#------------------------------------------------------------------------------ #$Date: 2016-04-03 05:02:24 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181214 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/93/2229359.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2229359_Fobs loop_ _publ_author_name 'Shakuntala, K.' 'Foro, Sabine' 'Gowda, B. Thimme' _publ_section_title ; 2-Chloro-N-[(2-methylphenyl)sulfonyl]acetamide ; _journal_coeditor_code DS2090 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o549 _journal_volume 67 _journal_year 2011 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 93.640 _cell_angle_beta 109.720 _cell_angle_gamma 102.520 _cell_length_a 7.4439 _cell_length_b 7.5195 _cell_length_c 10.5190 _exptl_crystal_F_000 256.00 _reflns_d_resolution_high 0.8381 _cod_data_source_file ds2090Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' SA79 P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 94.34 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 2195.21 2083.31 219.50 o 2 0 0 4561.57 4529.33 694.75 o 3 0 0 91.83 68.77 10.74 o 4 0 0 1.46 0.67 0.46 o 5 0 0 136.13 131.53 35.33 o 6 0 0 213.48 188.41 61.19 o 7 0 0 0.02 0.37 0.28 o 8 0 0 41.32 36.23 13.49 o -8 1 0 2.49 2.45 0.99 o -7 1 0 0.28 0.22 0.59 o -6 1 0 32.48 26.25 13.71 o -5 1 0 50.57 35.99 16.63 o -4 1 0 127.96 110.00 50.39 o -3 1 0 22.43 12.84 5.83 o -2 1 0 27.90 36.30 4.68 o -1 1 0 95.78 64.90 0.80 o 0 1 0 658.26 577.12 3.45 o 1 1 0 1909.56 2023.08 49.41 o 2 1 0 628.55 660.83 61.11 o 3 1 0 204.42 217.62 25.16 o 4 1 0 452.81 438.43 77.81 o 5 1 0 17.55 15.52 2.64 o 6 1 0 113.87 104.23 26.72 o 7 1 0 6.68 7.56 1.72 o -8 2 0 37.41 25.51 11.05 o -7 2 0 0.95 1.26 0.60 o -6 2 0 107.27 80.21 41.16 o -5 2 0 70.48 57.02 23.38 o -4 2 0 3.27 4.21 0.98 o -3 2 0 503.17 490.10 42.39 o -2 2 0 497.85 423.62 1.64 o -1 2 0 1011.42 895.26 31.87 o 0 2 0 102.49 122.85 0.66 o 1 2 0 1342.86 1323.77 15.04 o 2 2 0 194.37 220.90 3.90 o 3 2 0 24.74 18.94 2.08 o 4 2 0 318.33 336.66 41.48 o 5 2 0 18.85 21.03 3.59 o 6 2 0 20.71 19.79 3.25 o 7 2 0 0.10 0.59 0.34 o -8 3 0 9.16 7.92 0.35 o -7 3 0 70.69 61.98 17.16 o -6 3 0 24.73 21.57 5.76 o -5 3 0 120.88 