#------------------------------------------------------------------------------ #$Date: 2012-09-11 12:26:43 +0300 (Tue, 11 Sep 2012) $ #$Revision: 66590 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/45/2234546.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2234546_Fobs loop_ _publ_author_name 'W\"ohlert, Susanne' 'Wriedt, Mario' 'Jess, Inke' 'N\"ather, Christian' _publ_section_title ; Bis(dicyanamido-\kN)tetrakis(pyridazine-\kN)nickel(II) ; _journal_coeditor_code BT5900 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m696 _journal_volume 68 _journal_year 2012 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 81.364 _cell_angle_beta 66.027 _cell_angle_gamma 84.879 _cell_length_a 8.1796 _cell_length_b 8.4125 _cell_length_c 8.9643 _exptl_crystal_F_000 262.00 _reflns_d_resolution_high 0.8101 _[local]_cod_data_source_file bt5900Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Ni(dca)2(pyridazine)4 in P-1 at 170 K (ss551)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 81.81 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1547.19 1579.64 52.73 o 2 0 0 1.20 33.09 36.90 o 3 0 0 278.61 302.08 27.94 o 4 0 0 366.20 334.48 29.87 o 5 0 0 33.57 -175.79 203.71 o 6 0 0 5.32 -25.01 25.01 o 7 0 0 125.48 107.41 17.72 o 8 0 0 72.65 98.25 16.39 o 9 0 0 10.81 15.97 25.16 o -9 1 0 11.49 36.80 15.04 o -8 1 0 46.19 14.54 28.12 o -7 1 0 21.44 -14.71 47.71 o -6 1 0 56.18 56.50 20.69 o -5 1 0 243.81 223.66 22.22 o -4 1 0 75.18 78.20 23.30 o -3 1 0 1652.36 1602.77 24.47 o -2 1 0 3632.62 3827.06 37.59 o -1 1 0 86.23 55.03 38.47 o 0 1 0 1707.54 1540.10 43.84 o 1 1 0 93.18 69.77 35.96 o 2 1 0 3709.86 3670.49 37.94 o 3 1 0 457.42 404.25 21.51 o 4 1 0 178.31 142.88 27.69 o 5 1 0 370.40 570.43 130.54 o 6 1 0 24.84 -13.62 20.16 o 7 1 0 283.33 290.45 34.51 o 8 1 0 131.25 119.32 18.14 o 9 1 0 48.64 14.44 31.14 o -8 2 0 51.85 67.35 20.66 o -7 2 0 286.39 325.53 19.12 o -6 2 0 199.36 213.92 17.69 o -5 2 0 240.95 262.62 16.72 o -4 2 0 121.96 114.45 27.09 o -3 2 0 1450.16 1455.64 22.80 o -2 2 0 351.17 382.95 40.60 o -1 2 0 989.14 963.12 31.48 o 0 2 0 516.03 462.43 31.41 o 1 2 0 842.55 786.14 31.89 o 2 2 0 160.20 141.96 22.44 o 3 2 0 1618.75 1559.43 36.29 o 4 2 0 2299.24 2342.15 57.65 o 5 2 0 728.78 