#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/77/2227707.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2227707_Fobs loop_ _publ_author_name 'G\^az, \,Serban Andrei' 'Dobra, Ioana' 'Woiczechowski-Pop, Adrian' 'Varga, Richard A.' 'Grosu, Ion' _publ_section_title ; 3,9-Diisopropyl-2,4,8,10-tetrathiaspiro[5.5]undecane ; _journal_coeditor_code JH2201 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2618 _journal_volume 66 _journal_year 2010 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 128.418 _cell_angle_gamma 90.000 _cell_length_a 16.7012 _cell_length_b 10.2410 _cell_length_c 12.0631 _exptl_crystal_F_000 664.00 _reflns_d_resolution_high 0.8409 _[local]_cod_data_source_file jh2201Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 49alb in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 205.85 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 20743.94 23453.20 389.57 o 4 0 0 1876.15 1891.96 36.39 o 6 0 0 1321.99 1433.94 39.73 o 8 0 0 19325.71 19540.50 333.13 o 10 0 0 3822.09 3556.19 71.98 o 12 0 0 2.05 1.08 9.35 o 14 0 0 0.26 20.52 14.34 o 1 1 0 785.20 998.67 13.24 o 3 1 0 24717.53 27998.35 329.20 o 5 1 0 11885.36 13131.82 158.07 o 7 1 0 168.33 251.17 7.31 o 9 1 0 919.32 813.75 16.45 o 11 1 0 570.12 529.86 21.85 o 13 1 0 490.23 439.49 21.36 o 15 1 0 47.37 42.36 18.82 o 0 2 0 23072.21 26114.94 434.00 o 2 2 0 11828.86 13311.70 158.28 o 4 2 0 77.10 107.42 3.75 o 6 2 0 4055.22 4345.19 57.09 o 8 2 0 1406.51 1452.06 25.89 o 10 2 0 700.07 646.05 18.33 o 12 2 0 276.62 243.25 15.17 o 14 2 0 73.94 97.46 14.40 o 1 3 0 843.40 864.49 14.05 o 3 3 0 18583.36 20953.58 248.96 o 5 3 0 17923.84 19748.10 236.27 o 7 3 0 456.75 458.38 11.07 o 9 3 0 177.87 188.31 8.96 o 11 3 0 700.50 640.82 31.63 o 13 3 0 670.32 678.22 27.70 o 15 3 0 31.84 50.95 17.77 o 0 4 0 1217.36 1291.30 27.82 o 2 4 0 339.50 378.43 8.37 o 4 4 0 1240.71 1296.49 20.96 o 6 4 0 4.94 13.55 4.73 o 8 4 0 926.31 933.96 20.38 o 10 4 0 17.16 49.50 8.07 o 12 4 0 291.31 265.90 15.27 o 14 4 0 20.19 27.45 10.75 o 1 5 0 5322.84 5078.51 70.31 o 3 5 0 546.10 610.80 17.93 o 5 5 0 242.23 280.34 8.48 o 7 5 0 2025.12 1910.92 34.92 o 9 5 0 1659.90 1418.35 29.10 o 11 5 0 66.59 110.30 14.79 o 13 5 0 2.47 28.62 12.75 o 0 6 0 1306.09 1291.38 30.49 o 2 6 0 