#------------------------------------------------------------------------------ #$Date: 2011-04-13 11:12:47 +0300 (Wed, 13 Apr 2011) $ #$Revision: 17966 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2229328.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2229328_Fobs loop_ _publ_author_name 'Himmelspach, Alexander' 'Reiss, Guido J.' 'Finze, Maik' _publ_section_title ; 2-Azaniumylcarba-closo-dodecaborate ethanol monosolvate ; _journal_coeditor_code BR2161 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o704 _journal_volume 67 _journal_year 2011 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 97.519 _cell_angle_gamma 90.000 _cell_length_a 9.5753 _cell_length_b 9.2549 _cell_length_c 13.9095 _exptl_crystal_F_000 432.00 _reflns_d_resolution_high 0.7107 _[local]_cod_data_source_file br2161Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title 2-ammoniocarba-closo-dodecaborane _shelx_refln_list_code 4 _shelx_f_calc_maximum 115.35 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 10990.52 10782.14 49.97 o 3 0 0 837.03 853.44 7.42 o 4 0 0 4154.87 4461.85 28.50 o 5 0 0 10.62 5.54 0.27 o 6 0 0 564.17 581.00 4.73 o 7 0 0 33.58 30.84 0.37 o 8 0 0 138.74 119.38 0.63 o 9 0 0 290.06 271.26 1.52 o 10 0 0 16.02 16.62 0.70 o 11 0 0 0.66 0.48 0.73 o 12 0 0 50.99 47.56 1.06 o 13 0 0 38.59 35.16 1.11 o 2 1 0 343.34 366.68 1.96 o 3 1 0 889.67 909.92 4.17 o 4 1 0 566.77 611.98 2.56 o 5 1 0 1123.91 1313.61 4.83 o 6 1 0 366.32 368.90 2.06 o 7 1 0 518.26 500.43 2.13 o 8 1 0 22.54 18.44 0.28 o 9 1 0 0.56 0.93 0.34 o 10 1 0 8.95 8.37 0.44 o 11 1 0 305.39 300.72 2.49 o 12 1 0 0.41 1.00 0.60 o 13 1 0 0.31 0.50 0.66 o 0 2 0 13306.46 11941.99 127.65 o 1 2 0 36.76 38.90 0.31 o 2 2 0 341.94 380.13 1.71 o 3 2 0 0.40 1.09 0.13 o 4 2 0 311.46 378.15 1.74 o 5 2 0 43.57 37.04 0.29 o 6 2 0 7.31 6.88 0.18 o 7 2 0 80.45 76.62 0.56 o 8 2 0 70.22 64.05 0.40 o 9 2 0 181.83 172.52 0.88 o 10 2 0 83.81 84.91 0.58 o 11 2 0 96.23 99.67 0.92 o 12 2 0 4.57 3.83 0.61 o 13 2 0 76.92 79.71 1.01 o 1 3 0 5096.66 4947.22 27.21 o 2 3 0 529.08 497.05 3.25 o 3 3 0 0.16 3.63 0.24 o 4 3 0 8.20 10.93 0.23 o 5 3 0 293.82 248.60 