#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/04/2230482.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2230482_Fobs loop_ _publ_author_name 'Li, Shi-Jie' 'Miao, Dong-Liang' 'Song, Wen-Dong' 'Tong, Shao-Wei' _publ_section_title ; 3-Carboxy-5-(pyridinium-4-yl)benzoate: a redetermination ; _journal_coeditor_code SJ5133 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1353 _journal_volume 67 _journal_year 2011 _space_group_IT_number 43 _symmetry_space_group_name_Hall 'F 2 -2d' _symmetry_space_group_name_H-M 'F d d 2' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 15.5702 _cell_length_b 37.3769 _cell_length_c 7.2016 _exptl_crystal_F_000 2016.00 _reflns_d_resolution_high 0.8351 _[local]_cod_data_source_file sj5133Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 100920a in Fdd2' _shelx_refln_list_code 4 _shelx_f_calc_maximum 617.88 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z' 'x+1/4, -y+1/4, z+1/4' '-x+1/4, y+1/4, z+1/4' 'x, y+1/2, z+1/2' '-x, -y+1/2, z+1/2' 'x+1/4, -y+3/4, z+3/4' '-x+1/4, y+3/4, z+3/4' 'x+1/2, y, z+1/2' '-x+1/2, -y, z+1/2' 'x+3/4, -y+1/4, z+3/4' '-x+3/4, y+1/4, z+3/4' 'x+1/2, y+1/2, z' '-x+1/2, -y+1/2, z' 'x+3/4, -y+3/4, z+1/4' '-x+3/4, y+3/4, z+1/4' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 34902.41 37091.86 827.66 o 8 0 0 6427.89 9020.64 186.64 o 12 0 0 3752.84 3313.86 134.62 o 2 2 0 20527.90 26758.36 507.33 o 4 2 0 28703.23 22433.89 348.56 o 6 2 0 9867.97 11908.30 203.77 o 8 2 0 48905.57 53608.60 816.95 o 10 2 0 5961.86 6013.63 138.93 o 12 2 0 2280.81 2532.39 86.45 o 14 2 0 130.48 68.37 55.04 o 16 2 0 1242.31 1386.94 131.48 o 18 2 0 62.11 54.31 70.49 o 2 4 0 55741.64 64752.82 352.31 o 4 4 0 13257.26 12780.40 314.34 o 6 4 0 61178.68 56567.37 695.03 o 8 4 0 11687.38 14227.80 368.40 o 10 4 0 116.63 92.80 26.73 o 12 4 0 1.01 -0.17 22.64 o 14 4 0 13.77 -11.94 49.17 o 16 4 0 2224.99 2029.97 153.64 o 18 4 0 128.24 254.11 85.25 o 2 6 0 79510.52 73491.95 939.50 o 4 6 0 5092.66 4852.14 75.97 o 6 6 0 532.65 770.07 45.70 o 8 6 0 37.33 70.28 24.00 o 10 6 0 401.99 288.14 35.41 o 12 6 0 401.34 380.89 47.48 o 14 6 0 0.74 -16.90 37.21 o 16 6 0 0.83 226.11 304.48 o 18 6 0 200.19 197.16 86.28 o 0 8 0 6947.08 6839.58 86.51 o 2 8 0 1840.06 1457.93 53.07 o 4 8 0 5274.49 5698.34 85.82 o 6 8 0 10.34 49.86 23.52 o 8 8 0 1594.78 1558.32 69.66 o 10 8 0 3496.75 3831.17 133.26 o 12 8 0 33.84 