#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/77/2227708.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2227708_Fobs loop_ _publ_author_name 'Moreno-Fuquen, Rodolfo' 'Grande, Carlos' 'Zuluaga, Fabio' 'Ellena, Javier' 'De Simone, Carlos A.' _publ_section_title ; 2-(Phenylcarbonothioylsulfanyl)acetic acid ; _journal_coeditor_code JH2203 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2614 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 121.870 _cell_angle_gamma 90.000 _cell_length_a 13.1565 _cell_length_b 4.9522 _cell_length_c 17.3747 _exptl_crystal_F_000 439.96 _reflns_d_resolution_high 0.7701 _[local]_cod_data_source_file jh2203Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' import in P 21/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 69.02 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1838.75 1546.64 70.98 o 3 0 0 3538.87 3067.99 105.69 o 4 0 0 4763.52 3791.72 128.95 o 5 0 0 1394.99 1328.52 68.44 o 6 0 0 6.20 4.84 1.16 o 7 0 0 258.87 302.75 13.04 o 8 0 0 473.28 517.22 22.21 o 9 0 0 30.47 30.94 2.83 o 10 0 0 125.85 118.25 4.96 o 11 0 0 24.19 23.55 1.83 o 12 0 0 0.70 -1.34 1.34 o 13 0 0 2.30 3.72 2.02 o 14 0 0 15.66 18.77 2.62 o 1 1 0 8.59 12.73 1.17 o 4 1 0 259.60 240.55 11.31 o 5 1 0 582.02 621.69 23.82 o 6 1 0 437.96 405.67 14.18 o 7 1 0 157.71 156.19 5.39 o 8 1 0 14.03 17.29 0.74 o 9 1 0 43.21 44.27 1.70 o 10 1 0 31.71 35.45 2.93 o 11 1 0 9.78 7.49 0.80 o 12 1 0 19.88 18.66 2.41 o 13 1 0 16.86 17.54 1.76 o 14 1 0 2.91 2.81 1.62 o 0 2 0 268.05 279.76 5.44 o 1 2 0 2065.14 1997.00 29.23 o 2 2 0 37.22 42.27 2.22 o 3 2 0 2600.59 2729.37 97.33 o 4 2 0 96.41 105.93 5.89 o 5 2 0 1076.12 1176.03 62.39 o 6 2 0 193.52 232.06 10.18 o 7 2 0 156.17 162.14 8.95 o 8 2 0 2.10 2.12 0.63 o 9 2 0 40.29 43.55 3.78 o 10 2 0 34.17 33.00 4.39 o 11 2 0 21.04 19.86 3.23 o 12 2 0 23.52 24.83 7.61 o 13 2 0 38.10 32.37 5.16 o 1 3 0 349.70 392.46 5.03 o 2 3 0 19.71 17.49 0.77 o 3 3 0 107.83 124.97 6.51 o 4 3 0 138.58 139.96 4.96 o 5 3 0 19.09 17.09 1.17 o 6 3 0 59.12 53.13 2.77 o 7 3 0 0.42 0.60 0.38 o 8 3 0 15.15 12.93 0.70 o 9 3 0 28.84 23.51 2.23 o 10 3 0 0.60 0.30 0.60 o 11 3 0 7.33 8.28 1.07 o 12 3 0 2.99 1.80 1.10 o 0 4 0 17.68 