288.77 287.91 8.24 o 4 6 0 2759.46 2603.59 39.42 o 6 6 0 971.47 945.33 20.37 o 8 6 0 99.54 106.90 10.68 o 10 6 0 25.08 24.64 13.62 o 12 6 0 148.28 184.55 22.48 o 1 7 0 17.47 19.15 4.10 o 3 7 0 897.15 894.22 21.46 o 5 7 0 1674.48 1479.04 28.42 o 7 7 0 498.78 417.96 15.28 o 9 7 0 30.68 59.81 11.78 o 11 7 0 3.15 25.71 10.82 o 0 8 0 103.53 115.76 13.91 o 2 8 0 496.78 431.60 14.47 o 4 8 0 1555.30 1340.58 29.48 o 6 8 0 103.37 157.51 12.38 o 8 8 0 14.65 37.32 8.97 o 10 8 0 152.93 218.85 20.81 o 1 9 0 481.78 466.86 17.63 o 3 9 0 652.47 644.44 21.50 o 5 9 0 1243.66 1153.50 31.20 o 7 9 0 39.33 74.35 11.98 o 9 9 0 197.01 219.63 19.56 o 0 10 0 2134.36 1952.24 93.92 o 2 10 0 704.06 656.85 26.10 o 4 10 0 37.67 49.20 11.68 o 6 10 0 40.11 80.07 12.41 o 8 10 0 766.82 687.02 32.64 o 1 11 0 8.13 12.67 11.43 o 3 11 0 92.48 129.29 21.50 o 5 11 0 201.55 274.98 25.52 o 0 12 0 122.55 186.49 27.26 o 2 12 0 42.23 67.92 13.71 o -15 1 1 207.36 257.01 18.20 o -13 1 1 19.79 36.49 9.70 o -11 1 1 3316.43 3163.16 55.87 o -9 1 1 946.49 932.73 18.16 o -7 1 1 3115.15 3396.22 45.63 o -5 1 1 309.87 312.02 6.57 o -3 1 1 42373.75 47315.74 554.97 o -1 1 1 12441.93 14060.97 191.51 o 1 1 1 1893.44 2032.46 26.07 o 3 1 1 74.38 71.78 3.41 o 5 1 1 1616.13 1982.85 28.57 o 7 1 1 1474.36 1445.39 23.71 o 9 1 1 44.36 84.26 8.18 o 11 1 1 13.66 5.53 10.38 o 13 1 1 0.42 3.59 10.80 o -16 2 1 243.55 268.42 22.19 o -14 2 1 911.71 785.90 30.03 o -12 2 1 80.34 133.69 13.64 o -10 2 1 1315.53 1223.11 27.49 o -8 2 1 2984.37 3255.24 48.23 o -6 2 1 14086.14 14909.03 179.46 o -4 2 1 861.46 888.34 13.90 o -2 2 1 11879.84 13418.09 159.39 o 0 2 1 7384.80 8577.03 130.26 o 2 2 1 13047.07 14589.07 173.92 o 4 2 1 2676.33 2949.66 42.43 o 6 2 1 1812.10 1658.79 27.17 o 8 2 1 100.99 115.37 7.66 o 10 2 1 288.04 293.51 13.67 o 12 2 1 215.33 227.79 15.98 o 14 2 1 23.66 31.81 11.97 o -15 3 1 33.03 24.19 11.79 o -13 3 1 94.85 111.50 17.20 o -11 3 1 684.80 649.77 17.42 o -9 3 1 277.99 307.29 10.41 o -7 3 1 48.80 58.64 4.28 o -5 3 1 955.08 886.13 15.10 o -3 3 1 2303.68 2418.76 32.45 o -1 3 1 4051.49 4419.48 55.32 o 1 3 1 205.13 229.89 5.51 o 3 3 1 3820.71 4006.25 52.19 o 5 3 1 86.77 103.17 5.15 o 7 3 1 1360.26 1201.05 31.01 o 9 3 1 157.62 161.47 11.04 o 11 3 1 488.24 450.46 18.38 o 13 3 1 82.60 