784.66 26.46 o 6 2 0 79.88 68.51 21.47 o 7 2 0 483.20 536.69 21.47 o 8 2 0 156.35 166.66 18.19 o 9 2 0 16.23 -11.99 16.29 o -8 3 0 32.38 28.38 15.80 o -7 3 0 158.74 155.66 33.20 o -6 3 0 30.11 38.33 17.88 o -5 3 0 259.77 292.93 16.27 o -4 3 0 3.03 -6.32 19.57 o -3 3 0 249.89 249.03 18.14 o -2 3 0 179.19 136.10 34.01 o -1 3 0 50.38 30.90 21.10 o 0 3 0 278.36 302.07 32.32 o 1 3 0 2177.62 2043.02 24.31 o 2 3 0 766.21 707.97 37.00 o 3 3 0 189.37 161.32 61.92 o 4 3 0 824.71 857.62 19.68 o 5 3 0 1544.92 1580.81 31.74 o 6 3 0 565.92 564.40 34.07 o 7 3 0 5.87 12.90 18.44 o 8 3 0 39.80 14.88 16.58 o -8 4 0 18.34 26.22 15.74 o -7 4 0 141.58 109.56 14.23 o -6 4 0 7.87 17.19 48.77 o -5 4 0 200.41 204.14 21.53 o -4 4 0 128.65 164.02 20.68 o -3 4 0 178.56 178.62 21.76 o -2 4 0 468.51 466.69 18.83 o -1 4 0 228.95 252.58 24.36 o 0 4 0 379.17 366.61 23.65 o 1 4 0 1098.25 1021.34 21.74 o 2 4 0 7.80 -9.78 17.27 o 3 4 0 158.21 153.26 32.40 o 4 4 0 351.29 379.68 16.87 o 5 4 0 3.33 7.56 19.48 o 6 4 0 56.02 33.54 18.22 o 7 4 0 4.86 56.62 38.81 o 8 4 0 542.65 520.25 18.23 o -7 5 0 248.08 214.75 28.40 o -6 5 0 114.79 77.37 18.81 o -5 5 0 37.70 37.61 15.15 o -4 5 0 19.05 53.73 23.13 o -3 5 0 32.79 31.68 20.31 o -2 5 0 1380.31 1408.45 23.73 o -1 5 0 471.46 474.18 18.00 o 0 5 0 37.82 30.41 21.25 o 1 5 0 85.42 62.48 21.08 o 2 5 0 82.47 77.03 18.91 o 3 5 0 1.06 -12.16 15.75 o 4 5 0 83.49 129.38 18.18 o 5 5 0 84.82 100.46 16.96 o 6 5 0 714.79 695.27 16.79 o 7 5 0 3.73 10.38 14.68 o 8 5 0 274.86 274.75 19.56 o -7 6 0 7.57 18.71 23.55 o -6 6 0 19.55 46.20 20.17 o -5 6 0 107.70 100.83 14.38 o -4 6 0 459.30 504.45 19.02 o -3 6 0 80.29 67.57 19.42 o -2 6 0 99.73 120.49 16.43 o -1 6 0 0.79 2.95 16.35 o 0 6 0 121.22 128.56 16.58 o 1 6 0 273.42 301.59 18.45 o 2 6 0 43.36 37.62 18.13 o 3 6 0 147.67 163.72 18.19 o 4 6 0 60.59 84.24 19.76 o 5 6 0 210.40 192.14 15.21 o 6 6 0 151.79 166.25 16.38 o 7 6 0 11.84 -2.63 31.97 o -6 7 0 241.28 265.21 16.29 o -5 7 0 35.61 98.04 31.81 o -4 7 0 97.11 82.68 16.27 o -3 7 0 80.21 104.08 17.10 o -2 7 0 130.16 141.64 21.03 o -1 7 0 137.59 157.69 19.39 o 0 7 0 30.75 14.21 15.55 o 1 7 0 198.31 192.52 15.55 o 2 7 0 219.39 224.97 15.38 o 3 7 0 424.57 438.61 16.55 o 4 7 0 1.65 4.01 12.48 o 5 7 0 41.79 28.92 