#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/04/2230477.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2230477_Fobs loop_ _publ_author_name 'Ge, Guo-Di' 'Shen, Jin-Bei' 'Zhao, Guo-Liang' _publ_section_title ; Tris[6-methoxy-2-(phenyliminiomethyl)phenolato]-\k^4^O,O';\kO^1^-tris(thiocyanato-\kN)samarium(III) ; _journal_coeditor_code SJ5128 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m706 _journal_page_last m707 _journal_volume 67 _journal_year 2011 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 19.5821 _cell_length_b 20.3531 _cell_length_c 22.4764 _exptl_crystal_F_000 4072.00 _reflns_d_resolution_high 0.7714 _[local]_cod_data_source_file sj5128Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' a in Pbca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 560.19 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 141554.34 129185.42 1725.30 o 4 0 0 155289.08 154277.52 2081.73 o 6 0 0 26275.77 26358.77 402.52 o 8 0 0 129656.42 124568.74 2347.23 o 10 0 0 54712.25 54810.05 785.39 o 12 0 0 59487.94 59842.92 880.79 o 14 0 0 47959.66 47338.03 996.46 o 16 0 0 14041.63 13459.64 661.01 o 18 0 0 34056.44 35313.75 1385.19 o 20 0 0 799.63 767.63 346.30 o 22 0 0 8216.25 10412.67 853.56 o 24 0 0 5.53 -341.17 341.17 o 2 1 0 76533.86 75423.91 733.39 o 4 1 0 53869.29 48394.56 544.09 o 6 1 0 40900.06 41065.40 440.46 o 8 1 0 1115.89 1076.08 84.44 o 10 1 0 35204.58 35078.51 413.24 o 12 1 0 4027.37 4142.48 127.79 o 14 1 0 5780.72 5586.74 217.41 o 16 1 0 3474.77 3305.32 276.62 o 18 1 0 819.03 807.89 278.00 o 20 1 0 2931.79 2936.12 473.27 o 22 1 0 92.28 381.82 242.01 o 24 1 0 825.06 1015.14 543.50 o 0 2 0 245603.19 245328.17 3184.82 o 2 2 0 41856.09 40016.54 478.78 o 4 2 0 14930.62 14219.11 194.99 o 6 2 0 50676.95 50909.23 526.36 o 8 2 0 808.92 731.28 62.46 o 10 2 0 1638.42 1778.27 125.83 o 12 2 0 9366.03 9664.16 167.97 o 14 2 0 14900.92 14965.42 348.10 o 16 2 0 3374.35 3564.89 302.48 o 18 2 0 13219.38 13038.84 555.31 o 20 2 0 49.06 -76.97 211.21 o 22 2 0 1187.81 777.66 274.62 o 24 2 0 21.05 26.76 442.81 o 2 3 0 134917.53 134222.14 1360.52 o 4 3 0 191806.89 190678.00 1931.74 o 6 3 0 12766.61 11732.22 188.97 o 8 3 0 46957.61 47564.10 553.17 o 10 3 0 26986.06 28163.86 393.53 o 12 3 0 45426.61 47319.87 543.01 o 14 3 0 1224.81 1071.52 117.44 o 16 3 0 10931.19 10972.30 416.03 o 18 3 0 44.57 32.25 184.90 o 20 3 0 5444.32 6097.88 