#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:35:34 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181258 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/36/2233663.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2233663_Fobs loop_ _publ_author_name 'Zhao, Lei' 'Liu, Bingtao' 'Jin, Guanghua' 'Meng, Xiangru' _publ_section_title ; Diaquabis{1-[(1H-benzimidazol-2-yl)methyl]-1H-1,2,4-triazole-\kN^4^}bis(2,4,5-tricarboxybenzoato-\kO^1^)cadmium dihydrate ; _journal_coeditor_code WM2579 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m139 _journal_page_last m140 _journal_volume 68 _journal_year 2012 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 75.980 _cell_angle_beta 82.550 _cell_angle_gamma 70.600 _cell_length_a 7.7005 _cell_length_b 8.6131 _cell_length_c 17.4600 _exptl_crystal_F_000 554.00 _reflns_d_resolution_high 0.7600 _cod_data_source_file wm2579Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' p in P-1 New: P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 158.15 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1295.92 1274.37 11.84 o 2 0 0 6506.81 6493.86 37.98 o 3 0 0 1366.07 1349.47 10.21 o 4 0 0 2620.46 2507.07 31.10 o 5 0 0 918.78 880.45 9.74 o 6 0 0 274.57 284.75 7.41 o 7 0 0 122.19 120.08 5.74 o 8 0 0 672.82 662.50 20.07 o 9 0 0 196.57 189.09 14.91 o -9 1 0 102.41 100.21 18.80 o -8 1 0 126.60 113.53 9.10 o -7 1 0 86.44 93.86 12.18 o -6 1 0 566.57 556.17 11.77 o -5 1 0 1008.24 949.32 11.23 o -4 1 0 441.15 448.45 5.01 o -3 1 0 7723.21 8061.56 62.68 o -2 1 0 213.90 251.96 3.01 o -1 1 0 824.26 811.45 6.96 o 0 1 0 307.30 257.91 2.35 o 1 1 0 596.84 691.21 6.52 o 2 1 0 11325.00 10890.66 65.33 o 3 1 0 5015.97 4968.64 46.59 o 4 1 0 551.99 485.30 8.94 o 5 1 0 359.00 369.58 6.90 o 6 1 0 1266.04 1227.26 23.80 o 7 1 0 225.09 223.99 7.30 o 8 1 0 149.93 150.88 18.73 o 9 1 0 113.13 120.66 7.56 o -8 2 0 106.23 96.71 34.79 o -7 2 0 319.96 323.36 11.00 o -6 2 0 313.28 350.49 31.28 o -5 2 0 165.48 162.22 4.59 o -4 2 0 25.89 25.47 2.18 o -3 2 0 827.97 899.78 8.47 o -2 2 0 4069.34 4481.41 32.91 o -1 2 0 484.95 326.86 3.30 o 0 2 0 14.49 48.94 3.72 o 1 2 0 3051.29 2956.59 21.61 o 2 2 0 4437.74 4211.92 23.04 o 3 2 0 14457.23 14464.48 92.11 o 4 2 0 1184.32 966.14 14.57 o 5 2 0 80.84 85.61 6.14 o 6 2 0 374.06 392.25 10.35 o 7 2 0 908.37 871.15 19.11 o 8 2 0 132.35 140.56 6.10 o 9 2 0 302.09 298.40 21.10 o -8 3 0 68.72 66.77 22.07 o -7 3 0 90.76 103.53 29.71 o -6 3 0 138.28 