#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/93/2229377.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2229377_Fobs loop_ _publ_author_name 'Jones, Myron W.' 'Powell, Douglas R.' 'Richter-Addo, George B.' _publ_section_title ; Dinitrosylbis[tris(4-methylphenyl)phosphane]iron ; _journal_coeditor_code FK2034 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m331 _journal_volume 67 _journal_year 2011 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 114.508 _cell_angle_beta 93.158 _cell_angle_gamma 94.732 _cell_length_a 10.2400 _cell_length_b 19.4090 _cell_length_c 21.0400 _exptl_crystal_F_000 1520.00 _reflns_d_resolution_high 0.8107 _[local]_cod_data_source_file fk2034Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 08056 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 267.33 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 6920.34 7001.78 90.83 o 2 0 0 6152.93 6665.87 101.86 o 3 0 0 27.80 35.65 3.30 o 4 0 0 2734.00 2876.23 43.49 o 5 0 0 86.45 185.83 8.15 o 6 0 0 564.51 430.15 17.31 o 7 0 0 1953.07 1921.38 36.07 o 8 0 0 157.36 136.43 10.42 o 9 0 0 1676.39 1640.72 54.10 o 10 0 0 4394.12 4550.25 113.78 o 11 0 0 2708.46 2736.35 95.75 o 12 0 0 5.39 0.39 15.37 o -12 1 0 13.14 35.66 17.65 o -11 1 0 125.55 135.06 21.11 o -10 1 0 1090.88 1088.65 64.25 o -9 1 0 4142.27 4170.45 81.50 o -8 1 0 2.52 2.58 5.58 o -7 1 0 3444.65 3436.66 56.00 o -6 1 0 696.77 739.64 18.18 o -5 1 0 0.73 24.85 4.44 o -4 1 0 611.43 590.65 13.63 o -3 1 0 1066.40 1097.19 19.18 o -2 1 0 6.88 9.69 1.88 o -1 1 0 62519.58 65433.76 837.77 o 1 1 0 53347.14 55824.61 777.74 o 2 1 0 7853.99 8705.18 113.76 o 3 1 0 377.41 361.97 10.89 o 4 1 0 219.60 269.89 8.59 o 5 1 0 7.54 13.37 3.59 o 6 1 0 1426.13 1178.26 24.30 o 7 1 0 570.37 517.94 15.88 o 8 1 0 32.45 43.20 9.64 o 9 1 0 5436.04 5172.11 122.37 o 10 1 0 2476.03 2537.04 75.78 o 11 1 0 992.37 1003.52 62.32 o 12 1 0 638.15 617.36 78.16 o -12 2 0 171.73 171.67 24.68 o -11 2 0 41.57 42.16 19.60 o -10 2 0 2819.12 2876.60 80.77 o -9 2 0 1041.12 997.57 32.46 o -8 2 0 887.52 794.37 31.06 o -7 2 0 389.55 423.94 16.90 o -6 2 0 5311.13 5128.37 75.98 o -5 2 0 1765.17 1662.15 29.71 o -4 2 0 929.47 949.67 18.76 o -3 2 0 1667.61 1702.89 27.23 o -2 2 0 26994.22 29365.00 399.99 o -1 2 0 1013.93 995.89 15.15 o 0 2 