#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/94/2229402.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2229402_Fobs loop_ _publ_author_name 'Prasath, R.' 'Bhavana, P.' 'Ng, Seik Weng' 'Tiekink, Edward R. T.' _publ_section_title ; 2-Acetylanilinium chloride ; _journal_coeditor_code HG2797 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o623 _journal_volume 67 _journal_year 2011 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 102.569 _cell_angle_gamma 90.000 _cell_length_a 4.8979 _cell_length_b 15.8136 _cell_length_c 10.8203 _exptl_crystal_F_000 360.00 _reflns_d_resolution_high 0.8409 _[local]_cod_data_source_file hg2797Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 152.05 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 505.47 439.40 8.93 o 2 0 0 441.82 459.58 12.67 o 3 0 0 482.85 483.07 16.56 o 4 0 0 254.56 248.49 13.92 o 5 0 0 293.54 308.26 17.68 o 1 1 0 183.96 163.16 3.97 o 2 1 0 49.10 47.56 2.41 o 3 1 0 77.58 84.45 4.94 o 4 1 0 36.36 32.12 3.69 o 5 1 0 1.26 1.79 1.63 o 0 2 0 3985.64 3338.60 16.66 o 1 2 0 3917.15 3764.57 29.33 o 2 2 0 196.12 186.68 4.66 o 3 2 0 2.99 3.30 1.38 o 4 2 0 558.41 558.76 25.91 o 5 2 0 126.32 136.79 8.40 o 1 3 0 8.05 3.56 0.61 o 2 3 0 1147.17 1147.43 15.53 o 3 3 0 1418.28 1496.84 14.49 o 4 3 0 11.60 8.47 2.21 o 5 3 0 30.36 38.30 4.61 o 0 4 0 852.38 985.18 16.85 o 1 4 0 3212.48 3045.47 33.63 o 2 4 0 128.26 129.74 3.46 o 3 4 0 761.31 775.06 10.40 o 4 4 0 159.25 151.09 5.46 o 5 4 0 196.94 207.29 10.43 o 1 5 0 29.71 21.42 1.42 o 2 5 0 321.85 319.73 5.45 o 3 5 0 0.15 1.56 0.73 o 4 5 0 235.64 244.11 7.79 o 5 5 0 0.01 -1.67 2.09 o 0 6 0 21.03 21.69 1.88 o 1 6 0 4.28 5.53 0.66 o 2 6 0 139.78 143.99 5.46 o 3 6 0 48.18 53.77 3.97 o 4 6 0 1.67 1.38 1.74 o 5 6 0 27.86 23.36 3.68 o 1 7 0 3274.42 3284.19 22.68 o 2 7 0 1042.58 1015.54 10.38 o 3 7 0 979.43 972.56 16.36 o 4 7 0 0.51 -1.45 1.07 o 5 7 0 33.88 36.39 6.46 o 0 8 0 166.64 153.42 5.11 o 1 8 0 61.45 63.99 2.74 o 2 8 0 0.21 -0.10 0.50 o 3 8 0 101.06 27.75 46.36 o 4 8 0 568.71 567.55 11.58 o 5 8 0 0.50 -0.45 3.22 o 1 9 0 381.50 377.74 5.66 o 2 9 0 494.81 499.78 8.92 o 3 9 0 59.20 48.50 4.21 o 4 9 0 210.28 214.96 9.18 o 0 10 0 15.54 18.05 2.21 o 1 10 0 112.71 98.75 3.07 o 2 10 0 250.16 254.38 5.70 o 3 10 0 7.23 2.23 1.28 o 4 10 0 290.46 293.40 