170.35 17.89 o -5 3 0 478.54 417.59 8.89 o -4 3 0 252.79 251.16 4.31 o -3 3 0 374.80 357.48 3.94 o -2 3 0 791.73 862.15 8.10 o -1 3 0 177.91 173.21 2.53 o 0 3 0 5847.30 5526.87 31.19 o 1 3 0 1109.80 972.42 10.26 o 2 3 0 4732.07 5097.26 30.82 o 3 3 0 1577.84 1573.55 33.43 o 4 3 0 11064.55 11212.20 111.65 o 5 3 0 9.51 10.36 3.16 o 6 3 0 1869.29 1941.73 30.35 o 7 3 0 377.53 404.03 15.02 o 8 3 0 444.68 466.84 11.60 o 9 3 0 62.14 57.43 18.91 o 10 3 0 224.99 245.72 32.60 o -7 4 0 32.65 38.50 13.14 o -6 4 0 101.64 112.98 8.98 o -5 4 0 418.16 436.36 26.34 o -4 4 0 290.67 252.18 4.59 o -3 4 0 457.69 497.07 6.48 o -2 4 0 192.81 170.36 2.61 o -1 4 0 436.74 418.70 6.54 o 0 4 0 908.84 933.01 12.55 o 1 4 0 2270.93 2452.79 21.59 o 2 4 0 346.31 339.84 7.42 o 3 4 0 217.38 207.38 7.39 o 4 4 0 109.81 79.71 5.65 o 5 4 0 159.48 175.94 7.44 o 6 4 0 101.74 101.66 9.54 o 7 4 0 1562.17 1567.69 23.01 o 8 4 0 18.79 18.81 6.59 o 9 4 0 92.29 96.60 9.82 o 10 4 0 153.16 140.01 10.56 o -7 5 0 262.15 245.52 18.91 o -6 5 0 164.47 177.29 10.79 o -5 5 0 9.64 14.81 5.15 o -4 5 0 655.17 585.79 10.11 o -3 5 0 389.23 391.28 10.84 o -2 5 0 708.97 746.99 10.18 o -1 5 0 179.76 210.17 3.12 o 0 5 0 265.55 223.72 4.96 o 1 5 0 3508.81 3839.70 66.10 o 2 5 0 36.96 38.12 5.32 o 3 5 0 761.58 723.94 12.14 o 4 5 0 568.70 554.11 11.49 o 5 5 0 561.92 584.28 18.35 o 6 5 0 9.58 10.64 3.06 o 7 5 0 106.45 102.37 10.70 o 8 5 0 41.52 62.25 9.05 o 9 5 0 140.42 127.65 8.52 o -6 6 0 95.12 56.21 18.64 o -5 6 0 272.98 236.07 26.13 o -4 6 0 10.41 21.54 8.29 o -3 6 0 472.93 479.47 12.35 o -2 6 0 268.23 286.64 5.12 o -1 6 0 262.42 215.54 4.28 o 0 6 0 392.22 417.44 8.85 o 1 6 0 17.82 13.11 3.39 o 2 6 0 227.86 227.76 11.98 o 3 6 0 1.39 4.88 2.41 o 4 6 0 320.78 298.63 13.21 o 5 6 0 156.39 177.59 14.74 o 6 6 0 403.70 427.90 12.82 o 7 6 0 113.20 108.70 10.78 o 8 6 0 347.82 345.49 19.85 o 9 6 0 37.30 42.29 6.60 o -5 7 0 73.68 83.60 19.82 o -4 7 0 252.94 263.62 14.69 o -3 7 0 242.19 250.90 13.26 o -2 7 0 144.55 154.89 7.38 o -1 7 0 620.55 577.82 16.19 o 0 7 0 504.71 473.21 12.43 o 1 7 0 406.00 379.22 11.72 o 2 7 0 778.77 794.20 15.56 o 3 7 0 324.12 360.80 8.30 o 4 7 0 278.93 287.58 19.72 o 5 7 0 54.84 58.29 9.02 o 6 7 0 262.79 268.32 11.27 o 7 7 0 348.01 399.39 31.16 o 8 7 0 82.41 74.06 7.01 o 9 7 0 27.87 23.49 10.07 o -4 8 0 180.45 206.48 16.15 o -3 8 0 360.63 387.20 15.87 o -2 8 0 311.00 298.09 17.41 o -1 8 0 0.82 2.18 2.83 o 0 8 0 483.06 481.82 15.05 o 1 8 0 255.10 257.11 