100.67 17.14 o -4 3 0 226.22 197.12 22.04 o -3 3 0 284.55 306.19 6.41 o -2 3 0 1255.71 1078.65 38.23 o -1 3 0 1268.14 1209.01 17.37 o 0 3 0 698.47 633.71 7.82 o 1 3 0 118.23 88.95 0.98 o 2 3 0 122.58 136.78 3.37 o 3 3 0 412.06 424.29 16.72 o 4 3 0 184.01 200.44 14.53 o 5 3 0 13.64 13.80 1.45 o 6 3 0 19.46 22.05 5.11 o -8 4 0 12.81 13.13 0.40 o -7 4 0 29.05 28.68 0.81 o -6 4 0 92.43 93.19 16.38 o -5 4 0 6.22 7.17 0.84 o -4 4 0 28.86 30.36 1.88 o -3 4 0 3.26 3.50 0.19 o -2 4 0 73.35 69.64 3.98 o -1 4 0 16.06 15.48 0.55 o 0 4 0 189.29 179.90 1.19 o 1 4 0 66.23 67.35 0.76 o 2 4 0 0.96 1.52 0.26 o 3 4 0 139.24 136.92 1.32 o 4 4 0 76.09 70.65 4.39 o 5 4 0 0.71 0.40 0.23 o 6 4 0 5.16 4.61 0.83 o -7 5 0 11.62 15.89 0.53 o -6 5 0 298.19 339.04 25.51 o -5 5 0 260.95 278.51 21.63 o -4 5 0 0.05 3.20 0.37 o -3 5 0 725.71 634.46 38.01 o -2 5 0 758.63 651.69 8.21 o -1 5 0 149.47 136.86 2.00 o 0 5 0 255.70 224.06 1.86 o 1 5 0 2.19 2.80 0.29 o 2 5 0 65.10 62.55 5.54 o 3 5 0 343.41 323.19 21.21 o 4 5 0 31.18 27.88 3.95 o 5 5 0 34.12 39.58 7.34 o -7 6 0 0.04 0.06 0.36 o -6 6 0 10.71 12.23 1.73 o -5 6 0 36.29 36.37 4.53 o -4 6 0 60.67 65.27 3.55 o -3 6 0 34.53 33.44 1.06 o -2 6 0 634.22 574.07 3.55 o -1 6 0 73.97 69.87 1.90 o 0 6 0 162.47 134.86 7.14 o 1 6 0 185.21 161.39 10.66 o 2 6 0 8.34 8.62 0.89 o 3 6 0 78.90 70.46 7.19 o 4 6 0 39.84 38.36 4.77 o -6 7 0 79.35 90.51 8.16 o -5 7 0 20.34 22.91 1.97 o -4 7 0 0.31 0.75 0.24 o -3 7 0 62.36 64.39 0.95 o -2 7 0 53.31 54.53 3.05 o -1 7 0 4.51 4.85 0.28 o 0 7 0 47.94 43.77 2.17 o 1 7 0 51.81 49.04 2.22 o 2 7 0 16.55 13.95 0.37 o 3 7 0 0.73 0.50 0.17 o -5 8 0 95.38 113.48 5.51 o -4 8 0 117.36 126.43 1.79 o -3 8 0 48.88 57.20 1.24 o -2 8 0 145.26 150.09 4.13 o -1 8 0 15.52 18.45 0.40 o 0 8 0 0.91 1.19 0.24 o 1 8 0 144.53 157.64 5.02 o -2 -8 1 0.14 0.09 0.17 o -1 -8 1 109.90 110.72 3.07 o 0 -8 1 43.81 42.23 1.30 o 1 -8 1 7.35 6.39 0.40 o 2 -8 1 8.78 10.64 0.32 o 3 -8 1 50.34 56.15 2.13 o 4 -8 1 0.35 1.38 0.38 o 5 -8 1 1.69 3.07 0.22 o -3 -7 1 107.36 119.53 9.97 o -2 -7 1 176.10 184.04 12.35 o -1 -7 1 75.94 85.16 3.05 o 0 -7 1 306.30 331.78 11.17 o 1 -7 1 28.39 28.72 0.59 o 2 -7 1 80.96 94.62 2.16 o 3 -7 1 345.54 