776.77 o 22 3 0 2.98 -26.20 224.22 o 24 3 0 2882.74 4311.63 480.61 o 0 4 0 3306.11 3175.19 119.90 o 2 4 0 6994.86 6639.47 144.11 o 4 4 0 33662.08 32755.94 377.02 o 6 4 0 3031.82 3076.10 94.62 o 8 4 0 5513.88 5184.00 139.00 o 10 4 0 5149.98 5272.08 154.07 o 12 4 0 173.83 154.31 77.44 o 14 4 0 4465.74 4605.93 314.20 o 16 4 0 1082.36 969.11 171.39 o 18 4 0 177.63 461.77 290.18 o 20 4 0 2.88 50.43 211.17 o 22 4 0 95.22 -218.26 218.26 o 24 4 0 749.29 1043.71 330.20 o 2 5 0 174404.41 172838.63 1540.58 o 4 5 0 17598.42 17539.17 261.49 o 6 5 0 100839.20 97538.95 1002.85 o 8 5 0 12815.98 12807.68 265.47 o 10 5 0 17765.32 16797.89 289.85 o 12 5 0 67405.95 69214.03 1082.36 o 14 5 0 2588.24 2918.82 264.22 o 16 5 0 36122.21 36760.83 760.91 o 18 5 0 48.06 250.74 171.81 o 20 5 0 9178.93 9979.78 1186.23 o 22 5 0 40.34 -216.11 216.11 o 24 5 0 1403.66 954.66 323.45 o 0 6 0 14734.20 13650.62 283.18 o 2 6 0 9637.52 8957.91 179.15 o 4 6 0 110377.37 105117.91 984.96 o 6 6 0 9972.21 9521.74 177.32 o 8 6 0 14600.65 13904.53 252.53 o 10 6 0 41093.36 40818.33 552.28 o 12 6 0 20503.16 19821.89 618.61 o 14 6 0 11496.47 11371.52 531.81 o 16 6 0 16192.23 16386.13 494.16 o 18 6 0 8535.77 7726.27 1084.43 o 20 6 0 442.71 434.74 438.80 o 22 6 0 1945.81 1592.72 298.48 o 24 6 0 79.05 -252.54 252.54 o 2 7 0 21474.45 21946.46 282.10 o 4 7 0 387.31 280.33 56.81 o 6 7 0 2075.43 1997.42 81.08 o 8 7 0 22492.87 23754.49 342.29 o 10 7 0 10947.59 11295.66 233.46 o 12 7 0 20.36 13.97 157.44 o 14 7 0 1947.29 1877.04 264.52 o 16 7 0 2521.23 2488.65 214.32 o 18 7 0 286.57 398.84 221.89 o 20 7 0 1989.89 2299.08 523.46 o 22 7 0 364.34 289.24 299.64 o 24 7 0 75.91 259.92 359.60 o 0 8 0 150926.52 159199.72 1979.64 o 2 8 0 730.85 859.70 68.20 o 4 8 0 127966.88 124377.94 1119.22 o 6 8 0 35383.03 34526.57 435.22 o 8 8 0 82626.03 82363.46 1015.68 o 10 8 0 20973.07 21509.95 485.29 o 12 8 0 6255.84 6270.10 391.23 o 14 8 0 10337.51 9860.42 621.44 o 16 8 0 2664.73 3065.35 383.24 o 18 8 0 11296.06 11369.95 615.16 o 20 8 0 3.98 -167.86 190.07 o 22 8 0 3802.07 3804.18 407.62 o 24 8 0 17.05 -255.73 255.73 o 2 9 0 2186.50 2381.73 118.27 o 4 9 0 17267.61 18636.41 274.60 o 6 9 0 55031.14 57296.58 638.68 o 8 9 0 843.20 794.60 68.61 o 10 9 0 3727.72 3644.41 301.59 o 12 9 0 14114.97 14087.71 663.64 o 14 9 0 2710.38 2804.71 681.53 o 16 9 0 985.86 881.62 170.27 o 18 9 0 778.57 829.88 408.98 o 20 9 0 585.87 504.97 