#------------------------------------------------------------------------------ #$Date: 2012-09-11 12:26:43 +0300 (Tue, 11 Sep 2012) $ #$Revision: 66590 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/36/2233661.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2233661_Fobs loop_ _publ_author_name 'Uhrinov\'a, Anna' 'Kuch\'ar, Juraj' '\n~ with different types of fumarate bridging ; _journal_coeditor_code WM2574 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m92 _journal_page_last m93 _journal_volume 68 _journal_year 2012 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 68.677 _cell_angle_beta 70.141 _cell_angle_gamma 89.655 _cell_length_a 7.8998 _cell_length_b 9.8238 _cell_length_c 11.3815 _exptl_crystal_F_000 380.00 _reflns_d_resolution_high 0.7965 _[local]_cod_data_source_file wm2574Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 3aapM in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 140.08 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1450.28 1481.82 14.34 o 3 0 0 1428.66 1457.62 13.09 o 4 0 0 36.52 25.49 1.95 o 5 0 0 605.62 621.70 14.56 o 6 0 0 1015.68 1016.23 24.48 o 7 0 0 2.88 3.43 3.38 o 8 0 0 1.10 5.28 6.06 o 9 0 0 203.69 210.73 11.70 o -9 1 0 0.15 -0.66 6.13 o -8 1 0 185.85 199.16 10.49 o -7 1 0 22.17 23.29 10.63 o -6 1 0 168.36 159.08 7.70 o -5 1 0 3214.17 3384.42 46.36 o -4 1 0 3120.68 3328.09 19.30 o -3 1 0 352.82 368.72 4.26 o -2 1 0 171.59 153.64 1.95 o -1 1 0 260.47 282.12 2.51 o 1 1 0 11151.19 10774.72 107.34 o 2 1 0 283.94 283.81 3.68 o 3 1 0 111.19 135.82 2.82 o 4 1 0 1452.86 1455.02 14.69 o 5 1 0 1708.34 1756.71 13.47 o 6 1 0 124.16 119.33 3.78 o 7 1 0 656.59 688.98 17.86 o 8 1 0 220.05 237.60 11.62 o 9 1 0 48.52 43.38 5.66 o -9 2 0 84.86 84.84 8.28 o -8 2 0 33.81 35.50 4.67 o -7 2 0 204.80 209.36 9.74 o -6 2 0 133.71 136.80 13.26 o -5 2 0 417.61 383.19 12.39 o -4 2 0 2144.95 2274.75 16.95 o -3 2 0 33.12 53.06 1.42 o -2 2 0 73.36 76.34 1.12 o -1 2 0 80.85 90.34 1.54 o 0 2 0 1501.01 1486.10 10.69 o 1 2 0 3404.12 3468.82 47.71 o 2 2 0 422.40 376.21 4.54 o 3 2 0 796.98 712.68 6.00 o 4 2 0 1250.47 1268.52 11.62 o 5 2 0 38.86 40.15 1.85 o 6 2 0 275.28 273.32 6.59 o 7 2 0 272.06 274.93 13.61 o 8 2 0 71.24 70.82 12.62 o -9 3 0 1.05 0.00 1.74 o -8 3 0 325.52 343.66 24.93 o -7 3 0 196.10 211.69 11.64 o -6 3 0 10.34 17.00 2.85 o -5 3 0 871.68 819.00 15.67 o -4 3 0 1690.57 1675.66 8.81 o -3 3 0 1222.68 1274.86 9.00 o -2 3 0 356.92 318.91 