17.72 o 1 11 0 128.01 121.81 3.54 o 2 11 0 790.91 801.75 14.61 o 3 11 0 801.34 797.20 17.15 o 4 11 0 12.89 10.45 3.98 o 0 12 0 159.21 170.70 9.04 o 1 12 0 67.38 59.03 2.61 o 2 12 0 47.57 50.16 3.07 o 3 12 0 71.87 57.50 12.77 o 4 12 0 106.75 118.85 11.97 o 1 13 0 1.50 2.37 0.89 o 2 13 0 381.70 390.12 11.52 o 3 13 0 17.12 16.24 2.41 o 4 13 0 33.65 39.21 7.44 o 0 14 0 1245.13 1161.46 18.81 o 1 14 0 70.28 75.40 4.05 o 2 14 0 35.32 37.69 4.13 o 3 14 0 198.96 197.79 14.37 o 1 15 0 164.25 140.12 5.62 o 2 15 0 3.92 0.05 0.96 o 3 15 0 78.38 80.54 9.61 o 0 16 0 13.65 31.96 5.11 o 1 16 0 488.97 436.50 19.35 o 2 16 0 0.51 -4.38 2.92 o 1 17 0 20.58 21.52 4.96 o 2 17 0 7.18 6.69 3.68 o 0 18 0 444.57 434.96 18.51 o 1 18 0 104.91 129.05 11.38 o -5 1 1 54.06 58.96 9.18 o -4 1 1 481.94 498.28 17.64 o -3 1 1 458.20 455.39 11.45 o -2 1 1 854.75 848.60 10.35 o -1 1 1 572.43 557.13 7.53 o 0 1 1 1324.03 1076.26 10.53 o 1 1 1 495.59 559.49 5.04 o 2 1 1 2359.46 2386.16 18.15 o 3 1 1 684.95 660.75 13.72 o 4 1 1 125.50 133.06 7.20 o 5 1 1 70.94 67.10 8.86 o -5 2 1 22.60 14.16 3.17 o -4 2 1 16.90 14.71 2.64 o -3 2 1 222.81 265.16 8.81 o -2 2 1 1423.07 1440.71 13.39 o -1 2 1 1295.55 1363.81 11.93 o 0 2 1 4.65 3.57 1.06 o 1 2 1 200.62 222.85 3.11 o 2 2 1 96.51 94.88 2.93 o 3 2 1 5.97 10.17 1.55 o 4 2 1 54.16 55.78 5.44 o 5 2 1 48.60 49.67 5.62 o -5 3 1 5.71 5.13 2.17 o -4 3 1 172.42 174.76 8.36 o -3 3 1 652.47 645.42 13.63 o -2 3 1 1403.10 1404.77 16.59 o -1 3 1 2.87 3.26 0.68 o 0 3 1 446.63 481.89 3.39 o 1 3 1 4425.95 4355.53 18.39 o 2 3 1 490.39 464.91 7.65 o 3 3 1 2.33 0.89 0.70 o 4 3 1 36.95 34.43 3.11 o 5 3 1 131.10 132.17 8.25 o -5 4 1 32.84 26.28 3.30 o -4 4 1 154.10 170.37 8.30 o -3 4 1 31.36 36.60 3.39 o -2 4 1 16.96 12.73 1.33 o -1 4 1 1128.23 1176.58 7.65 o 0 4 1 1243.43 1220.03 8.98 o 1 4 1 992.59 960.43 13.35 o 2 4 1 78.97 82.83 2.72 o 3 4 1 701.79 705.08 11.80 o 4 4 1 28.50 24.53 2.93 o 5 4 1 93.15 87.92 6.63 o -5 5 1 2.01 1.52 1.50 o -4 5 1 1.05 -0.37 1.10 o -3 5 1 1397.64 1490.46 20.83 o -2 5 1 8.78 6.75 0.92 o -1 5 1 2.61 3.64 0.61 o 0 5 1 253.42 222.64 2.81 o 1 5 1 2261.09 2317.93 26.96 o 2 5 1 278.27 271.33 4.83 o 3 5 1 47.31 44.44 5.32 o 4 5 1 40.39 38.09 3.09 o 5 5 1 63.47 62.99 5.70 o -5 6 1 219.69 234.73 11.06 o -4 6 1 94.94 88.78 5.04 o -3 6 1 31.46 29.64 