226.95 o 22 9 0 452.46 468.81 253.24 o 0 10 0 62827.27 62858.29 940.52 o 2 10 0 385.25 337.26 62.11 o 4 10 0 66988.99 67025.35 728.60 o 6 10 0 524.03 614.32 119.38 o 8 10 0 10162.58 10123.50 234.07 o 10 10 0 3241.88 3082.89 195.13 o 12 10 0 7619.98 8158.97 510.57 o 14 10 0 864.28 897.03 162.82 o 16 10 0 69.40 -1.19 142.29 o 18 10 0 8870.82 9122.26 474.36 o 20 10 0 597.20 650.70 240.18 o 22 10 0 1473.44 1635.84 322.65 o 2 11 0 98585.67 96801.84 986.23 o 4 11 0 12239.22 11935.86 266.52 o 6 11 0 61510.98 61077.33 810.88 o 8 11 0 36634.94 36969.08 636.70 o 10 11 0 21271.50 21600.95 1065.87 o 12 11 0 7632.20 7970.46 441.33 o 14 11 0 275.72 268.34 148.10 o 16 11 0 9086.42 10114.48 340.38 o 18 11 0 5.57 49.27 177.08 o 20 11 0 8869.71 8650.70 526.68 o 22 11 0 26.87 -82.50 247.76 o 0 12 0 11792.13 11642.98 375.64 o 2 12 0 1366.11 1274.98 111.88 o 4 12 0 5787.40 5599.56 204.95 o 6 12 0 368.23 337.86 89.23 o 8 12 0 1148.49 1414.11 273.35 o 10 12 0 3597.24 3628.23 263.71 o 12 12 0 1110.61 1463.62 280.51 o 14 12 0 83.17 184.14 154.88 o 16 12 0 528.81 987.82 175.53 o 18 12 0 1302.66 1132.42 268.76 o 20 12 0 34.54 -65.44 290.19 o 22 12 0 2.15 367.81 454.68 o 2 13 0 26080.57 26069.92 438.56 o 4 13 0 1991.96 2086.98 164.78 o 6 13 0 25572.31 26631.80 487.91 o 8 13 0 6702.61 6633.37 406.12 o 10 13 0 13211.40 14242.08 852.00 o 12 13 0 2590.03 2725.93 258.67 o 14 13 0 212.75 348.39 262.36 o 16 13 0 4523.99 4807.91 494.54 o 18 13 0 151.55 102.62 214.24 o 20 13 0 4033.70 3816.41 417.62 o 22 13 0 2.80 -170.97 260.76 o 0 14 0 14082.10 14240.19 809.95 o 2 14 0 205.72 145.60 117.21 o 4 14 0 24082.63 23463.04 515.80 o 6 14 0 10285.39 10158.43 549.00 o 8 14 0 24676.73 24902.04 1055.57 o 10 14 0 3585.22 4297.82 367.75 o 12 14 0 4537.09 5045.25 436.56 o 14 14 0 3413.90 3774.26 363.47 o 16 14 0 396.80 469.36 178.38 o 18 14 0 5198.38 4616.90 426.58 o 20 14 0 260.92 499.85 277.71 o 2 15 0 1553.53 1309.59 274.54 o 4 15 0 1283.10 1187.33 181.77 o 6 15 0 4302.84 4885.92 420.56 o 8 15 0 1724.40 1054.29 330.59 o 10 15 0 113.31 -131.47 248.82 o 12 15 0 98.91 502.13 311.35 o 14 15 0 188.87 648.67 288.90 o 16 15 0 2.20 -123.70 186.03 o 18 15 0 10.40 -246.25 309.90 o 20 15 0 152.47 769.87 368.42 o 0 16 0 28106.51 28985.15 1373.65 o 2 16 0 1625.46 1288.63 205.28 o 4 16 0 45315.79 47700.41 963.00 o 6 16 0 13605.11 13740.34 858.69 o 8 16 0 23655.85 24701.00 1155.93 o 10 16 0 4992.29 