2.56 o -1 3 0 537.07 521.53 2.58 o 0 3 0 0.30 5.80 0.60 o 1 3 0 775.74 755.67 6.79 o 2 3 0 342.78 326.16 5.14 o 3 3 0 0.09 0.90 0.33 o 4 3 0 8.85 5.09 0.71 o 5 3 0 141.99 138.76 3.39 o 6 3 0 2.04 2.38 0.96 o 7 3 0 289.20 296.11 12.13 o 8 3 0 429.90 447.66 16.13 o -9 4 0 375.60 402.63 47.33 o -8 4 0 52.31 51.29 4.43 o -7 4 0 154.33 147.51 5.80 o -6 4 0 552.40 542.13 7.75 o -5 4 0 788.67 757.42 10.98 o -4 4 0 664.79 650.96 7.17 o -3 4 0 3712.98 3779.44 13.14 o -2 4 0 1149.59 1133.48 9.00 o -1 4 0 857.11 895.38 6.75 o 0 4 0 3545.64 3742.26 20.96 o 1 4 0 605.55 601.35 4.54 o 2 4 0 350.09 333.85 5.00 o 3 4 0 1813.42 1864.70 21.18 o 4 4 0 603.00 578.67 6.00 o 5 4 0 0.22 0.86 0.59 o 6 4 0 251.94 247.76 7.03 o 7 4 0 188.71 186.06 8.68 o 8 4 0 10.83 13.39 3.66 o -8 5 0 143.96 161.59 9.51 o -7 5 0 700.54 701.85 9.44 o -6 5 0 195.35 190.50 4.48 o -5 5 0 1016.94 1040.09 13.89 o -4 5 0 4039.25 4058.62 35.26 o -3 5 0 229.56 221.91 3.01 o -2 5 0 830.06 789.31 4.25 o -1 5 0 1001.62 940.94 8.54 o 0 5 0 1216.94 1352.89 6.93 o 1 5 0 1818.36 1879.38 18.07 o 2 5 0 1821.22 1807.62 12.49 o 3 5 0 34.45 29.81 2.22 o 4 5 0 372.45 390.79 8.08 o 5 5 0 216.52 218.19 6.50 o 6 5 0 19.90 16.64 2.12 o 7 5 0 103.90 102.06 5.07 o -8 6 0 78.83 94.90 7.42 o -7 6 0 5.96 7.33 2.14 o -6 6 0 196.73 188.33 5.84 o -5 6 0 472.00 442.07 17.36 o -4 6 0 1594.50 1563.75 10.58 o -3 6 0 1440.77 1441.79 9.04 o -2 6 0 470.37 474.23 3.72 o -1 6 0 95.87 112.77 2.10 o 0 6 0 520.05 483.88 3.89 o 1 6 0 262.13 243.52 6.51 o 2 6 0 17.49 19.41 1.41 o 3 6 0 939.08 956.93 12.29 o 4 6 0 78.45 83.87 4.96 o 5 6 0 2.98 2.19 0.99 o 6 6 0 225.39 233.06 7.50 o 7 6 0 128.00 126.50 8.16 o -8 7 0 416.63 432.72 33.73 o -7 7 0 69.39 65.18 13.00 o -6 7 0 60.86 59.50 11.62 o -5 7 0 75.58 80.08 2.92 o -4 7 0 28.55 27.09 1.45 o -3 7 0 98.15 95.60 2.39 o -2 7 0 61.38 58.71 1.64 o -1 7 0 210.16 205.29 2.50 o 0 7 0 31.82 32.70 1.18 o 1 7 0 335.65 339.16 5.95 o 2 7 0 431.16 438.60 7.13 o 3 7 0 37.79 35.03 2.57 o 4 7 0 546.48 569.20 12.92 o 5 7 0 82.51 89.60 5.55 o 6 7 0 53.27 52.22 4.48 o -7 8 0 32.85 37.18 10.18 o -6 8 0 203.28 212.22 21.85 o -5 8 0 245.19 244.25 8.25 o -4 8 0 344.82 332.46 5.93 o -3 8 0 239.90 226.15 4.55 o -2 8 0 300.72 298.27 4.81 o -1 8 0 164.40 160.72 3.65 o 0 8 0 160.26 158.03 3.38 o 1 8 0 369.31 382.55 6.90 o 2 8 0 1.11 1.92 1.26 o 3 8 0 394.97 405.80 8.84 o 4 8 0 145.68 153.20 9.00 o 5 8 0 46.93 44.29 3.73 o -6 9 0 24.11 15.98 7.57 o -5 9 0 182.62 183.91 6.99 o -4 9 0 433.56 436.82 9.06 o -3 9 0 3.25 2.85 1.00 o -2 9 0 149.72 151.79 3.74 o -1 9 0 643.44 628.88 7.67 o 0 9 0 23.57 22.85 1.60 o 1 9 0 1.94 1.18 0.87 o 2 9 0 229.30 238.56 8.18 o 3 9 0 4.40 4.08 1.60 o 4 9 0 137.11 142.41 8.87 o -5 10 0 38.62 35.01 5.19 o -4 10 0 17.89 21.79 2.27 o -3 10 0 337.71 332.90 8.07 o -2 10 0 129.35 130.59 5.95 o -1 10 0 133.08 124.01 5.75 o 0 10 0 381.38 365.14 10.34 o 1 10 0 61.33 64.26 3.55 o 2 10 0 11.23 6.66 1.75 o 3 10 0 179.53 176.87 7.71 o -3 11 0 18.26 14.75 2.00 o -2 11 0 137.78 140.01 6.55 o -1 11 0 179.64 190.23 8.88 o 0 11 0 0.22 -0.15 2.13 o 1 11 0 42.32 40.69 3.02 o 0 -11 1 16.78 16.90 2.55 o 1 -11 1 15.23 16.18 3.52 o 2 -11 1 111.77 117.89 6.18 o -2 -10 1 260.11 268.87 15.09 o -1 -10 1 1.89 -1.50 1.50 o 0 -10 1 184.60 178.89 6.33 o 1 -10 1 575.94 537.90 20.01 o 2 -10 1 124.13 113.28 7.32 o 3 -10 1 30.23 24.53 2.41 o 4 -10 1 473.81 490.92 10.89 o 5 -10 1 46.19 57.58 3.58 o -4 -9 1 226.25 230.36 11.56 o -3 -9 1 493.24 479.67 11.61 o -2 -9 1 27.54 28.45 3.11 o -1 -9 1 222.08 233.21 6.27 o 0 -9 1 89.05 88.82 3.65 o 1 -9 1 78.68 62.86 3.03 o 2 -9 1 301.02 298.88 7.38 o 3 -9 1 208.39 211.57 6.22 o 4 -9 1 2.95 1.97 0.97 o 5 -9 1 871.27 884.96 13.31 o 6 -9 1 247.11 237.42 14.26 o -5 -8 1 24.07 30.26 3.43 o -4 -8 1 142.59 137.12 5.83 o -3 -8 1 517.48 519.63 12.17 o -2 -8 1 162.86 160.10 4.79 o -1 -8 1 36.13 39.14 2.40 o 0 -8 1 3.90 6.31 1.05 o 1 -8 1 140.91 157.51 5.20 o 2 -8 1 26.50 25.17 2.48 o 3 -8 1 0.64 2.81 0.75 o 4 -8 1 712.60 705.77 10.62 o 5 -8 1 522.38 505.18 11.35 o 6 -8 1 164.27 161.68 9.59 o 7 -8 1 197.38 210.39 22.29 o -6 -7 1 54.79 53.38 4.11 o -5 -7 1 17.69 15.82 2.22 o -4 -7 1 3.94 3.12 1.19 o -3 -7 1 44.98 44.53 3.07 o -2 -7 1 18.19 16.16 2.18 o -1 -7 1 130.60 128.64 3.87 o 0 -7 1 676.22 703.17 11.53 o 1 -7 1 3.79 4.42 0.98 o 2 -7 1 360.47 358.27 4.14 o 3 -7 1 42.61 40.77 1.27 o 4 -7 1 39.46 38.01 1.30 o 5 -7 1 358.49 361.26 7.36 o 6 -7 1 149.93 145.60 17.03 o 7 -7 1 29.73 14.53 6.72 o 8 -7 1 156.32 174.96 21.09 o -6 -6 1 64.88 61.33 4.00 o -5 -6 1 296.15 302.47 8.37 o -4 -6 1 253.25 265.45 7.70 o -3 -6 1 550.92 577.11 10.67 o -2 -6 1 839.77 837.02 12.03 o -1 -6 1 300.06 290.90 4.22 o 0 -6 1 341.15 343.09 5.71 o 1 -6 1 733.99 751.87 6.20 o 2 -6 1 80.58 86.29 1.75 o 3 -6 1 401.26 404.41 5.05 o 4 -6 1 383.79 385.68 4.03 o 5 -6 1 227.65 229.11 3.23 o 6 -6 1 228.58 213.31 5.53 o 7 -6 1 167.40 177.82 18.91 