#------------------------------------------------------------------------------ #$Date: 2011-11-08 16:24:06 +0200 (Tue, 08 Nov 2011) $ #$Revision: 29951 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/21/2232107.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2232107_Fobs loop_ _publ_author_name 'He, Long' _publ_section_title ; 2,2-Diethyl 4-methyl 5-(4-nitrophenyl)-4-phenylpyrrolidine-2,2,4-tricarboxylate ; _journal_coeditor_code XU5319 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2593 _journal_volume 67 _journal_year 2011 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 9.7948 _cell_length_b 10.9356 _cell_length_c 22.3240 _exptl_crystal_F_000 992.00 _reflns_d_resolution_high 0.8092 _[local]_cod_data_source_file xu5319Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 100118-120K in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 106.08 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 0.07 6.25 0.27 o 4 0 0 3083.41 2991.29 15.75 o 6 0 0 75.84 91.27 3.73 o 8 0 0 1205.19 1184.69 13.02 o 10 0 0 2399.84 2589.01 11.64 o 1 1 0 9.00 18.60 0.78 o 2 1 0 0.89 3.15 0.59 o 3 1 0 6.62 13.19 0.43 o 4 1 0 274.83 248.68 1.98 o 5 1 0 1058.18 945.47 7.08 o 6 1 0 121.67 131.05 2.40 o 7 1 0 2.90 4.71 1.17 o 8 1 0 4.98 5.81 0.66 o 9 1 0 917.40 984.11 6.09 o 10 1 0 254.22 261.28 2.48 o 11 1 0 1.86 2.36 0.73 o 12 1 0 118.34 134.45 3.26 o 3 2 0 853.24 799.77 4.29 o 4 2 0 1345.90 1385.69 11.72 o 5 2 0 313.26 264.43 3.14 o 6 2 0 10.42 11.69 1.16 o 7 2 0 1771.71 1706.96 9.32 o 8 2 0 1847.96 1894.43 10.80 o 9 2 0 162.60 163.71 2.08 o 10 2 0 148.55 148.82 2.04 o 11 2 0 116.21 120.42 1.62 o 1 3 0 2418.47 2481.13 7.59 o 2 3 0 9301.54 8769.20 66.69 o 3 3 0 139.56 132.79 1.03 o 4 3 0 2156.64 2308.54 8.14 o 5 3 0 18.74 24.35 0.85 o 6 3 0 14.19 19.97 1.33 o 7 3 0 95.75 100.51 2.61 o 8 3 0 1095.05 1098.47 6.43 o 9 3 0 0.05 1.51 0.63 o 10 3 0 141.43 129.04 2.03 o 11 3 0 494.00 539.46 10.04 o 0 4 0 167.13 122.34 1.49 o 1 4 0 66.66 85.34 0.87 o 2 4 0 907.20 758.35 5.12 o 3 4 0 1466.52 1503.90 9.66 o 4 4 0 99.37 115.66 1.43 o 5 4 0 11.18 9.10 0.93 o 6 4 0 2.69 2.31 0.97 o 7 4 0 839.47 886.87 4.26 o 8 4 0 290.76 267.61 2.38 o 9 4 0 667.17 641.19 5.42 o 10 4 0 18.58 28.24 1.27 o 11 4 0 31.17 25.12 1.19 o 1 5 0 179.80 222.03 2.53 o 2 5 0 