15.77 o 6 7 0 36.37 15.50 16.49 o -5 8 0 40.47 26.16 22.33 o -4 8 0 68.00 120.65 26.29 o -3 8 0 47.92 82.97 27.25 o -2 8 0 143.95 158.93 11.53 o -1 8 0 323.72 341.85 17.64 o 0 8 0 23.49 28.66 13.59 o 1 8 0 90.90 94.53 13.57 o 2 8 0 10.49 23.10 14.68 o 3 8 0 166.87 192.35 16.01 o 4 8 0 79.43 102.54 28.12 o 5 8 0 20.60 7.16 19.21 o 6 8 0 0.43 -10.97 18.25 o -4 9 0 56.05 73.59 17.10 o -3 9 0 54.61 73.85 24.81 o -2 9 0 72.44 118.59 19.35 o -1 9 0 33.82 30.84 16.97 o 0 9 0 18.96 -9.79 15.33 o 1 9 0 268.54 267.13 15.65 o 2 9 0 91.43 126.70 19.60 o 3 9 0 22.43 4.63 19.19 o 4 9 0 10.63 1.07 21.52 o -1 10 0 141.15 133.41 13.93 o 0 10 0 80.17 28.53 13.99 o 1 10 0 28.68 13.24 16.03 o 2 10 0 23.12 16.62 18.08 o -1 -10 1 80.09 12.74 16.70 o 0 -10 1 36.48 40.82 11.75 o 1 -10 1 116.17 100.97 48.83 o -4 -9 1 0.58 13.84 17.98 o -3 -9 1 118.56 126.53 15.79 o -2 -9 1 56.04 70.83 16.12 o -1 -9 1 59.11 73.51 14.84 o 0 -9 1 44.64 52.64 13.02 o 1 -9 1 109.00 105.40 22.08 o 2 -9 1 70.92 67.10 23.88 o 3 -9 1 52.78 48.52 17.48 o 4 -9 1 104.11 65.57 24.37 o -5 -8 1 33.17 40.49 15.39 o -4 -8 1 5.21 16.95 19.46 o -3 -8 1 91.96 92.55 39.44 o -2 -8 1 165.13 153.39 13.85 o -1 -8 1 312.95 312.77 16.75 o 0 -8 1 125.44 157.41 11.78 o 1 -8 1 35.45 29.47 16.39 o 2 -8 1 265.67 275.99 16.36 o 3 -8 1 89.23 99.58 19.35 o 4 -8 1 64.43 94.55 18.64 o 5 -8 1 8.20 23.25 15.70 o -6 -7 1 182.58 186.90 13.99 o -5 -7 1 115.07 122.64 33.34 o -4 -7 1 74.91 66.17 18.40 o -3 -7 1 268.44 267.78 15.39 o -2 -7 1 265.60 226.48 25.91 o -1 -7 1 160.10 146.99 12.96 o 0 -7 1 120.94 99.71 15.21 o 1 -7 1 191.47 196.78 18.54 o 2 -7 1 168.86 149.07 28.21 o 3 -7 1 7.65 -5.53 17.09 o 4 -7 1 122.20 144.49 16.27 o 5 -7 1 272.36 277.97 35.78 o 6 -7 1 101.41 71.65 17.58 o -7 -6 1 2.01 -1.98 17.38 o -6 -6 1 114.61 119.26 17.41 o -5 -6 1 176.42 176.15 15.10 o -4 -6 1 452.78 459.29 16.73 o -3 -6 1 52.68 45.84 20.43 o -2 -6 1 3.09 -17.21 17.90 o -1 -6 1 231.37 265.49 16.45 o 0 -6 1 1.86 -3.35 16.18 o 1 -6 1 31.44 54.44 19.75 o 2 -6 1 570.73 569.03 20.63 o 3 -6 1 547.97 528.75 21.04 o 4 -6 1 132.69 113.90 18.07 o 5 -6 1 116.01 109.95 23.34 o 6 -6 1 30.91 32.09 14.60 o 7 -6 1 179.75 186.61 19.32 o -7 -5 1 10.64 21.33 24.16 o -6 -5 1 91.17 105.46 16.79 o -5 -5 1 52.06 