o 8 -6 1 76.20 82.98 14.90 o -7 -5 1 168.12 182.23 15.61 o -6 -5 1 398.33 394.44 9.64 o -5 -5 1 118.16 116.71 5.00 o -4 -5 1 257.32 252.10 6.83 o -3 -5 1 909.93 921.15 12.15 o -2 -5 1 4.10 7.98 3.54 o -1 -5 1 376.66 348.12 4.22 o 0 -5 1 2562.03 2734.38 10.84 o 1 -5 1 6.92 8.65 0.60 o 2 -5 1 1666.63 1680.81 8.48 o 3 -5 1 1641.12 1621.84 8.28 o 4 -5 1 2.19 1.80 0.46 o 5 -5 1 774.73 761.28 7.25 o 6 -5 1 126.65 127.09 2.78 o 7 -5 1 64.14 60.29 3.62 o 8 -5 1 84.09 86.85 13.97 o -7 -4 1 21.12 20.95 3.80 o -6 -4 1 4.52 4.81 1.25 o -5 -4 1 140.90 132.51 5.04 o -4 -4 1 21.02 17.04 1.12 o -3 -4 1 313.40 298.24 4.51 o -2 -4 1 1840.84 1891.59 15.05 o -1 -4 1 1746.02 1741.33 6.96 o 0 -4 1 174.39 198.33 5.63 o 1 -4 1 5167.46 5693.08 22.73 o 2 -4 1 600.24 566.59 3.89 o 3 -4 1 31.86 31.19 1.27 o 4 -4 1 1635.36 1585.16 10.75 o 5 -4 1 170.35 165.38 2.65 o 6 -4 1 168.49 165.17 4.10 o 7 -4 1 327.10 328.14 6.40 o 8 -4 1 179.22 174.26 7.99 o 9 -4 1 6.88 4.05 3.08 o -8 -3 1 118.59 105.44 8.24 o -7 -3 1 591.34 623.75 18.12 o -6 -3 1 31.34 33.68 2.69 o -5 -3 1 0.97 1.13 1.28 o -4 -3 1 3.65 1.69 0.72 o -3 -3 1 6.78 13.32 1.46 o -2 -3 1 325.51 350.02 4.43 o -1 -3 1 96.51 78.55 2.01 o 0 -3 1 163.91 149.45 1.76 o 1 -3 1 542.07 564.43 4.87 o 2 -3 1 290.88 235.64 2.58 o 3 -3 1 573.96 528.56 4.93 o 4 -3 1 322.25 314.73 4.55 o 5 -3 1 1324.29 1288.30 15.38 o 6 -3 1 664.12 666.29 11.11 o 7 -3 1 36.34 38.53 4.92 o 8 -3 1 105.92 106.05 7.49 o 9 -3 1 159.10 161.02 7.20 o -8 -2 1 5.46 7.31 2.76 o -7 -2 1 1.03 2.17 2.21 o -6 -2 1 148.91 138.83 4.90 o -5 -2 1 783.69 772.53 8.38 o -4 -2 1 374.70 373.74 8.47 o -3 -2 1 83.74 72.18 3.89 o -2 -2 1 185.67 159.02 3.22 o -1 -2 1 377.73 351.56 7.47 o 0 -2 1 4503.20 4569.86 26.24 o 1 -2 1 1594.88 1640.73 7.48 o 2 -2 1 7.06 13.70 0.46 o 3 -2 1 192.90 206.87 2.30 o 4 -2 1 450.63 420.62 7.77 o 5 -2 1 297.56 266.38 6.34 o 6 -2 1 106.80 117.62 12.23 o 7 -2 1 206.74 206.98 9.34 o 8 -2 1 95.12 100.60 7.33 o 9 -2 1 108.28 114.79 8.45 o -8 -1 1 383.96 387.34 17.39 o -7 -1 1 35.83 28.84 4.21 o -6 -1 1 1254.56 1256.57 12.94 o -5 -1 1 0.07 0.43 0.53 o -4 -1 1 3277.58 3473.60 21.64 o -3 -1 1 758.68 726.25 8.33 o -2 -1 1 13.61 8.73 1.15 o -1 -1 1 1004.80 1029.95 7.33 o 0 -1 1 5295.84 5463.69 50.49 o 1 -1 1 878.37 923.68 7.73 o 2 -1 1 59.43 62.65 1.03 o 3 -1 1 21.76 28.44 0.76 o 4 -1 1 28.27 28.62 1.11 o 5 -1 1 466.66 438.24 13.23 o 6 -1 1 426.72 412.80 11.97 o 7 -1 1 92.78 86.93 6.22 o 8 -1 1 