2.60 o -2 6 1 531.20 521.54 6.79 o -1 6 1 1632.41 1541.47 11.00 o 0 6 1 2200.11 2217.74 17.38 o 1 6 1 275.62 304.61 4.10 o 2 6 1 43.49 33.85 1.73 o 3 6 1 112.71 115.53 12.67 o 4 6 1 528.15 524.30 11.10 o 5 6 1 37.02 40.31 4.82 o -5 7 1 6.42 4.07 1.93 o -4 7 1 25.20 23.21 2.51 o -3 7 1 21.87 20.03 2.54 o -2 7 1 370.39 375.07 6.57 o -1 7 1 22.20 18.86 1.40 o 0 7 1 2849.80 3065.39 22.97 o 1 7 1 289.12 348.03 4.72 o 2 7 1 55.24 60.48 2.45 o 3 7 1 16.58 20.49 1.92 o 4 7 1 47.97 45.99 4.33 o 5 7 1 1.33 0.08 3.00 o -5 8 1 354.86 372.93 13.93 o -4 8 1 48.32 54.20 3.88 o -3 8 1 15.41 14.76 5.39 o -2 8 1 147.01 135.94 4.52 o -1 8 1 954.42 945.76 8.57 o 0 8 1 364.69 312.89 4.36 o 1 8 1 1458.79 1481.47 14.78 o 2 8 1 2.45 1.88 0.69 o 3 8 1 532.21 530.17 11.81 o 4 8 1 727.60 733.21 16.15 o 5 8 1 2.67 2.51 1.69 o -5 9 1 2.31 6.88 3.36 o -4 9 1 110.90 103.24 6.57 o -3 9 1 637.97 605.30 14.48 o -2 9 1 55.07 62.42 2.89 o -1 9 1 202.93 206.79 4.23 o 0 9 1 392.70 449.01 5.58 o 1 9 1 89.13 112.07 3.07 o 2 9 1 15.31 12.93 1.38 o 3 9 1 18.15 16.57 2.64 o 4 9 1 10.17 6.76 4.09 o -4 10 1 130.12 124.33 7.26 o -3 10 1 188.45 199.86 8.59 o -2 10 1 148.66 153.14 5.61 o -1 10 1 639.26 590.77 8.46 o 0 10 1 1247.61 1269.19 17.12 o 1 10 1 60.50 56.44 3.04 o 2 10 1 345.63 370.20 6.90 o 3 10 1 817.97 857.91 12.33 o 4 10 1 28.68 26.95 5.89 o -4 11 1 107.62 105.53 6.79 o -3 11 1 276.00 286.76 15.55 o -2 11 1 872.16 875.76 13.72 o -1 11 1 83.00 80.77 2.94 o 0 11 1 30.90 31.73 1.80 o 1 11 1 207.07 221.36 6.17 o 2 11 1 82.10 86.73 3.47 o 3 11 1 8.02 8.00 1.82 o 4 11 1 16.11 16.58 5.09 o -4 12 1 183.21 185.49 8.94 o -3 12 1 470.04 502.78 21.16 o -2 12 1 889.13 904.70 14.42 o -1 12 1 362.14 347.89 6.22 o 0 12 1 306.73 304.66 5.44 o 1 12 1 53.92 54.77 2.88 o 2 12 1 12.26 11.76 1.99 o 3 12 1 46.56 42.06 2.81 o 4 12 1 777.79 752.67 29.96 o -4 13 1 145.26 177.51 14.50 o -3 13 1 434.46 432.54 20.02 o -2 13 1 1.96 2.31 1.54 o -1 13 1 10.36 10.00 1.31 o 0 13 1 265.42 282.66 5.45 o 1 13 1 56.93 54.76 6.23 o 2 13 1 125.57 125.87 6.91 o 3 13 1 273.38 274.67 16.85 o -3 14 1 202.29 197.49 14.00 o -2 14 1 7.85 5.25 2.82 o -1 14 1 289.74 306.88 6.30 o 0 14 1 186.03 176.11 4.93 o 1 14 1 3.52 3.85 1.63 o 2 14 1 71.01 68.35 3.22 o 3 14 1 193.05 192.48 14.56 o -3 15 1 163.76 183.52 13.84 o -2 15 1 85.54 81.88 