0 55774.70 57200.59 729.01 o 1 2 0 1804.30 1821.89 25.89 o 2 2 0 1028.46 1113.65 18.01 o 3 2 0 460.77 465.63 10.55 o 4 2 0 670.55 776.57 19.74 o 5 2 0 29.87 35.56 5.16 o 6 2 0 305.94 289.76 10.93 o 7 2 0 852.32 735.07 19.82 o 8 2 0 13.53 10.44 6.62 o 9 2 0 296.61 310.55 36.35 o 10 2 0 1037.91 1204.62 56.29 o 11 2 0 2895.46 3122.41 91.99 o 12 2 0 8.53 11.26 49.61 o -12 3 0 1.26 -7.61 20.75 o -11 3 0 40.32 28.96 14.69 o -10 3 0 397.37 416.52 21.88 o -9 3 0 7.83 23.13 8.91 o -8 3 0 268.23 292.56 19.36 o -7 3 0 3378.86 3378.51 55.69 o -6 3 0 94.05 72.89 6.77 o -5 3 0 35.97 3.67 3.61 o -4 3 0 10.72 14.25 3.37 o -3 3 0 3095.05 3260.63 48.03 o -2 3 0 2102.19 2266.20 39.18 o -1 3 0 20370.60 22997.09 294.07 o 0 3 0 26994.31 28440.93 362.52 o 1 3 0 5356.91 5569.56 74.14 o 2 3 0 352.33 317.60 7.85 o 3 3 0 250.22 270.13 7.91 o 4 3 0 10854.84 12630.29 167.49 o 5 3 0 14210.91 15895.43 210.46 o 6 3 0 73.06 108.05 11.48 o 7 3 0 1213.70 1219.19 26.46 o 8 3 0 325.64 318.66 23.35 o 9 3 0 15.43 27.78 23.02 o 10 3 0 1433.71 1391.82 53.66 o 11 3 0 157.73 206.02 30.55 o 12 3 0 88.88 86.28 21.45 o -12 4 0 17.10 9.07 22.29 o -11 4 0 603.88 659.18 52.30 o -10 4 0 782.74 717.28 59.04 o -9 4 0 41.58 35.18 8.15 o -8 4 0 400.67 382.25 19.01 o -7 4 0 14.07 21.32 6.78 o -6 4 0 3111.20 3058.07 50.05 o -5 4 0 433.65 466.91 13.42 o -4 4 0 5714.14 5968.25 83.68 o -3 4 0 2675.94 2902.73 43.16 o -2 4 0 10.90 9.24 7.60 o -1 4 0 25524.66 27799.76 355.13 o 0 4 0 1649.66 1595.44 24.26 o 1 4 0 1720.96 1888.28 28.50 o 2 4 0 1030.33 1078.34 18.83 o 3 4 0 483.60 551.52 12.59 o 4 4 0 326.72 487.97 12.52 o 5 4 0 120.08 84.80 6.73 o 6 4 0 30.12 26.57 6.47 o 7 4 0 20.66 16.90 6.61 o 8 4 0 0.93 -3.67 11.99 o 9 4 0 635.41 712.57 71.93 o 10 4 0 1243.75 1192.56 50.06 o 11 4 0 1599.48 1706.13 72.31 o 12 4 0 264.05 297.78 31.09 o -12 5 0 72.74 84.76 25.90 o -11 5 0 26.33 27.91 19.21 o -10 5 0 154.92 169.27 19.00 o -9 5 0 1852.28 1882.33 39.89 o -8 5 0 874.39 782.31 24.74 o -7 5 0 418.64 485.67 23.47 o -6 5 0 209.78 214.57 10.13 o -5 5 0 1616.13 1368.00 26.53 o -4 5 0 3434.89 4038.99 63.42 o -3 5 0 19.11 33.61 4.21 o -2 5 0 439.89 419.05 10.07 o -1 5 0 5840.57 6136.12 82.92 o 0 5 0 561.78 471.95 15.27 o 1 5 0 279.14 232.62 7.34 o 2 5 0 19.12 19.76 3.12 o 3 5 0 3781.91 4578.88 65.55 o 4 5 0 