18.65 1.11 o 1 4 0 30.73 29.21 0.69 o 2 4 0 0.49 0.40 0.25 o 3 4 0 134.71 138.06 5.85 o 4 4 0 22.85 17.61 0.96 o 5 4 0 4.93 4.40 0.52 o 6 4 0 5.21 4.90 0.58 o 7 4 0 4.24 5.56 2.28 o 8 4 0 7.95 7.75 2.36 o 9 4 0 1.78 0.56 0.71 o 10 4 0 0.00 1.85 0.92 o 11 4 0 12.98 9.77 2.25 o 1 5 0 66.40 77.24 1.55 o 2 5 0 28.35 29.95 1.60 o 3 5 0 20.07 20.95 0.77 o 4 5 0 21.18 23.00 2.80 o 5 5 0 21.84 19.74 1.69 o 6 5 0 5.11 4.23 0.96 o 7 5 0 0.94 1.57 1.02 o 8 5 0 0.03 1.41 1.79 o 9 5 0 18.24 12.07 2.10 o 0 6 0 47.88 49.27 4.10 o 1 6 0 6.86 9.19 1.64 o 2 6 0 0.07 0.43 1.68 o 3 6 0 1.83 2.58 1.86 o -14 1 1 8.63 11.44 2.80 o -13 1 1 10.40 9.39 0.99 o -12 1 1 20.49 20.95 3.22 o -11 1 1 9.54 6.52 0.92 o -10 1 1 214.76 220.31 15.94 o -9 1 1 1.29 0.72 0.42 o -8 1 1 8.01 8.92 0.43 o -7 1 1 119.90 110.81 4.34 o -6 1 1 2567.55 2800.66 103.94 o -5 1 1 336.59 390.66 16.69 o -4 1 1 400.75 367.90 15.71 o -1 1 1 267.24 257.81 8.69 o 1 1 1 684.51 701.13 15.75 o 2 1 1 1177.91 1086.60 26.65 o 3 1 1 455.47 430.70 12.28 o 4 1 1 285.27 357.73 14.52 o 5 1 1 23.91 21.03 2.36 o 6 1 1 116.22 97.67 2.96 o 7 1 1 8.60 7.15 0.60 o 8 1 1 40.58 37.74 1.00 o 9 1 1 298.50 317.58 20.10 o 10 1 1 35.44 32.26 3.94 o 11 1 1 0.11 -0.35 0.62 o 12 1 1 10.18 9.66 1.22 o 13 1 1 15.72 14.62 2.41 o -14 2 1 10.22 7.63 1.67 o -13 2 1 0.01 0.54 0.85 o -12 2 1 59.92 63.98 6.11 o -11 2 1 15.75 16.11 2.65 o -10 2 1 51.89 47.93 5.34 o -9 2 1 0.96 0.69 0.58 o -8 2 1 192.44 186.88 10.40 o -7 2 1 30.65 32.14 1.80 o -6 2 1 63.95 67.69 2.79 o -5 2 1 12.12 16.99 2.93 o -4 2 1 2943.77 3141.98 207.06 o -3 2 1 146.15 167.50 6.01 o -2 2 1 484.38 472.77 10.59 o -1 2 1 8.84 10.09 0.26 o 0 2 1 47.48 39.85 0.61 o 1 2 1 579.59 565.80 11.47 o 2 2 1 0.24 3.27 0.35 o 3 2 1 592.58 641.06 18.82 o 4 2 1 265.33 293.93 15.18 o 5 2 1 1.62 0.31 0.25 o 6 2 1 41.06 40.79 2.22 o 7 2 1 170.66 167.41 8.36 o 8 2 1 8.84 10.36 0.76 o 9 2 1 1.81 0.99 0.52 o 10 2 1 0.01 -0.11 0.78 o 11 2 1 13.34 15.31 2.61 o 12 2 1 0.45 0.28 0.97 o 13 2 1 8.24 7.70 1.62 o -13 3 1 41.26 42.10 3.23 o -12 3 1 7.22 6.18 2.20 o -11 3 1 2.40 2.23 0.71 o -10 3 1 6.52 4.69 0.73 o -9 3 1 57.04 60.17 6.37 o -8 3 1 86.25 77.72 7.12 o -7 3 1 65.66 71.15 3.70 o -6 3 1 20.58 20.43 0.99 