8.43 o -1 15 1 156.29 168.98 7.76 o 0 15 1 0.07 0.79 1.98 o 1 15 1 470.79 454.84 16.15 o 2 15 1 356.94 357.75 18.78 o 3 15 1 9.63 16.47 5.26 o -3 16 1 79.35 72.50 9.21 o -2 16 1 4.53 1.94 2.46 o -1 16 1 93.36 97.57 6.14 o 0 16 1 3.87 5.59 2.68 o 1 16 1 13.02 9.86 3.90 o 2 16 1 80.60 67.12 8.71 o -2 17 1 75.82 67.41 8.32 o -1 17 1 10.88 6.09 2.47 o 0 17 1 47.48 38.20 3.99 o 1 17 1 291.56 317.27 17.82 o 2 17 1 267.50 290.54 18.12 o -1 18 1 46.94 49.39 6.69 o 0 18 1 2.86 -0.09 4.27 o 1 18 1 0.80 0.34 3.23 o -5 0 2 26.75 21.65 5.12 o -4 0 2 4.30 5.15 2.98 o -3 0 2 297.01 289.46 13.15 o -2 0 2 1351.70 1304.09 23.12 o -1 0 2 281.64 295.55 8.28 o 0 0 2 1427.13 1231.99 8.66 o 1 0 2 5050.91 4760.53 31.83 o 2 0 2 1083.03 1103.12 24.50 o 3 0 2 525.96 552.98 20.67 o 4 0 2 73.02 85.47 8.55 o 5 0 2 45.83 52.86 8.02 o -5 1 2 328.36 309.64 12.78 o -4 1 2 71.07 71.61 5.53 o -3 1 2 2.28 1.45 1.09 o -2 1 2 55.04 56.83 3.43 o -1 1 2 1072.09 957.05 10.61 o 0 1 2 999.07 977.39 5.58 o 1 1 2 23119.47 19870.01 64.80 o 2 1 2 394.01 448.90 7.64 o 3 1 2 89.55 92.48 4.28 o 4 1 2 152.23 160.82 11.74 o 5 1 2 12.33 7.73 2.47 o -5 2 2 202.74 195.22 10.30 o -4 2 2 68.58 66.36 5.34 o -3 2 2 8.87 4.35 1.45 o -2 2 2 5680.73 5668.44 38.29 o -1 2 2 5068.77 4759.55 33.86 o 0 2 2 963.10 1036.43 11.16 o 1 2 2 1331.68 1372.98 11.48 o 2 2 2 459.43 450.16 9.92 o 3 2 2 956.35 946.51 18.15 o 4 2 2 501.80 518.73 21.28 o 5 2 2 3.10 -0.95 1.60 o -5 3 2 33.34 31.88 6.02 o -4 3 2 26.73 26.84 3.52 o -3 3 2 81.64 83.08 5.05 o -2 3 2 61.11 59.73 2.89 o -1 3 2 179.71 163.84 4.59 o 0 3 2 827.80 813.42 7.83 o 1 3 2 73.25 90.75 2.91 o 2 3 2 85.27 77.82 3.46 o 3 3 2 3.64 3.63 0.95 o 4 3 2 77.38 78.32 5.65 o 5 3 2 162.48 163.90 13.77 o -5 4 2 156.75 158.95 9.33 o -4 4 2 5.26 4.80 3.34 o -3 4 2 796.58 839.62 15.84 o -2 4 2 668.03 822.44 9.36 o -1 4 2 634.98 671.35 14.71 o 0 4 2 1945.51 1883.45 9.25 o 1 4 2 356.18 358.86 4.74 o 2 4 2 81.27 81.00 2.67 o 3 4 2 146.59 146.50 6.42 o 4 4 2 21.11 18.43 2.94 o 5 4 2 26.17 25.45 5.87 o -5 5 2 141.85 150.27 25.09 o -4 5 2 490.21 512.13 14.61 o -3 5 2 878.33 901.53 14.35 o -2 5 2 138.80 129.90 4.48 o -1 5 2 92.80 87.95 2.31 o 0 5 2 3459.33 3383.45 19.62 o 1 5 2 1206.54 1175.11 21.33 o 2 5 2 917.30 896.05 13.84 o 3 5 2 2.39 0.25 0.73 o 4 5 2 246.48 242.20 10.90 o 5 5 2 107.26 