#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:35:34 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181258 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/36/2233662.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2233662_Fobs loop_ _publ_author_name 'Morrison, Shaunna M.' 'Downs, Robert T.' 'Yang, Hexiong' _publ_section_title ; Redetermination of kovdorskite, Mg~2~PO~4~(OH)·3H~2~O ; _journal_coeditor_code WM2577 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first i12 _journal_page_last i13 _journal_volume 68 _journal_year 2012 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yab' _symmetry_space_group_name_H-M 'P 1 21/a 1' _cell_angle_alpha 90.000 _cell_angle_beta 105.054 _cell_angle_gamma 90.000 _cell_length_a 10.4785 _cell_length_b 12.9336 _cell_length_c 4.7308 _exptl_crystal_F_000 436.00 _reflns_d_resolution_high 0.6610 _cod_data_source_file wm2577Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' kovd2 in P2(1)/a' _shelx_refln_list_code 4 _shelx_f_calc_maximum 114.38 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z' '-x, -y, -z' 'x-1/2, -y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2058.12 2229.18 27.66 o 4 0 0 629.19 571.03 7.67 o 6 0 0 11520.65 11400.92 194.80 o 8 0 0 3041.02 3029.69 43.37 o 10 0 0 244.67 239.71 8.93 o 12 0 0 435.22 422.82 10.68 o 2 1 0 203.16 230.23 2.32 o 3 1 0 649.23 659.56 6.38 o 4 1 0 905.27 902.99 9.30 o 5 1 0 231.61 239.56 2.92 o 6 1 0 16.96 18.89 0.91 o 7 1 0 908.40 921.78 9.28 o 8 1 0 1538.13 1538.90 17.26 o 9 1 0 0.06 -0.39 0.97 o 10 1 0 412.04 390.62 6.96 o 11 1 0 230.65 224.61 5.51 o 12 1 0 590.88 564.80 11.66 o 13 1 0 375.74 365.57 8.55 o 14 1 0 106.33 107.69 5.78 o 0 2 0 2542.79 2638.80 30.28 o 1 2 0 3048.43 3170.87 43.34 o 2 2 0 494.79 516.66 8.13 o 3 2 0 1068.24 1125.78 14.82 o 5 2 0 691.53 706.78 6.67 o 6 2 0 69.45 85.91 1.54 o 7 2 0 972.43 987.78 9.90 o 8 2 0 1001.99 983.92 9.98 o 9 2 0 202.74 196.26 3.94 o 10 2 0 493.88 489.67 10.22 o 11 2 0 5.57 3.66 1.79 o 12 2 0 97.33 96.66 4.10 o 13 2 0 340.33 342.57 18.75 o 14 2 0 730.31 711.26 22.25 o 15 2 0 135.18 144.02 7.06 o 1 3 0 59.08 60.60 0.77 o 2 3 0 40.82 39.05 2.40 o 3 3 0 2588.55 2717.08 38.76 o 4 3 0 378.59 392.16 6.31 o 5 3 0 1511.61 1506.83 19.96 o 6 3 0 321.49 305.53 5.16 o 7 3 0 996.03 1011.19 12.89 o 8 3 0 150.66 152.81 3.45 o 9 3 0 1095.56 1080.25 19.72 o 10 3 0 355.87 331.38 7.69 o 11 3 0 24.70 25.65 2.50 o 12 3 0 0.62 1.96 1.92 o 13 3 0 52.41 53.13 5.33 o 14 3 0 3.12 0.77 3.21 o 15 3 0 5.81 0.77 3.08 o 0 4 0 