364.07 13.12 o 4 -7 1 97.07 105.95 5.92 o 5 -7 1 38.40 40.39 4.64 o 6 -7 1 82.54 94.05 10.78 o -4 -6 1 9.19 8.32 0.31 o -3 -6 1 41.70 35.50 0.74 o -2 -6 1 2.74 2.00 0.27 o -1 -6 1 7.53 7.50 0.57 o 0 -6 1 1.21 1.34 0.21 o 1 -6 1 96.77 91.09 1.67 o 2 -6 1 35.72 37.45 0.98 o 3 -6 1 140.17 150.37 9.52 o 4 -6 1 47.14 47.87 3.87 o 5 -6 1 12.86 15.26 1.86 o 6 -6 1 23.38 25.72 3.26 o 7 -6 1 32.82 42.53 0.82 o -5 -5 1 108.90 102.87 14.64 o -4 -5 1 20.12 17.59 2.10 o -3 -5 1 412.80 346.64 26.12 o -2 -5 1 134.15 112.14 7.61 o -1 -5 1 92.38 73.02 1.76 o 0 -5 1 45.41 36.65 0.62 o 1 -5 1 4.24 5.01 0.42 o 2 -5 1 378.21 348.05 15.41 o 3 -5 1 649.59 658.30 55.21 o 4 -5 1 0.56 0.76 0.48 o 5 -5 1 68.21 68.86 5.59 o 6 -5 1 44.74 44.72 3.04 o 7 -5 1 0.09 0.08 0.37 o -6 -4 1 0.25 0.15 0.18 o -5 -4 1 61.27 61.79 7.30 o -4 -4 1 120.04 116.97 9.28 o -3 -4 1 17.60 15.42 0.57 o -2 -4 1 170.67 154.47 5.42 o -1 -4 1 323.62 276.31 3.72 o 0 -4 1 226.96 214.53 1.31 o 1 -4 1 86.67 58.61 0.65 o 2 -4 1 55.77 49.85 4.12 o 3 -4 1 460.54 464.26 20.66 o 4 -4 1 620.64 643.77 29.70 o 5 -4 1 10.51 11.07 1.70 o 6 -4 1 198.24 183.67 36.32 o 7 -4 1 117.22 98.26 24.91 o -7 -3 1 2.36 2.41 0.67 o -6 -3 1 33.84 30.52 6.18 o -5 -3 1 66.52 61.78 7.18 o -4 -3 1 24.31 23.95 2.62 o -3 -3 1 12.52 12.53 0.42 o -2 -3 1 128.92 135.42 1.02 o -1 -3 1 285.07 268.73 1.48 o 0 -3 1 122.22 105.82 0.74 o 1 -3 1 494.16 389.69 13.62 o 2 -3 1 14.02 14.89 0.81 o 3 -3 1 34.32 37.30 0.93 o 4 -3 1 0.23 0.43 0.42 o 5 -3 1 120.74 123.35 17.85 o 6 -3 1 19.53 19.07 4.67 o 7 -3 1 84.50 77.51 19.90 o 8 -3 1 19.54 17.53 0.53 o -7 -2 1 1.63 1.54 0.18 o -6 -2 1 44.83 47.66 10.14 o -5 -2 1 262.51 281.38 42.48 o -4 -2 1 22.10 22.27 2.82 o -3 -2 1 589.15 608.53 31.01 o -2 -2 1 691.45 632.87 3.16 o -1 -2 1 251.62 239.35 1.34 o 0 -2 1 6974.15 5056.53 39.50 o 1 -2 1 8343.82 8014.63 464.29 o 2 -2 1 557.62 521.32 28.68 o 3 -2 1 529.91 516.52 39.98 o 4 -2 1 170.63 193.31 23.35 o 5 -2 1 114.30 124.99 21.48 o 6 -2 1 115.16 105.43 23.43 o 7 -2 1 31.26 20.95 6.55 o 8 -2 1 7.43 7.52 2.98 o -8 -1 1 2.87 3.18 0.81 o -7 -1 1 1.43 1.69 0.63 o -6 -1 1 0.02 0.02 0.28 o -5 -1 1 28.46 31.97 8.00 o -4 -1 1 10.82 14.67 2.78 o -3 -1 1 