114.39 11.85 o -5 6 2 19.65 17.36 2.68 o -4 6 2 22.12 23.85 3.36 o -3 6 2 2.36 2.47 1.07 o -2 6 2 785.82 828.09 9.03 o -1 6 2 763.65 774.67 7.10 o 0 6 2 1480.57 1520.97 7.29 o 1 6 2 0.00 0.51 0.61 o 2 6 2 1026.54 1038.05 8.80 o 3 6 2 170.34 169.60 6.30 o 4 6 2 293.92 284.92 10.26 o 5 6 2 49.88 48.52 8.16 o -5 7 2 191.94 217.80 9.05 o -4 7 2 209.40 219.08 8.06 o -3 7 2 4.75 4.13 1.36 o -2 7 2 476.28 482.84 7.84 o -1 7 2 652.92 675.99 10.84 o 0 7 2 34.26 22.33 1.03 o 1 7 2 523.01 511.67 13.72 o 2 7 2 404.75 405.34 6.78 o 3 7 2 26.75 27.28 3.42 o 4 7 2 193.29 196.52 8.40 o 5 7 2 0.84 4.25 3.83 o -5 8 2 14.22 21.17 3.63 o -4 8 2 1.68 1.53 1.19 o -3 8 2 15.94 16.93 2.15 o -2 8 2 0.04 0.93 1.02 o -1 8 2 5.03 4.83 0.89 o 0 8 2 214.38 224.83 3.87 o 1 8 2 32.20 28.71 1.95 o 2 8 2 39.25 41.78 1.92 o 3 8 2 5.27 5.04 1.06 o 4 8 2 161.19 144.30 12.36 o -5 9 2 9.62 11.21 2.81 o -4 9 2 315.33 343.51 12.28 o -3 9 2 2036.52 2050.89 38.94 o -2 9 2 25.44 27.23 2.05 o -1 9 2 707.29 703.70 8.76 o 0 9 2 1201.25 1144.15 10.20 o 1 9 2 734.26 717.87 10.73 o 2 9 2 346.37 334.65 5.27 o 3 9 2 28.71 33.19 2.32 o 4 9 2 29.78 37.00 6.77 o -4 10 2 1.03 2.18 2.09 o -3 10 2 56.30 67.06 7.33 o -2 10 2 174.30 176.71 8.43 o -1 10 2 27.31 31.38 2.03 o 0 10 2 97.04 99.08 2.66 o 1 10 2 7.20 7.14 0.55 o 2 10 2 58.52 55.46 3.91 o 3 10 2 7.06 5.98 1.22 o 4 10 2 44.30 36.56 6.75 o -4 11 2 265.87 264.94 16.18 o -3 11 2 11.42 11.62 4.50 o -2 11 2 5.41 4.37 1.44 o -1 11 2 127.77 132.84 5.57 o 0 11 2 466.23 461.10 6.02 o 1 11 2 857.22 867.29 7.32 o 2 11 2 66.06 68.48 4.40 o 3 11 2 26.82 29.30 2.04 o 4 11 2 1.84 -0.89 3.79 o -4 12 2 13.73 12.67 2.67 o -3 12 2 25.82 23.47 3.07 o -2 12 2 970.92 977.75 25.03 o -1 12 2 58.94 58.51 2.98 o 0 12 2 101.54 101.05 3.02 o 1 12 2 0.00 0.53 0.34 o 2 12 2 129.73 128.36 8.04 o 3 12 2 183.46 171.54 13.35 o 4 12 2 58.39 61.65 9.24 o -4 13 2 142.88 154.31 9.80 o -3 13 2 55.33 64.75 5.15 o -2 13 2 174.41 178.64 11.13 o -1 13 2 22.27 20.88 2.21 o 0 13 2 285.02 286.15 6.31 o 1 13 2 658.18 655.45 11.85 o 2 13 2 37.18 43.98 3.87 o 3 13 2 52.18 53.25 7.89 o -3 14 2 80.18 84.77 5.96 o -2 14 2 52.41 50.86 4.29 o -1 14 2 518.97 482.69 13.05 o 0 14 2 8.74 4.12 1.07 o 1 14 2 13.57 13.12 1.51 o 2 14 2 26.24 23.37 5.23 o 3 14 2 239.11 223.59 16.18 o -3 15 2 101.52 100.61 6.56 