o -5 3 1 58.29 64.38 3.50 o -4 3 1 17.62 17.09 1.04 o -3 3 1 837.87 875.83 46.00 o -2 3 1 57.18 50.34 1.35 o -1 3 1 228.07 252.83 3.42 o 0 3 1 324.06 344.72 6.66 o 1 3 1 513.60 568.36 8.88 o 2 3 1 94.09 90.74 4.67 o 3 3 1 48.61 57.25 3.14 o 4 3 1 9.13 9.10 0.52 o 5 3 1 170.21 171.36 6.53 o 6 3 1 220.05 248.70 13.11 o 7 3 1 17.98 17.03 2.10 o 8 3 1 2.66 1.65 0.53 o 9 3 1 2.47 1.66 0.66 o 10 3 1 28.62 32.39 4.84 o 11 3 1 16.63 14.27 1.80 o 12 3 1 30.18 30.85 7.74 o -11 4 1 18.44 18.03 2.47 o -10 4 1 5.30 3.60 1.48 o -9 4 1 4.69 5.34 1.63 o -8 4 1 10.07 11.32 2.85 o -7 4 1 96.63 101.75 7.29 o -6 4 1 13.22 12.88 1.37 o -5 4 1 10.48 11.73 0.62 o -4 4 1 0.31 0.57 0.23 o -3 4 1 18.12 19.21 0.52 o -2 4 1 4.50 3.65 0.25 o -1 4 1 246.81 289.97 5.52 o 0 4 1 102.83 116.57 2.37 o 1 4 1 0.32 0.30 0.22 o 2 4 1 21.37 20.30 0.80 o 3 4 1 73.41 88.47 3.62 o 4 4 1 50.55 57.93 2.97 o 5 4 1 7.62 6.44 0.41 o 6 4 1 8.67 8.89 2.39 o 7 4 1 3.67 3.73 0.88 o 8 4 1 8.37 9.57 0.95 o 9 4 1 18.53 16.26 2.79 o 10 4 1 15.28 17.39 1.68 o -9 5 1 1.68 0.11 1.47 o -8 5 1 0.19 -0.17 1.21 o -7 5 1 0.13 0.96 0.89 o -6 5 1 8.70 7.22 1.01 o -5 5 1 9.93 12.52 4.84 o -4 5 1 0.04 2.63 1.03 o -3 5 1 5.61 2.55 0.35 o -2 5 1 24.24 33.14 1.31 o -1 5 1 11.13 13.68 0.51 o 0 5 1 18.92 21.31 0.65 o 1 5 1 1.71 3.60 0.41 o 2 5 1 0.10 -0.06 0.44 o 3 5 1 8.77 7.38 0.48 o 4 5 1 1.40 0.31 0.36 o 5 5 1 3.36 1.98 0.81 o 6 5 1 0.05 -0.35 0.92 o 7 5 1 2.55 2.14 0.91 o 8 5 1 5.20 5.17 1.54 o -5 6 1 0.23 1.64 1.42 o -3 6 1 3.43 5.40 2.06 o -2 6 1 0.22 2.74 1.95 o -1 6 1 6.73 8.04 1.72 o 0 6 1 0.55 2.54 2.97 o 1 6 1 10.58 19.49 3.18 o 2 6 1 6.02 6.14 2.77 o 3 6 1 0.03 1.66 1.88 o -15 0 2 0.00 2.64 1.65 o -14 0 2 0.06 -1.74 1.74 o -13 0 2 2.69 1.88 1.47 o -12 0 2 231.07 261.47 10.62 o -11 0 2 53.23 49.29 2.56 o -10 0 2 124.62 120.01 3.46 o -9 0 2 38.38 40.53 2.25 o -8 0 2 1481.70 1693.26 106.76 o -7 0 2 1977.88 1979.59 128.87 o -6 0 2 1129.46 1259.16 78.68 o -5 0 2 31.11 29.91 1.86 o -4 0 2 342.29 323.30 30.17 o -3 0 2 113.53 96.13 8.61 o -2 0 2 295.70 261.48 80.42 o 2 0 2 4638.14 3659.18 92.37 o 4 0 2 33.74 30.78 4.39 o 5 0 2 641.81 544.45 13.40 o 6 0 2 3.72 2.65 0.45 o 7 0 2 1507.38 1463.12 35.61 o 8 0 2 0.42 -0.46 