11.16 37.09 o 14 8 0 55.68 49.35 40.29 o 16 8 0 110.80 126.04 58.28 o 18 8 0 27.35 40.01 130.30 o 2 10 0 15433.40 13744.29 111.66 o 4 10 0 20284.79 22601.82 511.68 o 6 10 0 8.92 26.14 24.08 o 8 10 0 25.10 44.45 28.16 o 10 10 0 18.88 10.14 29.71 o 12 10 0 3085.79 3472.78 126.83 o 14 10 0 193.27 245.81 50.28 o 16 10 0 1.90 76.74 69.87 o 18 10 0 2.14 -12.10 75.26 o 0 12 0 8107.73 5965.19 96.90 o 2 12 0 11.04 93.68 20.63 o 4 12 0 7037.73 8464.24 108.65 o 6 12 0 2975.50 2456.00 70.68 o 8 12 0 1734.99 1424.82 99.70 o 10 12 0 155.14 99.53 41.41 o 12 12 0 6152.01 6453.74 173.14 o 14 12 0 5463.74 5393.36 194.58 o 16 12 0 51.31 68.60 87.74 o 2 14 0 13999.38 10183.66 107.65 o 4 14 0 1544.58 1540.94 48.81 o 6 14 0 70.76 110.42 25.76 o 8 14 0 384.32 381.88 39.73 o 10 14 0 8355.88 8915.50 182.95 o 12 14 0 8649.89 8984.73 280.82 o 14 14 0 456.28 335.69 58.61 o 16 14 0 40.77 70.72 102.15 o 0 16 0 2168.29 2037.75 66.59 o 2 16 0 13038.75 17774.65 227.78 o 4 16 0 3125.62 3609.95 72.59 o 6 16 0 63.89 16.78 22.13 o 8 16 0 1657.29 1493.10 66.00 o 10 16 0 4000.48 4060.26 129.02 o 12 16 0 21709.04 22500.21 323.81 o 14 16 0 279.29 232.26 58.67 o 16 16 0 297.18 357.31 73.34 o 2 18 0 32.26 171.13 19.79 o 4 18 0 42099.52 41381.88 368.17 o 6 18 0 943.31 1311.95 88.46 o 8 18 0 899.44 866.01 54.92 o 10 18 0 5654.65 5501.37 219.82 o 12 18 0 1225.08 1307.15 140.13 o 14 18 0 1007.50 992.05 102.55 o 16 18 0 526.47 578.15 85.27 o 0 20 0 352.35 212.28 34.29 o 2 20 0 2623.44 2381.07 53.19 o 4 20 0 1183.47 1753.80 57.17 o 6 20 0 2676.27 2262.82 68.42 o 8 20 0 35.54 24.91 27.96 o 10 20 0 1265.31 1217.01 95.26 o 12 20 0 5033.85 5579.87 203.26 o 14 20 0 0.02 -3.85 81.19 o 16 20 0 24.15 6.93 48.29 o 2 22 0 2008.86 2650.47 61.95 o 4 22 0 7149.72 7445.99 116.64 o 6 22 0 1777.17 1714.25 62.43 o 8 22 0 88.37 47.19 34.29 o 10 22 0 3458.72 3757.28 343.57 o 12 22 0 70.44 98.21 47.68 o 14 22 0 602.11 720.41 91.66 o 16 22 0 13.20 6.82 44.95 o 0 24 0 203.70 195.98 32.78 o 2 24 0 5326.64 4729.03 85.12 o 4 24 0 312.97 463.43 57.25 o 6 24 0 0.33 78.02 32.41 o 8 24 0 716.37 749.49 77.38 o 10 24 0 3381.74 3156.30 125.10 o 12 24 0 22.20 38.88 48.14 o 14 24 0 402.60 480.51 85.56 o 2 26 0 6630.43 5636.27 105.61 o 4 26 0 508.95 540.40 33.95 o 6 26 0 122.36 129.33 36.69 o 8 26 0 31.44 72.96 36.03 o 10 26 0 19.09 -24.14 33.07 o 12 26 0 7.10 -12.64 38.86 o 14 26 0 409.95 504.08 84.82 o 0 28 0 