1168.98 1285.31 14.02 o 1 4 0 1276.52 1303.88 10.39 o 2 4 0 0.17 -0.58 0.58 o 3 4 0 0.08 1.65 0.91 o 4 4 0 1827.33 1929.81 32.19 o 5 4 0 160.37 150.73 3.03 o 6 4 0 2130.65 2069.34 30.15 o 7 4 0 228.62 238.49 4.26 o 8 4 0 39.79 42.79 1.88 o 9 4 0 7.61 11.13 2.02 o 10 4 0 122.23 113.64 5.97 o 11 4 0 638.08 638.81 13.05 o 12 4 0 133.44 126.45 4.71 o 13 4 0 192.87 184.44 6.67 o 14 4 0 115.64 115.27 7.70 o 1 5 0 918.75 873.96 7.15 o 2 5 0 280.97 277.43 3.71 o 3 5 0 21.01 17.91 0.79 o 4 5 0 145.54 138.48 4.17 o 5 5 0 1501.36 1485.42 25.29 o 6 5 0 266.88 266.83 6.03 o 7 5 0 12.78 16.60 1.40 o 8 5 0 607.01 625.45 9.32 o 9 5 0 871.22 826.31 15.73 o 10 5 0 782.37 790.70 15.40 o 11 5 0 70.42 67.87 3.49 o 12 5 0 136.67 135.12 4.87 o 13 5 0 746.17 730.25 18.20 o 14 5 0 20.50 13.86 4.23 o 0 6 0 2050.42 1968.41 24.95 o 1 6 0 296.38 311.51 3.40 o 2 6 0 972.52 913.54 9.83 o 3 6 0 397.96 379.64 5.28 o 4 6 0 47.58 48.61 1.66 o 5 6 0 129.21 130.36 4.14 o 6 6 0 449.73 427.62 9.06 o 7 6 0 92.14 80.48 4.87 o 8 6 0 202.81 210.54 3.98 o 9 6 0 19.54 19.92 2.40 o 10 6 0 5.63 6.73 1.69 o 11 6 0 194.59 200.52 5.66 o 12 6 0 24.69 20.39 3.47 o 13 6 0 116.41 114.24 8.60 o 14 6 0 207.67 199.91 10.66 o 1 7 0 441.59 445.92 4.53 o 2 7 0 988.05 1013.38 10.59 o 3 7 0 13082.48 12090.40 235.86 o 4 7 0 2357.34 2325.50 33.78 o 5 7 0 1489.25 1433.80 24.91 o 6 7 0 548.79 552.02 11.20 o 7 7 0 4.36 4.02 2.06 o 8 7 0 317.09 334.29 8.19 o 9 7 0 1591.97 1605.66 40.99 o 10 7 0 31.91 34.63 2.17 o 11 7 0 847.51 867.04 21.56 o 12 7 0 375.58 366.85 24.34 o 13 7 0 56.74 55.06 6.67 o 14 7 0 121.39 126.18 9.63 o 0 8 0 7.25 7.95 1.06 o 1 8 0 11.11 14.36 0.88 o 2 8 0 15.41 16.44 0.81 o 3 8 0 209.62 217.78 4.54 o 4 8 0 7172.33 6777.76 149.05 o 5 8 0 18.42 18.99 2.89 o 6 8 0 1161.00 1136.71 20.66 o 7 8 0 0.04 1.60 2.04 o 8 8 0 31.24 28.84 2.96 o 9 8 0 179.69 178.53 6.00 o 10 8 0 1008.68 1036.15 25.06 o 11 8 0 230.32 235.68 9.15 o 12 8 0 96.73 96.01 8.47 o 13 8 0 123.53 119.76 9.50 o 1 9 0 124.31 125.79 2.31 o 2 9 0 587.51 621.86 6.96 o 3 9 0 950.42 993.55 15.51 o 4 9 0 2.99 4.04 1.33 o 5 9 0 17.85 18.28 1.50 o 6 9 0 577.05 548.14 11.54 o 7 9 0 923.12 931.63 17.85 o 8 9 0 668.43 631.24 13.29 o 9 9 0 59.06 64.96 4.14 o 10 9 0 6.35 11.83 3.38 o 11 9 0 662.32 661.63 18.05 o 12 9 0 0.23 6.42 4.62 o 13 9 0 1.58 5.77 4.75 o 0 10 0 207.04 209.47 3.96 o 1 10 0 740.93 758.76 8.47 o 2 10 0 5.17 7.24 0.85 o 3 10 0 1626.39 1661.63 25.00 o 4 10 0 568.40 560.62 9.73 o 5 10 0 1150.75 1141.83 17.92 o 6 10 0 117.25 119.36 6.71 o 7 10 0 178.14 