729.48 739.10 101.90 o -2 -1 1 795.67 739.02 48.33 o -1 -1 1 234.24 189.62 3.95 o 0 -1 1 538.39 373.42 7.65 o 1 -1 1 6.80 8.98 0.31 o 2 -1 1 1322.61 1479.55 67.19 o 3 -1 1 534.25 579.07 44.74 o 4 -1 1 326.12 357.10 53.80 o 5 -1 1 9.50 10.16 1.34 o 6 -1 1 225.35 196.36 50.36 o 7 -1 1 23.96 18.54 5.66 o 8 -1 1 3.03 3.00 0.98 o -8 0 1 48.30 41.29 15.98 o -7 0 1 31.51 21.60 10.52 o -6 0 1 18.20 17.95 8.69 o -5 0 1 253.49 197.24 95.94 o -4 0 1 182.72 163.33 83.44 o -3 0 1 1115.11 791.52 414.56 o -2 0 1 1445.95 602.78 462.69 o -1 0 1 534.63 395.84 11.60 o 0 0 1 1557.09 1687.77 6.69 o 1 0 1 1.73 3.58 0.11 o 2 0 1 522.69 595.11 32.49 o 3 0 1 202.67 253.21 14.93 o 4 0 1 3.87 3.46 0.25 o 5 0 1 62.31 72.80 13.35 o 6 0 1 36.38 33.27 8.54 o 7 0 1 3.48 2.63 0.41 o -8 1 1 13.22 10.14 5.10 o -7 1 1 266.51 173.31 121.72 o -6 1 1 103.86 65.75 54.58 o -5 1 1 415.15 242.25 206.05 o -4 1 1 378.83 175.41 175.10 o -3 1 1 0.22 0.24 0.42 o -2 1 1 208.91 136.71 11.81 o -1 1 1 5814.04 6920.38 75.78 o 0 1 1 33.96 87.29 1.59 o 1 1 1 8900.84 10754.18 34.70 o 2 1 1 637.58 634.52 46.62 o 3 1 1 1112.17 1241.62 115.96 o 4 1 1 685.92 716.92 92.73 o 5 1 1 0.03 0.35 0.23 o 6 1 1 32.82 33.37 7.14 o 7 1 1 10.52 12.96 3.31 o -8 2 1 12.89 12.60 0.41 o -7 2 1 40.89 31.06 21.41 o -6 2 1 2.43 1.27 0.72 o -5 2 1 6.06 10.86 6.13 o -4 2 1 44.10 28.45 22.35 o -3 2 1 428.20 408.63 4.78 o -2 2 1 20.79 21.97 0.70 o -1 2 1 106.98 120.10 1.73 o 0 2 1 47.85 65.89 0.79 o 1 2 1 247.62 285.40 3.34 o 2 2 1 671.44 699.90 6.17 o 3 2 1 174.56 190.03 15.38 o 4 2 1 759.72 793.17 88.36 o 5 2 1 210.83 208.62 32.50 o 6 2 1 16.70 16.72 2.90 o 7 2 1 18.41 19.40 4.58 o -8 3 1 24.24 23.74 0.69 o -7 3 1 183.85 140.57 66.43 o -6 3 1 26.27 19.09 9.79 o -5 3 1 449.23 418.44 58.05 o -4 3 1 16.07 22.60 0.74 o -3 3 1 38.62 58.01 3.31 o -2 3 1 181.35 151.60 3.83 o -1 3 1 479.51 449.36 12.94 o 0 3 1 1280.21 1229.63 3.71 o 1 3 1 275.37 270.45 2.24 o 2 3 1 195.98 210.92 2.17 o 3 3 1 66.02 70.98 1.68 o 4 3 1 106.57 119.51 10.28 o 5 3 1 42.92 39.85 5.20 o 6 3 1 0.06 1.00 0.19 o -8 4 1 0.12 -0.20 0.33 o -7 4 1 0.94 1.45 0.40 o -6 4 1 0.34 1.04 0.31 o -5 4 1 22.61 27.08 2.12 o -4 4 1 212.24 181.44 11.22 o -3 4 1 229.19 