109.62 14.84 o -14 4 1 0.01 0.00 9.95 o -12 4 1 15.71 17.80 7.16 o -10 4 1 166.83 164.54 10.15 o -8 4 1 289.43 310.44 9.16 o -6 4 1 323.52 433.45 10.31 o -4 4 1 282.02 298.51 9.06 o -2 4 1 1616.82 1676.27 26.19 o 0 4 1 6.49 8.25 1.83 o 2 4 1 2.93 22.42 3.50 o 4 4 1 527.31 516.16 11.44 o 6 4 1 1161.55 1112.12 20.51 o 8 4 1 227.48 220.18 9.49 o 10 4 1 20.94 19.61 7.59 o 12 4 1 134.15 158.75 17.74 o -15 5 1 9.53 10.85 17.87 o -13 5 1 12.60 17.31 10.05 o -11 5 1 21.98 56.47 9.50 o -9 5 1 537.54 542.03 17.92 o -7 5 1 62.48 74.09 5.90 o -5 5 1 400.59 394.36 9.88 o -3 5 1 2.47 8.00 2.69 o -1 5 1 27.34 33.62 4.41 o 1 5 1 28.31 54.41 4.09 o 3 5 1 0.47 12.83 3.08 o 5 5 1 98.13 144.04 6.84 o 7 5 1 188.89 170.25 8.31 o 9 5 1 101.97 138.04 14.38 o 11 5 1 36.42 62.27 12.54 o 13 5 1 4.83 35.02 16.34 o -14 6 1 76.12 63.16 21.01 o -12 6 1 42.32 43.39 11.10 o -10 6 1 70.80 107.52 11.00 o -8 6 1 22.62 28.85 5.77 o -6 6 1 410.52 372.68 15.23 o -4 6 1 0.05 6.81 3.35 o -2 6 1 197.65 190.76 6.69 o 0 6 1 64.66 87.83 4.92 o 2 6 1 593.77 622.85 14.04 o 4 6 1 150.59 158.14 9.65 o 6 6 1 331.60 297.75 11.19 o 8 6 1 82.53 102.82 11.44 o 10 6 1 58.69 79.73 11.77 o 12 6 1 1.51 20.61 12.84 o -13 7 1 68.45 100.56 15.20 o -11 7 1 145.39 187.73 16.86 o -9 7 1 130.01 179.99 13.99 o -7 7 1 1134.28 1025.80 34.78 o -5 7 1 598.89 604.85 15.87 o -3 7 1 752.05 765.68 15.86 o -1 7 1 1203.37 1190.47 32.57 o 1 7 1 351.01 309.49 10.35 o 3 7 1 738.72 639.70 16.23 o 5 7 1 351.20 324.67 11.87 o 7 7 1 874.02 776.44 24.67 o 9 7 1 49.80 77.66 12.05 o 11 7 1 146.32 193.08 24.72 o -12 8 1 203.54 229.97 19.15 o -10 8 1 611.49 581.10 22.32 o -8 8 1 92.49 132.97 13.54 o -6 8 1 1383.46 1329.70 32.95 o -4 8 1 0.02 10.28 5.50 o -2 8 1 1321.87 1225.91 44.59 o 0 8 1 32.42 38.97 5.97 o 2 8 1 2392.03 2153.98 38.02 o 4 8 1 1076.85 884.14 21.22 o 6 8 1 95.27 141.76 12.37 o 8 8 1 74.85 110.24 15.22 o 10 8 1 291.93 300.98 20.64 o -11 9 1 139.42 178.35 19.50 o -9 9 1 36.65 76.29 13.28 o -7 9 1 41.43 51.54 10.40 o -5 9 1 36.10 62.27 9.21 o -3 9 1 202.48 204.31 13.65 o -1 9 1 611.36 495.78 18.50 o 1 9 1 2.37 19.27 7.60 o 3 9 1 356.77 359.15 15.80 o 5 9 1 0.74 16.63 7.24 o 7 9 1 291.27 271.76 17.41 o 9 9 1 38.64 31.60 12.18 o -8 10 1 6.13 29.94 14.64 o -6 10 1 51.23 84.16 12.78 o -4 