178.37 5.93 o 8 10 0 2.89 3.14 2.36 o 9 10 0 126.50 140.93 5.95 o 10 10 0 90.25 82.74 10.65 o 11 10 0 131.61 126.63 10.27 o 12 10 0 38.31 48.76 6.93 o 13 10 0 16.66 14.76 5.52 o 1 11 0 13.99 12.60 1.35 o 2 11 0 198.38 205.04 4.43 o 3 11 0 1361.45 1360.05 24.05 o 4 11 0 77.36 81.17 6.88 o 5 11 0 166.06 166.03 5.63 o 6 11 0 63.92 65.56 4.02 o 7 11 0 274.17 273.76 7.71 o 8 11 0 450.22 478.40 11.35 o 9 11 0 21.02 24.29 3.39 o 10 11 0 106.12 104.84 6.88 o 11 11 0 330.90 347.82 16.31 o 12 11 0 55.62 53.13 7.83 o 0 12 0 933.07 892.52 26.66 o 1 12 0 457.65 431.91 10.19 o 2 12 0 1493.77 1484.21 23.84 o 3 12 0 160.74 152.41 8.60 o 4 12 0 119.83 118.49 8.34 o 5 12 0 57.00 55.71 4.84 o 6 12 0 163.61 155.31 5.67 o 7 12 0 30.55 32.73 3.49 o 8 12 0 35.40 35.98 4.86 o 9 12 0 0.25 -2.70 2.72 o 10 12 0 545.82 531.32 16.14 o 11 12 0 24.70 26.43 6.42 o 12 12 0 74.30 68.28 8.47 o 1 13 0 19.63 21.24 2.37 o 2 13 0 948.41 955.77 15.79 o 3 13 0 161.70 156.00 8.86 o 4 13 0 565.03 550.18 19.93 o 5 13 0 28.48 34.52 5.52 o 6 13 0 202.81 214.30 11.56 o 7 13 0 200.89 202.23 11.68 o 8 13 0 13.09 11.36 3.63 o 9 13 0 338.59 353.00 11.81 o 10 13 0 199.35 243.91 14.96 o 11 13 0 56.84 65.58 8.60 o 0 14 0 190.64 183.10 8.22 o 1 14 0 365.24 349.97 8.82 o 2 14 0 1349.25 1329.57 39.84 o 3 14 0 8.52 11.55 4.11 o 4 14 0 19.52 27.33 5.13 o 5 14 0 28.37 22.07 5.26 o 6 14 0 775.11 770.16 27.01 o 7 14 0 27.59 37.98 6.67 o 8 14 0 343.55 371.22 17.47 o 9 14 0 331.04 333.30 16.70 o 10 14 0 7.77 17.19 6.42 o 1 15 0 618.74 591.54 13.32 o 2 15 0 0.20 -3.21 3.21 o 3 15 0 6.64 8.21 4.23 o 4 15 0 41.31 44.27 5.90 o 5 15 0 83.37 88.30 8.34 o 6 15 0 478.06 456.20 18.76 o 7 15 0 755.03 761.76 27.78 o 8 15 0 361.62 378.68 18.11 o 9 15 0 92.46 111.15 10.91 o 0 16 0 0.05 -2.44 2.69 o 1 16 0 6.34 6.58 2.06 o 2 16 0 230.55 231.65 10.91 o 3 16 0 90.23 88.56 7.70 o 4 16 0 9.00 1.28 4.49 o 5 16 0 124.77 122.72 9.88 o 6 16 0 148.74 155.59 11.55 o 7 16 0 13.00 6.54 5.26 o 8 16 0 13.12 14.88 5.90 o 1 17 0 18.49 18.61 2.21 o 2 17 0 229.89 206.60 10.27 o 3 17 0 6.90 6.67 4.23 o 4 17 0 71.45 61.09 7.32 o 5 17 0 197.49 223.01 12.58 o 6 17 0 38.63 41.83 7.19 o 7 17 0 669.67 683.95 26.61 o 0 18 0 12.95 11.55 3.34 o 1 18 0 685.03 652.53 21.60 o 2 18 0 135.05 134.01 8.34 o 3 18 0 235.69 228.43 11.56 o 4 18 0 99.85 87.54 8.21 o 5 18 0 13.77 16.81 5.65 o 6 18 0 2.59 0.13 5.00 o 1 19 0 127.24 118.35 7.32 o 2 19 0 6.54 9.88 4.23 o 3 19 0 1.20 0.51 4.11 o -14 0 1 1.90 0.13 2.18 o -12 0 1 1295.47 1272.39 27.67 o -10 0 1 0.83 0.10 1.75 o -8 0 1 