1.87 o 6 3 0 211.92 208.96 0.93 o 7 3 0 9.24 7.65 0.28 o 8 3 0 142.67 143.34 0.97 o 9 3 0 107.24 107.43 0.87 o 10 3 0 8.75 9.27 0.46 o 11 3 0 31.42 30.90 0.65 o 12 3 0 180.09 185.05 1.32 o 0 4 0 1654.51 1886.93 10.07 o 1 4 0 7.14 7.46 0.19 o 2 4 0 165.17 230.86 1.41 o 3 4 0 123.04 132.22 0.95 o 4 4 0 892.22 883.22 3.96 o 5 4 0 446.57 436.15 2.48 o 6 4 0 832.78 847.35 5.17 o 7 4 0 0.00 0.09 0.35 o 8 4 0 113.72 114.73 0.61 o 9 4 0 104.91 103.54 0.73 o 10 4 0 430.90 428.74 2.80 o 11 4 0 21.13 22.76 0.59 o 12 4 0 10.32 9.92 0.71 o 1 5 0 1421.11 1598.97 8.04 o 2 5 0 98.09 101.73 0.57 o 3 5 0 97.09 76.91 0.46 o 4 5 0 0.00 0.10 0.16 o 5 5 0 1199.63 1177.76 5.36 o 6 5 0 28.61 30.25 0.51 o 7 5 0 88.15 92.07 0.79 o 8 5 0 34.68 33.80 0.51 o 9 5 0 169.00 167.16 1.00 o 10 5 0 64.57 69.25 0.73 o 11 5 0 53.77 51.48 1.18 o 12 5 0 7.83 7.24 0.73 o 0 6 0 573.17 565.25 6.85 o 1 6 0 88.64 92.43 0.61 o 2 6 0 16.33 17.53 0.33 o 3 6 0 29.85 30.07 0.30 o 4 6 0 347.81 351.33 2.14 o 5 6 0 266.22 266.64 1.80 o 6 6 0 278.60 289.57 2.99 o 7 6 0 330.38 336.39 2.05 o 8 6 0 1.91 2.24 0.51 o 9 6 0 44.63 43.60 0.80 o 10 6 0 24.23 22.20 0.63 o 11 6 0 51.65 51.88 0.79 o 1 7 0 88.43 82.44 0.50 o 2 7 0 851.51 808.01 4.29 o 3 7 0 51.83 46.90 0.52 o 4 7 0 199.57 194.44 1.73 o 5 7 0 0.36 0.46 0.50 o 6 7 0 27.18 27.18 0.65 o 7 7 0 174.77 178.02 1.91 o 8 7 0 79.54 76.67 1.01 o 9 7 0 192.45 188.03 1.55 o 10 7 0 0.16 0.34 0.64 o 11 7 0 7.69 7.53 0.74 o 0 8 0 663.83 574.55 2.64 o 1 8 0 14.50 14.52 0.35 o 2 8 0 135.09 119.53 1.08 o 3 8 0 6.30 6.62 0.41 o 4 8 0 130.78 133.42 1.49 o 5 8 0 12.97 11.73 0.62 o 6 8 0 43.39 43.71 0.72 o 7 8 0 350.39 349.54 1.81 o 8 8 0 308.24 303.75 3.73 o 9 8 0 655.89 663.54 5.24 o 10 8 0 327.85 337.23 2.56 o 1 9 0 16.12 13.80 0.44 o 2 9 0 79.98 75.28 0.91 o 3 9 0 179.38 177.97 1.40 o 4 9 0 4.75 5.05 0.59 o 5 9 0 332.74 335.78 2.99 o 6 9 0 4.84 4.50 0.67 o 7 9 0 97.16 96.60 1.27 o 8 9 0 43.05 41.57 0.92 o 9 9 0 380.63 375.58 2.77 o 0 10 0 67.10 67.74 0.95 o 1 10 0 170.30 170.20 1.41 o 2 10 0 6.68 6.36 0.52 o 3 10 0 491.41 500.96 3.46 o 4 10 0 15.33 16.56 0.70 o 5 10 0 7.78 7.98 0.69 o 6 10 0 108.24 108.67 1.00 o 7 10 