10 1 12.63 31.75 8.42 o -2 10 1 46.25 61.20 10.22 o 0 10 1 30.28 46.38 11.18 o 2 10 1 178.76 214.75 16.63 o 4 10 1 21.08 24.37 10.23 o 6 10 1 21.93 78.58 18.41 o -7 11 1 76.09 109.59 14.37 o -5 11 1 69.19 55.46 15.90 o -3 11 1 228.87 258.42 16.83 o -1 11 1 513.22 458.30 22.44 o 1 11 1 0.26 18.94 10.83 o 3 11 1 43.04 77.45 14.22 o 5 11 1 156.98 195.56 22.94 o -2 12 1 62.68 68.99 12.93 o 0 12 1 13.86 45.68 17.84 o -16 0 2 624.04 587.15 48.05 o -14 0 2 146.44 173.17 24.27 o -12 0 2 343.73 315.97 18.64 o -10 0 2 2014.32 1947.97 42.54 o -8 0 2 8876.61 8406.99 147.62 o -6 0 2 5648.69 5691.73 100.12 o -4 0 2 154.32 170.51 5.87 o -2 0 2 4756.16 5499.84 93.91 o 0 0 2 2033.90 2404.56 43.24 o 2 0 2 22578.95 24387.62 407.98 o 4 0 2 76.32 78.95 6.69 o 6 0 2 201.16 200.93 9.43 o 8 0 2 752.45 599.65 24.05 o 10 0 2 1296.10 1129.58 50.02 o 12 0 2 6.03 27.57 13.46 o -17 1 2 106.79 116.32 17.70 o -15 1 2 21.21 33.24 10.71 o -13 1 2 1031.30 950.92 25.01 o -11 1 2 172.34 172.18 9.57 o -9 1 2 132.39 163.86 6.05 o -7 1 2 1534.43 1452.37 24.02 o -5 1 2 6067.16 6607.92 87.10 o -3 1 2 1568.67 1783.07 24.94 o -1 1 2 520.35 571.66 8.96 o 1 1 2 1693.74 1885.67 25.23 o 3 1 2 436.48 492.57 9.45 o 5 1 2 2763.90 2594.84 39.37 o 7 1 2 200.67 175.42 8.57 o 9 1 2 78.43 102.41 9.33 o 11 1 2 55.26 65.98 11.93 o 13 1 2 191.70 201.31 23.84 o -16 2 2 10.55 27.27 11.13 o -14 2 2 42.28 56.32 10.66 o -12 2 2 289.79 257.46 12.04 o -10 2 2 736.50 770.12 17.59 o -8 2 2 478.11 472.25 12.52 o -6 2 2 1241.00 1254.70 21.21 o -4 2 2 14440.21 15895.77 202.60 o -2 2 2 468.86 489.91 8.20 o 0 2 2 808.38 812.46 12.65 o 2 2 2 600.86 592.59 10.82 o 4 2 2 5606.93 5658.42 72.30 o 6 2 2 883.77 767.85 16.85 o 8 2 2 159.60 169.25 9.22 o 10 2 2 30.22 45.31 9.15 o 12 2 2 35.62 40.33 11.52 o -15 3 2 44.93 65.10 13.87 o -13 3 2 575.49 550.84 23.04 o -11 3 2 690.09 674.83 17.39 o -9 3 2 0.53 16.15 6.97 o -7 3 2 1420.31 1432.06 22.42 o -5 3 2 2124.42 2157.07 30.04 o -3 3 2 5690.18 5714.58 70.90 o -1 3 2 2876.80 3176.77 47.93 o 1 3 2 2537.10 2527.58 34.34 o 3 3 2 1375.36 1416.88 22.31 o 5 3 2 835.64 794.44 18.75 o 7 3 2 772.86 714.97 17.28 o 9 3 2 107.72 162.06 13.03 o 11 3 2 117.90 163.52 15.18 o 13 3 2 32.61 49.35 11.64 o -16 4 2 44.10 60.64 16.98 o -14 4 2 30.08 66.73 11.50 o -12 