0.46 o 9 0 2 505.41 510.85 18.78 o 10 0 2 27.86 27.32 1.80 o 11 0 2 62.98 66.23 3.34 o 12 0 2 16.83 23.59 2.30 o 13 0 2 31.36 32.65 2.73 o -15 1 2 3.17 4.38 1.67 o -14 1 2 50.62 53.26 3.72 o -13 1 2 4.99 6.05 0.95 o -12 1 2 1.34 1.21 0.62 o -11 1 2 5.91 6.48 0.69 o -10 1 2 415.45 448.48 28.34 o -9 1 2 193.25 188.02 9.86 o -8 1 2 12.19 12.55 0.74 o -7 1 2 2.42 7.64 3.09 o -6 1 2 8.11 5.84 0.30 o -5 1 2 288.73 301.09 13.97 o -4 1 2 264.16 278.96 9.82 o -3 1 2 2484.49 2586.77 223.09 o -2 1 2 34.79 38.56 4.07 o -1 1 2 4027.45 3680.83 79.36 o 0 1 2 1465.95 1330.52 26.67 o 1 1 2 220.56 198.32 3.27 o 2 1 2 195.39 160.41 4.44 o 3 1 2 1044.22 941.86 16.40 o 4 1 2 1642.18 1649.10 45.41 o 5 1 2 1774.50 1708.20 41.45 o 6 1 2 1.65 48.19 45.38 o 7 1 2 353.62 342.43 14.09 o 8 1 2 198.00 198.16 9.22 o 9 1 2 167.26 167.94 15.04 o 10 1 2 1.95 1.17 0.60 o 11 1 2 27.40 28.85 2.13 o 12 1 2 5.16 4.69 1.81 o 13 1 2 4.12 3.82 1.16 o -14 2 2 6.57 5.93 1.24 o -13 2 2 22.49 21.86 5.69 o -12 2 2 41.44 32.55 3.90 o -11 2 2 14.95 13.69 1.97 o -10 2 2 55.97 56.47 3.41 o -9 2 2 35.08 37.69 2.69 o -8 2 2 7.34 9.39 0.45 o -7 2 2 44.25 48.69 2.34 o -6 2 2 746.41 807.62 38.94 o -5 2 2 1011.35 1110.22 50.25 o -4 2 2 14.80 10.20 0.62 o -3 2 2 1226.05 1240.05 34.73 o -2 2 2 49.11 59.11 1.17 o -1 2 2 307.64 315.27 6.96 o 0 2 2 250.52 251.01 4.09 o 1 2 2 2.83 2.52 0.17 o 2 2 2 1582.88 1716.27 50.43 o 3 2 2 109.33 104.08 2.29 o 4 2 2 89.72 107.99 5.70 o 5 2 2 221.02 227.46 8.74 o 6 2 2 948.55 1049.79 51.22 o 7 2 2 9.24 8.87 0.61 o 8 2 2 11.53 11.58 1.49 o 9 2 2 20.01 20.27 1.08 o 10 2 2 59.22 80.46 3.98 o 11 2 2 10.60 7.02 1.99 o 12 2 2 26.85 33.08 6.51 o -13 3 2 1.05 0.09 1.65 o -12 3 2 1.99 0.82 1.03 o -11 3 2 2.67 2.40 1.45 o -10 3 2 11.13 9.84 1.85 o -9 3 2 50.51 45.35 4.79 o -8 3 2 13.06 13.30 1.67 o -7 3 2 51.47 48.39 2.71 o -6 3 2 3.35 2.05 0.29 o -5 3 2 3.48 3.56 0.25 o -4 3 2 403.08 417.09 14.35 o -3 3 2 458.87 465.96 10.48 o -2 3 2 13.46 12.69 0.87 o -1 3 2 149.18 146.70 3.32 o 0 3 2 167.80 190.27 4.37 o 1 3 2 152.38 152.33 3.45 o 2 3 2 0.39 -0.16 0.23 o 3 3 2 2.09 2.78 0.25 o 4 3 2 63.93 78.58 3.40 o 5 3 2 44.30 35.35 2.01 o 6 3 2 12.08 8.59 0.55 o 7 3 2 3.09 2.29 0.53 o 8 3 2 25.20 20.46 