0 1.20 1.07 0.75 o 8 10 0 56.10 57.37 0.99 o 1 11 0 63.09 62.71 1.38 o 2 11 0 114.55 119.17 1.47 o 3 11 0 13.09 14.45 0.69 o 4 11 0 82.53 85.10 1.10 o 5 11 0 46.56 44.56 0.90 o 6 11 0 68.02 68.28 1.00 o 7 11 0 12.87 14.18 0.86 o 0 12 0 13.66 13.41 0.92 o 1 12 0 125.24 129.79 1.77 o 2 12 0 70.60 78.52 1.00 o 3 12 0 268.35 282.95 4.11 o 4 12 0 52.74 57.87 1.32 o 5 12 0 4.48 4.37 0.89 o -13 1 1 45.55 43.56 0.79 o -12 1 1 71.26 73.40 0.79 o -11 1 1 37.45 39.82 0.61 o -10 1 1 52.61 58.63 0.52 o -9 1 1 25.14 21.66 0.39 o -8 1 1 124.92 118.48 0.74 o -7 1 1 28.54 23.25 0.24 o -6 1 1 809.23 818.55 4.12 o -5 1 1 29.65 29.88 0.23 o -4 1 1 1712.19 1868.12 7.55 o -3 1 1 49.56 53.75 0.34 o -2 1 1 125.18 126.88 0.67 o 2 1 1 33.06 39.71 0.31 o 3 1 1 144.55 122.50 0.79 o 4 1 1 3.05 9.04 0.25 o 5 1 1 258.29 261.72 1.24 o 6 1 1 267.47 254.31 1.32 o 7 1 1 601.57 597.99 3.07 o 8 1 1 262.59 251.58 1.45 o 9 1 1 34.08 33.79 0.40 o 10 1 1 2.01 1.51 0.51 o 11 1 1 77.35 74.40 0.83 o 12 1 1 10.69 10.93 0.68 o 13 1 1 26.10 24.49 0.72 o -13 2 1 12.02 12.27 0.75 o -12 2 1 114.00 118.70 0.84 o -11 2 1 335.62 351.11 2.38 o -10 2 1 48.12 50.88 0.53 o -9 2 1 1.24 3.17 0.38 o -8 2 1 72.14 66.06 0.55 o -7 2 1 1607.68 1536.06 6.70 o -6 2 1 255.00 248.79 1.20 o -5 2 1 1222.99 1252.60 5.70 o -4 2 1 456.77 496.31 2.26 o -3 2 1 97.63 109.23 1.33 o -2 2 1 481.20 444.79 1.87 o -1 2 1 417.83 359.74 1.53 o 0 2 1 82.89 61.12 0.46 o 1 2 1 445.23 413.76 3.03 o 2 2 1 34.66 30.34 0.27 o 3 2 1 77.18 84.12 0.72 o 4 2 1 92.24 87.68 0.47 o 5 2 1 395.02 387.63 2.57 o 6 2 1 68.80 60.07 0.67 o 7 2 1 358.78 335.34 1.73 o 8 2 1 322.19 300.90 1.58 o 9 2 1 10.38 8.67 0.37 o 10 2 1 78.64 79.58 0.63 o 11 2 1 13.13 13.48 0.59 o 12 2 1 221.90 226.25 1.80 o 13 2 1 38.49 37.73 0.91 o -13 3 1 134.02 134.78 1.17 o -12 3 1 211.07 215.74 1.58 o -11 3 1 397.25 419.07 2.71 o -10 3 1 349.22 357.27 2.01 o -9 3 1 0.19 0.96 0.37 o -8 3 1 82.73 70.90 0.48 o -7 3 1 33.36 24.92 0.38 o -6 3 1 364.61 340.58 1.59 o -5 3 1 415.15 430.50 2.14 o -4 3 1 179.00 204.74 1.43 o -3 3 1 57.86 54.37 0.32 o -2 3 1 282.72 321.20 2.08 o -1 3 1 422.26 415.77 2.90 o 0 3 1 147.21 146.73 1.28 o 