4 2 604.77 611.15 17.46 o -10 4 2 16.11 23.53 5.13 o -8 4 2 562.19 541.35 14.92 o -6 4 2 211.46 206.19 8.08 o -4 4 2 3314.55 3184.76 43.74 o -2 4 2 204.13 213.53 6.03 o 0 4 2 1840.24 1800.85 28.56 o 2 4 2 5.66 8.48 2.59 o 4 4 2 864.65 779.20 15.54 o 6 4 2 683.98 634.54 18.16 o 8 4 2 74.97 104.05 11.59 o 10 4 2 347.51 323.11 17.92 o 12 4 2 6.66 32.88 12.94 o -15 5 2 243.49 273.46 35.06 o -13 5 2 1.05 14.17 12.06 o -11 5 2 29.45 48.41 7.07 o -9 5 2 2268.92 1994.78 47.86 o -7 5 2 4307.65 4119.49 56.44 o -5 5 2 274.38 228.40 12.78 o -3 5 2 33.04 35.19 3.77 o -1 5 2 4900.79 4976.39 69.67 o 1 5 2 9816.14 9746.40 129.87 o 3 5 2 596.70 594.06 13.06 o 5 5 2 215.59 204.72 8.93 o 7 5 2 127.39 150.33 11.06 o 9 5 2 1688.96 1497.87 62.45 o 11 5 2 389.90 400.79 22.37 o -14 6 2 113.60 77.05 31.39 o -12 6 2 613.13 542.31 26.89 o -10 6 2 63.53 91.35 9.99 o -8 6 2 179.26 196.76 16.16 o -6 6 2 120.56 123.62 7.44 o -4 6 2 3836.22 3594.93 49.70 o -2 6 2 1853.12 1768.21 27.21 o 0 6 2 53.95 64.26 5.87 o 2 6 2 123.05 128.74 7.99 o 4 6 2 1968.19 1868.33 43.18 o 6 6 2 1111.78 1036.52 25.42 o 8 6 2 0.18 1.14 7.42 o 10 6 2 94.29 109.06 16.52 o -13 7 2 288.47 281.53 20.42 o -11 7 2 118.45 166.73 14.01 o -9 7 2 0.47 11.75 6.29 o -7 7 2 12.95 14.15 5.22 o -5 7 2 708.13 662.97 16.18 o -3 7 2 950.86 860.96 28.40 o -1 7 2 216.42 215.16 8.85 o 1 7 2 21.95 37.31 5.67 o 3 7 2 182.09 177.51 10.48 o 5 7 2 416.11 405.80 17.51 o 7 7 2 65.63 87.83 11.78 o 9 7 2 12.34 28.48 10.78 o -12 8 2 207.91 227.44 22.16 o -10 8 2 187.61 204.59 14.95 o -8 8 2 110.54 150.38 15.63 o -6 8 2 396.42 378.36 21.27 o -4 8 2 672.40 651.51 31.78 o -2 8 2 884.69 858.00 22.00 o 0 8 2 200.89 219.46 10.90 o 2 8 2 390.70 396.07 13.48 o 4 8 2 459.88 443.55 14.80 o 6 8 2 567.62 530.93 22.14 o 8 8 2 24.12 49.27 12.69 o -11 9 2 108.22 146.67 26.35 o -9 9 2 379.00 339.97 19.31 o -7 9 2 405.27 395.25 19.47 o -5 9 2 51.76 62.16 9.10 o -3 9 2 435.69 339.58 15.20 o -1 9 2 215.22 231.72 13.28 o 1 9 2 779.90 773.83 24.55 o 3 9 2 3.59 15.63 7.30 o 5 9 2 149.03 185.73 14.14 o 7 9 2 9.55 23.85 11.48 o -10 10 2 39.98 57.06 13.23 o -8 10 2 870.20 798.72 30.86 o -6 10 2 144.24 180.05 17.75 o -4 10 2 311.32 304.70 15.05 o -2 10 2 9.01 26.62 8.15 o 0 10 2 1269.88 1142.66 32.43 o 2 10 2 415.11 405.81 