3.28 o 9 3 2 2.53 3.94 0.87 o 10 3 2 13.11 15.38 3.41 o 11 3 2 1.37 1.49 1.04 o -11 4 2 5.21 3.36 1.63 o -10 4 2 2.06 0.99 1.77 o -9 4 2 13.99 15.03 0.95 o -8 4 2 24.64 23.97 1.17 o -7 4 2 7.11 8.32 0.99 o -6 4 2 0.73 3.18 3.61 o -5 4 2 139.92 138.61 4.37 o -4 4 2 4.72 3.63 0.24 o -3 4 2 47.64 49.64 1.85 o -2 4 2 0.75 0.94 0.20 o -1 4 2 104.08 99.25 2.44 o 0 4 2 83.93 86.88 1.60 o 1 4 2 1.08 0.68 0.24 o 2 4 2 58.23 56.61 2.70 o 3 4 2 38.83 31.20 0.94 o 4 4 2 12.63 11.31 0.98 o 5 4 2 7.50 6.78 0.51 o 6 4 2 21.25 21.85 4.11 o 7 4 2 7.18 6.99 1.70 o 8 4 2 15.01 14.54 1.07 o 9 4 2 6.57 4.30 1.16 o 10 4 2 2.57 3.94 1.23 o -9 5 2 0.10 0.98 2.06 o -8 5 2 3.64 3.41 1.81 o -7 5 2 21.36 14.83 1.30 o -6 5 2 16.12 14.74 2.23 o -5 5 2 0.01 0.44 0.75 o -4 5 2 2.56 3.15 0.93 o -3 5 2 19.24 15.92 1.04 o -2 5 2 14.57 15.42 0.61 o -1 5 2 93.78 111.41 2.07 o 0 5 2 50.25 53.44 1.83 o 1 5 2 40.99 40.67 1.05 o 2 5 2 36.37 39.77 1.57 o 3 5 2 4.98 4.60 0.54 o 4 5 2 26.06 27.05 3.09 o 5 5 2 28.18 23.45 3.04 o 6 5 2 5.49 4.20 0.90 o 7 5 2 0.10 0.87 1.57 o 8 5 2 13.61 6.85 1.71 o -5 6 2 0.59 -0.99 1.30 o -4 6 2 0.18 3.06 1.91 o -3 6 2 0.01 -0.44 2.61 o -2 6 2 3.76 6.81 2.95 o -1 6 2 15.72 14.77 1.92 o 0 6 2 2.41 3.93 2.67 o 1 6 2 17.96 19.91 2.68 o 2 6 2 12.08 11.19 2.30 o -15 1 3 2.82 4.58 1.10 o -14 1 3 2.97 3.46 2.26 o -13 1 3 33.39 36.33 3.92 o -12 1 3 11.49 9.66 0.92 o -11 1 3 4.09 4.77 0.62 o -10 1 3 6.36 5.11 0.53 o -9 1 3 102.33 122.19 6.37 o -8 1 3 197.22 220.45 15.38 o -7 1 3 1377.84 1506.05 85.97 o -6 1 3 87.98 94.69 5.16 o -5 1 3 14.96 17.10 1.10 o -4 1 3 1961.28 1991.51 70.14 o -3 1 3 639.35 648.38 17.95 o -2 1 3 1723.09 1645.67 33.15 o -1 1 3 2931.51 2862.52 41.12 o 0 1 3 586.48 522.94 13.23 o 1 1 3 1232.19 1175.34 28.77 o 2 1 3 349.21 321.71 6.51 o 3 1 3 1693.05 1472.38 25.02 o 4 1 3 12.68 11.83 0.42 o 5 1 3 263.51 257.01 7.31 o 6 1 3 393.02 368.95 9.43 o 7 1 3 141.97 136.20 7.66 o 8 1 3 60.70 61.70 3.85 o 9 1 3 61.28 60.82 3.88 o 10 1 3 20.16 22.77 3.19 o 11 1 3 0.35 -0.50 1.12 o 12 1 3 74.04 80.58 10.71 o -14 2 3 2.49 2.81 0.88 o -13 2 3 15.83 17.65 1.57 o -12 2 3 58.69 62.12 6.31 o -11 2 3 44.98 43.27 2.80 o -10 2 3 22.55 22.60 1.07 o -9 2 3 396.46 425.55 23.16 