1 3 1 15.62 16.02 0.34 o 2 3 1 81.01 75.88 0.50 o 3 3 1 151.45 159.93 0.92 o 4 3 1 469.75 480.60 2.95 o 5 3 1 261.85 246.11 1.48 o 6 3 1 294.33 269.84 1.67 o 7 3 1 594.53 558.07 2.82 o 8 3 1 237.08 218.77 1.26 o 9 3 1 37.03 37.17 0.56 o 10 3 1 103.15 104.89 1.12 o 11 3 1 281.86 287.12 2.10 o 12 3 1 36.96 37.64 0.80 o -12 4 1 122.69 125.28 1.36 o -11 4 1 355.23 357.67 2.55 o -10 4 1 305.29 302.17 1.95 o -9 4 1 116.11 120.67 1.00 o -8 4 1 13.76 12.44 0.40 o -7 4 1 537.85 504.79 3.23 o -6 4 1 304.45 300.52 1.58 o -5 4 1 44.74 49.28 0.35 o -4 4 1 162.06 168.74 1.02 o -3 4 1 590.05 601.67 3.45 o -2 4 1 66.59 64.00 0.52 o -1 4 1 688.70 772.73 4.12 o 0 4 1 7.51 8.66 0.22 o 1 4 1 16.21 32.47 0.58 o 2 4 1 726.35 735.79 3.11 o 3 4 1 176.66 178.66 1.05 o 4 4 1 39.22 35.74 0.34 o 5 4 1 286.89 290.28 2.13 o 6 4 1 246.16 247.81 1.35 o 7 4 1 33.32 29.69 0.38 o 8 4 1 37.40 40.59 0.44 o 9 4 1 248.91 252.00 1.56 o 10 4 1 265.81 262.38 2.82 o 11 4 1 91.88 90.98 0.82 o 12 4 1 57.55 60.76 0.90 o -12 5 1 19.96 18.84 0.70 o -11 5 1 218.38 225.42 1.87 o -10 5 1 125.29 119.37 0.83 o -9 5 1 12.95 13.22 0.52 o -8 5 1 15.91 17.05 0.49 o -7 5 1 0.22 0.27 0.45 o -6 5 1 33.94 30.97 0.65 o -5 5 1 546.28 525.65 3.49 o -4 5 1 30.97 32.44 0.32 o -3 5 1 131.88 125.28 1.03 o -2 5 1 1722.70 1742.94 6.51 o -1 5 1 38.72 45.57 0.51 o 0 5 1 10.40 14.94 0.27 o 1 5 1 11.07 13.79 0.25 o 2 5 1 201.25 183.57 1.13 o 3 5 1 11.64 11.58 0.20 o 4 5 1 69.94 69.41 0.60 o 5 5 1 92.38 89.68 0.73 o 6 5 1 106.58 109.89 0.75 o 7 5 1 46.54 44.25 0.51 o 8 5 1 8.35 8.14 0.46 o 9 5 1 130.09 128.61 1.04 o 10 5 1 271.98 271.51 2.05 o 11 5 1 13.07 13.59 0.63 o 12 5 1 9.71 9.09 0.78 o -11 6 1 6.76 6.96 0.64 o -10 6 1 46.17 44.52 0.81 o -9 6 1 29.73 32.04 0.65 o -8 6 1 0.00 0.00 0.54 o -7 6 1 66.90 65.80 0.65 o -6 6 1 127.07 123.36 0.99 o -5 6 1 3.33 4.35 0.44 o -4 6 1 105.68 95.44 0.82 o -3 6 1 110.07 84.06 0.98 o -2 6 1 87.29 93.58 0.71 o -1 6 1 1307.40 1260.68 5.23 o 0 6 1 1.71 2.17 0.25 o 1 6 1 72.78 74.32 0.67 o 2 6 1 662.10 651.08 2.97 o 3 6 1 988.67 944.24 6.36 o 4 6 1 0.37 0.27 0.29 o 5 6 1 270.84 277.50 2.27 o 6 6 1 250.73 240.77 1.68 o 7 6 1 5.33 6.22 