43.44 15.56 o -4 -5 1 13.91 22.10 20.40 o -3 -5 1 19.95 28.73 21.87 o -2 -5 1 158.52 173.49 19.12 o -1 -5 1 1037.77 1067.91 21.68 o 0 -5 1 55.95 58.04 14.68 o 1 -5 1 321.49 341.09 25.01 o 2 -5 1 388.22 390.26 17.65 o 3 -5 1 584.09 641.03 30.29 o 4 -5 1 185.91 131.85 28.63 o 5 -5 1 280.50 298.99 16.25 o 6 -5 1 12.34 11.09 12.74 o 7 -5 1 128.98 95.74 17.14 o 8 -5 1 61.47 31.49 13.21 o -8 -4 1 47.19 24.71 20.00 o -7 -4 1 72.48 89.21 21.92 o -6 -4 1 76.57 26.55 16.49 o -5 -4 1 1.84 -3.42 15.83 o -4 -4 1 294.57 294.36 18.54 o -3 -4 1 293.62 275.47 23.24 o -2 -4 1 195.64 204.15 28.88 o -1 -4 1 856.55 840.13 24.57 o 0 -4 1 1135.66 1233.81 25.82 o 1 -4 1 99.51 139.36 51.88 o 2 -4 1 129.34 140.53 31.21 o 3 -4 1 808.38 825.57 32.00 o 4 -4 1 0.90 -3.05 17.89 o 5 -4 1 60.07 76.76 17.52 o 6 -4 1 169.07 178.15 28.95 o 7 -4 1 163.11 194.55 12.76 o 8 -4 1 23.98 23.63 15.55 o -8 -3 1 108.13 86.39 14.84 o -7 -3 1 157.86 138.91 15.74 o -6 -3 1 9.12 -3.06 14.97 o -5 -3 1 431.43 475.30 40.04 o -4 -3 1 474.47 477.34 21.21 o -3 -3 1 140.20 163.60 18.81 o -2 -3 1 212.46 154.24 20.71 o -1 -3 1 5.39 127.18 120.93 o 0 -3 1 2751.91 2771.62 28.47 o 1 -3 1 6.09 3.16 20.47 o 2 -3 1 14.76 4.95 23.71 o 3 -3 1 12.23 -1.61 23.26 o 4 -3 1 22.16 38.79 16.63 o 5 -3 1 325.25 364.70 47.87 o 6 -3 1 122.19 104.09 12.86 o 7 -3 1 181.75 151.63 11.80 o 8 -3 1 267.52 263.07 13.30 o 9 -3 1 48.34 20.96 11.46 o -8 -2 1 112.97 117.93 17.74 o -7 -2 1 475.96 442.09 20.32 o -6 -2 1 409.78 414.37 24.62 o -5 -2 1 336.91 299.83 25.10 o -4 -2 1 184.28 211.43 26.17 o -3 -2 1 184.62 247.93 96.92 o -2 -2 1 14.96 6.98 19.56 o -1 -2 1 913.49 934.21 32.03 o 0 -2 1 4259.16 4270.44 97.36 o 1 -2 1 2483.66 2441.50 96.42 o 2 -2 1 11.74 -10.54 28.34 o 3 -2 1 1777.39 1722.61 37.86 o 4 -2 1 1492.47 1449.81 41.29 o 5 -2 1 361.49 414.34 20.17 o 6 -2 1 66.94 53.29 19.80 o 7 -2 1 284.97 274.96 17.96 o 8 -2 1 63.86 45.88 36.12 o 9 -2 1 0.62 0.49 13.39 o -8 -1 1 183.25 184.20 18.12 o -7 -1 1 187.34 205.94 14.99 o -6 -1 1 205.04 237.12 16.79 o -5 -1 1 558.98 598.47 18.88 o -4 -1 1 390.07 365.92 19.62 o -3 -1 1 652.57 622.17 17.99 o -2 -1 1 28.17 34.94 19.54 o -1 -1 1 1527.68 1452.52 55.69 o 0 -1 1 1788.28 1607.16 46.01 o 2 -1 1 4771.15 4652.94 52.47 o 3 -1 1 499.98 