27.79 o 2 8 0 97.55 95.46 5.19 o 3 8 0 250.34 276.54 9.10 o 4 8 0 197.70 223.76 15.83 o 5 8 0 759.93 745.39 14.74 o 6 8 0 146.33 131.78 10.80 o 7 8 0 188.52 150.94 7.65 o 8 8 0 54.30 50.65 6.74 o -1 9 0 189.79 194.88 9.70 o 0 9 0 379.31 407.44 15.22 o 1 9 0 489.12 501.88 11.73 o 2 9 0 19.83 19.19 4.62 o 3 9 0 645.25 673.12 22.20 o 4 9 0 361.59 385.40 10.15 o 5 9 0 220.21 228.87 8.11 o 6 9 0 83.43 93.57 14.62 o 7 9 0 0.35 4.62 3.15 o 8 9 0 61.44 41.80 11.63 o 0 10 0 354.28 355.60 17.17 o 1 10 0 180.09 188.30 16.08 o 2 10 0 176.81 190.18 11.41 o 3 10 0 84.01 75.45 8.94 o 4 10 0 283.17 282.88 10.36 o 5 10 0 16.28 18.02 3.68 o 6 10 0 134.27 114.42 10.13 o -6 -10 1 80.94 54.66 15.97 o -5 -10 1 15.14 14.52 4.42 o -4 -10 1 178.32 161.31 9.70 o -3 -10 1 301.56 263.06 12.23 o -2 -10 1 101.56 111.34 25.35 o -1 -10 1 200.36 177.47 10.14 o 0 -10 1 97.89 65.12 27.25 o -7 -9 1 87.26 60.26 14.68 o -6 -9 1 48.72 35.99 8.73 o -5 -9 1 241.74 242.26 8.94 o -4 -9 1 242.54 256.05 13.65 o -3 -9 1 309.55 290.76 14.16 o -2 -9 1 20.36 28.77 4.58 o -1 -9 1 156.32 158.57 8.87 o 0 -9 1 299.15 302.75 14.37 o 1 -9 1 346.24 356.48 14.16 o -8 -8 1 164.45 182.82 12.63 o -7 -8 1 106.99 99.87 7.94 o -6 -8 1 54.24 62.00 8.95 o -5 -8 1 1332.73 1315.80 42.65 o -4 -8 1 471.11 520.49 15.27 o -3 -8 1 233.34 249.16 7.12 o -2 -8 1 35.73 33.23 6.54 o -1 -8 1 91.10 92.35 9.24 o 0 -8 1 1351.11 1316.48 35.79 o 1 -8 1 57.06 52.89 10.86 o 2 -8 1 123.76 127.69 7.38 o 4 -8 1 174.36 237.26 20.35 o -9 -7 1 110.82 71.02 18.77 o -8 -7 1 501.00 514.86 16.28 o -7 -7 1 160.77 143.19 9.04 o -6 -7 1 220.88 205.34 6.75 o -5 -7 1 33.90 35.26 8.87 o -4 -7 1 132.70 150.51 6.90 o -3 -7 1 61.31 55.03 7.47 o -2 -7 1 361.05 354.43 9.89 o -1 -7 1 308.37 276.78 8.70 o 0 -7 1 359.85 352.02 10.36 o 1 -7 1 224.50 246.69 10.52 o 2 -7 1 38.48 46.95 15.41 o 3 -7 1 258.88 230.13 10.32 o 4 -7 1 244.12 224.54 29.54 o 5 -7 1 1.78 3.95 5.94 o -9 -6 1 97.53 77.68 12.93 o -8 -6 1 6.22 5.50 2.88 o -7 -6 1 480.67 478.86 13.50 o -6 -6 1 64.55 72.83 13.61 o -5 -6 1 262.24 252.90 9.43 o -4 -6 1 73.94 84.93 14.20 o -3 -6 1 385.61 437.49 12.30 o -2 -6 1 1234.98 1287.65 17.02 o -1 -6 1 890.84 938.82 20.33 o 0 -6 1 2.64 2.50 1.20 o 1 -6 1 522.77 516.12 8.79 o 2 -6 1 37.31 38.55 4.35 o 3 -6 1 252.86 240.99 17.01 o 4 -6 1 129.57 138.27 10.51 o 5 -6 1 95.17 104.60 17.75 o 6 -6 1 203.07 208.50 18.80 o -9 -5 1 158.81 144.48 9.32 o -8 -5 1 67.53 76.85 14.99 o -7 -5 1 5.61 11.28 2.93 o -6 -5 1 19.78 