0.50 o 8 6 1 19.31 18.74 0.55 o 9 6 1 82.18 81.65 0.96 o 10 6 1 1.39 1.32 0.61 o 11 6 1 0.20 0.00 0.70 o -11 7 1 2.89 2.57 0.70 o -10 7 1 17.66 18.76 0.69 o -9 7 1 11.69 11.17 0.65 o -8 7 1 8.82 7.94 0.61 o -7 7 1 30.79 29.27 0.68 o -6 7 1 18.03 17.74 0.59 o -5 7 1 117.28 118.49 1.18 o -4 7 1 415.96 384.37 2.18 o -3 7 1 3.12 2.21 0.34 o -2 7 1 1677.95 1626.79 8.53 o -1 7 1 80.78 70.90 0.70 o 0 7 1 25.43 19.94 0.35 o 1 7 1 12.92 9.66 0.31 o 2 7 1 942.42 857.67 3.51 o 3 7 1 12.87 9.94 0.31 o 4 7 1 3.16 1.51 0.43 o 5 7 1 86.26 84.12 0.85 o 6 7 1 11.26 12.06 0.58 o 7 7 1 104.04 106.14 1.12 o 8 7 1 57.41 60.30 0.76 o 9 7 1 0.01 0.00 0.63 o 10 7 1 0.09 0.00 0.68 o 11 7 1 32.85 33.54 0.84 o -10 8 1 15.00 15.84 0.76 o -9 8 1 8.33 11.70 0.70 o -8 8 1 135.90 134.19 1.30 o -7 8 1 2.76 2.51 0.63 o -6 8 1 1.13 0.82 0.62 o -5 8 1 16.93 20.39 0.65 o -4 8 1 138.15 133.08 1.36 o -3 8 1 128.66 104.68 0.63 o -2 8 1 39.51 32.48 0.41 o -1 8 1 277.01 261.63 2.20 o 0 8 1 25.71 20.34 0.38 o 1 8 1 125.70 119.56 0.53 o 2 8 1 61.39 61.05 0.50 o 3 8 1 89.84 81.02 0.59 o 4 8 1 16.08 15.73 0.52 o 5 8 1 84.78 81.00 0.79 o 6 8 1 13.13 12.58 0.65 o 7 8 1 3.28 3.31 0.67 o 8 8 1 2.92 3.56 0.71 o 9 8 1 53.38 54.04 0.88 o 10 8 1 0.17 0.12 0.75 o -9 9 1 76.01 75.11 1.09 o -8 9 1 1.48 2.40 0.70 o -7 9 1 91.07 88.20 1.34 o -6 9 1 148.13 149.66 1.51 o -5 9 1 20.28 20.56 0.70 o -4 9 1 130.57 129.50 0.91 o -3 9 1 23.56 22.26 0.54 o -2 9 1 0.02 0.04 0.42 o -1 9 1 63.71 63.47 0.81 o 0 9 1 128.25 119.13 0.62 o 1 9 1 5.64 6.56 0.37 o 2 9 1 18.43 14.12 0.43 o 3 9 1 73.07 74.68 0.61 o 4 9 1 521.88 524.44 3.54 o 5 9 1 0.51 0.34 0.64 o 6 9 1 160.00 158.46 1.52 o 7 9 1 20.02 22.25 0.80 o 8 9 1 28.92 30.61 0.83 o 9 9 1 16.22 18.98 0.83 o -8 10 1 47.58 49.38 0.92 o -7 10 1 6.30 6.41 0.71 o -6 10 1 1.14 0.70 0.69 o -5 10 1 334.98 329.76 2.51 o -4 10 1 0.69 0.41 0.57 o -3 10 1 344.19 357.26 4.39 o -2 10 1 5.96 5.40 0.55 o -1 10 1 13.79 15.43 0.55 o 0 10 1 8.47 8.46 0.52 o 1 10 1 106.48 108.35 1.09 o 2 10 1 50.08 50.08 0.79 o 3 10 1 530.11 529.85 3.29 o 4 10 1 37.54 38.37 0.74 o 5 10 1 382.50 382.33 4.04 o 6 10 1 2.11 2.09 0.77 o 7 10 1 0.09 0.07 0.75 o 