464.75 19.67 o 4 -1 1 214.05 205.53 39.49 o 5 -1 1 355.50 386.46 25.73 o 6 -1 1 7.51 35.15 20.37 o 7 -1 1 105.73 105.91 15.84 o 8 -1 1 48.17 5.37 16.07 o 9 -1 1 21.38 19.15 17.41 o -8 0 1 82.61 58.76 18.11 o -7 0 1 206.54 210.67 14.78 o -6 0 1 101.32 123.50 16.89 o -5 0 1 122.18 160.16 21.13 o -4 0 1 121.13 137.88 27.88 o -3 0 1 4952.44 5288.43 28.66 o -2 0 1 2701.23 2659.77 32.21 o -1 0 1 823.84 789.88 41.64 o 1 0 1 2105.51 1933.54 50.00 o 2 0 1 217.31 233.81 33.34 o 3 0 1 60.25 58.00 19.60 o 4 0 1 109.72 66.45 48.38 o 5 0 1 85.70 59.27 22.04 o 6 0 1 1.24 -20.78 20.78 o 7 0 1 188.68 201.75 18.72 o 8 0 1 122.52 145.25 16.26 o 9 0 1 63.50 63.57 21.32 o -8 1 1 1.68 3.81 18.01 o -7 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27.67 17.64 o -7 3 1 140.04 123.56 12.62 o -6 3 1 7.33 5.16 14.38 o -5 3 1 39.94 16.71 17.48 o -4 3 1 263.77 231.75 19.72 o -3 3 1 20.99 42.79 27.79 o -2 3 1 690.17 639.94 37.31 o -1 3 1 228.60 201.58 18.10 o 0 3 1 794.54 700.65 23.91 o 1 3 1 2144.03 2033.19 31.15 o 2 3 1 3103.27 3072.42 26.80 o 3 3 1 2567.02 2556.35 74.25 o 4 3 1 388.34 338.73 26.84 o 5 3 1 280.73 293.70 20.97 o 6 3 1 425.27 445.79 17.90 o 7 3 1 222.70 222.00 27.93 o 8 3 1 29.26 43.49 36.08 o 9 3 1 35.09 26.03 28.05 o -8 4 1 33.71 25.50 11.29 o -7 4 1 46.23 68.01 16.01 o -6 4 1 244.77 235.85 37.65 o -5 4 1 178.65 213.04 39.86 o -4 4 1 191.96 208.30 22.32 o -3 4 1 6.03 38.36 29.11 o -2 4 1 223.51 236.22 26.54 o -1 4 1 67.77 102.40 31.38 o 0 4 1 526.82 506.37 23.90 o 1 4 1 1647.86 1606.58 61.19 o 2 4 1 505.94 522.82 39.63 o 3 4 1 684.06 700.29 24.93 o 4 4 1 129.75 106.72 19.34 o 5 4 1 340.21 347.99 20.22 o 6 4 1 148.69 169.44 16.10 o 7 4 1 8.12 20.82 16.25 o 8 4 1 150.01 147.79 17.99 o -7 5 1 29.06 39.18 23.54 o -6 5 1 136.23 107.67 13.82 o -5 5 1 1.18 5.52 13.18 o -4 5 1 102.16 101.31 15.02 o -3 5 1 140.82 137.60 20.20 o -2 5 1 262.08 278.71 15.03 o -1 5 1 365.63 392.49 17.74 o 0 5 1 0.92 17.90 17.22 o 1 5 1 4.21 16.57 28.05 o 2 5 1 12.04 24.88 16.94 o 3 5 1 815.24 825.81 31.92 o 4 5 1 62.48 67.05 22.05 o 5 5 1 366.78 359.56 18.21 o 6 5 1 591.97 590.25 16.83 o 7 5 1 441.60 348.82 47.52 o 8 5 1 35.71 19.13 20.78 o -6 6 1 81.60 49.78 30.73 o -5 6 1 6.26 4.59 18.28 o -4 6 1 104.80 121.11 22.60 o -3 6 1 