719.58 706.11 3.32 o 3 5 0 1986.93 2022.13 6.86 o 4 5 0 97.60 118.00 1.72 o 5 5 0 26.07 28.13 1.19 o 6 5 0 24.72 19.12 1.22 o 7 5 0 1850.93 1809.77 13.62 o 8 5 0 722.67 677.67 7.63 o 9 5 0 11.86 10.06 0.85 o 10 5 0 38.05 47.58 1.52 o 11 5 0 1.94 4.69 0.91 o 0 6 0 318.83 314.31 4.88 o 1 6 0 395.61 427.70 4.90 o 2 6 0 251.85 287.87 2.53 o 3 6 0 0.25 1.34 0.69 o 4 6 0 1.90 3.45 0.86 o 5 6 0 1071.92 1052.91 7.47 o 6 6 0 214.03 212.16 2.25 o 7 6 0 108.31 97.42 1.67 o 8 6 0 126.23 115.30 2.17 o 9 6 0 110.74 106.08 1.87 o 10 6 0 165.40 179.08 2.74 o 1 7 0 687.87 698.96 5.19 o 2 7 0 0.11 3.01 0.79 o 3 7 0 142.97 140.01 2.31 o 4 7 0 20.36 19.00 1.24 o 5 7 0 520.77 478.10 4.39 o 6 7 0 764.91 754.90 4.93 o 7 7 0 290.23 284.98 4.37 o 8 7 0 1.75 0.12 0.75 o 9 7 0 20.61 19.31 1.04 o 10 7 0 0.04 0.35 0.63 o 0 8 0 831.17 827.83 6.84 o 1 8 0 0.64 1.33 0.78 o 2 8 0 25.84 25.88 1.36 o 3 8 0 50.62 46.72 1.30 o 4 8 0 147.50 153.02 2.21 o 5 8 0 793.56 795.78 7.97 o 6 8 0 429.25 413.22 6.70 o 7 8 0 163.40 156.61 3.29 o 8 8 0 83.08 80.99 1.56 o 9 8 0 3.67 3.78 0.80 o 1 9 0 7.09 8.21 0.58 o 2 9 0 84.97 87.29 1.35 o 3 9 0 722.47 672.80 3.84 o 4 9 0 738.60 706.59 5.37 o 5 9 0 504.20 466.84 8.72 o 6 9 0 356.33 350.45 14.81 o 7 9 0 353.45 350.27 4.56 o 8 9 0 99.01 111.18 2.27 o 9 9 0 190.44 182.11 3.95 o 0 10 0 73.19 86.83 1.86 o 1 10 0 118.89 115.14 1.95 o 2 10 0 1.63 1.30 0.79 o 3 10 0 31.14 28.04 1.34 o 4 10 0 209.19 209.43 3.75 o 5 10 0 3.21 5.18 1.35 o 6 10 0 3.15 2.64 1.31 o 7 10 0 32.90 29.32 1.80 o 8 10 0 39.72 34.00 1.15 o 1 11 0 35.51 34.29 1.18 o 2 11 0 82.14 88.37 2.00 o 3 11 0 3.71 3.47 0.91 o 4 11 0 15.76 14.99 1.17 o 5 11 0 38.60 32.16 1.55 o 6 11 0 4.04 7.72 0.95 o 7 11 0 56.91 65.95 2.51 o 0 12 0 245.07 224.00 7.81 o 1 12 0 67.34 71.40 2.07 o 2 12 0 26.27 22.23 1.45 o 3 12 0 174.06 160.66 2.43 o 4 12 0 10.01 9.60 1.01 o 5 12 0 7.78 5.38 0.71 o 1 13 0 39.65 44.62 1.72 o 2 13 0 26.74 26.27 1.39 o 3 13 0 111.20 120.37 3.57 o 1 0 1 47.98 51.01 0.46 o 2 0 1 813.02 738.03 2.75 o 3 0 1 5860.37 5570.35 23.58 o 4 0 1 245.82 234.91 1.62 o 5 0 1 1716.60 1698.70 5.80 o 6 0 1 0.03 1.88 0.75 o 7 0 1 408.34 397.71 4.62 o 8 0 1 19.12 18.11 0.75 o 9 0 1 320.32 347.02 2.92 o 10 0 1 39.04 39.85 1.26 o 11 0 1 0.00 1.74 0.71 o 12 0 1 84.45 90.31 2.77 o -12 1 1 22.28 