8 10 1 0.26 0.00 0.79 o -7 11 1 37.19 35.97 0.89 o -6 11 1 0.49 0.48 0.72 o -5 11 1 2.46 1.71 0.74 o -4 11 1 471.63 468.11 4.11 o -3 11 1 68.76 72.12 0.85 o -2 11 1 478.59 488.18 3.44 o -1 11 1 40.82 39.15 0.70 o 0 11 1 7.43 7.45 0.63 o 1 11 1 34.61 35.54 0.70 o 2 11 1 157.38 165.23 1.91 o 3 11 1 46.56 50.93 0.86 o 4 11 1 104.21 106.42 1.10 o 5 11 1 0.20 0.00 0.71 o 6 11 1 1.88 1.48 0.75 o 7 11 1 2.51 2.51 0.83 o -5 12 1 14.22 13.60 0.90 o -4 12 1 80.59 81.79 1.43 o -3 12 1 162.06 166.83 1.38 o -2 12 1 77.95 83.55 1.01 o -1 12 1 12.50 11.62 0.76 o 0 12 1 0.14 0.00 0.65 o 1 12 1 278.26 292.25 2.81 o 2 12 1 13.21 12.31 0.85 o 3 12 1 206.86 208.85 2.63 o 4 12 1 0.32 0.00 0.86 o 5 12 1 0.49 0.65 0.87 o 0 13 1 0.01 0.00 0.80 o -13 0 2 33.73 31.83 0.98 o -12 0 2 83.91 82.97 1.31 o -11 0 2 37.73 39.83 0.84 o -10 0 2 162.54 157.44 1.40 o -9 0 2 2.09 3.54 0.45 o -8 0 2 215.15 196.24 1.57 o -7 0 2 26.86 25.05 0.31 o -6 0 2 364.10 385.66 2.44 o -5 0 2 783.77 822.29 4.73 o -4 0 2 4.03 8.89 0.21 o -3 0 2 15.28 15.46 0.22 o -2 0 2 2358.94 2487.31 9.29 o 2 0 2 3773.00 3547.17 25.15 o 3 0 2 1692.37 1665.76 5.22 o 4 0 2 8.72 20.77 0.33 o 5 0 2 0.02 0.44 0.27 o 6 0 2 69.59 63.22 0.90 o 7 0 2 163.51 139.42 2.07 o 8 0 2 115.00 103.04 0.76 o 9 0 2 48.45 43.62 0.85 o 10 0 2 1.15 2.16 0.66 o 11 0 2 26.30 24.01 0.98 o 12 0 2 32.64 31.38 1.09 o 13 0 2 86.70 87.61 1.19 o -13 1 2 7.74 6.77 0.68 o -12 1 2 77.35 79.77 0.73 o -11 1 2 2.37 2.23 0.50 o -10 1 2 0.39 0.86 0.42 o -9 1 2 427.92 398.94 1.86 o -8 1 2 353.25 332.42 1.30 o -7 1 2 53.29 43.05 0.34 o -6 1 2 40.69 47.03 0.31 o -5 1 2 107.74 145.77 0.86 o -4 1 2 213.92 211.61 1.15 o -3 1 2 516.17 549.72 2.26 o -2 1 2 65.48 47.70 0.26 o 1 1 2 11819.94 11101.34 94.92 o 2 1 2 223.61 253.87 1.14 o 3 1 2 0.45 2.77 0.19 o 4 1 2 2.93 5.15 0.17 o 5 1 2 3.07 6.94 0.19 o 6 1 2 246.44 246.36 0.87 o 7 1 2 135.90 155.02 1.04 o 8 1 2 82.97 71.69 0.52 o 9 1 2 2.04 0.84 0.44 o 10 1 2 25.73 27.43 0.57 o 11 1 2 43.57 43.88 0.65 o 12 1 2 13.30 15.34 0.75 o 13 1 2 55.56 57.90 0.89 o -13 2 2 26.63 29.08 0.73 o -12 2 2 114.92 116.58 1.10 o -11 2 2 41.75 42.86 0.58 o -10 2 2 214.07 213.84 1.43 o -9 2 2 1.55 1.61 0.37 o -8 2 2 6.23 9.01 0.32 o -7 2 2 5.66 5.96 0.22 o -6 2 2 14.79 20.50 0.22 o -5 2 2 158.70 162.82 0.83 o -4 2 2 283.44 358.68 1.82 o -3 2 2 154.87 163.16 0.83 o -2 2 2 517.39 569.17 3.24 o -1 2 2 63.19 67.75 0.33 o 0 2 2 491.01 446.13 2.37 o 1 2 2 96.84 92.62 0.64 o 2 2 2 3033.39 3167.96 16.10 o 3 2 2 14.55 10.08 0.18 o 4 2 2 96.79 140.12 0.63 o 5 2 2 71.84 76.79 0.53 o 6 2 2 0.96 0.72 0.21 o 7 2 2 20.62 16.57 0.28 o 8 2 2 70.00 64.55 0.58 o 9 2 2 5.27 5.87 0.40 o 10 2 2 57.06 55.23 0.66 o 11 2 2 127.19 126.79 1.48 o 12 2 2 103.22 105.91 1.18 o -13 3 2 8.55 9.01 0.75 o -12 3 2 75.83 78.82 0.95 o -11 3 2 11.24 9.67 0.51 o -10 3 2 11.17 10.74 0.47 o -9 3 2 122.82 118.02 0.74 o -8 3 2 67.12 58.48 0.44 o -7 3 2 67.35 78.79 0.64 o -6 3 2 121.93 125.13 0.71 o -5 3 2 8.93 7.20 0.29 o -4 3 2 396.20 405.33 2.33 o -3 3 2 1558.78 1665.43 9.35 o -2 3 2 90.88 76.11 0.69 o -1 3 2 31.05 36.33 0.34 o 0 3 2 142.85 129.46 0.81 o 1 3 2 1354.32 1293.24 6.61 o 2 3 2 793.51 794.09 3.59 o 3 3 2 6.97 3.11 0.35 o 4 3 2 124.56 142.38 0.96 o 5 3 2 1.59 0.89 0.21 o 6 3 2 182.33 174.46 1.48 o 7 3 2 12.55 13.64 0.37 o 8 3 2 2.08 2.62 0.36 o 9 3 2 0.32 0.37 0.39 o 10 3 2 11.10 10.70 0.54 o 11 3 2 1.12 0.91 0.56 o 12 3 2 61.76 64.85 0.91 o -12 4 2 5.55 5.66 0.67 o -11 4 2 2.33 3.21 0.55 o -10 4 2 13.33 13.78 0.55 o -9 4 2 11.50 13.84 0.45 o -8 4 2 1.43 1.43 0.43 o -7 4 2 13.12 12.71 0.34 o -6 4 2 260.04 255.56 1.20 o -5 4 2 3.31 2.87 0.29 o -4 4 2 8.90 2.19 0.40 o -3 4 2 246.88 258.21 1.69 o -2 4 2 438.40 553.36 4.17 o -1 4 2 202.89 203.56 1.20 o 0 4 2 401.34 462.24 2.21 o 1 4 2 0.62 0.19 0.16 o 2 4 2 92.45 124.21 0.95 o 3 4 2 4.52 10.38 0.21 o 4 4 2 26.65 21.93 0.28 o 5 4 2 0.57 0.81 0.17 o 6 4 2 0.40 0.82 0.31 o 7 4 2 15.61 14.93 0.36 o 8 4 2 102.59 107.30 1.00 o 9 4 2 20.92 22.88 0.45 o 10 4 2 0.16 0.12 0.53 o 11 4 2 0.36 0.00 0.66 o 12 4 2 32.08 34.57 0.84 o -12 5 2 24.06 23.92 0.68 o -11 5 2 128.65 125.44 1.13 o -10 5 2 31.07 31.45 0.65 o -9 5 2 296.35 295.48 2.03 o -8 5 2 6.60 6.41 0.48 o -7 5 2 16.47 20.38 0.49 o -6 5 2 175.25 176.26 1.03 o -5 5 2 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