192.82 223.86 26.77 o -2 6 1 309.91 310.84 22.26 o -1 6 1 191.14 207.36 20.11 o 0 6 1 42.86 48.57 14.34 o 1 6 1 289.77 303.79 14.85 o 2 6 1 70.15 98.02 30.02 o 3 6 1 224.99 209.17 17.38 o 4 6 1 160.28 218.11 20.66 o 5 6 1 218.18 235.65 16.14 o 6 6 1 160.08 141.09 34.57 o 7 6 1 258.46 272.45 16.83 o 8 6 1 28.01 34.64 15.62 o -6 7 1 121.90 97.20 28.84 o -5 7 1 118.96 112.21 16.79 o -4 7 1 138.30 169.71 27.91 o -3 7 1 5.55 0.19 16.96 o -2 7 1 70.75 74.26 23.75 o -1 7 1 255.14 261.87 16.48 o 0 7 1 182.19 170.33 16.07 o 1 7 1 301.56 337.78 16.28 o 2 7 1 3.54 -8.42 18.63 o 3 7 1 5.62 -4.65 15.19 o 4 7 1 80.65 98.51 17.58 o 5 7 1 22.39 12.71 17.15 o 6 7 1 130.37 175.64 32.12 o 7 7 1 80.30 65.19 22.21 o -5 8 1 53.39 40.62 25.61 o -4 8 1 119.71 65.52 26.30 o -3 8 1 2.46 -0.39 19.02 o -2 8 1 165.00 172.55 13.38 o -1 8 1 38.79 49.21 23.46 o 0 8 1 4.72 9.53 32.19 o 1 8 1 45.02 28.89 13.58 o 2 8 1 172.58 159.25 13.87 o 3 8 1 81.41 84.61 20.47 o 4 8 1 95.22 87.99 13.51 o 5 8 1 6.40 23.65 20.40 o 6 8 1 8.20 13.60 15.39 o -3 9 1 3.35 -4.69 17.35 o -2 9 1 110.81 86.13 14.81 o -1 9 1 51.86 46.69 15.00 o 0 9 1 71.45 70.70 15.40 o 1 9 1 45.48 46.88 15.40 o 2 9 1 178.57 115.89 24.22 o 3 9 1 39.59 59.19 19.05 o 4 9 1 39.08 27.11 19.07 o 5 9 1 2.34 23.80 18.14 o -1 10 1 126.63 121.51 28.97 o 0 10 1 134.03 134.08 12.28 o 1 10 1 6.18 -13.37 20.24 o 2 10 1 31.97 38.42 24.84 o 3 10 1 16.09 5.88 19.08 o -3 -9 2 7.12 -11.22 12.73 o -2 -9 2 68.52 63.44 16.45 o -1 -9 2 112.85 108.68 14.46 o 0 -9 2 54.94 23.70 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66.90 18.45 o 2 0 9 246.56 223.37 32.37 o 3 0 9 81.54 86.40 27.77 o 4 0 9 1.71 16.51 16.13 o 5 0 9 368.88 381.70 20.40 o 6 0 9 35.56 53.39 20.33 o 7 0 9 49.51 41.19 13.82 o 8 0 9 42.89 47.21 15.07 o 2 1 9 258.07 250.37 20.99 o 3 1 9 196.61 189.38 17.11 o 4 1 9 52.75 46.65 16.74 o 5 1 9 360.30 338.92 19.63 o 6 1 9 224.85 229.99 17.28 o 7 1 9 137.49 139.39 18.27 o 8 1 9 75.49 54.68 19.04 o 0 2 9 22.51 34.44 33.48 o 1 2 9 26.56 14.94 24.11 o 2 2 9 157.20 148.07 17.97 o 3 2 9 250.72 245.56 14.33 o 4 2 9 271.92 247.58 17.26 o 5 2 9 228.15 227.05 23.42 o 6 2 9 289.50 281.24 17.23 o 7 2 9 219.33 234.07 18.28 o 8 2 9 63.11 47.49 15.77 o -1 3 9 1.33 -0.58 23.90 o 0 3 9 92.88 