15073.77 16322.07 478.88 o 2 28 0 1946.31 2037.61 61.78 o 4 28 0 961.80 913.17 60.98 o 6 28 0 0.92 -5.91 36.61 o 8 28 0 1932.89 1861.58 96.88 o 10 28 0 1665.15 1441.58 94.71 o 12 28 0 51.28 20.79 43.99 o 14 28 0 419.17 410.20 81.07 o 2 30 0 14219.48 14912.31 187.60 o 4 30 0 353.68 248.75 41.45 o 6 30 0 285.56 252.70 119.45 o 8 30 0 4714.31 4365.93 149.98 o 10 30 0 537.89 724.49 74.78 o 12 30 0 89.70 139.93 55.05 o 0 32 0 611.56 726.58 84.54 o 2 32 0 64.55 271.79 59.94 o 4 32 0 705.78 695.55 56.87 o 6 32 0 645.88 460.15 51.34 o 8 32 0 220.25 207.33 48.88 o 10 32 0 931.03 775.67 78.81 o 12 32 0 188.99 379.65 74.54 o 2 34 0 128.03 99.03 46.42 o 4 34 0 734.04 792.09 63.03 o 6 34 0 12.08 -39.55 31.68 o 8 34 0 5.29 26.52 46.42 o 10 34 0 1181.04 929.44 83.80 o 12 34 0 180.98 88.97 54.81 o 0 36 0 1460.95 1767.93 201.68 o 2 36 0 34.08 -6.01 52.57 o 4 36 0 164.50 177.02 49.53 o 6 36 0 1399.29 1633.90 98.29 o 8 36 0 83.59 325.54 218.10 o 10 36 0 21.42 22.37 41.68 o 2 38 0 44.25 52.06 69.38 o 4 38 0 119.73 71.28 46.04 o 6 38 0 13.32 19.32 50.53 o 8 38 0 115.11 89.16 46.88 o 0 40 0 214.10 216.08 124.41 o 2 40 0 348.36 455.63 83.89 o 4 40 0 117.16 28.11 89.71 o 6 40 0 887.53 846.93 157.15 o 8 40 0 2.86 -19.75 49.22 o 2 42 0 243.61 290.44 84.81 o 4 42 0 121.20 221.32 124.41 o 6 42 0 1059.61 1223.15 201.68 o 0 44 0 29.24 90.36 119.17 o 2 44 0 53.48 66.72 85.18 o 1 1 1 1997.03 1635.68 32.58 o 3 1 1 621.31 413.06 17.62 o 5 1 1 574.81 564.01 17.81 o 7 1 1 6105.24 7016.54 93.57 o 9 1 1 4137.56 5193.39 70.84 o 11 1 1 654.07 732.33 44.50 o 13 1 1 2204.01 2090.99 79.30 o 15 1 1 891.42 746.34 71.36 o 17 1 1 178.38 132.39 56.03 o 1 3 1 13628.06 16055.88 353.67 o 3 3 1 14904.08 16057.82 212.47 o 5 3 1 10465.97 8427.42 132.73 o 7 3 1 12162.86 11849.96 118.38 o 9 3 1 880.72 857.18 37.40 o 11 3 1 2155.63 2188.88 60.60 o 13 3 1 38.07 51.73 30.77 o 15 3 1 2359.86 2271.04 95.28 o 17 3 1 736.47 600.31 68.36 o 1 5 1 2479.02 1876.66 34.06 o 3 5 1 10971.64 12115.08 154.87 o 5 5 1 1362.44 1403.88 36.51 o 7 5 1 220.16 336.30 20.12 o 9 5 1 4126.21 4738.32 79.79 o 11 5 1 205.70 203.16 25.12 o 13 5 1 81.48 129.99 29.99 o 15 5 1 111.41 106.35 39.40 o 17 5 1 523.30 517.56 66.11 o 1 7 1 41349.37 44465.44 598.05 o 3 7 1 6732.28 6087.77 126.11 o 5 7 1 4496.91 4456.58 61.65 o 7 7 1 1275.01 1250.81 32.97 o 9 7 1 1205.57 1328.65 38.47 o 11 7 1 1733.34 1716.82 54.92 o 13 7 1 