#------------------------------------------------------------------------------ #$Date: 2012-09-11 12:26:43 +0300 (Tue, 11 Sep 2012) $ #$Revision: 66590 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/45/2234568.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2234568_Fobs loop_ _publ_author_name 'Zhang, Guo-Chun' 'Qiao, Cheng-Fang' 'Zhou, Chun-Sheng' 'Xia, Zheng-Qiang' _publ_section_title ; 2-(5-Amino-2H-tetrazol-2-yl)acetic acid ; _journal_coeditor_code CV5277 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1330 _journal_volume 68 _journal_year 2012 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 90.850 _cell_angle_gamma 90.000 _cell_length_a 18.3812 _cell_length_b 4.4429 _cell_length_c 14.8456 _exptl_crystal_F_000 592.00 _reflns_d_resolution_high 0.8108 _[local]_cod_data_source_file cv5277Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' xb4776_0m in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 216.45 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 801.01 601.54 15.06 o 4 0 0 31881.38 28285.19 557.87 o 6 0 0 9305.26 8361.61 120.15 o 8 0 0 1599.10 1653.84 29.51 o 10 0 0 101.57 83.42 3.77 o 12 0 0 2218.18 2295.87 42.14 o 14 0 0 220.96 233.64 11.67 o 16 0 0 223.82 246.67 13.11 o 18 0 0 545.43 505.59 27.54 o 20 0 0 2.64 -0.43 5.59 o 22 0 0 117.55 156.19 21.08 o 1 1 0 4280.69 4286.94 92.94 o 3 1 0 1945.42 2032.80 34.22 o 5 1 0 1525.35 1471.23 21.59 o 7 1 0 1040.59 1103.39 13.67 o 9 1 0 269.09 266.62 5.79 o 11 1 0 187.65 190.03 5.41 o 13 1 0 0.95 3.93 2.22 o 15 1 0 17.16 7.25 2.87 o 17 1 0 19.58 22.12 4.83 o 19 1 0 0.16 -0.33 3.92 o 21 1 0 2.27 -0.75 4.65 o 0 2 0 1775.18 1718.56 46.47 o 2 2 0 78.96 101.83 13.34 o 4 2 0 159.05 145.87 12.91 o 6 2 0 514.19 522.10 15.34 o 8 2 0 242.12 308.75 12.05 o 10 2 0 487.09 447.02 9.23 o 12 2 0 241.96 271.57 10.81 o 14 2 0 120.01 108.46 6.93 o 16 2 0 208.26 190.15 11.46 o 18 2 0 82.35 83.06 8.32 o 20 2 0 3.91 0.43 5.16 o 1 3 0 744.86 752.67 21.73 o 3 3 0 2077.14 2177.66 50.13 o 5 3 0 75.13 58.73 8.18 o 7 3 0 4.38 -1.45 3.18 o 9 3 0 16.41 16.97 7.75 o 11 3 0 372.31 394.24 11.07 o 13 3 0 218.34 250.82 15.68 o 15 3 0 15.55 29.64 6.82 o 17 3 0 84.16 84.16 10.64 o 0 4 0 282.40 345.09 22.37 o 2 4 0 10.09 0.76 4.40 o 4 4 0 189.23 208.28 14.43 o 6 4 