2225.82 2276.12 32.09 o -6 0 1 1038.17 1035.75 15.04 o -4 0 1 2692.85 2942.22 37.68 o -2 0 1 3606.29 3657.41 39.12 o 0 0 1 580.98 577.53 6.99 o 2 0 1 8130.72 7825.27 91.47 o 4 0 1 159.17 164.42 2.96 o 6 0 1 4416.84 4415.85 55.21 o 8 0 1 19.50 23.17 2.37 o 10 0 1 3.01 6.79 2.06 o 12 0 1 879.33 858.74 19.29 o -15 1 1 15.02 18.09 3.08 o -14 1 1 9.30 7.57 2.95 o -13 1 1 207.27 217.64 4.75 o -12 1 1 2.30 3.10 1.37 o -11 1 1 324.47 311.92 6.05 o -10 1 1 333.37 314.59 6.01 o -9 1 1 404.75 408.29 6.30 o -8 1 1 1295.65 1286.10 18.11 o -7 1 1 5370.80 5368.83 55.06 o -6 1 1 1844.32 1844.50 19.67 o -5 1 1 231.07 273.95 3.35 o -4 1 1 1732.40 1700.89 14.65 o -3 1 1 0.37 1.56 0.49 o -2 1 1 2277.70 2152.71 20.81 o -1 1 1 1126.10 1123.20 9.79 o 0 1 1 2448.23 2575.58 20.35 o 1 1 1 1074.75 1125.69 9.13 o 2 1 1 102.68 122.89 1.45 o 3 1 1 7447.83 7528.84 58.98 o 4 1 1 49.61 53.83 1.19 o 5 1 1 1041.78 1090.92 10.13 o 6 1 1 640.57 627.58 8.22 o 7 1 1 61.08 62.49 1.67 o 8 1 1 9.61 8.44 1.14 o 9 1 1 1238.87 1217.05 18.46 o 10 1 1 522.61 505.61 8.63 o 11 1 1 7.64 7.04 1.50 o 12 1 1 27.57 29.35 2.61 o 13 1 1 7.54 9.50 2.82 o 14 1 1 306.66 317.73 10.40 o -15 2 1 103.63 119.37 6.93 o -14 2 1 310.83 332.52 12.59 o -13 2 1 127.72 133.94 6.22 o -12 2 1 417.50 428.18 9.64 o -11 2 1 2.51 5.52 0.95 o -10 2 1 185.37 187.62 4.41 o -9 2 1 955.91 971.90 13.11 o -8 2 1 22.67 26.74 1.30 o -7 2 1 123.44 137.17 2.23 o -6 2 1 0.01 -0.17 0.66 o -5 2 1 1214.80 1260.36 12.81 o -4 2 1 2079.02 2087.62 18.82 o -3 2 1 10819.07 10329.48 134.33 o -2 2 1 1915.16 1919.91 17.42 o -1 2 1 290.31 286.93 2.70 o 0 2 1 1018.62 1133.66 10.03 o 1 2 1 2996.58 2977.51 24.45 o 2 2 1 6166.11 6098.02 49.84 o 3 2 1 2957.83 3459.23 28.71 o 4 2 1 1989.18 2115.25 21.46 o 5 2 1 972.87 960.16 10.15 o 6 2 1 203.12 196.93 2.79 o 7 2 1 152.02 153.91 2.43 o 8 2 1 17.98 20.37 1.16 o 9 2 1 646.53 630.15 10.08 o 10 2 1 2448.24 2337.32 40.57 o 11 2 1 66.60 65.76 3.49 o 12 2 1 5.13 5.87 2.09 o 13 2 1 54.10 52.49 5.01 o 14 2 1 10.32 8.98 3.21 o -15 3 1 11.97 18.73 4.11 o -14 3 1 376.35 364.96 14.13 o -13 3 1 87.73 81.82 4.10 o -12 3 1 23.76 24.44 2.57 o -11 3 1 948.19 938.49 17.96 o -10 3 1 120.24 112.18 4.11 o -9 3 1 116.26 112.18 3.95 o -8 3 1 353.87 333.52 4.28 o -7 3 1 27.83 31.18 1.03 o -6 3 1 424.81 483.32 5.75 o -5 3 1 107.99 126.20 1.98 o -4 3 1 4168.28 4675.27 42.01 o -3 3 1 7482.30 7218.72 68.76 o -2 3 1 792.11 891.07 8.29 o -1 3 1 3474.00 3474.59 29.61 o 0 3 1 238.60 252.40 2.63 o 1 3 1 794.55 777.21 6.71 o 2 3 1 233.17 279.52 3.01 o 3 3 