1172.12 1150.88 115.17 o 15 7 1 161.11 122.04 37.76 o 17 7 1 257.57 248.74 57.60 o 1 9 1 4553.59 5926.29 140.53 o 3 9 1 7024.86 7367.77 123.73 o 5 9 1 5071.12 4940.49 80.24 o 7 9 1 2911.86 2601.39 47.94 o 9 9 1 1511.92 1316.86 137.77 o 11 9 1 1041.33 1147.50 47.49 o 13 9 1 1470.42 1370.58 60.01 o 15 9 1 555.65 664.73 56.71 o 17 9 1 181.90 227.52 72.15 o 1 11 1 2640.21 2212.60 35.21 o 3 11 1 7940.23 7494.43 74.28 o 5 11 1 27046.05 26006.15 523.91 o 7 11 1 633.31 374.90 26.63 o 9 11 1 5184.21 5036.08 97.03 o 11 11 1 1109.56 1116.16 52.19 o 13 11 1 481.73 473.78 41.99 o 15 11 1 441.12 441.19 60.69 o 17 11 1 161.87 144.44 60.68 o 1 13 1 12277.22 10134.80 125.52 o 3 13 1 15818.30 19070.73 172.57 o 5 13 1 5169.68 5862.79 69.85 o 7 13 1 1332.14 1401.90 44.28 o 9 13 1 219.52 180.63 25.23 o 11 13 1 10819.38 10922.79 150.29 o 13 13 1 4545.21 4803.79 119.15 o 15 13 1 1326.71 1484.54 89.02 o 17 13 1 152.62 121.91 62.94 o 1 15 1 11587.66 11140.18 75.84 o 3 15 1 58239.10 63356.52 419.03 o 5 15 1 33602.98 34024.97 382.12 o 7 15 1 8387.88 7500.79 143.66 o 9 15 1 4618.41 4474.56 85.25 o 11 15 1 17687.63 17413.94 333.99 o 13 15 1 576.21 621.07 52.54 o 15 15 1 368.16 457.10 56.38 o 17 15 1 503.53 663.83 76.84 o 1 17 1 2429.07 2889.22 36.56 o 3 17 1 2578.31 2842.75 40.82 o 5 17 1 6291.49 6778.33 84.78 o 7 17 1 1597.93 1435.81 51.52 o 9 17 1 2074.86 2267.39 69.64 o 11 17 1 14272.98 15003.55 213.28 o 13 17 1 10750.39 11544.54 212.93 o 15 17 1 615.41 799.11 88.92 o 17 17 1 348.05 567.37 77.93 o 1 19 1 1042.95 691.15 21.57 o 3 19 1 7224.85 6697.11 73.76 o 5 19 1 1783.80 1831.73 41.40 o 7 19 1 73.09 54.63 21.92 o 9 19 1 506.75 451.41 38.41 o 11 19 1 91.75 95.65 28.92 o 13 19 1 7445.48 8305.35 244.78 o 15 19 1 334.13 330.77 48.73 o 1 21 1 2429.61 1723.64 35.45 o 3 21 1 2469.63 2284.28 50.44 o 5 21 1 5127.43 5016.69 75.26 o 7 21 1 1885.46 1921.96 62.30 o 9 21 1 71.97 70.66 25.94 o 11 21 1 157.06 185.52 38.95 o 13 21 1 1887.19 1944.65 92.74 o 15 21 1 163.07 96.96 41.74 o 1 23 1 16.52 13.14 12.69 o 3 23 1 1806.35 1566.50 81.33 o 5 23 1 47.64 31.22 17.45 o 7 23 1 153.20 162.32 27.95 o 9 23 1 291.30 276.05 33.68 o 11 23 1 127.55 58.46 29.96 o 13 23 1 154.12 184.40 115.61 o 15 23 1 290.39 251.27 51.20 o 1 25 1 905.36 728.76 25.53 o 3 25 1 1271.47 1210.88 36.53 o 5 25 1 306.91 302.41 25.50 o 7 25 1 888.13 834.20 47.12 o 9 25 1 1437.08 1492.35 69.05 o 11 25 1 184.91 