27.03 1.72 o -11 1 1 114.12 115.21 1.80 o -10 1 1 31.69 35.62 1.31 o -9 1 1 80.32 82.25 1.65 o -8 1 1 21.90 24.29 0.85 o -7 1 1 42.54 38.48 3.10 o -6 1 1 121.39 124.29 4.55 o -5 1 1 1535.58 1625.19 18.19 o -4 1 1 772.20 735.25 3.43 o -3 1 1 3902.73 3719.08 21.23 o -2 1 1 1748.19 1570.18 20.32 o 0 1 1 1781.97 1687.09 16.38 o 2 1 1 1744.28 1557.16 11.27 o 3 1 1 3911.28 3734.48 26.86 o 4 1 1 770.78 740.09 9.17 o 5 1 1 1543.26 1616.93 12.17 o 6 1 1 120.75 127.41 3.77 o 7 1 1 43.03 43.24 4.03 o 8 1 1 21.74 23.13 0.85 o 9 1 1 79.06 79.38 1.69 o 10 1 1 31.11 34.88 1.22 o 11 1 1 114.63 118.46 1.88 o -11 2 1 48.40 45.94 1.09 o -10 2 1 683.15 726.28 4.66 o -9 2 1 471.44 463.87 3.85 o -8 2 1 129.76 125.75 1.70 o -7 2 1 214.23 218.95 4.30 o -6 2 1 593.61 567.02 4.39 o -5 2 1 470.99 429.29 4.99 o -4 2 1 576.77 575.49 6.72 o -3 2 1 64.51 77.86 2.76 o -2 2 1 11197.58 10399.20 88.46 o -1 2 1 497.76 467.29 1.76 o 1 2 1 496.78 467.42 3.16 o 2 2 1 11252.07 9952.57 80.72 o 3 2 1 63.62 75.77 0.83 o 4 2 1 583.75 583.93 6.50 o 5 2 1 475.13 417.94 3.97 o 6 2 1 596.76 577.41 6.54 o 7 2 1 213.58 223.88 3.58 o 8 2 1 130.71 124.21 1.62 o 9 2 1 471.28 457.58 3.34 o 10 2 1 684.60 736.21 4.22 o 11 2 1 48.56 45.48 1.12 o -11 3 1 32.23 36.98 1.29 o -10 3 1 456.63 472.54 4.18 o -9 3 1 422.94 442.56 3.17 o -8 3 1 446.09 413.17 2.68 o -7 3 1 188.11 185.35 3.46 o -6 3 1 1599.80 1632.16 9.90 o -5 3 1 349.79 377.40 3.78 o -4 3 1 61.26 60.79 1.00 o -3 3 1 7111.01 6947.89 41.21 o -2 3 1 815.36 804.52 3.72 o -1 3 1 4643.64 4423.99 19.03 o 0 3 1 8844.95 7960.43 36.81 o 1 3 1 4646.71 4360.85 18.82 o 2 3 1 811.37 796.97 5.42 o 3 3 1 7131.45 6852.56 64.73 o 4 3 1 61.60 59.45 1.92 o 5 3 1 349.38 373.50 3.48 o 6 3 1 1603.12 1615.64 17.10 o 7 3 1 186.56 186.48 4.55 o 8 3 1 441.52 407.70 2.36 o 9 3 1 419.03 445.83 3.25 o 10 3 1 457.67 466.50 4.09 o 11 3 1 31.57 35.48 1.24 o -11 4 1 94.90 96.44 1.92 o -10 4 1 295.04 299.97 3.18 o -9 4 1 39.93 47.94 1.48 o -8 4 1 542.88 529.38 3.41 o -7 4 1 276.30 279.29 2.48 o -6 4 1 118.97 122.10 2.44 o -5 4 1 1314.24 1301.53 5.31 o -4 4 1 691.22 714.38 5.02 o -3 4 1 534.38 504.95 3.60 o -2 4 1 981.81 1039.32 5.11 o -1 4 1 1969.63 2050.59 7.59 o 0 4 1 494.00 537.78 3.77 o 1 4 1 1962.72 2040.78 4.97 o 2 4 1 969.21 1028.14 2.81 o 3 4 1 543.93 513.78 