5314.39 557.28 o 12 16 0 7738.96 8881.58 674.32 o 14 16 0 8794.05 9494.66 705.10 o 16 16 0 544.15 319.17 438.80 o 18 16 0 2470.94 2850.55 485.78 o 20 16 0 68.51 -138.84 335.40 o 2 17 0 5317.58 4058.92 812.20 o 4 17 0 9721.21 10500.49 618.45 o 6 17 0 2122.29 2835.16 515.28 o 8 17 0 1292.10 980.54 349.50 o 10 17 0 3559.92 4502.84 565.94 o 12 17 0 2169.92 2200.60 457.88 o 14 17 0 702.23 791.03 363.29 o 16 17 0 3032.92 3053.81 360.73 o 18 17 0 1.02 -114.79 328.02 o 0 18 0 1200.36 1533.65 457.56 o 2 18 0 219.50 85.79 425.50 o 4 18 0 11013.34 10790.30 651.45 o 6 18 0 247.05 450.83 323.53 o 8 18 0 1609.93 2086.45 481.93 o 10 18 0 13.13 -240.81 268.06 o 12 18 0 2516.73 3381.54 554.08 o 14 18 0 488.72 530.83 260.33 o 16 18 0 630.29 692.06 277.21 o 18 18 0 532.15 2.57 406.58 o 2 19 0 15351.12 15907.91 769.06 o 4 19 0 818.73 1204.81 386.38 o 6 19 0 25327.37 26290.76 1349.60 o 8 19 0 6604.37 6963.48 745.18 o 10 19 0 4912.91 5063.65 649.95 o 12 19 0 6234.57 6241.70 701.57 o 14 19 0 2303.23 2571.45 366.24 o 16 19 0 4207.58 4985.61 617.24 o 0 20 0 86.57 915.12 456.92 o 2 20 0 869.32 796.07 437.04 o 4 20 0 864.38 682.55 693.24 o 6 20 0 8.58 456.92 364.90 o 8 20 0 3052.94 3599.90 606.98 o 10 20 0 676.34 258.12 365.54 o 12 20 0 822.17 1165.23 450.51 o 14 20 0 424.42 231.48 277.03 o 16 20 0 1.05 210.02 415.56 o 2 21 0 1294.10 502.33 449.55 o 4 21 0 10.27 431.91 342.45 o 6 21 0 2862.21 3586.75 644.82 o 8 21 0 2409.56 1933.50 525.22 o 10 21 0 179.43 1049.48 453.39 o 12 21 0 521.86 92.68 246.23 o 14 21 0 510.19 772.18 325.15 o 0 22 0 9286.41 7454.71 963.22 o 2 22 0 145.25 217.94 271.84 o 4 22 0 4049.52 4187.64 718.89 o 6 22 0 2741.96 3128.23 665.98 o 8 22 0 2482.75 2503.61 581.65 o 10 22 0 1683.78 1887.97 546.70 o 12 22 0 1364.43 1439.86 481.77 o 2 23 0 46.95 545.23 414.92 o 4 23 0 255.87 -24.05 376.12 o 6 23 0 3.49 -40.72 396.32 o 8 23 0 368.25 117.36 388.30 o 10 23 0 27.26 -117.22 299.85 o 12 23 0 3.21 -262.81 262.81 o 0 24 0 14591.71 15138.29 2301.44 o 2 24 0 483.60 489.31 502.45 o 4 24 0 7501.27 6089.72 897.49 o 6 24 0 1326.53 904.62 346.53 o 8 24 0 2777.81 3316.59 506.71 o 10 24 0 1472.50 1282.79 391.45 o 2 25 0 2647.84 3408.97 543.11 o 4 25 0 131.51 -90.14 312.16 o 6 25 0 1583.78 1565.53 409.93 o 8 25 0 1252.69 790.07 509.83 o 0 26 0 30.14 205.20 360.30 o 2 26 0 0.13 -124.08 324.88 o 4 26 0 14.30 316.48 514.32 o 1 1 1 75772.71 76132.44 655.45 o 2 1 1 