153.22 38.06 o 13 25 1 154.90 204.28 44.32 o 15 25 1 82.69 84.61 44.91 o 1 27 1 2732.42 2407.89 91.19 o 3 27 1 1124.96 1151.16 37.91 o 5 27 1 53.44 135.81 51.03 o 7 27 1 13.73 11.20 25.90 o 9 27 1 1309.20 1247.87 71.00 o 11 27 1 78.75 80.66 31.13 o 13 27 1 37.32 61.54 36.87 o 1 29 1 9631.18 9750.96 171.11 o 3 29 1 88.82 64.91 19.92 o 5 29 1 259.36 212.62 25.31 o 7 29 1 1368.27 1253.57 57.92 o 9 29 1 1280.21 1028.36 62.36 o 11 29 1 258.09 343.55 45.24 o 13 29 1 49.20 42.39 36.88 o 1 31 1 19073.09 19426.56 246.25 o 3 31 1 1496.33 1352.44 49.71 o 5 31 1 1675.41 1633.47 68.64 o 7 31 1 5416.85 5599.21 285.43 o 9 31 1 494.88 464.43 48.01 o 11 31 1 203.49 143.19 37.30 o 13 31 1 110.37 99.59 45.53 o 1 33 1 21112.52 24218.74 281.76 o 3 33 1 903.40 963.29 52.27 o 5 33 1 51.25 28.38 26.76 o 7 33 1 1969.35 1542.33 67.64 o 9 33 1 224.21 165.44 40.86 o 11 33 1 464.78 503.84 53.54 o 1 35 1 8967.90 10567.36 164.19 o 3 35 1 567.35 626.41 49.89 o 5 35 1 29.50 -17.38 27.32 o 7 35 1 59.17 136.06 39.87 o 9 35 1 784.65 702.19 57.37 o 11 35 1 203.05 226.39 47.60 o 1 37 1 171.01 366.07 53.99 o 3 37 1 156.26 117.16 39.02 o 5 37 1 560.33 489.42 56.26 o 7 37 1 1175.24 1372.63 88.94 o 9 37 1 665.91 730.43 74.08 o 1 39 1 253.83 334.65 62.54 o 3 39 1 410.67 467.27 52.48 o 5 39 1 32.50 -0.46 34.37 o 7 39 1 442.40 369.43 58.62 o 1 41 1 705.08 845.04 85.25 o 3 41 1 929.54 1224.61 110.47 o 5 41 1 490.07 651.65 85.25 o 7 41 1 130.49 96.37 50.07 o 1 43 1 32.83 51.72 47.55 o 3 43 1 191.49 257.00 78.28 o 2 0 2 381780.19 374763.63 8542.03 o 6 0 2 28578.57 33021.38 279.42 o 10 0 2 1434.00 1275.75 80.00 o 14 0 2 3216.42 2967.31 139.44 o 18 0 2 429.08 408.10 90.54 o 0 2 2 326374.88 357453.66 20836.09 o 2 2 2 104740.01 111425.84 2604.17 o 4 2 2 6141.24 6185.93 83.72 o 6 2 2 32851.48 32160.12 647.20 o 8 2 2 12762.03 13480.44 119.76 o 10 2 2 6088.26 6264.86 298.26 o 12 2 2 492.41 488.05 41.62 o 14 2 2 727.55 617.40 51.68 o 16 2 2 77.72 66.09 42.51 o 18 2 2 257.25 411.34 67.41 o 2 4 2 75984.05 77642.73 522.42 o 4 4 2 10226.93 7312.92 211.25 o 6 4 2 1457.48 1455.05 37.88 o 8 4 2 8726.17 8417.33 103.72 o 10 4 2 549.88 677.54 35.61 o 12 4 2 315.06 296.24 38.32 o 14 4 2 185.79 151.26 36.54 o 16 4 2 162.70 151.29 44.98 o 18 4 2 137.67 186.49 62.28 o 0 6 2 26700.64 24551.07 799.07 o 2 6 2 12587.64 13143.38 134.92 o 4 6 2 8909.25 8476.98 132.23 o 6 6 2 851.10 870.42 34.77 o 8 6 2 