0 131.50 141.27 12.56 o 8 4 0 129.62 122.91 11.85 o 10 4 0 169.16 157.46 13.98 o 12 4 0 23.05 27.25 6.82 o 14 4 0 41.01 50.77 15.06 o 1 5 0 61.47 73.04 10.16 o 3 5 0 42.41 48.17 9.19 o 5 5 0 22.82 28.14 7.41 o 7 5 0 35.84 25.21 7.72 o 9 5 0 0.60 -1.29 7.75 o -21 1 1 117.47 102.33 16.14 o -19 1 1 124.56 114.07 9.48 o -17 1 1 2.82 4.83 2.88 o -15 1 1 570.82 572.73 14.60 o -13 1 1 39.32 40.76 4.16 o -11 1 1 717.81 813.75 18.69 o -9 1 1 882.99 836.94 11.79 o -7 1 1 91.27 83.35 4.24 o -5 1 1 171.67 153.65 4.39 o -3 1 1 46851.85 42970.66 627.64 o -1 1 1 2540.97 2350.22 54.22 o 1 1 1 15710.14 15208.52 178.25 o 3 1 1 2798.01 2599.92 28.78 o 5 1 1 936.52 934.76 11.25 o 7 1 1 536.22 543.72 7.46 o 9 1 1 1361.25 1469.25 15.84 o 11 1 1 63.20 64.12 3.09 o 13 1 1 613.80 630.01 12.89 o 15 1 1 460.67 439.51 19.02 o 17 1 1 20.13 30.57 6.29 o 19 1 1 99.45 100.35 21.08 o 21 1 1 14.77 9.90 8.82 o -20 2 1 14.52 17.13 5.52 o -18 2 1 8.74 15.69 4.87 o -16 2 1 95.62 82.09 7.83 o -14 2 1 141.23 155.82 8.33 o -12 2 1 15.37 14.40 3.25 o -10 2 1 63.80 73.12 5.23 o -8 2 1 19.87 24.59 3.62 o -6 2 1 970.08 1049.48 24.33 o -4 2 1 53.16 47.94 5.45 o -2 2 1 328.44 331.17 11.26 o 0 2 1 920.12 905.74 20.68 o 2 2 1 461.82 402.37 12.46 o 4 2 1 353.58 342.29 15.49 o 6 2 1 227.26 260.64 23.02 o 8 2 1 1381.39 1451.77 25.76 o 10 2 1 51.33 53.98 3.85 o 12 2 1 38.90 42.45 3.77 o 14 2 1 140.84 150.54 14.42 o 16 2 1 51.39 44.66 6.17 o 18 2 1 7.15 10.28 4.37 o 20 2 1 73.70 60.23 9.99 o -17 3 1 0.01 0.51 4.48 o -15 3 1 22.42 27.75 6.44 o -13 3 1 109.31 103.44 8.38 o -11 3 1 18.25 13.98 4.31 o -9 3 1 496.07 491.87 18.80 o -7 3 1 226.83 239.24 21.08 o -5 3 1 84.49 75.85 7.89 o -3 3 1 652.58 693.04 20.68 o -1 3 1 20.14 21.98 4.71 o 1 3 1 0.47 -1.17 3.66 o 3 3 1 64.37 67.12 7.11 o 5 3 1 13.40 8.84 4.03 o 7 3 1 262.84 197.66 23.67 o 9 3 1 93.89 84.09 6.86 o 11 3 1 272.75 254.17 11.10 o 13 3 1 0.28 -3.35 3.81 o 15 3 1 201.98 232.98 16.22 o 17 3 1 8.35 -1.68 5.57 o -14 4 1 17.00 35.71 12.48 o -12 4 1 0.16 6.13 5.97 o -10 4 1 150.20 132.32 12.68 o -8 4 1 70.23 66.79 12.05 o -6 4 1 13.80 15.87 13.55 o -4 4 1 40.81 23.86 9.25 o -2 4 1 13.67 11.52 5.38 o 0 4 1 131.62 96.39 9.88 o 2 4 1 3.35 0.09 6.02 o 4 4 1 23.75 23.55 6.41 o 6 4 1 5.23 5.47 4.94 o 8 4 1 127.59 133.87 12.25 