126.89 138.79 8.54 o 9 -1 1 125.10 128.73 8.95 o -8 0 1 134.61 141.72 9.29 o -7 0 1 162.71 165.92 9.05 o -6 0 1 2.10 1.67 0.71 o -5 0 1 2398.87 2372.84 23.71 o -4 0 1 1506.35 1538.26 11.58 o -3 0 1 5.33 4.76 0.90 o -2 0 1 107.46 108.72 4.69 o -1 0 1 4954.58 5266.84 22.92 o 2 0 1 8.35 8.06 0.81 o 3 0 1 20.59 20.60 0.57 o 4 0 1 1316.76 1323.13 8.60 o 5 0 1 1475.22 1511.73 11.48 o 6 0 1 156.19 124.59 16.33 o 7 0 1 167.63 173.37 8.79 o 8 0 1 278.35 286.09 12.20 o 9 0 1 1.98 2.43 4.68 o -9 1 1 125.45 139.13 9.84 o -8 1 1 23.37 22.31 4.11 o -7 1 1 2.37 3.67 3.87 o -6 1 1 488.29 496.74 13.95 o -5 1 1 562.24 553.62 13.33 o -4 1 1 1676.90 1725.06 20.88 o -3 1 1 620.90 617.27 6.27 o -2 1 1 1.25 0.74 0.63 o -1 1 1 82.63 64.47 0.84 o 1 1 1 564.58 572.54 5.99 o 2 1 1 70.74 61.22 1.37 o 3 1 1 1264.56 1253.01 6.07 o 4 1 1 146.24 138.34 2.80 o 5 1 1 483.12 495.90 5.93 o 6 1 1 368.64 377.63 5.45 o 7 1 1 44.27 45.27 7.65 o 8 1 1 105.27 113.04 7.92 o 9 1 1 169.66 183.41 10.75 o -9 2 1 32.53 38.81 5.28 o -8 2 1 49.80 49.94 10.20 o -7 2 1 74.12 63.98 13.85 o -6 2 1 3.50 3.43 2.91 o -5 2 1 724.19 686.45 14.80 o -4 2 1 16.33 11.18 2.04 o -3 2 1 1717.38 1818.33 18.62 o -2 2 1 102.44 74.89 1.06 o -1 2 1 963.61 986.50 5.37 o 0 2 1 695.35 699.83 4.81 o 1 2 1 577.48 578.38 4.71 o 2 2 1 330.62 331.45 3.06 o 3 2 1 247.57 254.86 2.49 o 4 2 1 1240.22 1255.97 8.78 o 5 2 1 208.45 196.74 4.56 o 6 2 1 18.49 19.39 1.82 o 7 2 1 314.98 319.15 9.20 o 8 2 1 214.43 230.98 11.20 o 9 2 1 14.34 19.63 9.63 o -9 3 1 644.27 651.26 29.70 o -8 3 1 11.38 6.26 4.89 o -7 3 1 253.89 260.64 15.85 o -6 3 1 379.59 387.80 12.39 o -5 3 1 325.71 349.56 13.86 o -4 3 1 601.08 536.76 11.66 o -3 3 1 331.51 291.87 3.88 o -2 3 1 3.05 1.61 0.29 o -1 3 1 2.28 3.33 0.38 o 0 3 1 436.67 442.07 6.98 o 1 3 1 39.11 44.81 1.01 o 2 3 1 391.22 372.65 3.48 o 3 3 1 2375.77 2380.91 13.56 o 4 3 1 399.10 396.23 4.93 o 5 3 1 283.66 296.95 4.85 o 6 3 1 749.67 745.08 17.19 o 7 3 1 20.14 21.93 2.48 o 8 3 1 216.39 219.12 10.97 o -8 4 1 847.84 839.02 27.18 o -7 4 1 291.38 275.78 19.20 o -6 4 1 16.35 16.27 1.94 o -5 4 1 445.82 424.80 7.94 o -4 4 1 610.81 630.30 13.26 o -3 4 1 157.32 142.01 2.72 o -2 4 1 1419.64 1426.14 5.78 o -1 4 1 1276.25 1278.94 8.05 o 0 4 1 67.15 69.07 1.05 o 1 4 1 538.94 511.18 6.30 o 2 4 1 1632.90 1629.05 13.23 o 3 4 1 77.22 80.63 2.52 o 4 4 1 357.58 363.20 7.05 o 5 4 1 25.14 26.25 1.89 o 6 4 1 34.47 38.86 2.80 o 7 4 1 475.11 439.37 19.22 o 8 4 1 