1692.14 1833.16 50.57 o 10 6 2 3987.80 4016.46 77.28 o 12 6 2 124.50 107.56 29.87 o 14 6 2 135.23 124.88 34.16 o 16 6 2 712.11 653.56 72.98 o 2 8 2 17893.00 16945.37 193.27 o 4 8 2 1688.88 1266.81 36.46 o 6 8 2 736.65 816.47 37.77 o 8 8 2 1507.81 1567.98 48.52 o 10 8 2 562.00 504.88 35.33 o 12 8 2 941.36 964.77 52.26 o 14 8 2 93.54 67.13 33.63 o 16 8 2 79.12 125.66 47.13 o 0 10 2 9239.59 7966.20 107.05 o 2 10 2 3420.43 3778.62 82.88 o 4 10 2 5122.45 5310.08 103.86 o 6 10 2 846.49 887.42 35.19 o 8 10 2 893.30 788.01 37.47 o 10 10 2 1469.57 1451.49 53.54 o 12 10 2 516.50 465.75 38.29 o 14 10 2 2858.10 2733.74 227.54 o 16 10 2 465.77 408.38 59.28 o 2 12 2 1121.33 1497.42 39.63 o 4 12 2 4500.15 4725.48 68.76 o 6 12 2 856.31 813.37 34.38 o 8 12 2 1619.72 1490.26 48.34 o 10 12 2 3339.80 3492.37 88.72 o 12 12 2 5268.44 5801.07 122.07 o 14 12 2 1655.21 1663.02 97.80 o 16 12 2 173.25 157.35 48.77 o 0 14 2 7362.06 6346.15 108.29 o 2 14 2 13053.94 12889.21 234.47 o 4 14 2 5242.48 5277.76 80.83 o 6 14 2 4350.32 4274.88 72.17 o 8 14 2 1456.67 1412.99 56.31 o 10 14 2 253.02 253.30 34.89 o 12 14 2 10391.43 11001.58 237.68 o 14 14 2 614.72 532.21 63.23 o 16 14 2 954.87 870.64 80.53 o 2 16 2 72.38 52.40 19.15 o 4 16 2 2364.23 2651.65 68.85 o 6 16 2 2176.99 2332.59 67.93 o 8 16 2 666.44 682.96 42.16 o 10 16 2 13854.45 14042.01 181.43 o 12 16 2 1702.62 1682.96 70.00 o 14 16 2 2559.94 2953.65 125.25 o 16 16 2 5.61 35.08 49.22 o 0 18 2 8093.73 8939.96 123.30 o 2 18 2 4541.97 4931.62 84.36 o 4 18 2 475.58 508.52 31.24 o 6 18 2 5336.76 5206.08 101.50 o 8 18 2 391.64 388.14 36.82 o 10 18 2 6906.61 7047.04 136.58 o 12 18 2 1289.79 1357.40 73.60 o 14 18 2 1450.36 1748.35 152.97 o 16 18 2 248.80 313.14 63.81 o 2 20 2 7599.48 8864.23 169.62 o 4 20 2 3248.83 3272.50 67.02 o 6 20 2 5106.11 5429.76 106.00 o 8 20 2 52.70 23.85 26.86 o 10 20 2 4676.04 4849.64 198.73 o 12 20 2 682.82 699.72 54.42 o 14 20 2 533.35 569.56 59.21 o 16 20 2 62.82 52.41 48.34 o 0 22 2 8175.22 6638.43 224.71 o 2 22 2 2784.14 2824.39 59.48 o 4 22 2 215.86 275.17 27.57 o 6 22 2 122.48 171.21 28.45 o 8 22 2 1189.00 1126.98 55.75 o 10 22 2 957.48 865.23 52.31 o 12 22 2 1612.14 1664.59 75.49 o 14 22 2 164.70 151.07 39.12 o 2 24 2 244.23 319.05 25.79 o 4 24 2 2671.52 2718.10 66.35 o 6 24 2 2.49 -19.14 24.26 o 8 24 2 1322.94 1114.02 57.93 o 10 24 2 152.80 145.90 31.97 o 12 24 2 806.52 848.20 