#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/77/2227710.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2227710_Fobs loop_ _publ_author_name 'Daran, Jean-Claude' 'Audin, Catherine' 'Deydier, Eric' 'Manoury, Eric' 'Poli, Rinaldo' _publ_section_title ; 1-(Diphenylphosphinothioyl)-2-[(4-methylphenyl)methoxymethyl]ferrocene ; _journal_coeditor_code JH2205 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1417 _journal_page_last m1418 _journal_volume 66 _journal_year 2010 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 78.192 _cell_angle_beta 88.526 _cell_angle_gamma 86.917 _cell_length_a 9.0614 _cell_length_b 14.9924 _cell_length_c 19.1180 _exptl_crystal_F_000 1120.00 _reflns_d_resolution_high 0.8401 _[local]_cod_data_source_file jh2205Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' EricDT6 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 270.58 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 25458.97 30872.71 1049.24 o 3 0 0 1676.64 2007.26 101.74 o 4 0 0 56.54 65.58 70.99 o 5 0 0 263.85 272.53 84.22 o 6 0 0 410.76 383.05 93.42 o 7 0 0 780.85 671.68 64.11 o 8 0 0 69.81 18.89 51.85 o -8 1 0 78.35 44.62 55.06 o -7 1 0 18.09 14.67 12.75 o -6 1 0 198.14 156.98 15.46 o -5 1 0 99.36 160.57 19.53 o -4 1 0 1503.67 1376.58 33.29 o -3 1 0 2000.49 2148.36 80.69 o -2 1 0 112.67 138.17 8.96 o 2 1 0 2019.60 2255.58 67.31 o 3 1 0 5627.14 6215.74 250.10 o 4 1 0 344.54 280.43 42.34 o 5 1 0 490.14 629.90 95.66 o 6 1 0 1184.45 1483.23 152.51 o 7 1 0 218.25 153.05 91.33 o 8 1 0 348.09 304.96 67.75 o -8 2 0 4.39 -14.14 14.14 o -7 2 0 588.70 514.11 23.50 o -6 2 0 2229.43 2138.64 49.19 o -5 2 0 303.78 359.49 17.69 o -4 2 0 30.69 35.37 8.72 o -3 2 0 1772.55 1652.13 41.16 o -2 2 0 12747.22 13106.44 152.79 o -1 2 0 562.75 507.11 18.63 o 1 2 0 941.63 897.43 19.34 o 2 2 0 661.91 778.07 24.28 o 3 2 0 90.87 112.68 6.26 o 4 2 0 1513.05 1608.32 47.66 o 5 2 0 416.32 398.58 19.65 o 6 2 0 25.66 6.54 9.68 o 7 2 0 1177.18 952.55 127.45 o 8 2 0 179.40 153.74 99.30 o -9 3 0 11.47 -22.74 22.74 o -8 3 0 1382.29 1282.54 45.83 o -7 3 0 1834.10 1627.57 53.58 o -6 3 0 3454.16 3346.95 66.54 o -5 3 0 702.21 793.53 24.55 o -4 3 0 269.44 214.28 12.84 o -3 3 0 8.63 17.51 9.36 o 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26.23 o -5 5 0 452.38 607.98 21.59 o -4 5 0 9380.46 9531.48 149.15 o -3 5 0 1994.29 2027.99 35.66 o -2 5 0 381.57 375.75 17.50 o -1 5 0 3224.05 2886.99 49.20 o 0 5 0 200.52 226.77 13.89 o 1 5 0 4944.50 4677.26 63.32 o 2 5 0 13.45 -6.82 9.13 o 3 5 0 1717.00 1610.25 28.09 o 4 5 0 185.58 176.72 11.86 o 5 5 0 1159.89 1295.81 26.91 o 6 5 0 8.25 8.32 28.04 o 7 5 0 526.36 590.08 48.76 o 8 5 0 740.25 590.13 143.54 o 9 5 0 63.81 8.74 99.84 o -9 6 0 50.24 51.51 41.61 o -8 6 0 378.84 354.29 37.19 o -7 6 0 1396.58 1368.38 58.68 o -6 6 0 445.51 408.71 23.42 o -5 6 0 91.39 86.74 16.76 o -4 6 0 151.28 180.86 18.90 o -3 6 0 3914.85 3838.83 62.59 o -2 6 0 1528.69 1638.34 40.33 o -1 6 0 319.07 304.33 17.70 o 0 6 0 3300.80 3040.21 52.92 o 1 6 0 2048.73 2248.15 40.05 o 2 6 0 1800.94 1934.54 34.99 o 3 6 0 797.78 808.11 21.49 o 4 6 0 6692.17 6835.90 95.54 o 5 6 0 4396.18 4474.50 74.20 o 6 6 0 1648.41 1544.05 35.29 o 7 6 0 351.71 439.23 131.43 o 8 6 0 122.41 175.34 36.11 o 9 6 0 47.97 89.94 108.27 o -9 7 0 5.66 91.80 49.19 o -8 7 0 424.01 404.14 41.38 o -7 7 0 1915.49 1936.68 81.41 o -6 7 0 2045.96 2049.62 75.79 o -5 7 0 648.41 778.49 52.86 o -4 7 0 3017.40 2982.21 58.81 o -3 7 0 29.69 19.43 13.46 o -2 7 0 1095.03 1017.82 27.97 o -1 7 0 1375.22 1332.70 32.92 o 0 7 0 370.73 359.26 19.03 o 1 7 0 2081.70 1870.93 37.18 o 2 7 0 274.57 309.09 19.52 o 3 7 0 7175.47 7224.30 104.71 o 4 7 0 692.11 638.33 16.92 o 5 7 0 639.43 662.15 23.88 o 6 7 0 8.01 17.79 16.84 o 7 7 0 1491.31 1477.07 91.26 o 8 7 0 377.13 309.02 44.28 o -9 8 0 292.87 415.53 61.56 o -8 8 0 711.16 797.34 77.26 o -7 8 0 1935.38 1941.87 83.84 o -6 8 0 115.05 138.23 28.45 o -5 8 0 243.92 265.95 23.94 o -4 8 0 1225.20 1389.94 41.26 o -3 8 0 4810.66 4753.98 83.39 o -2 8 0 166.88 161.42 21.73 o -1 8 0 410.15 444.25 20.63 o 0 8 0 6330.18 6211.47 99.24 o 1 8 0 537.68 748.36 92.99 o 2 8 0 23.97 40.56 13.87 o 3 8 0 1282.12 1231.58 26.36 o 4 8 0 491.65 483.97 17.88 o 5 8 0 698.07 644.56 30.82 o 6 8 0 1244.94 1227.11 83.60 o 7 8 0 5.53 17.89 25.12 o 8 8 0 470.91 478.30 94.12 o 9 8 0 65.34 36.27 40.45 o -8 9 0 72.08 105.49 56.69 o -7 9 0 659.17 664.05 54.92 o -6 9 0 587.95 675.10 53.92 o -5 9 0 51.58 44.76 24.53 o -4 9 0 2351.09 2268.03 52.28 o -3 9 0 249.67 219.51 19.88 o -2 9 0 3285.03 3211.94 64.71 o -1 9 0 35.93 71.36 16.08 o 0 9 0 218.98 212.41 18.11 o 1 9 0 2241.95 2172.11 48.94 o 2 9 0 362.82 393.35 21.75 o 3 9 0 6047.34 5979.35 98.87 o 4 9 0 13.46 11.03 11.68 o 5 9 0 538.52 521.33 28.25 o 6 9 0 34.42 -4.37 41.45 o 7 9 0 1191.44 1109.18 73.13 o 8 9 0 558.40 583.54 167.51 o 9 9 0 151.54 150.57 47.95 o -8 10 0 308.43 421.10 72.46 o -7 10 0 1010.67 1152.31 99.45 o -6 10 0 868.68 802.38 89.83 o -5 10 0 59.42 50.27 30.43 o -4 10 0 180.41 173.70 23.72 o -3 10 0 1805.60 1745.28 53.02 o -2 10 0 137.66 203.49 30.86 o -1 10 0 352.16 369.90 30.46 o 0 10 0 141.33 129.54 18.34 o 1 10 0 1262.58 1222.38 37.26 o 2 10 0 888.84 848.99 28.81 o 3 10 0 121.79 133.93 18.51 o 4 10 0 387.84 373.82 22.30 o 5 10 0 879.00 877.45 33.34 o 6 10 0 940.85 909.32 66.60 o 7 10 0 266.82 114.82 47.50 o 8 10 0 1596.99 1479.98 104.56 o 9 10 0 138.78 52.90 49.50 o -8 11 0 137.27 99.53 66.97 o -7 11 0 10.95 -23.28 62.10 o -6 11 0 145.54 112.16 65.93 o -5 11 0 350.11 336.99 40.76 o -4 11 0 206.38 255.72 44.58 o -3 11 0 2872.44 2861.49 69.56 o -2 11 0 3222.24 3200.67 74.66 o -1 11 0 318.14 358.17 25.67 o 0 11 0 100.90 96.01 21.12 o 1 11 0 2714.92 2651.59 59.19 o 2 11 0 