198.80 207.63 10.87 o -8 5 1 18.80 25.28 4.05 o -7 5 1 121.51 124.81 4.17 o -6 5 1 499.86 493.34 7.45 o -5 5 1 217.64 216.07 3.26 o -4 5 1 565.94 555.15 8.40 o -3 5 1 1652.08 1641.94 13.71 o -2 5 1 878.66 862.78 5.90 o -1 5 1 25.50 20.37 0.83 o 0 5 1 454.01 410.02 4.26 o 1 5 1 817.33 834.78 10.68 o 2 5 1 60.98 48.43 1.66 o 3 5 1 808.57 769.72 9.35 o 4 5 1 112.06 118.10 4.28 o 5 5 1 74.52 72.91 5.69 o 6 5 1 34.07 39.54 3.07 o 7 5 1 256.87 233.78 13.13 o 8 5 1 31.88 28.32 10.79 o -8 6 1 265.08 282.41 12.73 o -7 6 1 224.78 225.73 7.25 o -6 6 1 4.29 3.15 1.02 o -5 6 1 118.80 118.07 3.69 o -4 6 1 253.37 240.98 12.53 o -3 6 1 15.85 17.13 1.05 o -2 6 1 680.77 678.02 7.83 o -1 6 1 695.86 675.90 9.90 o 0 6 1 190.33 189.99 2.24 o 1 6 1 1338.08 1316.57 20.34 o 2 6 1 1444.95 1478.64 9.44 o 3 6 1 118.16 116.53 5.12 o 4 6 1 314.92 308.85 7.18 o 5 6 1 47.26 49.22 3.21 o 6 6 1 62.82 62.02 3.97 o 7 6 1 71.88 75.51 9.10 o -7 7 1 38.93 41.49 9.13 o -6 7 1 217.47 254.08 23.71 o -5 7 1 123.97 120.36 3.99 o -4 7 1 39.41 41.86 2.17 o -3 7 1 1124.42 1127.21 7.72 o -2 7 1 396.38 394.88 4.29 o -1 7 1 625.94 615.03 8.66 o 0 7 1 434.35 423.76 3.74 o 1 7 1 185.47 180.87 3.53 o 2 7 1 45.46 44.23 1.94 o 3 7 1 861.79 847.57 16.65 o 4 7 1 13.90 12.74 1.84 o 5 7 1 112.81 112.16 4.93 o 6 7 1 92.35 102.63 6.70 o -7 8 1 105.03 101.18 17.06 o -6 8 1 0.19 -8.81 8.81 o -5 8 1 270.06 272.95 8.72 o -4 8 1 399.62 390.12 8.76 o -3 8 1 194.91 185.05 4.21 o -2 8 1 390.15 392.51 5.38 o -1 8 1 428.18 443.41 4.66 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5.29 o 4 5 11 260.97 263.92 6.05 o 5 5 11 134.60 123.02 5.10 o 6 5 11 273.11 285.41 6.69 o 7 5 11 2.56 3.12 1.06 o 8 5 11 8.37 5.41 1.29 o -3 6 11 37.08 35.42 4.77 o -2 6 11 41.61 37.63 3.21 o -1 6 11 55.88 58.34 3.56 o 0 6 11 540.84 531.36 8.82 o 1 6 11 15.47 12.88 1.35 o 2 6 11 3.49 4.03 1.19 o 3 6 11 114.23 118.58 3.99 o 4 6 11 1.68 2.42 0.89 o 5 6 11 732.29 724.04 12.44 o 6 6 11 333.84 333.09 7.27 o 7 6 11 112.00 102.29 4.17 o -2 7 11 16.60 6.76 6.42 o -1 7 11 0.39 0.11 0.74 o 0 7 11 378.84 383.19 6.70 o 1 7 11 1271.63 1298.12 19.79 o 2 7 11 9.82 11.12 1.40 o 3 7 11 19.75 21.78 1.79 o 4 7 11 136.00 136.68 5.50 o 5 7 11 12.42 13.19 1.97 o 6 7 11 107.48 111.42 4.34 o 7 7 11 120.68 119.63 5.60 o -2 8 11 38.40 40.17 13.19 o -1 8 11 77.71 77.45 4.76 o 0 8 11 67.83 70.34 4.27 o 1 8 11 99.16 108.81 4.37 o 2 8 11 110.37 109.56 4.64 o 3 8 11 17.70 13.09 1.83 o 4 8 11 5.72 