33.44 11.49 o -5 -5 1 364.58 367.12 11.29 o -4 -5 1 1122.56 1132.03 15.58 o -3 -5 1 572.70 550.13 9.89 o -2 -5 1 142.44 141.60 4.51 o -1 -5 1 1350.30 1304.34 24.50 o 0 -5 1 277.45 272.25 7.33 o 1 -5 1 419.35 420.35 8.09 o 2 -5 1 676.76 699.94 9.65 o 3 -5 1 384.86 375.80 8.83 o 4 -5 1 634.79 628.74 16.98 o 5 -5 1 99.18 107.85 24.83 o 6 -5 1 239.43 226.33 33.26 o 7 -5 1 419.86 445.99 30.12 o -9 -4 1 87.27 83.45 10.81 o -8 -4 1 586.05 596.86 15.04 o -7 -4 1 515.23 542.88 15.50 o -6 -4 1 2176.11 2184.12 42.94 o -5 -4 1 1031.52 1047.46 15.09 o -4 -4 1 2992.15 3216.32 75.45 o -3 -4 1 1513.12 1602.02 20.42 o -2 -4 1 1120.83 1076.97 20.47 o -1 -4 1 869.15 795.48 10.39 o 0 -4 1 1090.26 1130.26 13.20 o 1 -4 1 253.77 209.30 3.39 o 2 -4 1 3385.20 3624.93 53.74 o 3 -4 1 50.18 42.63 3.73 o 4 -4 1 437.99 419.98 8.54 o 5 -4 1 185.59 176.54 4.53 o 6 -4 1 0.89 3.46 5.55 o 7 -4 1 115.47 128.04 34.95 o -9 -3 1 155.99 146.81 12.84 o -8 -3 1 174.90 185.80 7.10 o -7 -3 1 709.58 712.69 14.27 o -6 -3 1 723.10 706.36 12.98 o -5 -3 1 313.65 298.99 11.20 o -4 -3 1 596.43 637.53 10.71 o -3 -3 1 1364.39 1411.81 27.00 o -2 -3 1 2237.04 2278.51 19.92 o -1 -3 1 3151.47 3258.37 21.72 o 0 -3 1 120.23 103.09 2.48 o 1 -3 1 556.76 661.24 7.38 o 2 -3 1 1.19 12.38 1.73 o 3 -3 1 181.33 195.31 2.69 o 4 -3 1 47.08 50.86 4.53 o 5 -3 1 862.20 911.55 9.10 o 6 -3 1 176.45 170.50 7.95 o 7 -3 1 49.65 57.46 20.31 o 8 -3 1 176.90 193.53 37.99 o -9 -2 1 70.89 71.24 17.28 o -8 -2 1 285.47 287.84 14.18 o -7 -2 1 917.42 912.19 19.80 o -6 -2 1 106.29 106.59 9.95 o -5 -2 1 991.57 963.06 17.19 o -4 -2 1 31.31 43.13 3.65 o -3 -2 1 1310.83 1430.14 12.49 o -2 -2 1 684.30 693.82 7.26 o -1 -2 1 22.29 49.72 2.58 o 0 -2 1 960.32 794.50 7.36 o 1 -2 1 2989.53 3159.78 16.56 o 2 -2 1 5665.59 5909.68 42.61 o 3 -2 1 1892.38 1933.59 15.64 o 4 -2 1 342.71 301.94 4.02 o 5 -2 1 1056.21 1094.76 14.26 o 6 -2 1 193.62 192.94 5.42 o 7 -2 1 63.17 53.17 6.83 o 8 -2 1 218.84 212.01 29.54 o -9 -1 1 155.09 137.59 15.83 o -8 -1 1 390.52 381.75 17.28 o -7 -1 1 63.44 64.06 8.39 o -6 -1 1 655.79 736.71 14.55 o -5 -1 1 149.53 148.90 5.09 o -4 -1 1 4244.65 4188.36 36.07 o -3 -1 1 5066.51 4737.32 33.58 o 0 -1 1 7482.34 7047.35 62.47 o 1 -1 1 6509.09 6749.74 68.16 o 2 -1 1 15228.71 15232.81 108.44 o 3 -1 1 1864.92 1864.08 20.26 o 4 -1 1 184.97 210.26 4.45 o 5 -1 1 246.71 209.55 9.74 o 6 -1 1 1414.97 1512.57 29.98 o 7 -1 1 747.05 774.36 18.71 o 8 -1 1 324.87 329.11 10.78 o 9 -1 1 168.10 192.88 