21.03 o 4 10 2 47.38 71.12 13.93 o 6 10 2 29.53 33.66 24.63 o -7 11 2 21.56 46.38 13.10 o -5 11 2 153.56 191.88 17.53 o -3 11 2 511.94 494.10 25.02 o -1 11 2 4.54 21.68 10.37 o 1 11 2 82.21 73.64 13.91 o 3 11 2 81.23 133.10 16.48 o -2 12 2 7.99 30.44 12.26 o -17 1 3 24.28 42.13 12.42 o -15 1 3 49.08 86.85 11.08 o -13 1 3 28.46 50.07 8.04 o -11 1 3 75.34 88.13 8.32 o -9 1 3 1447.89 1297.61 23.19 o -7 1 3 387.50 376.19 9.07 o -5 1 3 363.93 336.70 6.79 o -3 1 3 311.97 320.37 6.96 o -1 1 3 4452.09 5279.64 65.25 o 1 1 3 167.88 171.80 5.40 o 3 1 3 38.23 27.91 3.74 o 5 1 3 29.14 36.68 5.51 o 7 1 3 296.57 302.98 12.78 o 9 1 3 0.81 9.07 5.93 o 11 1 3 72.56 88.33 13.89 o -16 2 3 75.90 90.06 15.60 o -14 2 3 524.07 424.85 16.52 o -12 2 3 188.44 176.24 9.94 o -10 2 3 420.71 375.84 11.02 o -8 2 3 111.76 113.03 5.31 o -6 2 3 3414.63 3542.00 50.01 o -4 2 3 3775.34 4104.87 56.11 o -2 2 3 21.18 20.35 2.31 o 0 2 3 2744.71 2924.10 38.64 o 2 2 3 1833.05 1727.46 25.46 o 4 2 3 1347.62 1278.99 23.39 o 6 2 3 39.61 53.65 6.72 o 8 2 3 896.94 759.31 21.10 o 10 2 3 57.85 84.91 10.91 o 12 2 3 159.18 217.03 20.25 o -17 3 3 47.09 65.27 16.72 o -15 3 3 148.74 165.03 15.89 o -13 3 3 50.89 74.95 9.36 o -11 3 3 453.13 412.58 12.66 o -9 3 3 2003.61 1831.31 31.28 o -7 3 3 1065.62 992.61 16.71 o -5 3 3 1145.61 1065.23 16.89 o -3 3 3 29.66 41.13 3.37 o -1 3 3 8363.87 8812.84 115.69 o 1 3 3 182.68 202.30 6.06 o 3 3 3 3012.52 3006.65 42.18 o 5 3 3 988.96 961.79 21.90 o 7 3 3 1055.94 937.05 23.29 o 9 3 3 579.33 533.31 20.20 o 11 3 3 315.77 324.75 17.52 o -16 4 3 1.18 27.26 12.37 o -14 4 3 23.62 39.51 9.48 o -12 4 3 70.45 67.86 8.03 o -10 4 3 1362.05 1252.63 38.11 o -8 4 3 112.80 117.74 5.38 o -6 4 3 1339.95 1393.62 22.03 o -4 4 3 28.95 40.42 4.05 o -2 4 3 1436.68 1358.78 22.85 o 0 4 3 2535.81 2558.90 39.07 o 2 4 3 1055.67 1118.17 19.37 o 4 4 3 604.66 565.38 14.45 o 6 4 3 0.98 16.69 5.27 o 8 4 3 675.48 620.00 39.73 o 10 4 3 4.73 25.12 14.45 o -15 5 3 133.15 130.47 16.48 o -13 5 3 54.40 90.82 13.08 o -11 5 3 120.13 135.36 10.60 o -9 5 3 11.64 21.08 6.68 o -7 5 3 887.52 829.59 17.76 o -5 5 3 74.29 95.14 5.04 o -3 5 3 57.50 50.17 3.53 o -1 5 3 35.50 47.53 4.87 o 1 5 3 258.85 284.58 9.35 o 3 5 3 102.64 126.81 8.28 o 5 5 3 241.23 227.31 13.05 o 7 5 3 5.95 25.06 