99.72 20.34 o 1 3 9 6.08 16.82 18.92 o 2 3 9 30.05 28.24 19.49 o 3 3 9 77.16 70.10 13.68 o 4 3 9 84.19 75.50 24.59 o 5 3 9 68.15 77.73 20.27 o 6 3 9 229.60 230.32 21.63 o 7 3 9 72.46 85.69 17.03 o 8 3 9 0.57 -8.37 19.88 o -1 4 9 13.43 -3.21 23.58 o 0 4 9 93.35 105.77 18.11 o 1 4 9 122.04 123.03 15.42 o 2 4 9 34.19 24.61 13.45 o 3 4 9 21.98 -6.92 19.40 o 4 4 9 25.10 11.51 19.52 o 5 4 9 0.88 -17.57 17.57 o 6 4 9 79.53 81.01 20.66 o 7 4 9 171.63 178.68 17.04 o 8 4 9 170.45 180.94 14.47 o 0 5 9 78.04 60.30 17.20 o 1 5 9 47.74 43.32 14.65 o 2 5 9 0.75 11.42 18.13 o 3 5 9 165.29 173.12 21.84 o 4 5 9 71.88 70.42 20.07 o 5 5 9 17.45 44.80 29.01 o 6 5 9 5.70 -3.03 19.43 o 7 5 9 28.27 -4.70 19.04 o 1 6 9 95.62 32.09 23.03 o 2 6 9 134.47 106.37 37.13 o 3 6 9 144.59 124.78 21.29 o 4 6 9 25.88 5.99 19.03 o 5 6 9 9.31 -7.67 15.00 o 6 6 9 36.94 27.31 14.96 o 2 7 9 29.85 7.51 17.85 o 3 7 9 27.51 39.83 17.92 o 4 7 9 98.56 104.48 18.50 o 5 7 9 43.17 52.73 14.45 o 4 -2 10 54.79 50.71 21.79 o 5 -2 10 332.64 323.08 16.02 o 6 -2 10 0.53 -0.25 16.20 o 3 -1 10 106.79 99.70 22.50 o 4 -1 10 1.52 -11.82 25.38 o 5 -1 10 21.70 9.19 25.96 o 6 -1 10 44.79 29.55 18.65 o 3 0 10 47.96 62.73 31.04 o 4 0 10 24.55 34.25 25.77 o 5 0 10 17.83 4.24 26.54 o 6 0 10 51.93 41.09 19.06 o 7 0 10 64.52 44.96 16.59 o 2 1 10 112.03 112.96 31.38 o 3 1 10 125.29 125.38 31.96 o 4 1 10 57.51 69.34 19.03 o 5 1 10 38.85 51.95 18.90 o 6 1 10 211.88 181.41 27.41 o 7 1 10 125.34 128.72 27.49 o 1 2 10 136.72 153.94 38.65 o 2 2 10 48.61 49.65 22.63 o 3 2 10 200.55 202.05 19.41 o 4 2 10 158.77 154.31 19.34 o 5 2 10 148.63 151.90 25.27 o 6 2 10 95.40 121.40 18.59 o 7 2 10 65.06 59.91 12.85 o 1 3 10 38.44 43.12 21.58 o 2 3 10 148.19 154.75 18.56 o 3 3 10 491.92 470.49 19.87 o 4 3 10 101.04 97.34 20.67 o 5 3 10 23.27 45.68 33.86 o 6 3 10 46.21 39.29 23.20 o 7 3 10 69.69 86.51 14.55 o 1 4 10 32.24 19.37 21.08 o 2 4 10 5.77 9.13 17.17 o 3 4 10 45.17 35.46 17.81 o 4 4 10 135.77 146.68 30.03 o 5 4 10 193.26 176.48 15.14 o 6 4 10 188.81 149.70 18.17 o 2 5 10 32.64 49.70 13.72 o 3 5 10 19.65 25.36 13.92 o 4 5 10 62.55 34.54 17.32 o 5 5 10 40.47 45.62 19.02 o 6 5 10 193.27 160.76 20.58 o 4 1 11 3.53 2.25 23.52 o 4 2 11 99.89 69.74 23.14 o 5 2 11 57.48 47.57 17.37 o