2.84 o 4 4 1 686.76 716.29 4.00 o 5 4 1 1309.86 1262.98 9.35 o 6 4 1 116.04 120.66 2.38 o 7 4 1 270.88 267.01 2.19 o 8 4 1 543.96 534.72 3.26 o 9 4 1 39.61 47.55 1.12 o 10 4 1 292.72 302.49 3.17 o 11 4 1 94.52 93.37 2.30 o -11 5 1 2.45 3.13 0.85 o -10 5 1 24.75 28.21 1.27 o -9 5 1 27.77 26.49 1.03 o -8 5 1 864.40 841.13 4.84 o -7 5 1 4.00 4.65 0.70 o -6 5 1 253.47 253.60 3.25 o -5 5 1 487.16 498.28 4.03 o -4 5 1 901.42 924.82 7.52 o -3 5 1 362.61 378.16 2.73 o -2 5 1 1926.19 1933.36 9.38 o -1 5 1 200.50 193.90 1.78 o 0 5 1 203.83 250.32 1.74 o 1 5 1 196.66 191.18 2.13 o 2 5 1 1919.34 1934.21 13.17 o 3 5 1 364.46 378.65 3.00 o 4 5 1 909.12 945.83 5.89 o 5 5 1 486.33 500.27 4.53 o 6 5 1 247.74 249.59 2.89 o 7 5 1 4.14 4.46 0.69 o 8 5 1 868.37 836.97 8.92 o 9 5 1 27.60 27.73 1.13 o 10 5 1 24.89 27.87 1.31 o 11 5 1 2.72 4.28 0.86 o -10 6 1 31.17 32.03 1.35 o -9 6 1 133.40 133.83 2.31 o -8 6 1 61.77 57.23 1.79 o -7 6 1 652.53 663.12 6.33 o -6 6 1 348.37 329.58 3.86 o -5 6 1 16.86 19.55 1.23 o -4 6 1 632.40 644.05 4.68 o -3 6 1 1022.72 1043.51 5.62 o -2 6 1 78.37 107.16 1.70 o -1 6 1 1955.77 2056.21 10.28 o 0 6 1 684.43 754.77 4.59 o 1 6 1 1943.30 2024.44 18.76 o 2 6 1 78.27 106.53 1.61 o 3 6 1 1016.40 1030.99 4.97 o 4 6 1 633.43 645.21 5.48 o 5 6 1 17.39 19.32 1.21 o 6 6 1 350.68 332.08 2.63 o 7 6 1 650.84 647.10 5.32 o 8 6 1 60.99 55.35 1.75 o 9 6 1 133.15 129.42 2.66 o 10 6 1 30.84 30.81 1.38 o -10 7 1 19.87 18.12 1.18 o -9 7 1 8.30 8.44 0.86 o -8 7 1 38.16 32.54 1.35 o -7 7 1 408.56 413.75 4.07 o -6 7 1 193.82 185.42 2.17 o -5 7 1 113.50 111.26 1.70 o -4 7 1 528.45 506.69 4.47 o -3 7 1 548.74 587.18 4.06 o -2 7 1 595.46 585.70 5.64 o -1 7 1 460.74 481.36 3.36 o 0 7 1 371.82 433.51 4.23 o 1 7 1 462.05 480.40 3.81 o 2 7 1 595.49 581.51 4.20 o 3 7 1 550.67 581.21 5.04 o 4 7 1 536.93 513.71 4.06 o 5 7 1 110.65 108.49 1.60 o 6 7 1 193.97 185.04 3.34 o 7 7 1 411.70 410.24 6.07 o 8 7 1 38.70 32.57 1.23 o 9 7 1 8.62 8.76 0.88 o 10 7 1 21.09 19.43 1.18 o -9 8 1 90.66 92.02 2.43 o -8 8 1 39.93 35.05 1.23 o -7 8 1 62.19 67.53 1.79 o -6 8 1 42.56 40.91 1.68 o -5 8 1 257.70 256.38 2.73 o -4 8 1 67.93 63.81 2.40 o -3 8 1 384.53 381.49 3.02 o -2 8 1 13.73 12.05 1.10 o -1 8 1 303.25 321.93 3.09 o 0 8 1 6.31 11.68 0.99 o 1 8 1 302.13 313.87 3.08 o 2 8 1 