3225.11 3665.84 55.26 o 5 5 0 2910.78 2940.00 47.30 o 6 5 0 2009.12 1961.14 35.77 o 7 5 0 73.93 71.11 13.15 o 8 5 0 135.51 112.80 18.79 o 9 5 0 2250.51 2302.33 71.63 o 10 5 0 4740.87 4963.84 126.47 o 11 5 0 504.90 555.15 37.95 o -12 6 0 102.70 123.50 30.66 o -11 6 0 460.61 374.42 32.43 o -10 6 0 815.11 866.62 39.07 o -9 6 0 343.83 311.43 19.82 o -8 6 0 268.84 208.00 23.33 o -7 6 0 1093.88 1051.91 27.62 o -6 6 0 658.16 610.21 17.26 o -5 6 0 5923.74 6321.93 90.73 o -4 6 0 5345.68 5400.58 77.55 o -3 6 0 267.25 286.36 9.45 o -2 6 0 717.01 637.05 15.41 o -1 6 0 142.92 165.70 9.23 o 0 6 0 16186.82 16815.14 218.46 o 1 6 0 350.78 332.89 10.60 o 2 6 0 1104.68 1047.08 20.02 o 3 6 0 658.08 642.63 18.98 o 4 6 0 3792.29 4343.42 64.67 o 5 6 0 97.45 124.39 7.88 o 6 6 0 619.61 661.04 19.61 o 7 6 0 300.94 322.80 22.66 o 8 6 0 125.69 114.92 17.52 o 9 6 0 32.04 70.63 16.92 o 10 6 0 415.75 408.28 31.40 o 11 6 0 708.54 836.52 46.00 o -11 7 0 126.25 83.32 30.70 o -10 7 0 177.22 219.57 22.41 o -9 7 0 952.79 938.07 31.47 o -8 7 0 291.74 273.20 17.35 o -7 7 0 273.25 251.93 13.27 o -6 7 0 1997.56 2188.59 39.68 o -5 7 0 7258.26 7613.58 107.64 o -4 7 0 1032.87 1202.29 23.79 o -3 7 0 1670.09 1710.52 29.80 o -2 7 0 1470.98 1688.18 28.65 o -1 7 0 1673.78 1458.43 25.12 o 0 7 0 15859.46 17397.00 226.98 o 1 7 0 1383.98 1140.36 21.45 o 2 7 0 601.22 578.58 14.81 o 3 7 0 14.66 13.04 3.80 o 4 7 0 162.75 231.72 10.28 o 5 7 0 2918.89 3145.33 51.20 o 6 7 0 1119.33 1088.36 30.14 o 7 7 0 174.47 137.39 18.21 o 8 7 0 842.26 779.65 37.98 o 9 7 0 494.19 490.12 32.11 o 10 7 0 4462.11 4847.46 127.35 o 11 7 0 643.19 688.05 45.26 o -12 8 0 0.07 -1.23 21.44 o -11 8 0 353.72 340.36 40.19 o -10 8 0 1142.81 1082.75 47.47 o -9 8 0 187.85 160.03 16.13 o -8 8 0 729.22 664.73 25.49 o -7 8 0 4431.36 4036.35 125.88 o -6 8 0 569.56 574.76 17.08 o -5 8 0 1043.88 1084.69 37.01 o -4 8 0 8259.32 8374.93 116.89 o -3 8 0 1435.75 1692.58 29.86 o -2 8 0 2071.75 2208.88 36.10 o -1 8 0 2944.23 3139.73 47.90 o 0 8 0 139.48 123.71 5.89 o 1 8 0 1170.74 1047.27 21.03 o 2 8 0 50.80 47.94 4.67 o 3 8 0 0.33 0.45 3.42 o 4 8 0 850.91 832.96 19.72 o 5 8 0 531.09 535.35 34.43 o 6 8 0 723.38 746.18 33.04 o 7 8 0 88.79 115.56 17.38 o 8 8 0 1.48 12.02 11.22 o 9 8 0 1638.88 1746.78 63.17 o 10 8 0 106.02 124.78 23.20 o 11 8 