Crystallography Open Database

Information card for entry 2229338

Preview

Coordinates	2229338.cif
Structure factors	2229338.hkl
Original IUCr paper	HTML

Structure parameters

Chemical name	Bis(μ-<i>N</i>-nitroso-<i>N</i>-phenylhydroxylaminato)- κ^3^<i>O</i>,<i>O</i>':<i>O</i>';κ^3^<i>O</i>':<i>O</i>,<i>O</i>'- bis[(<i>N</i>-nitroso-<i>N</i>-phenylhydroxylaminato- κ^2^<i>O</i>,<i>O</i>')lead(II)]
Formula	C24 H20 N8 O8 Pb2
Calculated formula	C24 H20 N8 O8 Pb2
SMILES	[Pb]123([O]([Pb]45([O]3=NN(O4)c3ccccc3)[O]=NN(O5)c3ccccc3)=NN(O1)c1ccccc1)[O]=NN(O2)c1ccccc1
Title of publication	Bis(μ-<i>N</i>-nitroso-<i>N</i>-phenylhydroxylaminato)-κ^3^<i>O</i>,<i>O</i>':<i>O</i>';κ^3^<i>O</i>':<i>O</i>,<i>O</i>'-bis[(<i>N</i>-nitroso-<i>N</i>-phenylhydroxylaminato-κ^2^<i>O</i>,<i>O</i>')lead(II)]
Authors of publication	Najafi, Ezzatollah; Amini, Mostafa M.; Ng, Seik Weng
Journal of publication	Acta Crystallographica Section E
Year of publication	2011
Journal volume	67
Journal issue	3
Pages of publication	m377
a	9.6149 ± 0.0005 Å
b	11.534 ± 0.0006 Å
c	13.2724 ± 0.0007 Å
α	82.459 ± 0.001°
β	79.28 ± 0.001°
γ	67.369 ± 0.001°
Cell volume	1331.95 ± 0.12 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0303
Residual factor for significantly intense reflections	0.026
Weighted residual factors for significantly intense reflections	0.0685
Weighted residual factors for all reflections included in the refinement	0.0706
Goodness-of-fit parameter for all reflections included in the refinement	1.06
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	Yes

Version history

Revision	Date	Message	Files
181214 (current)	2016-04-03	hkl/2/22/ (antanas@echidna) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 2/22/93.	2229338.cif 2229338.hkl
176789	2016-02-20	cif/2/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 2/22.	2229338.cif 2229338.hkl
120072	2014-07-11	Adding DOIs to range 2 structures.	2229338.cif 2229338.hkl
88064	2013-08-29	Adding _cod_database_fobs_code data item to all COD CIFs that have Fobs deposited and did not have this data item yet.	2229338.cif 2229338.hkl
26848	2011-09-28	cif/2/, hkl/2/, html/ Reorganising CIFs of the range 2* into the "prefix-directory" tree.	2229338.cif 2229338.hkl
17966	2011-04-13	hkl/: adding the rest of Fobs files for the recent IUCr deposit.	2229338.cif 2229338.hkl
17383	2011-04-07	../uploads/cif-deposit/cod/cif Adding structures of 2229338 via cif-deposit CGI script.	2229338.cif