o -2 15 2 4.65 3.76 1.63 o -1 15 2 23.18 18.09 2.17 o 0 15 2 106.16 108.74 4.17 o 1 15 2 41.79 28.11 2.33 o 2 15 2 216.49 210.28 15.09 o 3 15 2 40.40 46.42 7.70 o -3 16 2 207.22 204.91 14.65 o -2 16 2 194.98 187.92 8.47 o -1 16 2 300.78 312.89 12.80 o 0 16 2 183.10 173.43 14.27 o 1 16 2 77.59 75.11 9.21 o 2 16 2 68.84 68.51 9.20 o -2 17 2 4.76 4.82 1.88 o -1 17 2 21.62 20.67 3.13 o 0 17 2 39.00 32.44 3.71 o 1 17 2 91.41 79.75 9.55 o 2 17 2 3.70 -1.43 4.29 o -1 18 2 57.76 55.37 4.95 o 0 18 2 107.24 100.97 10.09 o 1 18 2 0.98 1.83 2.89 o -5 1 3 39.36 45.12 5.31 o -4 1 3 454.45 440.47 13.68 o -3 1 3 386.99 385.31 10.92 o -2 1 3 0.83 2.52 0.87 o -1 1 3 2544.06 2502.14 42.60 o 0 1 3 3425.35 3432.81 14.99 o 1 1 3 1687.26 1653.66 18.24 o 2 1 3 84.44 92.40 3.07 o 3 1 3 81.91 78.95 3.48 o 4 1 3 82.44 93.49 6.36 o 5 1 3 249.40 253.21 11.80 o -5 2 3 292.31 290.51 12.62 o -4 2 3 110.75 99.32 6.60 o -3 2 3 246.84 265.06 9.06 o -2 2 3 7.68 10.15 1.57 o -1 2 3 168.78 148.47 4.55 o 0 2 3 178.03 188.71 2.49 o 1 2 3 353.23 359.58 5.96 o 2 2 3 12.22 14.01 1.26 o 3 2 3 261.96 268.27 6.31 o 4 2 3 51.77 44.28 4.43 o 5 2 3 57.37 54.83 5.74 o -5 3 3 650.64 657.95 18.91 o -4 3 3 195.12 192.87 10.00 o -3 3 3 232.58 250.16 8.85 o -2 3 3 336.08 392.11 7.68 o -1 3 3 17.36 14.00 1.49 o 0 3 3 1606.82 1570.66 28.07 o 1 3 3 485.48 482.50 4.98 o 2 3 3 1130.24 1164.67 10.64 o 3 3 3 136.00 140.09 5.17 o 4 3 3 591.71 568.84 15.36 o 5 3 3 34.55 43.01 5.01 o -5 4 3 38.81 32.40 4.54 o -4 4 3 35.80 38.22 4.22 o -3 4 3 516.83 495.92 12.49 o -2 4 3 85.41 60.00 3.79 o -1 4 3 782.35 784.19 8.96 o 0 4 3 20.32 22.98 1.49 o 1 4 3 382.30 388.23 4.33 o 2 4 3 272.89 273.89 7.96 o 3 4 3 197.88 188.23 7.32 o 4 4 3 29.98 31.61 2.97 o 5 4 3 19.29 22.74 5.74 o -5 5 3 70.77 68.08 6.32 o -4 5 3 281.58 291.32 14.55 o -3 5 3 9.93 13.27 2.31 o -2 5 3 118.66 148.22 4.95 o -1 5 3 1499.26 1526.34 12.82 o 0 5 3 692.55 670.52 6.64 o 1 5 3 195.30 191.83 4.04 o 2 5 3 42.24 49.39 2.56 o 3 5 3 17.14 17.01 3.97 o 4 5 3 35.28 36.85 3.90 o 5 5 3 71.46 72.25 6.57 o -5 6 3 68.37 69.24 6.31 o -4 6 3 2.77 2.51 1.65 o -3 6 3 125.34 108.70 6.27 o -2 6 3 2247.25 2334.70 17.15 o -1 6 3 73.53 70.06 2.40 o 0 6 3 96.64 92.48 2.17 o 1 6 3 93.50 120.51 3.54 o 2 6 3 2419.14 2458.96 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