o 10 4 1 56.29 41.52 6.20 o 12 4 1 76.71 71.09 12.91 o 14 4 1 92.65 105.85 18.93 o -9 5 1 5.67 2.15 8.18 o -7 5 1 4.07 2.70 8.18 o -5 5 1 0.55 -5.57 4.71 o -3 5 1 8.73 12.64 6.41 o -1 5 1 9.20 13.64 6.49 o 1 5 1 13.35 2.50 17.21 o 3 5 1 0.67 -3.13 5.01 o 5 5 1 100.49 115.39 12.80 o 7 5 1 54.18 49.85 14.41 o 9 5 1 37.01 20.22 9.04 o -22 0 2 129.75 112.74 18.07 o -20 0 2 10.03 6.59 4.84 o -18 0 2 414.28 405.99 17.14 o -16 0 2 122.38 106.23 9.72 o -14 0 2 359.14 366.30 17.43 o -12 0 2 29.43 28.76 5.16 o -10 0 2 1067.53 1058.66 29.04 o -8 0 2 1021.48 995.32 23.02 o -6 0 2 2011.85 1824.14 31.63 o -4 0 2 4958.57 4535.83 66.63 o -2 0 2 3009.28 2592.91 57.66 o 0 0 2 3403.33 3275.77 68.42 o 2 0 2 354.71 287.75 5.48 o 4 0 2 1595.51 1329.65 17.62 o 6 0 2 119.06 108.83 4.96 o 8 0 2 488.08 535.10 10.08 o 10 0 2 371.61 389.52 8.86 o 12 0 2 288.79 308.56 11.06 o 14 0 2 319.51 290.64 12.91 o 16 0 2 0.00 -1.29 3.87 o 18 0 2 79.19 96.38 15.06 o 20 0 2 21.90 16.78 8.61 o 22 0 2 10.54 19.79 9.47 o -21 1 2 5.28 2.62 4.27 o -19 1 2 60.70 56.49 7.02 o -17 1 2 2.29 -0.77 2.59 o -15 1 2 25.23 25.14 3.80 o -13 1 2 0.37 -1.69 1.75 o -11 1 2 15.45 17.35 2.76 o -9 1 2 2549.99 2561.00 31.84 o -7 1 2 547.78 568.23 10.24 o -5 1 2 6870.18 7114.76 85.66 o -3 1 2 5771.41 5831.00 69.90 o -1 1 2 595.87 578.34 10.76 o 1 1 2 422.66 421.02 7.64 o 3 1 2 2301.53 2205.19 22.21 o 5 1 2 5337.69 5436.14 51.02 o 7 1 2 734.85 793.26 10.48 o 9 1 2 994.77 943.05 12.17 o 11 1 2 10.32 13.71 1.86 o 13 1 2 80.22 77.70 5.01 o 15 1 2 238.25 264.19 21.20 o 17 1 2 258.69 233.25 15.82 o 19 1 2 166.60 165.51 18.29 o 21 1 2 13.15 5.95 8.61 o -20 2 2 3.28 -0.10 4.10 o -18 2 2 10.16 6.48 4.10 o -16 2 2 36.54 33.23 6.55 o -14 2 2 1.97 1.23 2.57 o -12 2 2 340.92 340.27 11.52 o -10 2 2 417.35 411.02 13.77 o -8 2 2 545.89 632.66 14.38 o -6 2 2 7505.08 7536.18 119.57 o -4 2 2 635.19 707.43 36.36 o -2 2 2 3106.43 3051.16 75.30 o 0 2 2 167.20 177.05 8.06 o 2 2 2 1372.93 1332.78 27.06 o 4 2 2 520.76 530.68 14.84 o 6 2 2 551.04 537.55 9.30 o 8 2 2 6.77 9.47 2.15 o 10 2 2 109.61 120.58 6.55 o 12 2 2 873.37 805.67 15.43 o 14 2 2 11.87 9.81 3.58 o 16 2 2 368.55 373.61 14.26 o 18 2 2 41.07 35.19 7.75 o 20 2 2 6.88 5.31 14.20 o -17 3 2 11.26 19.36 11.19 o -15 3 2 15.54 8.00 6.23 o -13 3 2 