14.51 11.73 1.12 o 3 8 1 386.90 389.92 3.25 o 4 8 1 67.56 64.26 1.45 o 5 8 1 259.23 263.97 3.16 o 6 8 1 42.46 45.86 2.04 o 7 8 1 61.72 68.65 1.85 o 8 8 1 40.20 35.45 1.15 o 9 8 1 90.28 97.95 1.74 o -9 9 1 65.62 72.53 2.61 o -8 9 1 76.39 71.23 1.84 o -7 9 1 70.81 70.15 1.90 o -6 9 1 169.54 169.17 3.42 o -5 9 1 174.78 165.36 6.08 o -4 9 1 563.47 563.77 5.45 o -3 9 1 123.04 130.74 1.90 o -2 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2.18 o 1 11 1 92.47 91.17 1.86 o 2 11 1 42.47 42.87 1.95 o 3 11 1 17.48 20.00 1.30 o 4 11 1 145.87 143.68 2.51 o 5 11 1 198.03 201.64 5.69 o 6 11 1 49.40 48.59 1.57 o 7 11 1 145.44 154.79 3.62 o -5 12 1 30.11 27.18 1.08 o -4 12 1 148.59 168.15 2.62 o -3 12 1 298.10 295.73 3.29 o -2 12 1 41.17 34.33 1.36 o -1 12 1 61.85 50.17 1.41 o 0 12 1 61.33 55.70 1.48 o 1 12 1 61.36 52.67 1.58 o 2 12 1 40.61 35.02 1.39 o 3 12 1 295.25 295.41 3.21 o 4 12 1 145.96 160.57 2.16 o 5 12 1 30.08 27.50 1.08 o -3 13 1 43.52 38.65 2.04 o -2 13 1 59.67 63.66 1.90 o -1 13 1 9.24 11.02 1.11 o 0 13 1 48.91 46.25 1.60 o 1 13 1 9.53 11.69 1.44 o 2 13 1 58.64 63.99 1.94 o 3 13 1 44.08 42.07 1.48 o 2 0 2 145.54 143.00 1.46 o 3 0 2 525.35 542.84 1.70 o 4 0 2 147.65 175.18 1.81 o 5 0 2 1430.92 1462.84 7.13 o 6 0 2 49.19 48.15 1.39 o 8 0 2 92.06 86.49 1.46 o 9 0 2 119.96 116.37 1.60 o 10 0 2 484.31 544.15 4.33 o 11 0 2 2.70 1.98 0.72 o 12 0 2 5.29 6.47 1.27 o -12 1 2 120.76 127.20 2.40 o -11 1 2 323.11 347.71 4.34 o -10 1 2 121.02 123.86 1.83 o -9 1 2 29.50 31.62 1.09 o -8 1 2 615.33 629.23 6.26 o -7 1 2 576.38 599.30 10.18 o -6 1 2 449.04 459.06 3.74 o -5 1 2 380.49 351.03 3.25 o -4 1 2 30.17 36.63 0.86 o -3 1 2 2942.83 2733.06 10.00 o -2 1 2 10958.45 9648.08 81.42 o -1 1 2 4657.40 4093.24 44.88 o 3 1 2 2953.66 2720.98 8.76 o 4 1 2 29.30 36.58 0.90 o 5 1 2 380.07 371.85 6.01 o 6 1 2 448.20 440.90 4.41 o 7 1 2 579.29 601.50 8.86 o 8 1 2 619.78 637.61 7.89 o 9 1 2 29.83 31.87 1.13 o 10 1 2 122.84 129.05 2.12 o 11 1 2 320.02 354.31 3.29 o -11 2 2 113.18 121.05 1.78 o -10 2 2 174.11 183.73 2.18 o -9 2 2 39.18 40.65 1.17 o -8 2 2 97.03 91.96 2.20 o -7 2 2 191.65 193.48 3.22 o -6 2 2 107.29 119.65 2.93 o -5 2 2 523.70 487.62 3.63 o -4 2 2 1067.84 1129.99 7.48 o -3 2 2 4544.13 4453.75 31.59 o -1 2 2 664.89 641.65 11.43 o 1 2 2 662.38 