0 1349.88 1487.69 63.58 o -12 9 0 2.50 -13.14 18.52 o -11 9 0 1263.58 1312.65 75.00 o -10 9 0 1015.26 1083.18 45.45 o -9 9 0 36.90 31.29 10.70 o -8 9 0 2397.08 2339.60 54.54 o -7 9 0 507.92 495.57 21.02 o -6 9 0 1108.42 1126.75 31.57 o -5 9 0 7919.51 8388.54 118.80 o -4 9 0 1772.93 1697.01 31.93 o -3 9 0 8811.50 9257.49 127.46 o -2 9 0 72.30 117.57 6.70 o -1 9 0 7452.63 8459.55 116.43 o 0 9 0 5247.35 5603.67 80.41 o 1 9 0 2360.55 2256.66 37.95 o 2 9 0 3.75 5.76 3.46 o 3 9 0 214.15 249.36 10.53 o 4 9 0 2993.54 3032.56 50.25 o 5 9 0 1861.63 1890.16 43.64 o 6 9 0 274.52 252.91 20.70 o 7 9 0 134.37 120.38 21.75 o 8 9 0 186.22 194.17 23.31 o 9 9 0 104.26 92.49 19.08 o 10 9 0 2305.49 2403.99 81.46 o -11 10 0 466.17 512.27 50.11 o -10 10 0 479.93 468.93 31.46 o -9 10 0 24.81 22.52 29.55 o -8 10 0 507.66 438.52 22.03 o -7 10 0 471.18 433.78 25.81 o -6 10 0 2400.24 2422.13 53.10 o -5 10 0 145.92 148.59 12.10 o -4 10 0 6224.22 6219.99 127.97 o -3 10 0 2155.80 1999.40 44.70 o -2 10 0 2036.98 2132.36 36.72 o -1 10 0 4094.52 4309.24 64.83 o 0 10 0 4.94 11.00 3.64 o 1 10 0 74.72 48.72 5.49 o 2 10 0 4453.26 4464.72 68.13 o 3 10 0 1687.60 1673.54 32.41 o 4 10 0 462.82 463.77 15.44 o 5 10 0 3463.03 3263.59 79.72 o 6 10 0 348.87 366.29 25.00 o 7 10 0 3.44 2.64 10.48 o 8 10 0 404.86 465.48 31.81 o 9 10 0 2584.63 2650.61 84.03 o 10 10 0 11.65 24.60 20.44 o -11 11 0 12.81 -18.90 19.60 o -10 11 0 531.28 579.21 34.64 o -9 11 0 128.88 138.18 20.24 o -8 11 0 2018.59 1776.18 56.97 o -7 11 0 349.80 322.40 18.54 o -6 11 0 968.56 949.27 29.79 o -5 11 0 1926.22 1773.17 47.90 o -4 11 0 1214.37 1136.62 71.77 o -3 11 0 11180.86 11409.93 183.06 o -2 11 0 761.35 719.30 19.94 o -1 11 0 162.74 116.11 7.80 o 0 11 0 5429.26 5354.06 79.52 o 1 11 0 1834.63 1821.90 54.16 o 2 11 0 43.77 38.63 5.84 o 3 11 0 2934.96 2868.21 49.28 o 4 11 0 1221.20 1187.83 28.65 o 5 11 0 4055.01 4085.18 79.46 o 6 11 0 336.37 305.68 29.20 o 7 11 0 1845.68 1828.20 62.61 o 8 11 0 1283.90 1369.78 128.45 o 9 11 0 62.43 94.73 23.17 o 10 11 0 1232.48 1318.34 82.30 o -11 12 0 283.57 238.23 41.34 o -10 12 0 585.05 634.75 37.19 o -9 12 0 10.75 10.21 13.16 o -8 12 0 104.54 116.06 19.52 o -7 12 0 2239.41 2130.30 52.84 o -6 12 0 369.82 392.68 21.74 o -5 12 0 125.89 148.27 12.99 o -4 12 0 5037.35 4940.47 90.89 o -3 12 0 92.40 104.40 10.71 o -2 12 0 1188.40 1178.48 31.22 o -1 12 0 2935.26 3065.74 50.78 o 0 12 0 40.16 44.65 5.89 o 1 12 0 1979.59 1951.30 36.85 o 2 12 0 6571.97 6605.58 97.58 o 3 12 0 356.99 290.19 16.46 o 4 12 0 2137.77 2108.93 65.41 o 5 12 0 1017.46 986.34 113.16 o 6 12 0 5.64 19.18 14.14 o 7 12 0 1873.34 1900.38 64.83 o 8 12 0 186.92 182.85 24.64 o 9 12 0 1565.06 1538.02 62.71 o -10 13 0 1569.68 1768.81 64.72 o -9 13 0 1657.72 1646.09 60.39 o -8 13 0 214.87 208.96 26.78 o -7 13 0 204.28 230.69 49.14 o -6 13 0 2500.28 2533.45 57.85 o -5 13 0 5550.98 5680.96 104.38 o -4 13 0 400.34 461.63 20.26 o -3 13 0 7348.34 7305.28 125.99 o -2 13 0 884.30 925.89 27.99 o -1 13 0 2832.66 2830.00 58.00 o 0 13 0 175.59 242.10 13.61 o 1 13 0 578.98 527.71 26.64 o 2 13 0 2338.97 2342.79 87.89 o 3 13 0 9996.65 9853.22 243.29 o 4 13 0 459.65 442.21 24.75 o 5 13 0 334.58 299.09 23.16 o 6 13 0 3673.55 3694.35 98.52 o 7 13 0 170.37 153.35 22.25 o 8 13 0 1956.81 2139.22 74.01 o 9 13 0 785.60 974.32 49.23 o -10 14 0 462.34 539.37 38.42 o -9 14 0 2.49 25.78 15.54 o -8 14 0 637.73 599.61 36.03 o -7 14 0 1756.78 1698.42 59.65 o -6 14 0 793.93 698.09 48.11 o -5 14 0 1201.42 1280.01 37.32 o -4 14 0 8002.15 7853.72 136.63 o -3 14 0 2939.74 3008.17 70.86 o -2 14 0 75.13 65.25 9.71 o -1 14 0 1971.07 1910.12 45.14 o 0 14 0 8044.69 8035.14 117.03 o 1 14 0 34.07 34.77 7.30 o 2 14 0 122.77 119.56 9.50 o 3 14 0 468.92 438.30 20.63 o 4 14 0 1950.43 1974.58 48.75 o 5 14 0 751.22 755.36 36.70 o 6 14 0 545.98 595.57 34.79 o 7 14 0 1570.86 1706.88 63.03 o 8 14 0 44.68 41.48 17.74 o -10 15 0 200.39 227.86 29.37 o -9 15 0 1868.91 1892.78 70.93 o -8 15 0 1025.31 1042.35 48.89 o -7 15 0 238.37 265.26 26.41 o -6 15 0 1949.98 2116.25 124.15 o -5 15 0 1782.09 1869.96 61.64 o -4 15 0 447.28 490.90 31.62 o -3 15 0 1351.08 1301.69 37.19 o -2 15 0 243.83 217.01 15.36 o -1 15 0 526.14 534.92 25.41 o 0 15 0 1412.59 1477.57 39.33 o 1 15 0 3411.07 3337.33 58.40 o 2 15 0 224.14 234.09 13.63 o 3 15 0 3.06 -1.59 7.57 o 4 15 0 1.84 3.11 8.52 o 5 15 0 112.20 129.51 25.17 o 6 15 0 690.48 701.81 56.83 o 7 15 0 127.87 111.76 21.38 o 8 15 0 701.86 788.28 44.56 o -9 16 0 9.85 -5.65 18.79 o -8 16 0 599.96 603.29 47.80 o -7 16 0 749.99 803.00 41.76 o -6 16 0 1051.05 1044.85 46.15 o -5 16 0 590.00 585.35 