12.51 o -9 0 1 63.96 45.89 16.20 o -8 0 1 390.42 372.70 14.01 o -7 0 1 402.68 428.32 10.40 o -6 0 1 7.80 7.86 2.30 o -5 0 1 539.20 579.94 6.86 o -4 0 1 2068.96 2116.35 21.71 o -3 0 1 19.29 30.01 2.11 o -2 0 1 355.87 299.95 3.29 o -1 0 1 1238.59 1397.67 8.55 o 1 0 1 1494.85 1517.83 10.44 o 2 0 1 301.76 418.33 4.16 o 3 0 1 156.28 131.53 2.80 o 4 0 1 1427.61 1455.59 18.59 o 5 0 1 1447.64 1441.24 18.85 o 6 0 1 437.65 450.50 11.93 o 7 0 1 87.59 80.32 5.71 o 8 0 1 158.00 146.98 19.88 o 9 0 1 193.81 195.00 15.00 o -9 1 1 208.66 188.80 13.57 o -7 1 1 273.12 258.05 9.73 o -6 1 1 33.45 29.29 4.85 o -5 1 1 1504.44 1562.11 17.87 o -4 1 1 3418.77 3421.59 42.33 o -3 1 1 2547.38 2682.91 20.58 o -2 1 1 1.55 2.27 0.88 o -1 1 1 9416.91 9060.52 55.38 o 0 1 1 22.56 28.68 0.99 o 1 1 1 4273.38 4060.47 21.66 o 2 1 1 1003.16 1283.88 9.99 o 3 1 1 746.73 580.96 5.50 o 4 1 1 297.40 265.24 5.61 o 5 1 1 4554.15 4628.84 64.35 o 6 1 1 674.41 692.24 18.30 o 7 1 1 76.04 80.90 5.08 o 8 1 1 116.81 116.17 9.11 o 9 1 1 57.04 59.51 18.14 o -8 2 1 8.87 7.48 2.00 o -7 2 1 93.09 96.53 7.85 o -6 2 1 793.77 810.34 36.15 o -5 2 1 178.73 161.26 2.19 o -4 2 1 631.08 684.40 7.81 o -3 2 1 21.09 34.03 2.78 o -2 2 1 47.55 30.50 1.55 o -1 2 1 2542.41 2237.60 12.20 o 0 2 1 134.11 158.98 2.19 o 1 2 1 1301.73 1230.39 11.19 o 2 2 1 25011.15 22894.39 309.04 o 3 2 1 3635.47 3388.61 20.99 o 4 2 1 3136.16 3062.32 32.29 o 5 2 1 233.25 247.62 5.48 o 6 2 1 562.56 561.56 14.37 o 7 2 1 531.84 545.87 21.01 o 8 2 1 167.98 176.78 6.69 o 9 2 1 431.91 454.62 13.84 o -8 3 1 57.34 59.27 15.87 o -7 3 1 129.26 135.78 13.16 o -6 3 1 825.53 836.18 45.96 o -5 3 1 64.54 55.64 3.53 o -4 3 1 127.69 140.07 3.77 o -3 3 1 5.36 3.29 0.95 o -2 3 1 321.00 356.04 6.03 o -1 3 1 2564.79 2370.15 15.00 o 0 3 1 135.01 95.88 2.38 o 1 3 1 204.79 234.94 3.65 o 2 3 1 2976.62 3216.22 21.80 o 3 3 1 2766.69 3010.25 25.69 o 4 3 1 402.00 429.65 15.05 o 6 3 1 572.95 583.60 13.50 o 7 3 1 80.50 86.46 7.66 o 8 3 1 779.13 747.74 26.92 o 9 3 1 143.25 122.81 14.03 o 10 3 1 88.34 97.52 25.17 o -7 4 1 43.08 57.93 13.53 o -6 4 1 184.59 178.63 20.52 o -5 4 1 703.25 635.37 16.32 o -4 4 1 43.06 48.35 4.37 o -3 4 1 2158.59 2309.63 23.03 o -2 4 1 234.24 199.72 3.58 o -1 4 1 4275.76 4797.70 42.42 o 0 4 1 4280.61 4347.93 41.76 o 1 4 1 62.92 52.86 5.55 o 2 4 1 1000.71 986.08 13.59 o 3 4 1 2366.09 2414.34 25.56 o 4 4 1 1338.42 1432.85 24.69 o 5 4 1 1160.59 1116.86 20.26 o 6 4 1 34.88 39.73 6.00 o 7 4 1 1160.37 1189.13 17.90 