3.81 1.84 o 5 8 11 107.18 106.19 5.45 o 6 8 11 94.75 88.88 4.82 o -1 9 11 28.08 27.22 3.21 o 0 9 11 174.23 173.08 7.32 o 1 9 11 263.74 273.66 9.20 o 2 9 11 12.59 12.37 2.34 o 3 9 11 174.37 174.06 6.12 o 4 9 11 103.09 100.51 5.12 o 5 9 11 24.53 19.67 2.39 o 0 10 11 163.12 165.55 7.42 o 1 10 11 9.61 8.04 2.10 o 2 10 11 102.82 107.41 6.08 o 3 10 11 23.17 24.76 3.24 o 4 10 11 7.94 4.48 1.80 o 2 -2 12 182.64 201.38 7.33 o 3 -2 12 101.36 115.42 5.41 o 4 -2 12 7.96 9.48 1.95 o 5 -2 12 10.72 11.43 2.01 o 1 -1 12 87.25 87.77 3.83 o 2 -1 12 111.59 114.49 6.59 o 3 -1 12 23.59 23.15 2.57 o 4 -1 12 112.63 127.67 5.86 o 5 -1 12 261.18 270.96 10.35 o 6 -1 12 9.61 6.24 3.77 o 0 0 12 221.74 213.81 7.05 o 1 0 12 227.20 227.24 7.06 o 2 0 12 72.17 69.75 5.01 o 3 0 12 385.66 390.85 11.54 o 4 0 12 6.14 8.00 1.76 o 5 0 12 40.23 42.26 4.28 o 6 0 12 97.09 108.99 6.56 o 7 0 12 0.44 -2.10 2.10 o -1 1 12 84.95 94.60 4.82 o 0 1 12 3.43 3.35 1.28 o 1 1 12 31.95 40.74 3.80 o 2 1 12 71.68 81.46 5.21 o 3 1 12 3.74 5.06 1.70 o 4 1 12 157.84 163.24 5.79 o 5 1 12 328.80 348.75 11.28 o 6 1 12 158.79 157.16 7.72 o 7 1 12 29.70 29.02 3.63 o -1 2 12 23.18 19.96 2.28 o 0 2 12 74.35 72.27 4.02 o 1 2 12 173.48 153.39 6.89 o 2 2 12 40.51 30.29 3.25 o 3 2 12 174.76 175.49 5.83 o 4 2 12 393.11 404.30 9.07 o 5 2 12 2.95 3.19 1.31 o 6 2 12 273.31 282.72 10.06 o 7 2 12 100.81 103.16 6.30 o -2 3 12 437.26 476.02 10.50 o -1 3 12 340.48 352.00 8.34 o 0 3 12 5.58 5.45 1.65 o 1 3 12 201.38 191.27 8.41 o 2 3 12 149.63 155.54 6.65 o 3 3 12 36.50 36.18 2.78 o 4 3 12 126.91 131.35 6.32 o 5 3 12 258.92 265.61 7.35 o 6 3 12 13.65 12.49 1.86 o 7 3 12 62.04 69.74 5.29 o -2 4 12 41.51 31.73 2.83 o -1 4 12 20.23 18.69 3.25 o 0 4 12 484.24 475.91 10.71 o 1 4 12 26.31 27.07 2.66 o 2 4 12 216.64 212.60 6.31 o 3 4 12 180.30 185.22 6.08 o 4 4 12 149.68 158.81 5.70 o 5 4 12 91.81 89.99 5.34 o 6 4 12 250.40 246.97 12.11 o 7 4 12 4.12 3.33 1.49 o -2 5 12 27.29 26.94 3.04 o -1 5 12 337.20 336.25 9.13 o 0 5 12 11.56 11.85 1.86 o 1 5 12 704.68 716.13 22.59 o 2 5 12 137.91 142.93 4.91 o 3 5 12 0.31 0.52 0.95 o 4 5 12 48.95 51.74 2.90 o 5 5 12 399.58 398.75 10.14 o 6 5 12 3.00 2.57 1.05 o 7 5 12 154.38 153.43 5.20 o -2 6 12 12.77 13.38 2.91 o -1 6 12 46.22 36.48 3.08 o 0 6 12 217.73 214.44 6.88 o 1 6 12 536.48 553.44 12.78 o 2 6 12 1.83 2.23 0.94 o 3 6 12 24.36 24.84 2.05 o 4 6 12 193.05 193.08 5.44 o 5 6 12 3.20 3.26 1.66 o 6 6 12 356.78 359.69 7.87 o 7 6 12 