278716.59 279946.25 2105.12 o 3 1 1 8151.44 7476.72 78.13 o 4 1 1 15214.20 15545.45 142.55 o 5 1 1 98308.19 100420.45 678.79 o 6 1 1 145749.25 141634.89 860.56 o 7 1 1 2267.94 2381.33 57.01 o 8 1 1 62436.87 61108.84 451.08 o 9 1 1 37632.75 36715.54 307.37 o 10 1 1 33722.54 32894.64 291.73 o 11 1 1 7217.07 7572.03 108.03 o 12 1 1 27932.21 28496.24 248.96 o 13 1 1 15450.02 15497.84 188.61 o 14 1 1 7018.39 7595.79 166.29 o 15 1 1 156.85 132.96 87.03 o 16 1 1 16338.20 17204.09 361.73 o 17 1 1 2004.13 1664.49 154.48 o 18 1 1 1004.98 856.78 161.33 o 19 1 1 4264.36 4153.48 280.33 o 20 1 1 9390.33 10146.08 394.03 o 21 1 1 1664.64 1391.44 207.78 o 22 1 1 14.25 -124.27 156.97 o 23 1 1 797.03 827.37 199.64 o 24 1 1 2568.77 2574.82 323.70 o 25 1 1 322.93 322.38 210.59 o 0 2 1 235714.97 235727.19 2743.05 o 2 2 1 2963.44 3416.05 46.67 o 3 2 1 29433.47 28075.63 262.46 o 4 2 1 3064.22 3434.68 71.53 o 5 2 1 613.07 590.64 43.14 o 6 2 1 16861.75 16646.09 162.97 o 7 2 1 32851.45 33504.43 275.12 o 8 2 1 26303.42 24790.13 225.91 o 9 2 1 4389.41 4456.91 91.22 o 10 2 1 4186.51 4197.64 88.85 o 11 2 1 16064.85 16327.48 185.60 o 12 2 1 12163.52 12906.45 168.21 o 13 2 1 703.69 599.13 56.98 o 14 2 1 10283.48 10398.10 189.68 o 15 2 1 5518.77 5573.64 288.45 o 16 2 1 2689.57 2760.10 187.88 o 17 2 1 293.04 328.49 116.05 o 18 2 1 6459.43 6407.05 298.99 o 19 2 1 1179.35 1173.24 306.06 o 20 2 1 941.29 1266.28 194.90 o 21 2 1 390.01 569.61 181.12 o 22 2 1 2843.54 2988.21 273.13 o 23 2 1 247.04 247.71 188.14 o 24 2 1 243.29 528.94 210.32 o 25 2 1 172.79 103.38 201.94 o 1 3 1 61.55 66.26 17.59 o 2 3 1 7531.19 6484.99 80.51 o 3 3 1 67958.66 64298.36 492.42 o 4 3 1 5246.42 5803.37 121.20 o 5 3 1 27958.96 28349.55 267.25 o 6 3 1 45160.79 44322.23 370.28 o 7 3 1 552.15 449.11 37.29 o 8 3 1 7536.94 7536.58 116.33 o 9 3 1 3841.38 3842.08 95.26 o 10 3 1 3262.36 3259.27 71.32 o 11 3 1 4008.76 4229.57 91.14 o 12 3 1 112.28 37.43 41.65 o 13 3 1 498.41 530.39 69.35 o 14 3 1 2039.75 2168.67 123.48 o 15 3 1 17.21 105.71 76.12 o 16 3 1 398.72 444.15 103.84 o 17 3 1 315.07 371.25 113.29 o 18 3 1 13.03 -5.51 137.92 o 19 3 1 704.87 838.78 162.10 o 20 3 1 614.79 407.99 177.11 o 21 3 1 7.13 112.94 157.06 o 22 3 1 108.93 106.07 166.77 o 23 3 1 305.22 155.58 183.00 o 24 3 1 253.52 514.59 212.61 o 25 3 1 23.73 -154.95 201.58 o 0 4 1 138130.16 137697.75 1410.54 o 1 4 1 17298.67 16670.75 175.09 o 2 4 1 