20.86 13.65 19.30 o 3 11 0 213.07 242.12 22.13 o 4 11 0 437.52 436.70 23.59 o 5 11 0 2579.42 2491.67 69.47 o 6 11 0 1206.10 984.73 142.49 o 7 11 0 1837.96 1866.59 125.44 o 8 11 0 43.42 59.63 54.75 o -7 12 0 93.74 22.81 64.73 o -6 12 0 440.17 327.91 81.28 o -5 12 0 817.78 839.06 67.04 o -4 12 0 525.21 499.82 45.49 o -3 12 0 1291.60 1359.45 55.84 o -2 12 0 543.73 525.80 38.02 o -1 12 0 243.60 232.90 25.24 o 0 12 0 969.67 956.51 43.96 o 1 12 0 3053.63 2955.97 65.87 o 2 12 0 246.77 308.75 29.06 o 3 12 0 9.47 -22.94 22.94 o 4 12 0 13.83 -4.76 18.21 o 5 12 0 225.34 238.08 23.83 o 6 12 0 789.60 780.63 84.68 o 7 12 0 6.69 -52.05 54.83 o 8 12 0 1099.87 1164.91 95.74 o -6 13 0 4.02 -57.92 73.01 o -5 13 0 141.88 155.36 40.45 o -4 13 0 1036.86 1156.66 75.51 o -3 13 0 29.97 13.07 31.44 o -2 13 0 859.10 849.89 46.91 o -1 13 0 846.51 823.13 45.79 o 0 13 0 8.60 -25.66 25.66 o 1 13 0 1886.73 1907.02 59.37 o 2 13 0 10.34 33.57 29.63 o 3 13 0 152.45 161.58 35.62 o 4 13 0 106.64 69.72 27.96 o 5 13 0 52.55 -9.63 31.09 o 6 13 0 29.63 5.65 62.95 o 7 13 0 254.14 428.29 75.48 o -6 14 0 241.38 163.72 84.22 o -5 14 0 14.18 41.32 49.28 o -4 14 0 3.35 -0.17 39.95 o -3 14 0 782.30 932.04 50.89 o -2 14 0 1040.05 1044.07 52.59 o -1 14 0 1524.06 1571.25 84.87 o 0 14 0 419.04 399.35 40.03 o 1 14 0 1955.10 1928.17 67.54 o 2 14 0 80.89 142.67 52.84 o 3 14 0 15.60 -34.04 34.04 o 4 14 0 59.37 37.99 24.47 o 5 14 0 31.65 52.08 36.47 o 6 14 0 303.36 331.31 73.47 o -5 15 0 99.55 13.22 80.35 o -4 15 0 77.59 62.85 142.18 o -3 15 0 67.36 34.87 41.93 o -2 15 0 25.71 34.43 37.71 o -1 15 0 560.13 672.49 64.56 o 0 15 0 1212.06 1303.42 62.71 o 1 15 0 64.36 111.64 40.25 o 2 15 0 118.57 129.33 39.94 o 3 15 0 77.27 -29.76 36.57 o 4 15 0 537.14 572.56 50.25 o 5 15 0 56.82 74.11 39.83 o -3 16 0 988.69 1057.48 82.32 o -2 16 0 2.24 -40.61 40.61 o -1 16 0 80.54 94.86 40.88 o 0 16 0 31.75 78.54 45.72 o 1 16 0 860.97 818.93 57.44 o 2 16 0 27.96 -7.44 39.52 o 3 16 0 45.45 28.62 40.21 o 4 16 0 59.00 5.55 38.28 o -1 17 0 210.98 259.52 66.20 o 0 17 0 1185.71 1213.75 124.23 o 1 17 0 30.11 21.15 43.68 o 2 17 0 532.98 592.66 92.39 o 3 17 0 1.43 -41.41 41.41 o -2 -17 1 131.48 85.03 70.39 o -1 -17 1 645.90 891.77 100.28 o 0 -17 1 344.59 387.88 54.43 o 1 -17 1 47.98 115.31 46.53 o -4 -16 1 139.78 81.79 40.51 o -3 -16 1 344.40 376.12 67.69 o -2 -16 1 1418.39 1306.01 68.76 o -1 -16 1 23.94 11.96 41.60 o 0 -16 1 8.01 -2.77 42.04 o 1 -16 1 1432.69 1442.10 75.00 o 2 -16 1 87.78 73.97 49.25 o 3 -16 1 85.66 -3.68 56.54 o -5 -15 1 430.68 468.78 102.20 o -4 -15 1 53.74 -35.14 35.14 o -3 -15 1 618.77 715.35 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15.38 19.10 57.38 o -7 -12 1 6.86 -48.19 48.19 o -6 -12 1 149.55 149.05 48.95 o -5 -12 1 627.31 641.82 29.54 o -4 -12 1 70.74 38.80 17.06 o -3 -12 1 31.61 18.77 25.21 o -2 -12 1 684.68 658.73 34.42 o -1 -12 1 