220.54 8.29 o -2 4 1 30.39 20.82 0.41 o -1 4 1 317.69 297.87 1.56 o 0 4 1 7.92 9.29 0.43 o 1 4 1 310.33 305.70 3.90 o 2 4 1 157.76 166.53 3.83 o 3 4 1 81.97 86.89 3.51 o 4 4 1 145.77 142.88 10.65 o 5 4 1 2.14 2.74 0.36 o -8 5 1 59.34 71.49 1.05 o -7 5 1 0.48 0.98 0.35 o -6 5 1 311.90 325.18 31.61 o -5 5 1 124.14 104.98 11.07 o -4 5 1 13.52 15.07 0.38 o -3 5 1 6.82 8.12 0.29 o -2 5 1 100.81 91.79 0.98 o -1 5 1 77.81 87.83 1.40 o 0 5 1 149.07 137.56 1.23 o 1 5 1 102.17 106.67 2.96 o 2 5 1 12.71 12.39 0.60 o 3 5 1 78.44 70.45 4.19 o 4 5 1 8.24 6.58 0.73 o 5 5 1 9.30 6.69 0.96 o -7 6 1 133.61 157.90 1.75 o -6 6 1 49.88 55.92 4.10 o -5 6 1 302.98 286.59 22.19 o -4 6 1 627.32 546.81 16.12 o -3 6 1 11.96 13.44 0.50 o -2 6 1 546.10 470.80 5.83 o -1 6 1 341.25 304.33 8.30 o 0 6 1 0.10 0.27 0.26 o 1 6 1 77.77 73.21 4.83 o 2 6 1 145.85 134.58 8.96 o 3 6 1 1.68 1.51 0.42 o 4 6 1 54.53 58.07 6.90 o -6 7 1 25.61 27.19 2.14 o -5 7 1 10.39 11.06 0.34 o -4 7 1 60.46 59.27 0.90 o -3 7 1 40.68 36.95 0.72 o -2 7 1 91.67 80.36 4.16 o -1 7 1 378.11 323.88 11.33 o 0 7 1 170.63 149.32 6.56 o 1 7 1 39.69 34.71 1.91 o 2 7 1 151.94 150.84 9.98 o 3 7 1 1.00 0.21 0.20 o -5 8 1 22.83 28.35 0.51 o -4 8 1 0.39 0.57 0.20 o -3 8 1 24.25 25.14 0.89 o -2 8 1 75.02 77.91 1.04 o -1 8 1 43.57 45.22 1.81 o 0 8 1 13.29 11.41 0.99 o 1 8 1 6.13 9.90 0.26 o -2 -8 2 5.70 5.52 0.20 o -1 -8 2 0.87 0.57 0.42 o 0 -8 2 17.07 19.42 0.55 o 1 -8 2 8.20 7.97 0.29 o 2 -8 2 127.57 139.09 2.49 o 3 -8 2 0.51 0.73 0.20 o 4 -8 2 42.64 44.14 2.05 o -3 -7 2 17.37 19.06 1.83 o -2 -7 2 211.43 216.27 12.24 o -1 -7 2 30.89 34.14 0.77 o 0 -7 2 297.92 321.15 2.21 o 1 -7 2 0.40 0.58 0.28 o 2 -7 2 54.46 60.80 0.95 o 3 -7 2 41.84 46.25 3.39 o 4 -7 2 27.24 33.07 2.23 o 5 -7 2 0.60 0.40 0.20 o 6 -7 2 2.24 2.91 0.16 o -5 -6 2 16.71 20.04 1.69 o -4 -6 2 60.86 67.66 5.86 o -3 -6 2 20.38 21.04 0.86 o -2 -6 2 18.39 22.41 1.36 o -1 -6 2 129.70 123.34 2.80 o 0 -6 2 3.37 3.41 0.28 o 1 -6 2 426.13 434.96 10.25 o 2 -6 2 74.55 77.26 3.41 o 3 -6 2 353.52 371.82 21.38 o 4 -6 2 343.28 349.34 30.35 o 5 -6 2 70.60 77.05 6.09 o 6 -6 2 9.95 9.72 1.38 o -5 -5 2 76.11 72.13 6.16 o -4 -5 2 114.60 108.50 9.88 o -3 -5 2 8.41 