241.68 272.00 17.09 o -11 3 2 12.39 15.28 5.99 o -9 3 2 271.09 291.37 11.39 o -7 3 2 44.39 37.57 6.67 o -5 3 2 124.52 120.55 12.56 o -3 3 2 1.36 -1.81 2.86 o -1 3 2 9.88 -0.41 3.00 o 1 3 2 2.41 -0.72 5.16 o 3 3 2 106.97 108.81 8.94 o 5 3 2 320.33 261.25 11.95 o 7 3 2 127.90 115.11 7.63 o 9 3 2 118.13 124.03 9.61 o 11 3 2 196.24 222.76 13.12 o 13 3 2 5.86 3.69 2.97 o 15 3 2 26.10 20.29 7.53 o 17 3 2 52.05 57.77 9.37 o -14 4 2 9.43 -0.43 8.61 o -12 4 2 12.24 7.53 7.75 o -10 4 2 38.85 45.76 8.67 o -8 4 2 2.32 0.82 4.65 o -6 4 2 85.39 77.02 13.34 o -4 4 2 16.08 6.81 5.59 o -2 4 2 79.82 54.86 8.20 o 0 4 2 47.89 45.25 7.61 o 2 4 2 33.38 47.31 9.04 o 4 4 2 2.94 7.00 4.85 o 6 4 2 291.38 307.42 16.12 o 8 4 2 53.14 52.75 6.40 o 10 4 2 44.62 52.21 8.15 o 12 4 2 27.15 24.61 7.16 o 14 4 2 2.42 9.02 12.48 o -7 5 2 0.00 -0.65 5.48 o -5 5 2 1.21 -2.58 5.38 o -3 5 2 19.91 22.34 7.28 o -1 5 2 17.81 20.58 6.84 o 1 5 2 6.75 -6.45 4.71 o 3 5 2 0.40 -1.93 5.27 o 5 5 2 9.22 7.01 6.20 o 7 5 2 23.38 19.94 6.92 o -21 1 3 34.71 42.90 6.97 o -19 1 3 62.99 70.87 6.65 o -17 1 3 15.29 13.83 5.47 o -15 1 3 4.92 3.60 2.43 o -13 1 3 42.89 50.97 6.39 o -11 1 3 88.08 90.97 5.56 o -9 1 3 1161.86 1207.49 15.32 o -7 1 3 113.06 154.75 6.12 o -5 1 3 7.23 4.85 1.36 o -3 1 3 3672.79 3521.64 38.71 o -1 1 3 7545.15 7219.39 75.13 o 1 1 3 108.57 120.99 3.51 o 3 1 3 0.32 0.29 0.75 o 5 1 3 1071.11 1040.79 12.31 o 7 1 3 7.26 8.06 1.42 o 9 1 3 955.93 997.32 11.97 o 11 1 3 464.80 498.41 8.01 o 13 1 3 215.59 225.96 12.89 o 15 1 3 94.75 74.27 8.52 o 17 1 3 19.66 18.55 5.48 o 19 1 3 34.89 32.52 11.19 o 21 1 3 0.16 0.17 4.30 o -20 2 3 0.26 3.87 4.49 o -18 2 3 3.08 4.73 3.60 o -16 2 3 86.19 85.18 12.30 o -14 2 3 25.49 30.07 4.71 o -12 2 3 86.56 82.31 6.73 o -10 2 3 112.44 91.21 6.60 o -8 2 3 44.89 59.81 5.11 o -6 2 3 270.12 228.59 10.02 o -4 2 3 821.19 788.46 20.23 o -2 2 3 59.53 59.17 5.78 o 0 2 3 825.77 868.15 23.45 o 2 2 3 1211.31 1191.10 17.52 o 4 2 3 10.63 12.47 2.11 o 6 2 3 1215.06 1267.10 16.42 o 8 2 3 17.31 19.43 2.54 o 10 2 3 50.81 85.52 6.27 o 12 2 3 98.30 88.19 5.03 o 14 2 3 208.98 187.16 11.05 o 16 2 3 53.26 37.78 5.82 o 18 2 3 152.34 177.31 14.45 o 20 2 3 4.24 4.24 5.33 o -17 3 3 0.43 10.76 6.02 o -15 3 3 7.10 8.26 6.06 o -13 3 3 32.62 27.97 7.11 o -11 3 3 