7.59 o 9 5 3 0.36 9.68 10.87 o 11 5 3 34.85 52.83 14.32 o -14 6 3 100.48 135.19 17.13 o -12 6 3 17.07 14.73 7.67 o -10 6 3 93.82 140.41 10.84 o -8 6 3 26.77 35.36 6.26 o -6 6 3 504.96 528.35 18.87 o -4 6 3 688.55 619.34 17.92 o -2 6 3 720.90 660.78 15.27 o 0 6 3 887.40 809.24 18.02 o 2 6 3 54.57 90.28 9.10 o 4 6 3 1460.51 1464.64 31.55 o 6 6 3 149.42 172.10 12.55 o 8 6 3 605.23 573.58 25.07 o 10 6 3 3.95 7.58 12.37 o -13 7 3 395.78 393.13 18.45 o -11 7 3 29.13 48.23 8.91 o -9 7 3 183.22 186.07 12.03 o -7 7 3 258.95 278.54 11.27 o -5 7 3 2249.95 2007.84 38.49 o -3 7 3 12.85 28.59 5.85 o -1 7 3 1625.90 1403.14 44.87 o 1 7 3 25.47 29.98 5.91 o 3 7 3 773.58 668.47 24.27 o 5 7 3 5.62 17.56 6.89 o 7 7 3 759.66 716.70 34.92 o 9 7 3 101.32 125.45 17.26 o -12 8 3 67.52 81.90 12.32 o -10 8 3 963.66 835.70 42.16 o -8 8 3 204.65 193.52 26.28 o -6 8 3 385.42 361.08 13.66 o -4 8 3 95.09 115.00 10.01 o -2 8 3 644.25 629.87 18.93 o 0 8 3 61.10 79.87 10.16 o 2 8 3 465.84 409.65 19.58 o 4 8 3 317.63 268.07 12.96 o 6 8 3 5.24 29.92 9.36 o 8 8 3 0.26 0.00 10.22 o -11 9 3 126.91 191.06 19.84 o -9 9 3 99.91 153.64 16.10 o -7 9 3 121.24 168.86 16.53 o -5 9 3 116.42 136.43 12.77 o -3 9 3 84.86 113.38 12.34 o -1 9 3 187.91 187.87 11.88 o 1 9 3 3.90 10.98 8.13 o 3 9 3 17.70 47.13 11.65 o 5 9 3 0.00 35.30 10.15 o 7 9 3 30.94 47.09 16.55 o -10 10 3 16.32 10.65 13.59 o -8 10 3 93.52 105.30 15.04 o -6 10 3 69.95 77.13 12.12 o -4 10 3 1.10 15.73 8.53 o -2 10 3 3.67 15.08 8.22 o 0 10 3 5.61 24.00 9.25 o 2 10 3 4.31 22.78 9.11 o 4 10 3 0.86 0.71 12.23 o -7 11 3 20.29 71.79 15.91 o -5 11 3 115.05 150.12 15.45 o -3 11 3 10.05 23.63 9.80 o -1 11 3 69.87 88.82 14.85 o 1 11 3 1.84 21.40 12.03 o 3 11 3 13.39 50.43 15.67 o -18 0 4 20.58 37.07 17.56 o -16 0 4 459.10 418.23 24.68 o -14 0 4 1361.79 1286.95 86.39 o -12 0 4 12.99 15.31 15.45 o -10 0 4 399.48 395.33 17.82 o -8 0 4 6923.62 6726.08 119.17 o -6 0 4 6131.61 6589.55 233.75 o -4 0 4 1571.31 1610.70 37.38 o -2 0 4 1209.64 1434.75 29.79 o 0 0 4 9572.61 10026.89 172.40 o 2 0 4 3743.95 3824.59 85.49 o 4 0 4 836.32 742.60 26.65 o 6 0 4 17.52 15.45 7.90 o 8 0 4 1027.76 939.36 38.04 o 10 0 4 470.20 472.07 38.15 o -17 1 4 17.32 19.79 10.01 o -15 1 4 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