34.94 o -4 16 0 2114.76 2256.88 69.80 o -3 16 0 45.17 35.85 16.13 o -2 16 0 324.23 329.57 27.74 o -1 16 0 421.98 466.07 22.13 o 0 16 0 1526.89 1536.65 41.31 o 1 16 0 11.94 22.15 9.03 o 2 16 0 894.95 920.37 30.77 o 3 16 0 0.49 2.06 9.49 o 4 16 0 33.96 84.25 16.47 o 5 16 0 216.81 272.17 25.74 o 6 16 0 533.20 537.76 35.16 o 7 16 0 1285.91 1389.75 58.08 o -8 17 0 267.35 239.95 28.90 o -7 17 0 75.52 69.94 19.32 o -6 17 0 844.60 943.37 45.81 o -5 17 0 151.63 185.93 23.54 o -4 17 0 620.51 595.45 34.98 o -3 17 0 450.50 343.45 26.17 o -2 17 0 1.03 7.74 8.78 o -1 17 0 59.03 61.91 11.85 o 0 17 0 244.35 286.65 24.34 o 1 17 0 143.78 161.18 15.98 o 2 17 0 330.13 334.03 25.05 o 3 17 0 360.25 340.20 32.12 o 4 17 0 2.10 -0.36 12.20 o 5 17 0 534.36 542.93 34.28 o 6 17 0 221.41 251.00 28.28 o -8 18 0 131.65 147.59 26.67 o -7 18 0 2788.22 2880.06 91.07 o -6 18 0 14.93 30.06 17.10 o -5 18 0 1086.72 969.14 63.90 o -4 18 0 942.27 999.42 108.47 o -3 18 0 471.33 465.41 31.48 o -2 18 0 1620.86 1621.08 76.77 o -1 18 0 30.58 28.37 13.88 o 0 18 0 581.63 609.97 26.98 o 1 18 0 118.17 129.82 19.72 o 2 18 0 152.93 161.49 21.71 o 3 18 0 12.07 18.67 13.69 o 4 18 0 139.75 188.05 34.66 o 5 18 0 794.49 771.64 82.69 o -7 19 0 4.56 -6.31 14.62 o -6 19 0 637.04 706.58 76.46 o -5 19 0 125.32 157.96 28.90 o -4 19 0 841.60 822.70 43.19 o -3 19 0 806.30 803.38 59.21 o -2 19 0 80.29 68.89 22.21 o -1 19 0 5.32 8.81 14.08 o 0 19 0 146.89 122.87 20.99 o 1 19 0 229.56 211.28 23.96 o 2 19 0 278.12 315.73 36.20 o 3 19 0 563.37 584.59 50.95 o 4 19 0 64.59 73.54 27.82 o -6 20 0 53.70 79.66 21.05 o -5 20 0 699.79 779.94 44.19 o -4 20 0 271.50 266.08 32.01 o -3 20 0 984.94 1072.65 49.53 o -2 20 0 369.00 393.80 32.03 o -1 20 0 23.96 16.42 15.32 o 0 20 0 825.61 733.91 55.64 o 1 20 0 4.19 -12.66 12.72 o 2 20 0 2.55 12.19 14.43 o 3 20 0 87.72 94.68 27.43 o -4 21 0 1482.57 1637.34 68.78 o -3 21 0 130.49 132.35 24.15 o -2 21 0 90.01 76.65 20.17 o -1 21 0 140.27 200.28 26.89 o 0 21 0 41.57 120.58 31.66 o 1 21 0 82.99 52.26 26.59 o 0 -22 1 415.28 420.59 48.65 o 1 -22 1 54.09 21.13 26.21 o 2 -22 1 464.04 473.01 36.19 o -2 -21 1 0.32 -5.66 13.92 o -1 -21 1 63.15 107.20 29.74 o 0 -21 1 93.48 143.48 32.35 o 1 -21 1 10.88 21.21 20.60 o 2 -21 1 2612.47 2670.73 84.17 o 3 -21 1 337.06 363.74 72.35 o 4 -21 1 20.22 -10.40 15.39 o 5 -21 1 11.81 15.14 16.23 o -4 -20 1 680.95 682.11 56.64 o -3 -20 1 2.24 19.44 15.84 o -2 -20 1 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32.20 o 7 8 2 236.23 265.43 22.69 o 8 8 2 11.06 32.63 15.91 o 9 8 2 186.55 186.42 27.74 o 10 8 2 3237.22 3327.24 100.20 o -11 9 2 146.44 215.79 25.50 o -10 9 2 34.59 41.64 17.37 o -9 9 2 43.31 45.40 15.05 o -8 9 2 464.23 455.19 28.09 o -7 9 2 505.97 467.67 20.44 o -6 9 2 4184.88 4164.95 95.26 o -5 9 2 1328.08 1353.45 57.56 o -4 9 2 431.57 389.54 13.21 o -3 9 2 847.11 829.62 19.28 o -2 9 2 421.73 436.49 13.01 o -1 9 2 385.18 378.84 10.95 o 0 9 2 527.76 434.60 16.43 o 1 9 2 1795.89 1663.86 31.09 o 2 9 2 1478.25 1463.40 34.13 o 3 9 2 439.46 414.17 14.02 o 4 9 2 2746.46 2615.72 75.66 o 5 9 2 76.21 107.85 11.16 o 6 9 2 11.98 8.01 8.98 o 7 9 2 384.82 299.91 24.97 o 8 9 2 5.72 6.85 12.86 o 9 9 2 1245.88 1212.06 53.01 o 10 9 2 149.69 156.03 25.40 o -11 10 2 81.44 42.13 27.51 o -10 10 2 425.68 391.14 30.83 o -9 10 2 0.29 -9.62 11.93 o -8 10 2 278.94 275.90 32.12 o -7 10 2 3606.78 3634.17 93.08 o -6 10 2 290.34 284.26 15.95 o -5 10 2 11843.59 12186.70 197.30 o -4 10 2 149.53 146.17 9.02 o -3 10 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201.46 o -6 -13 3 72.45 93.81 12.84 o -5 -13 3 826.93 839.13 41.67 o -4 -13 3 310.38 324.82 17.29 o -3 -13 3 54.36 49.20 9.05 o -2 -13 3 1818.75 1765.45 34.78 o -1 -13 3 232.91 205.93 10.32 o 0 -13 3 1446.17 1431.79 29.05 o 1 -13 3 2.26 2.26 4.99 o 2 -13 3 4940.02 4494.98 292.13 o 3 -13 3 449.22 453.25 30.76 o 4 -13 3 110.97 78.66 10.70 o 5 -13 3 147.11 110.72 12.50 o 6 -13 3 267.43 262.14 17.13 o 7 -13 3 2884.36 2798.94 63.16 o 8 -13 3 3442.14 3332.98 73.40 o 9 -13 3 449.94 420.14 24.20 o 10 -13 3 21.82 25.59 21.59 o 11 -13 3 115.86 119.04 33.81 o -10 -12 3 103.20 111.64 23.56 o -9 -12 3 726.23 805.21 43.22 o -8 -12 3 1546.37 1664.05 61.27 o -7 -12 3 636.91 713.75 37.37 o -6 -12 3 29.73 40.60 9.09 o -5 -12 3 663.60 607.89 31.70 o -4 -12 3 1085.97 1023.37 30.51 o -3 -12 3 39.44 12.47 6.55 o -2 -12 3 232.37 272.62 11.38 o -1 -12 3 23.53 23.22 7.01 o 0 -12 3 109.92 158.08 8.61 o 1 -12 3 54.72 28.20 6.17 o 2 -12 3 1944.62 2139.02 46.44 o 3 -12 3 1860.10 1789.80 51.22 o 4 -12 3 547.65 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