6.20 8.73 5.15 o -9 3 3 6.55 1.72 6.67 o -7 3 3 45.16 56.49 8.06 o -5 3 3 23.97 19.42 5.45 o -3 3 3 56.81 65.38 7.75 o -1 3 3 5.48 5.06 3.61 o 1 3 3 36.85 41.05 6.06 o 3 3 3 6.47 5.09 3.61 o 5 3 3 36.56 36.32 4.52 o 7 3 3 0.09 -1.73 2.21 o 9 3 3 1.60 -0.84 3.11 o 11 3 3 13.98 20.94 5.81 o 13 3 3 14.62 7.01 3.03 o 15 3 3 0.28 0.87 5.58 o 17 3 3 0.13 2.89 4.62 o -14 4 3 13.06 9.47 7.30 o -12 4 3 1.10 -5.29 6.19 o -10 4 3 1.98 9.99 5.06 o -8 4 3 17.37 21.87 15.71 o -6 4 3 4.71 -2.01 4.23 o -4 4 3 45.43 53.79 12.26 o -2 4 3 6.44 11.41 5.01 o 0 4 3 32.52 42.07 8.61 o 2 4 3 49.38 63.45 8.50 o 4 4 3 100.83 95.68 9.86 o 6 4 3 0.85 0.47 3.27 o 8 4 3 27.59 25.64 6.20 o 10 4 3 17.56 18.66 5.80 o 12 4 3 8.26 6.27 4.92 o 14 4 3 9.73 26.26 7.23 o -7 5 3 5.50 5.18 6.37 o -5 5 3 37.41 30.04 7.89 o -3 5 3 3.85 8.09 7.75 o -1 5 3 12.99 7.99 6.20 o 1 5 3 3.26 2.87 6.02 o 3 5 3 50.92 47.74 7.01 o 5 5 3 0.35 1.53 4.03 o 7 5 3 75.53 98.83 28.40 o -22 0 4 41.38 61.83 9.88 o -20 0 4 86.39 100.67 11.71 o -18 0 4 21.51 16.06 8.39 o -16 0 4 337.53 358.46 15.51 o -14 0 4 133.81 137.83 10.65 o -12 0 4 890.54 1039.47 25.39 o -10 0 4 310.00 260.70 14.20 o -8 0 4 178.75 161.84 8.82 o -6 0 4 217.04 187.77 5.10 o -4 0 4 31403.55 29615.81 426.38 o -2 0 4 1077.07 981.21 17.78 o 0 0 4 7546.98 7261.36 126.07 o 2 0 4 117.37 100.30 3.90 o 4 0 4 2056.96 2116.71 33.19 o 6 0 4 4301.96 4713.61 58.46 o 8 0 4 600.39 639.64 12.62 o 10 0 4 3270.04 3451.17 45.10 o 12 0 4 358.13 376.92 12.49 o 14 0 4 1.27 -1.72 4.30 o 16 0 4 38.04 49.48 10.76 o 18 0 4 0.12 10.33 7.31 o 20 0 4 7.09 1.29 6.45 o 22 0 4 13.14 32.27 11.19 o -21 1 4 19.16 22.21 4.93 o -19 1 4 4.87 13.23 3.96 o -17 1 4 24.04 29.54 4.58 o -15 1 4 159.54 164.21 8.74 o -13 1 4 123.85 108.21 8.20 o -11 1 4 210.45 214.80 7.55 o -9 1 4 127.00 143.98 4.69 o -7 1 4 941.21 878.31 13.06 o -5 1 4 753.20 717.80 9.56 o -3 1 4 14813.34 14832.55 150.88 o -1 1 4 57.54 76.16 3.49 o 1 1 4 7395.11 7487.33 78.12 o 3 1 4 3.04 11.53 1.51 o 5 1 4 98.71 105.44 3.23 o 7 1 4 757.98 702.44 42.42 o 9 1 4 0.93 1.35 1.20 o 11 1 4 268.92 276.99 6.70 o 13 1 4 101.18 82.46 4.57 o 15 1 4 56.47 59.10 8.61 o 17 1 4 64.61 39.63 6.98 o 19 1 4 54.82 42.19 7.91 o 21 1 4 0.24 -2.55 4.40 o -20 2 4 11.13 27.54 10.76 o -18 2 4 31.91 40.11 14.83 o -16 2 4 7.74 10.94 4.11 o -14 2 4 269.81 268.74 11.15 o -12 2 4 7.52 0.66 2.77 o -10 2 4 50.22 41.72 4.68 o -8 2 4 267.13 271.77 7.41 o -6 2 4 1588.42 1695.37 22.73 o -4 2 4 873.63 871.36 13.46 o -2 2 4 1622.75 1656.44 22.76 o 0 2 4 1284.98 1249.86 16.59 o 2 2 4 2074.08 2085.41 26.98 o 4 2 4 359.40 380.04 9.81 o 6 2 4 540.05 530.39 9.14 o 8 2 4 105.47 137.11 6.67 o 10 2 4 334.41 345.57 9.11 o 12 2 4 181.82 182.77 7.00 o 14 2 4 382.56 366.94 21.07 o 16 2 4 10.26 10.07 7.10 o 18 2 4 8.08 7.72 4.76 o 20 2 4 12.63 6.73 5.76 o -17 3 4 2.69 4.30 5.93 o -15 3 4 1.99 5.38 5.57 o -13 3 4 73.14 74.10 11.19 o -11 3 4 2.38 -1.66 4.73 o -9 3 4 142.14 110.19 12.26 o -7 3 4 65.78 79.58 9.28 o -5 3 4 3.43 5.00 4.40 o -3 3 4 0.17 3.64 3.92 o -1 3 4 340.92 360.55 33.13 o 1 3 4 13.98 13.64 3.29 o 3 3 4 42.41 53.07 6.12 o 5 3 4 242.10 265.11 10.66 o 7 3 4 152.12 142.94 8.23 o 9 3 4 584.16 652.61 20.63 o 11 3 4 181.55 171.94 16.35 o 13 3 4 260.87 282.15 14.07 o 15 3 4 65.87 79.90 8.39 o 17 3 4 0.57 -2.76 4.65 o -14 4 4 3.63 4.09 7.00 o -12 4 4 0.11 2.15 6.37 o -10 4 4 18.65 17.64 9.25 o -8 4 4 8.64 20.44 6.69 o -6 4 4 209.51 219.01 16.78 o -4 4 4 177.88 218.53 18.07 o -2 4 4 184.71 189.06 18.72 o 0 4 4 81.99 78.89 9.68 o 2 4 4 7.38 6.56 3.85 o 4 4 4 2.55 1.16 3.04 o 6 4 4 18.58 9.21 5.59 o 8 4 4 36.38 26.88 6.80 o 10 4 4 7.91 -0.30 4.10 o 12 4 4 0.20 -2.86 4.30 o 14 4 4 3.67 -3.44 10.76 o -7 5 4 4.91 11.19 7.00 o -5 5 4 1.76 4.69 6.37 o -3 5 4 71.41 100.07 28.83 o -1 5 4 3.22 -0.35 4.44 o 1 5 4 79.85 112.53 9.83 o 3 5 4 0.48 1.67 4.16 o 5 5 4 18.03 15.90 6.52 o 7 5 4 3.25 6.33 5.26 o -21 1 5 10.23 8.70 4.46 o -19 1 5 180.30 168.21 10.15 o -17 1 5 166.55 185.75 16.23 o -15 1 5 139.58 141.67 8.13 o -13 1 5 501.15 492.55 12.33 o -11 1 5 93.66 140.38 27.48 o -9 1 5 120.01 128.23 7.20 o -7 1 5 6494.86 6419.68 60.77 o -5 1 5 525.95 557.32 8.35 o -3 1 5 1153.37 1192.62 16.25 o -1 1 5 2339.96 2282.57 27.15 o 1 1 5 54.32 69.60 7.14 o 3 1 5 13.87 7.23 1.16 o 5 1 5 132.32 157.36 5.45 o 7 1 5 192.02 198.20 5.63 o 9 1 5 405.39 402.00 8.94 o 11 1 5 739.61 712.04 11.60 o 13 1 5 32.22 37.21 6.27 o 15 1 5 10.09 10.04 4.10 o 17 1 5 261.94 259.29 16.88 o 19 1 5 17.32 5.41 6.45 o 21 1 5 32.05 22.88 7.28 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