56.99 o 14 24 2 209.70 173.00 41.22 o 0 26 2 10054.94 9086.04 180.89 o 2 26 2 1647.27 1714.02 54.75 o 4 26 2 716.65 707.56 39.35 o 6 26 2 2240.50 2120.80 73.74 o 8 26 2 484.49 487.37 45.96 o 10 26 2 79.38 23.86 33.23 o 12 26 2 154.91 99.24 36.64 o 14 26 2 35.72 34.49 32.92 o 2 28 2 3521.84 3718.57 80.65 o 4 28 2 2596.52 2517.19 79.94 o 6 28 2 1422.75 1286.06 60.89 o 8 28 2 1250.73 898.05 53.83 o 10 28 2 398.55 309.81 45.90 o 12 28 2 125.93 143.93 42.63 o 0 30 2 9931.90 10786.73 205.25 o 2 30 2 132.77 159.68 29.85 o 4 30 2 1982.08 1771.28 64.71 o 6 30 2 1619.37 1392.10 131.19 o 8 30 2 681.37 639.57 53.76 o 10 30 2 480.57 407.54 50.59 o 12 30 2 435.18 486.45 57.57 o 2 32 2 2218.39 2284.78 76.25 o 4 32 2 940.68 938.17 52.58 o 6 32 2 48.69 62.63 34.30 o 8 32 2 1705.16 1415.28 84.53 o 10 32 2 552.78 622.70 57.82 o 12 32 2 958.00 1212.89 78.27 o 0 34 2 993.70 1209.81 83.43 o 2 34 2 275.97 303.01 37.52 o 4 34 2 230.46 192.86 35.05 o 6 34 2 508.44 482.08 70.80 o 8 34 2 3.10 -7.10 37.67 o 10 34 2 153.87 180.74 51.14 o 2 36 2 337.37 328.31 38.46 o 4 36 2 65.75 99.68 37.23 o 6 36 2 133.57 102.45 42.46 o 8 36 2 23.65 14.24 34.00 o 10 36 2 349.50 271.64 53.80 o 0 38 2 103.73 78.84 42.91 o 2 38 2 357.98 276.24 48.49 o 4 38 2 241.68 187.51 47.48 o 6 38 2 3.38 11.24 38.64 o 8 38 2 541.97 587.47 69.89 o 2 40 2 31.14 64.39 45.17 o 4 40 2 369.76 372.36 56.93 o 6 40 2 377.34 373.89 63.13 o 0 42 2 0.26 -13.07 72.36 o 2 42 2 113.01 136.33 51.27 o 4 42 2 149.40 137.52 45.39 o 1 1 3 2730.75 2153.34 74.34 o 3 1 3 293.80 378.98 29.55 o 5 1 3 3735.25 4095.93 77.63 o 7 1 3 1801.67 2174.73 50.96 o 9 1 3 1968.66 1793.91 59.89 o 11 1 3 571.96 536.35 43.37 o 13 1 3 1339.77 1177.86 66.24 o 15 1 3 786.48 817.18 63.42 o 17 1 3 164.58 113.64 58.13 o 1 3 3 5584.09 5812.88 113.67 o 3 3 3 1811.22 1818.45 52.09 o 5 3 3 100.44 78.85 20.79 o 7 3 3 3207.14 3540.40 65.02 o 9 3 3 543.33 656.44 36.13 o 11 3 3 2861.94 2974.83 82.62 o 13 3 3 166.50 146.74 35.34 o 15 3 3 103.47 62.53 39.83 o 17 3 3 378.66 337.69 71.19 o 1 5 3 3964.31 4840.54 87.75 o 3 5 3 8646.70 8448.35 93.37 o 5 5 3 5205.12 5070.20 78.10 o 7 5 3 1614.39 1734.65 53.33 o 9 5 3 141.94 120.97 24.41 o 11 5 3 38.89 15.45 23.79 o 13 5 3 1519.83 1506.19 74.93 o 15 5 3 831.22 689.65 64.59 o 17 5 3 416.94 401.76 67.51 o 1 7 3 4162.11 3954.91 73.70 o 3 7 3 520.98 409.89 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