o -8 2 3 28.19 27.79 0.76 o -7 2 3 16.06 16.13 1.02 o -6 2 3 313.51 345.34 14.22 o -5 2 3 955.17 987.89 29.51 o -4 2 3 366.30 405.80 10.91 o -3 2 3 250.66 287.07 11.00 o -2 2 3 325.65 353.36 7.30 o -1 2 3 1757.50 1726.99 23.44 o 0 2 3 114.10 114.91 2.78 o 1 2 3 77.50 68.21 2.02 o 2 2 3 91.91 89.11 2.44 o 3 2 3 539.44 592.38 13.69 o 4 2 3 33.00 24.05 0.76 o 5 2 3 310.63 319.36 13.51 o 6 2 3 218.12 232.97 9.45 o 7 2 3 122.09 128.22 9.91 o 8 2 3 28.39 29.82 3.73 o 9 2 3 47.93 52.11 6.39 o 10 2 3 53.92 69.32 8.36 o 11 2 3 0.00 3.53 2.07 o 12 2 3 0.37 0.84 1.41 o -13 3 3 0.01 -0.66 0.83 o -12 3 3 6.00 5.57 0.94 o -11 3 3 74.21 66.89 6.80 o -10 3 3 84.37 88.04 5.17 o -9 3 3 21.09 19.61 1.58 o -8 3 3 88.49 81.32 2.54 o -7 3 3 226.21 226.82 9.81 o -6 3 3 343.32 371.36 8.32 o -5 3 3 46.17 49.22 1.50 o -4 3 3 372.86 387.84 15.80 o -3 3 3 28.69 24.29 1.27 o -2 3 3 25.46 22.85 0.71 o -1 3 3 315.76 368.43 6.68 o 0 3 3 940.22 1036.70 22.14 o 1 3 3 608.41 653.68 18.25 o 2 3 3 75.38 80.40 4.31 o 3 3 3 0.65 0.27 0.34 o 4 3 3 414.98 445.81 13.80 o 5 3 3 262.62 287.26 14.80 o 6 3 3 52.92 57.58 4.60 o 7 3 3 14.50 13.51 1.98 o 8 3 3 18.98 21.95 3.55 o 9 3 3 136.30 168.27 30.37 o 10 3 3 0.22 -0.26 1.11 o 11 3 3 11.40 13.68 2.87 o -12 4 3 4.37 3.28 1.67 o -11 4 3 11.09 8.28 1.82 o -10 4 3 0.11 1.62 1.18 o -9 4 3 33.72 28.57 2.33 o -8 4 3 68.61 78.48 8.32 o -7 4 3 1.85 2.03 0.30 o -6 4 3 9.52 9.76 0.59 o -5 4 3 1.95 1.98 0.53 o -4 4 3 250.64 277.49 10.01 o -3 4 3 19.08 20.47 1.72 o -2 4 3 164.23 185.44 2.94 o -1 4 3 1.44 1.11 0.24 o 0 4 3 34.48 36.42 0.87 o 1 4 3 3.27 2.84 0.35 o 2 4 3 278.54 312.96 16.63 o 3 4 3 241.34 252.39 11.80 o 4 4 3 18.08 17.34 1.34 o 5 4 3 0.55 0.57 0.56 o 6 4 3 15.51 20.57 3.89 o 7 4 3 78.72 93.12 13.03 o 8 4 3 4.33 2.45 1.69 o 9 4 3 7.49 7.97 1.86 o -10 5 3 1.73 0.78 1.52 o -9 5 3 3.90 4.11 1.62 o -8 5 3 1.41 1.45 1.19 o -7 5 3 0.18 -0.26 1.76 o -6 5 3 3.76 5.80 1.10 o -5 5 3 0.48 -0.90 0.90 o -4 5 3 0.16 0.07 0.92 o -3 5 3 0.04 0.49 0.80 o -2 5 3 20.44 25.15 1.04 o -1 5 3 28.66 33.19 0.93 o 0 5 3 46.51 61.65 1.77 o 1 5 3 0.00 0.09 0.54 o 2 5 3 1.59 1.58 0.46 o 3 5 3 0.27 0.20 0.47 o 4 5 3 3.54 7.84 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