5.11 o -8 9 1 2382.34 2394.73 28.68 o -7 9 1 179.92 181.82 6.28 o -6 9 1 2888.71 2905.79 31.86 o -5 9 1 164.15 176.81 5.54 o -4 9 1 1531.74 1506.92 16.82 o -3 9 1 596.59 607.11 8.67 o -2 9 1 4806.85 4970.25 44.59 o -1 9 1 2049.13 2115.87 20.55 o 0 9 1 5803.60 6009.54 47.26 o 1 9 1 1693.16 1728.67 16.24 o 2 9 1 3246.40 3308.29 26.72 o 3 9 1 2121.58 2156.35 21.57 o 4 9 1 1977.36 1966.72 22.71 o 5 9 1 1763.61 1735.94 21.49 o 6 9 1 865.98 875.63 14.55 o 7 9 1 1197.23 1169.16 17.97 o 8 9 1 186.13 194.28 7.96 o 9 9 1 942.94 907.50 25.99 o -9 10 1 143.71 133.96 9.50 o -8 10 1 303.08 314.55 14.75 o -7 10 1 91.65 87.03 6.28 o -6 10 1 89.17 100.97 5.40 o -5 10 1 25.13 31.46 3.39 o -4 10 1 180.03 210.90 6.10 o -3 10 1 42.86 48.98 3.01 o -2 10 1 74.01 98.40 7.75 o -1 10 1 4.31 8.32 2.44 o 0 10 1 2.46 9.99 4.68 o 1 10 1 101.56 106.12 4.89 o 2 10 1 124.52 134.38 4.98 o 3 10 1 221.96 237.09 7.31 o 4 10 1 297.05 293.74 8.11 o 5 10 1 110.61 126.54 10.11 o 6 10 1 32.37 30.22 3.77 o 7 10 1 16.93 17.09 3.67 o 8 10 1 2.17 -0.42 3.42 o 9 10 1 105.82 114.81 11.01 o -8 11 1 1681.02 1704.65 38.47 o -7 11 1 137.34 141.03 7.96 o -6 11 1 2468.24 2504.38 35.97 o -5 11 1 676.93 677.05 17.21 o -4 11 1 2145.43 2263.90 29.42 o -3 11 1 510.48 526.35 12.37 o -2 11 1 2861.92 2947.38 35.03 o -1 11 1 1571.15 1639.79 20.69 o 0 11 1 2975.29 3021.78 31.70 o 1 11 1 1679.46 1722.67 21.46 o 2 11 1 1168.93 1210.70 17.25 o 3 11 1 1428.85 1407.34 21.42 o 4 11 1 1783.28 1791.05 30.73 o 5 11 1 1342.15 1334.81 19.27 o 6 11 1 420.43 423.60 10.66 o 7 11 1 996.79 1007.82 17.48 o 8 11 1 3.13 5.70 5.05 o -7 12 1 151.11 166.88 14.00 o -6 12 1 4741.78 4829.35 89.82 o -5 12 1 2146.43 2152.85 44.42 o -4 12 1 7849.85 7861.69 114.15 o -3 12 1 1637.93 1674.67 36.56 o -2 12 1 5017.80 5130.14 64.85 o -1 12 1 2245.72 2328.00 36.35 o 0 12 1 5463.83 5547.90 58.60 o 1 12 1 3329.68 3459.85 40.92 o 2 12 1 2693.06 2722.75 30.61 o 3 12 1 980.01 989.89 18.03 o 4 12 1 34.25 45.88 5.53 o 5 12 1 3159.82 3182.03 35.33 o 6 12 1 1479.50 1469.14 24.27 o -5 13 1 333.38 307.76 22.14 o -4 13 1 1006.69 993.37 28.61 o -3 13 1 404.67 421.49 17.98 o -2 13 1 269.54 277.20 11.83 o -1 13 1 294.62 328.36 12.83 o 0 13 1 107.70 138.67 9.14 o 1 13 1 352.40 374.04 13.58 o 2 13 1 186.13 199.11 10.17 o 3 13 1 382.86 395.48 21.17 o 4 13 1 55.54 47.61 7.69 o 5 13 1 400.69 421.12 24.09 o -2 14 1 6800.98 7118.19 106.49 o -1 14 1 2263.04 2340.80 39.21 o 0 14 1 5884.17 6073.10 96.30 o 1 14 1 3458.02 3596.77 91.63 o -13 0 2 15.95 20.47 10.31 o -12 0 2 3136.04 3099.25 57.70 o -11 0 2 978.54 954.48 26.61 o -10 0 2 7394.99 7459.19 148.64 o -9 0 2 3267.36 3387.23 44.05 o -8 0 2 8894.27 8928.96 153.38 o -7 0 2 9732.72 9773.33 102.64 o -6 0 2 12011.83 12037.01 106.17 o -5 0 2 40499.12 41334.57 365.09 o -4 0 2 21752.69 21794.54 198.01 o -3 0 2 44190.13 44006.56 383.20 o -2 0 2 8958.91 9126.35 84.49 o -1 0 2 17068.31 16781.76 209.91 o 0 0 2 4234.91 4291.07 38.61 o 1 0 2 55303.55 49835.27 1536.51 o 2 0 2 3009.32 3078.72 28.25 o 3 0 2 43285.38 41688.66 366.26 o 4 0 2 774.37 696.00 11.77 o 5 0 2 33795.97 32975.93 328.71 o 6 0 2 439.43 457.84 10.69 o 7 0 2 44309.18 41449.99 526.38 o 8 0 2 1068.76 1048.92 19.48 o 9 0 2 15617.62 15357.17 160.00 o 10 0 2 425.79 414.25 22.98 o 11 0 2 7625.18 7428.26 110.02 o 12 0 2 271.50 313.49 17.07 o -13 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