o 8 4 1 53.85 53.22 10.57 o 9 4 1 170.29 183.44 10.97 o 10 4 1 68.22 60.62 15.50 o -7 5 1 16.13 10.40 7.40 o -6 5 1 236.00 233.33 26.20 o -5 5 1 210.11 243.52 26.11 o -4 5 1 363.73 387.35 7.99 o -3 5 1 1185.14 1176.69 22.13 o -2 5 1 62.18 69.82 3.65 o -1 5 1 5.61 2.04 1.70 o 0 5 1 343.92 312.06 4.89 o 1 5 1 4.79 4.06 4.48 o 2 5 1 1046.91 961.47 15.28 o 3 5 1 433.91 414.99 9.13 o 4 5 1 125.90 124.30 6.98 o 5 5 1 235.22 193.47 10.07 o 6 5 1 1776.93 1846.57 17.10 o 7 5 1 56.36 63.78 10.60 o 8 5 1 110.86 121.82 12.92 o 9 5 1 5.19 6.74 3.08 o -6 6 1 267.29 215.81 25.25 o -5 6 1 160.98 148.44 12.39 o -4 6 1 31.37 20.40 8.87 o -3 6 1 429.56 456.24 8.92 o -2 6 1 1128.77 1042.07 18.45 o -1 6 1 36.71 57.98 6.21 o 0 6 1 851.41 811.14 12.88 o 1 6 1 546.78 523.48 12.06 o 2 6 1 528.61 503.36 15.86 o 3 6 1 606.88 576.50 14.73 o 4 6 1 37.79 56.84 8.55 o 5 6 1 101.29 130.73 15.73 o 6 6 1 849.94 804.71 17.92 o 7 6 1 12.00 5.24 3.64 o 8 6 1 91.98 96.37 5.94 o 9 6 1 169.09 179.19 9.48 o -5 7 1 371.19 368.38 18.31 o -4 7 1 60.18 64.24 26.99 o -3 7 1 38.86 33.28 16.08 o -2 7 1 605.64 564.16 11.42 o -1 7 1 438.15 373.09 8.82 o 0 7 1 779.96 783.22 12.85 o 1 7 1 154.73 180.60 11.28 o 2 7 1 30.04 45.97 7.76 o 3 7 1 1549.09 1639.25 35.14 o 4 7 1 298.48 277.14 14.19 o 5 7 1 433.76 429.43 13.29 o 6 7 1 311.65 315.80 15.93 o 7 7 1 382.03 388.31 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124.33 131.75 32.54 o -1 2 21 0.99 4.68 2.94 o 0 2 21 49.56 48.44 10.40 o 1 2 21 10.05 5.56 3.49 o 2 2 21 49.09 31.08 12.29 o 3 2 21 37.19 22.81 9.07 o 4 2 21 27.72 12.90 14.41 o -2 3 21 29.41 19.31 7.54 o -1 3 21 603.24 584.41 36.99 o 0 3 21 120.18 127.94 25.81 o 1 3 21 611.70 680.45 40.80 o 2 3 21 126.39 143.77 9.56 o 3 3 21 594.47 609.56 15.62 o 4 3 21 319.61 349.70 26.07 o 5 3 21 74.59 59.20 17.11 o -1 4 21 217.13 211.31 18.61 o 0 4 21 457.22 421.91 15.75 o 1 4 21 124.22 134.66 10.91 o 2 4 21 119.16 125.81 10.39 o 3 4 21 29.30 23.34 7.67 o 4 4 21 181.70 191.71 22.45 o 5 4 21 144.32 132.92 10.44 o -1 5 21 280.39 308.04 40.41 o 0 5 21 91.23 73.64 35.81 o 1 5 21 2.41 7.63 3.58 o 2 5 21 150.62 151.66 17.63 o 3 5 21 65.56 49.70 9.83 o 4 5 21 140.79 134.70 25.38 o 5 5 21 0.69 7.78 5.07 o 0 6 21 82.41 59.46 28.13 o 1 6 21 125.27 117.35 15.25 o 2 6 21 200.96 205.73 24.41 o 3 6 21 611.74 562.74 27.38 o 4 6 21 44.61 45.58 16.46 o -1 0 22 152.57 138.55 14.85 o 0 0 22 193.45 229.52 40.07 o 1 0 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