47.12 48.30 3.11 o -1 7 12 26.39 19.34 6.02 o 0 7 12 111.01 108.75 5.20 o 1 7 12 396.90 403.71 8.86 o 2 7 12 518.76 553.58 15.40 o 3 7 12 2.30 1.80 1.13 o 4 7 12 23.99 22.67 2.39 o 5 7 12 224.49 215.69 7.27 o 6 7 12 44.72 47.08 3.02 o -1 8 12 33.74 35.31 4.35 o 0 8 12 274.29 282.80 9.09 o 1 8 12 90.38 96.35 4.54 o 2 8 12 106.89 101.25 5.93 o 3 8 12 88.02 95.26 4.71 o 4 8 12 12.42 13.09 1.96 o 5 8 12 0.26 0.20 1.16 o 6 8 12 80.27 79.34 3.92 o 0 9 12 5.38 1.50 2.20 o 1 9 12 131.87 134.90 7.34 o 2 9 12 89.05 98.83 5.86 o 3 9 12 2.43 0.78 0.99 o 4 9 12 108.32 111.71 5.26 o 2 10 12 6.83 6.39 1.94 o 2 0 13 135.30 134.73 7.26 o 3 0 13 87.43 78.25 5.50 o 4 0 13 220.68 231.14 8.02 o 5 0 13 180.57 195.96 9.51 o 1 1 13 109.93 103.29 6.27 o 2 1 13 67.57 66.75 5.07 o 3 1 13 184.01 192.22 8.31 o 4 1 13 27.74 26.71 2.91 o 5 1 13 105.86 109.63 5.59 o 6 1 13 79.42 90.54 6.24 o 0 2 13 0.69 -1.58 1.58 o 1 2 13 36.86 38.96 3.82 o 2 2 13 65.26 70.46 5.47 o 3 2 13 24.28 19.00 2.17 o 4 2 13 138.53 146.19 5.78 o 5 2 13 247.97 255.25 8.14 o 6 2 13 6.10 6.25 2.23 o 0 3 13 147.90 147.00 9.52 o 1 3 13 8.12 5.85 1.73 o 2 3 13 15.83 19.46 2.78 o 3 3 13 55.72 60.19 3.75 o 4 3 13 13.59 13.79 1.97 o 5 3 13 17.63 19.70 2.04 o 6 3 13 271.92 285.10 10.49 o 0 4 13 1.66 1.87 1.28 o 1 4 13 593.06 605.68 14.09 o 2 4 13 48.11 52.80 3.41 o 3 4 13 3.85 2.34 1.09 o 4 4 13 113.28 119.18 5.84 o 5 4 13 76.07 76.89 4.22 o 6 4 13 0.01 0.79 1.18 o 0 5 13 193.08 196.94 7.65 o 1 5 13 45.46 46.00 3.72 o 2 5 13 230.80 246.14 7.04 o 3 5 13 21.63 22.09 2.35 o 4 5 13 32.60 31.25 2.73 o 5 5 13 164.17 153.16 5.88 o 6 5 13 126.88 127.18 6.60 o 0 6 13 1.06 1.63 1.09 o 1 6 13 282.11 291.37 7.63 o 2 6 13 275.99 296.90 8.83 o 3 6 13 11.93 9.09 1.42 o 4 6 13 53.04 51.79 3.04 o 5 6 13 126.56 125.33 4.71 o 6 6 13 2.46 3.70 1.28 o 0 7 13 142.39 133.28 7.46 o 1 7 13 23.46 22.56 2.59 o 2 7 13 0.33 -0.47 1.12 o 3 7 13 11.73 8.01 1.69 o 4 7 13 24.31 21.24 2.48 o 5 7 13 40.45 38.54 3.26 o 1 8 13 142.80 145.60 7.27 o 2 8 13 279.61 281.16 8.22 o 3 8 13 218.75 212.10 7.21 o 4 8 13 6.28 8.21 1.73 o 2 3 14 9.36 6.18 2.28 o 3 3 14 1.59 1.16 1.25 o 4 3 14 8.22 9.92 1.81 o 2 4 14 187.91 194.01 6.69 o 3 4 14 284.46 282.92 10.96 o 4 4 14 95.58 94.12 4.81 o 5 4 14 17.31 17.17 2.40 o 2 5 14 88.00 87.10 4.52 o 3 5 14 8.40 8.83 1.74 o 4 5 14 118.32 120.83 5.43 o 5 5 14 14.14 15.88 2.25 o 2 6 14 109.90 110.11 5.09 o 3 6 14 160.05 162.37 6.47 o 4 6 14 0.39 -0.86 1.75 o