1 592.03 549.50 5.37 o 4 3 1 1134.87 1212.97 13.96 o 5 3 1 383.98 393.40 6.19 o 6 3 1 889.35 898.49 12.42 o 7 3 1 727.00 715.60 10.45 o 8 3 1 7.03 6.29 1.71 o 9 3 1 140.32 138.02 5.09 o 10 3 1 25.06 27.28 2.48 o 11 3 1 378.01 352.55 8.37 o 12 3 1 20.46 18.46 2.99 o 13 3 1 94.57 90.23 6.67 o 14 3 1 266.88 269.54 11.30 o -15 4 1 254.00 279.29 12.20 o -14 4 1 552.26 538.15 19.28 o -13 4 1 321.95 315.07 12.23 o -12 4 1 51.16 51.94 4.07 o -11 4 1 0.04 0.49 1.79 o -10 4 1 13.52 14.67 2.07 o -9 4 1 317.72 309.23 8.26 o -8 4 1 359.55 357.49 6.78 o -7 4 1 752.39 785.05 14.18 o -6 4 1 721.68 717.03 11.41 o -5 4 1 1219.59 1290.81 15.65 o -4 4 1 130.74 141.96 1.84 o -3 4 1 729.72 741.89 6.99 o -2 4 1 0.00 1.46 0.41 o -1 4 1 5581.35 5953.28 50.51 o 0 4 1 14.06 7.37 0.55 o 1 4 1 4718.85 4607.79 39.23 o 2 4 1 459.52 569.30 5.34 o 3 4 1 705.00 723.09 8.67 o 4 4 1 38.54 40.74 1.39 o 5 4 1 540.34 524.91 7.76 o 6 4 1 43.90 46.79 2.39 o 7 4 1 306.00 294.64 5.67 o 8 4 1 101.06 100.26 4.11 o 9 4 1 502.52 487.39 10.28 o 10 4 1 28.75 26.81 2.47 o 11 4 1 2.76 1.65 1.90 o 12 4 1 1.06 0.38 2.27 o 13 4 1 0.36 2.82 3.34 o 14 4 1 0.80 -2.57 3.34 o -15 5 1 9.13 15.27 4.49 o -14 5 1 156.98 148.14 8.86 o -13 5 1 669.89 647.95 22.63 o -12 5 1 38.51 40.49 3.09 o -11 5 1 21.20 18.21 2.33 o -10 5 1 14.55 15.05 2.11 o -9 5 1 84.05 78.41 3.59 o -8 5 1 947.93 875.41 16.42 o -7 5 1 3389.86 3229.56 46.56 o -6 5 1 2637.04 2633.58 38.16 o -5 5 1 25.88 28.80 1.41 o -4 5 1 1451.95 1587.92 15.31 o -3 5 1 29.67 48.23 1.51 o -2 5 1 3179.23 3225.14 28.87 o -1 5 1 3260.41 3516.48 30.14 o 0 5 1 12717.83 13222.00 151.67 o 1 5 1 1379.39 1283.50 11.82 o 2 5 1 349.28 417.37 4.86 o 3 5 1 0.57 0.06 0.75 o 4 5 1 195.48 204.70 3.42 o 5 5 1 299.30 275.53 4.63 o 6 5 1 1654.92 1672.85 22.40 o 7 5 1 2736.04 2751.09 36.03 o 8 5 1 287.64 287.52 6.85 o 9 5 1 440.76 420.11 9.19 o 10 5 1 400.66 395.53 8.98 o 11 5 1 798.32 782.32 15.63 o 12 5 1 681.79 661.03 16.09 o 13 5 1 5.23 2.95 3.72 o 14 5 1 90.17 95.10 7.57 o -14 6 1 352.88 349.63 15.16 o -13 6 1 120.99 120.80 5.97 o -12 6 1 105.74 107.24 4.54 o -11 6 1 281.65 273.72 7.79 o -10 6 1 1249.99 1222.45 22.62 o -9 6 1 173.72 166.31 5.54 o -8 6 1 153.29 159.39 5.32 o -7 6 1 228.30 220.02 6.45 o -6 6 1 31.08 30.01 2.33 o -5 6 1 190.03 188.69 3.63 o -4 6 1 1866.33 1932.03 23.30 o -3 6 1 494.97 510.64 5.42 o -2 6 1 392.73 427.89 4.64 o -1 6 1 695.47 739.89 7.16 o 0 6 1 223.13 241.25 2.82 o 1 6 1 86.26 96.30 1.65 o 2 6 1 95.10 94.33 1.89 o 3 6 1 78.53 72.50 1.91 o 4 6 1 2216.17 2171.51 