8.04 0.33 o -2 -5 2 0.07 0.09 0.26 o -1 -5 2 75.80 72.54 0.91 o 0 -5 2 189.00 175.33 1.40 o 1 -5 2 74.93 124.42 11.01 o 2 -5 2 615.62 654.31 49.33 o 3 -5 2 97.01 103.11 5.82 o 4 -5 2 240.16 269.34 11.84 o 5 -5 2 69.04 76.18 4.64 o 6 -5 2 4.79 4.65 0.60 o 7 -5 2 54.79 54.35 12.46 o -6 -4 2 0.17 0.56 0.20 o -5 -4 2 60.18 59.10 7.35 o -4 -4 2 501.03 452.88 48.25 o -3 -4 2 62.99 53.63 3.07 o -2 -4 2 903.44 743.51 27.31 o -1 -4 2 562.56 475.35 2.89 o 0 -4 2 802.68 706.84 19.40 o 1 -4 2 1962.19 2000.26 126.75 o 2 -4 2 47.63 58.05 4.20 o 3 -4 2 175.39 173.61 2.07 o 4 -4 2 106.21 94.66 6.18 o 5 -4 2 17.85 13.61 2.54 o 6 -4 2 47.46 45.71 8.77 o 7 -4 2 118.47 101.64 22.98 o -7 -3 2 3.05 2.21 0.70 o -6 -3 2 4.60 4.48 0.66 o -5 -3 2 0.14 0.07 0.43 o -4 -3 2 96.61 95.85 5.91 o -3 -3 2 9.79 6.36 0.36 o -2 -3 2 6.48 4.34 0.18 o -1 -3 2 764.35 561.13 2.17 o 0 -3 2 1273.91 1085.63 46.73 o 1 -3 2 73.38 55.88 3.36 o 2 -3 2 272.07 251.31 1.54 o 3 -3 2 190.53 179.36 11.33 o 4 -3 2 2.30 6.04 1.58 o 5 -3 2 253.70 236.26 32.49 o 6 -3 2 0.03 0.21 0.50 o 7 -3 2 128.24 108.97 28.35 o -7 -2 2 4.90 3.92 1.11 o -6 -2 2 1.48 -0.17 0.37 o -5 -2 2 74.57 74.98 10.03 o -4 -2 2 63.25 52.44 3.91 o -3 -2 2 1028.21 1022.96 19.04 o -2 -2 2 309.19 268.27 4.87 o -1 -2 2 20.66 17.78 0.44 o 0 -2 2 2708.57 2493.11 134.28 o 1 -2 2 1471.58 1312.71 3.86 o 2 -2 2 0.17 0.95 0.20 o 3 -2 2 3.72 5.26 0.22 o 4 -2 2 87.91 95.58 9.53 o 5 -2 2 1.42 1.66 0.31 o 6 -2 2 11.45 13.13 2.67 o 7 -2 2 0.99 1.26 0.20 o -8 -1 2 0.56 0.47 0.27 o -7 -1 2 78.63 68.05 22.26 o -6 -1 2 185.79 167.12 51.32 o -5 -1 2 64.41 66.96 16.63 o -4 -1 2 520.72 450.48 85.69 o -3 -1 2 2.53 6.69 0.28 o -2 -1 2 778.57 607.17 2.06 o -1 -1 2 3363.38 2757.16 130.25 o 0 -1 2 1247.02 1259.54 7.56 o 1 -1 2 1518.79 1598.57 46.12 o 2 -1 2 597.37 563.63 28.75 o 3 -1 2 66.84 70.02 3.46 o 4 -1 2 341.87 363.30 33.42 o 5 -1 2 28.31 30.98 4.22 o 6 -1 2 51.75 49.10 9.63 o 7 -1 2 18.38 15.50 4.48 o -8 0 2 6.63 5.77 2.33 o -7 0 2 11.97 9.88 4.76 o -6 0 2 53.22 32.96 22.10 o -5 0 2 29.44 26.12 17.23 o -4 0 2 0.02 0.19 0.18 o -3 0 2 68.13 61.88 17.53 o -2 0 2 149.71 123.25 1.54 o -1 0 2 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