34938.32 34234.23 292.80 o 3 4 1 15896.63 14900.21 150.22 o 4 4 1 303747.28 302027.53 1969.42 o 5 4 1 41663.68 41890.93 331.90 o 6 4 1 4245.76 4318.94 94.94 o 7 4 1 21038.05 20015.44 235.64 o 8 4 1 58117.07 55900.10 483.58 o 9 4 1 3393.70 3341.73 123.24 o 10 4 1 33655.91 33241.24 305.28 o 11 4 1 10354.97 10440.77 151.33 o 12 4 1 5106.49 5107.27 163.78 o 13 4 1 997.33 959.70 85.90 o 14 4 1 17364.23 18315.15 393.94 o 15 4 1 1595.92 1524.68 104.76 o 16 4 1 1255.65 1022.77 123.72 o 17 4 1 2877.12 2839.89 252.39 o 18 4 1 12972.28 14527.94 404.00 o 19 4 1 113.19 302.09 138.90 o 20 4 1 567.00 275.06 154.24 o 21 4 1 1407.57 1375.03 346.62 o 22 4 1 2481.52 3460.43 285.35 o 23 4 1 320.18 450.67 192.16 o 24 4 1 74.61 -90.19 185.75 o 25 4 1 109.21 40.00 213.76 o 1 5 1 2166.46 2360.91 57.67 o 2 5 1 21850.34 20965.60 198.19 o 3 5 1 1250.70 1280.32 45.42 o 4 5 1 263.79 345.10 30.77 o 5 5 1 135.12 162.89 26.18 o 6 5 1 22089.87 21570.33 207.25 o 7 5 1 2672.14 2803.90 90.34 o 8 5 1 1299.20 1376.42 95.46 o 9 5 1 521.32 536.78 57.84 o 10 5 1 621.70 442.22 56.66 o 11 5 1 204.64 124.40 47.88 o 12 5 1 1814.84 1701.10 92.42 o 13 5 1 495.57 378.47 111.18 o 14 5 1 1145.12 1191.19 120.23 o 15 5 1 875.50 927.72 120.91 o 16 5 1 6111.15 6016.85 201.57 o 17 5 1 2211.69 2128.50 157.91 o 18 5 1 845.75 696.49 142.87 o 19 5 1 19.53 -92.49 123.49 o 20 5 1 504.37 599.11 160.91 o 21 5 1 32.79 93.52 166.06 o 22 5 1 54.83 -133.59 164.73 o 23 5 1 243.37 48.91 296.39 o 24 5 1 830.54 800.02 214.67 o 0 6 1 52158.80 51617.72 669.60 o 1 6 1 11869.95 12361.29 133.56 o 2 6 1 634.66 679.19 42.00 o 3 6 1 33933.48 33892.41 294.67 o 4 6 1 10682.82 10045.84 124.19 o 5 6 1 8.89 19.04 24.19 o 6 6 1 1633.22 1854.96 63.44 o 7 6 1 9871.49 9360.22 168.73 o 8 6 1 42903.98 43675.64 424.18 o 9 6 1 1272.71 1236.73 81.23 o 10 6 1 1542.33 1568.74 85.00 o 11 6 1 26502.42 26047.04 437.00 o 12 6 1 342.16 100.88 86.14 o 13 6 1 745.42 748.38 101.80 o 14 6 1 5308.96 5098.50 385.71 o 15 6 1 10877.13 11069.80 301.39 o 16 6 1 4160.58 4673.87 336.44 o 17 6 1 859.83 822.63 117.58 o 18 6 1 5683.87 6075.24 323.78 o 19 6 1 800.44 571.96 185.22 o 20 6 1 713.52 401.75 153.71 o 21 6 1 160.77 191.09 149.80 o 22 6 1 2891.35 2700.26 364.65 o 23 6 1 261.72 222.75 221.64 o 24 6 1 12.30 96.79 192.41 o 1 7 1 31004.81 29410.07 249.43 o 2 7 1 90707.48 88927.19 613.08 o 3 7 1 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