26.24 o 5 6 1 1376.17 1366.84 20.28 o 6 6 1 5761.81 5608.92 71.95 o 7 6 1 16.79 17.35 1.34 o 8 6 1 124.07 112.50 3.93 o 9 6 1 277.03 273.86 6.71 o 10 6 1 120.11 119.57 5.76 o 11 6 1 104.21 100.99 4.44 o 12 6 1 442.91 408.59 16.45 o 13 6 1 0.32 -1.28 3.72 o -14 7 1 41.21 37.73 6.03 o -13 7 1 60.64 68.15 7.32 o -12 7 1 0.78 -0.28 3.18 o -11 7 1 546.61 529.43 11.43 o -10 7 1 9.25 10.73 1.97 o -9 7 1 368.93 393.99 7.67 o -8 7 1 12.35 13.57 1.91 o -7 7 1 688.43 673.82 11.29 o -6 7 1 1406.68 1400.77 19.07 o -5 7 1 642.56 679.73 9.89 o -4 7 1 2611.42 2716.50 35.93 o -3 7 1 4068.38 4027.17 40.82 o -2 7 1 627.93 650.40 6.12 o -1 7 1 5.01 7.85 0.70 o 0 7 1 65.09 80.18 1.47 o 1 7 1 2116.75 2213.43 21.37 o 2 7 1 7.96 10.04 1.03 o 3 7 1 2106.24 2017.96 26.84 o 4 7 1 33.51 35.38 1.50 o 5 7 1 115.77 116.59 2.62 o 6 7 1 249.99 247.27 4.36 o 7 7 1 1.69 3.19 0.90 o 8 7 1 1026.88 1026.58 16.48 o 9 7 1 1427.10 1404.46 25.50 o 10 7 1 957.72 950.23 19.73 o 11 7 1 0.05 -0.96 6.61 o 12 7 1 114.92 105.77 8.73 o 13 7 1 6.24 4.36 4.62 o -14 8 1 67.32 71.36 7.96 o -13 8 1 57.18 43.12 6.55 o -12 8 1 354.48 362.72 12.46 o -11 8 1 207.93 226.27 19.07 o -10 8 1 24.98 24.39 4.03 o -9 8 1 517.84 541.29 9.83 o -8 8 1 600.93 610.58 10.67 o -7 8 1 5.23 8.37 1.81 o -6 8 1 12.77 12.73 1.34 o -5 8 1 411.91 402.94 6.52 o -4 8 1 394.02 388.69 6.28 o -3 8 1 1261.97 1280.58 14.42 o -2 8 1 1094.03 1170.95 10.54 o -1 8 1 74.89 76.92 1.54 o 0 8 1 758.15 772.89 8.05 o 1 8 1 226.92 232.19 3.22 o 2 8 1 1208.77 1253.06 15.66 o 3 8 1 0.88 4.16 1.21 o 4 8 1 200.20 200.38 3.83 o 5 8 1 271.00 261.90 5.16 o 6 8 1 54.45 45.52 3.22 o 7 8 1 1052.71 1010.84 23.79 o 8 8 1 50.07 55.26 3.74 o 9 8 1 17.65 14.24 3.43 o 10 8 1 19.80 19.54 3.75 o 11 8 1 23.02 30.41 5.52 o 12 8 1 24.97 23.10 5.39 o 13 8 1 46.85 44.27 6.54 o -14 9 1 16.98 19.50 5.52 o -13 9 1 234.03 223.81 12.58 o -12 9 1 389.61 379.11 16.57 o -11 9 1 158.12 179.28 10.98 o -10 9 1 160.65 167.88 13.80 o -9 9 1 80.08 85.09 3.07 o -8 9 1 456.87 446.28 9.33 o -7 9 1 51.06 53.60 2.75 o -6 9 1 31.62 26.80 1.63 o -5 9 1 1059.51 1036.89 14.65 o -4 9 1 1659.25 1652.69 22.31 o -3 9 1 841.42 875.98 9.48 o -2 9 1 155.85 158.93 2.35 o -1 9 1 2611.48 2648.46 22.91 o 0 9 1 1469.24 1472.41 14.51 o 1 9 1 670.29 704.43 7.51 o 2 9 1 39.19 42.18 1.99 o 3 9 1 43.20 38.81 2.48 o 4 9 1 348.40 341.71 5.78 o 5 9 1 813.70 838.45 13.50 o 6 9 1 35.04 39.59 3.22 o 7 9 1 578.66 605.18 12.88 o 8 9 1 82.08 87.67 4.69 o 9 9 1 500.38 535.17 15.30 o 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