646.34 7.97 o 3 2 2 4548.69 4362.81 37.30 o 4 2 2 1066.89 1123.21 7.75 o 5 2 2 526.52 478.48 3.72 o 6 2 2 105.82 115.63 2.45 o 7 2 2 189.95 192.77 3.39 o 8 2 2 96.03 90.68 1.36 o 9 2 2 40.62 40.20 1.22 o 10 2 2 174.42 194.34 2.27 o 11 2 2 113.33 120.33 1.73 o -11 3 2 73.86 78.14 1.84 o -10 3 2 1.81 2.86 0.91 o -9 3 2 265.13 270.40 2.72 o -8 3 2 63.53 64.08 1.27 o -7 3 2 569.76 548.53 6.01 o -6 3 2 82.32 95.58 1.78 o -5 3 2 202.43 197.11 1.86 o -4 3 2 1021.78 1027.38 6.47 o -3 3 2 1740.24 1630.89 11.94 o -2 3 2 1262.28 1193.49 4.12 o -1 3 2 666.46 621.21 2.05 o 0 3 2 1207.06 1059.56 7.13 o 1 3 2 666.88 627.05 2.52 o 2 3 2 1257.64 1203.48 5.85 o 3 3 2 1742.15 1661.89 6.11 o 4 3 2 1029.20 1034.53 7.86 o 5 3 2 205.39 199.32 2.62 o 6 3 2 80.88 90.97 3.01 o 7 3 2 575.21 549.71 5.78 o 8 3 2 62.92 61.89 1.05 o 9 3 2 266.62 279.23 2.67 o 10 3 2 2.34 2.46 0.77 o 11 3 2 73.23 79.51 1.58 o -11 4 2 54.65 56.74 1.55 o -10 4 2 77.30 83.33 1.60 o -9 4 2 169.83 161.02 2.36 o -8 4 2 842.59 796.80 4.72 o -7 4 2 81.90 84.09 1.46 o -6 4 2 803.99 793.03 5.79 o -5 4 2 137.50 139.92 2.07 o -4 4 2 1460.31 1443.86 6.51 o -3 4 2 435.81 512.75 2.88 o -2 4 2 2217.53 2184.31 9.46 o 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172.66 5.34 o -1 4 25 89.97 93.88 2.37 o 0 4 25 6.20 6.41 0.86 o 1 4 25 88.94 96.03 2.06 o 2 4 25 164.01 172.32 5.16 o 3 4 25 114.57 101.96 2.21 o -2 5 25 33.54 34.89 1.37 o -1 5 25 3.89 4.01 1.23 o 0 5 25 2.20 4.54 0.71 o 1 5 25 3.84 3.90 0.69 o 2 5 25 34.59 31.03 1.98 o 0 0 26 358.68 324.67 6.26 o 1 0 26 5.36 4.76 0.80 o 2 0 26 13.54 13.36 0.96 o 3 0 26 25.63 18.82 0.99 o 4 0 26 37.54 38.26 1.96 o -3 1 26 21.55 20.78 1.22 o -2 1 26 140.53 147.93 2.77 o -1 1 26 107.25 101.49 2.49 o 0 1 26 67.76 66.30 2.12 o 1 1 26 105.62 101.66 1.95 o 2 1 26 140.47 143.46 2.38 o 3 1 26 21.05 20.29 1.00 o -3 2 26 34.05 28.38 1.03 o -2 2 26 80.30 76.77 1.98 o -1 2 26 122.95 122.80 3.94 o 0 2 26 92.68 93.86 3.33 o 1 2 26 123.03 112.52 3.15 o 2 2 26 78.64 76.58 3.92 o 3 2 26 33.27 31.47 1.75 o -2 3 26 5.59 6.90 1.04 o -1 3 26 10.29 10.83 1.60 o 0 3 26 1.17 -0.14 0.76 o 1 3 26 10.05 11.13 1.03 o 2 3 26 5.71 5.72 1.30 o -1 4 26 295.45 327.45 5.29 o 0 4 26 42.79 41.50 2.08 o 1 4 26 297.37 308.43 5.08 o 1 0 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