1626.96 1588.59 52.20 o 0 -12 1 309.23 338.99 28.79 o 1 -12 1 76.71 51.44 30.63 o 2 -12 1 158.81 152.33 31.39 o 3 -12 1 249.88 263.09 33.98 o 4 -12 1 2436.32 2386.50 88.99 o 5 -12 1 438.25 378.91 44.18 o 6 -12 1 10.83 3.40 63.96 o 7 -12 1 20.90 -65.12 65.12 o -8 -11 1 940.57 925.39 116.16 o -7 -11 1 2.99 -31.37 44.15 o -6 -11 1 1780.80 1786.25 99.19 o -5 -11 1 169.69 177.03 18.98 o -4 -11 1 435.14 504.48 26.64 o -3 -11 1 1846.94 1807.17 44.17 o -2 -11 1 481.14 443.15 24.26 o -1 -11 1 3841.80 3767.53 75.93 o 0 -11 1 1037.61 1071.06 37.63 o 1 -11 1 1154.48 1013.09 40.00 o 2 -11 1 1264.82 1260.51 45.19 o 3 -11 1 85.95 98.40 27.92 o 4 -11 1 13.54 19.83 28.96 o 5 -11 1 12.79 -31.34 32.55 o 6 -11 1 340.15 333.46 54.23 o 7 -11 1 109.42 77.18 61.40 o -9 -10 1 435.02 408.88 61.33 o -8 -10 1 52.56 118.89 47.73 o -7 -10 1 0.95 72.80 60.71 o -6 -10 1 200.95 170.88 115.89 o -5 -10 1 858.60 886.44 33.06 o -4 -10 1 100.50 102.78 15.74 o -3 -10 1 9.37 13.50 15.46 o -2 -10 1 2069.50 2062.40 45.96 o -1 -10 1 86.35 64.52 19.05 o 0 -10 1 1091.15 1090.56 33.06 o 1 -10 1 1099.99 1141.13 37.22 o 2 -10 1 4405.54 4408.20 84.52 o 3 -10 1 1058.19 1101.46 37.49 o 4 -10 1 1330.12 1354.62 53.45 o 5 -10 1 60.63 30.49 31.84 o 6 -10 1 43.29 34.68 40.94 o 7 -10 1 120.81 127.30 64.19 o 8 -10 1 44.53 28.31 57.92 o -9 -9 1 884.74 800.61 73.47 o -8 -9 1 1188.32 1026.77 165.19 o -7 -9 1 388.62 436.22 84.26 o -6 -9 1 443.26 429.16 69.72 o -5 -9 1 346.67 290.04 23.48 o -4 -9 1 66.37 37.41 12.31 o -3 -9 1 108.72 88.23 17.44 o -2 -9 1 941.83 962.13 27.88 o -1 -9 1 4008.83 3720.69 71.31 o 0 -9 1 660.07 644.54 24.41 o 1 -9 1 4003.92 3828.01 67.79 o 2 -9 1 98.92 77.80 18.25 o 3 -9 1 51.91 32.60 17.71 o 4 -9 1 29.60 23.45 18.32 o 5 -9 1 511.27 526.05 54.49 o 6 -9 1 1399.50 1251.98 110.28 o 7 -9 1 410.44 398.40 55.84 o 8 -9 1 926.84 941.03 87.16 o -9 -8 1 1456.48 1207.56 73.97 o -8 -8 1 0.26 -38.00 38.00 o -7 -8 1 0.49 -14.07 38.10 o -6 -8 1 1094.33 1026.47 43.99 o -5 -8 1 721.96 752.43 28.29 o -4 -8 1 555.80 510.94 18.56 o -3 -8 1 184.78 190.59 15.39 o -2 -8 1 1410.12 1349.49 31.14 o -1 -8 1 542.27 597.49 19.64 o 0 -8 1 338.49 320.42 20.45 o 1 -8 1 1295.26 1354.39 34.29 o 2 -8 1 8461.52 8343.21 140.29 o 3 -8 1 254.67 293.80 23.59 o 4 -8 1 1536.00 1580.91 40.92 o 5 -8 1 39.79 48.97 23.41 o 6 -8 1 1369.24 1392.37 56.74 o 7 -8 1 0.04 16.30 35.11 o 8 -8 1 387.79 354.43 60.86 o 9 -8 1 858.14 998.87 83.76 o -9 -7 1 510.56 314.45 120.03 o -8 -7 1 799.87 758.95 55.65 o -7 -7 1 677.67 731.32 39.20 o -6 -7 1 219.87 238.15 18.40 o -5 -7 1 32.54 12.03 15.12 o -4 -7 1 20.81 -5.49 9.01 o -3 -7 1 270.13 266.67 13.41 o -2 -7 1 2250.76 2340.64 45.83 o -1 -7 1 4719.03 4527.64 66.60 o 0 -7 1 1836.90 1814.01 38.97 o 1 -7 1 6275.44 5951.64 94.75 o 2 -7 1 147.54 150.39 15.85 o 3 -7 1 4.12 -12.68 12.88 o 4 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