#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:38:35 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181267 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/45/2234573.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2234573_Fobs loop_ _publ_author_name 'Praveen, Aletti S.' 'Yathirajan, Hemmige S.' 'Narayana, Badiadka' 'Gerber, Thomas' 'Hosten, Eric' 'Betz, Richard' _publ_section_title ; 4-[(1E)-3-(2,6-Dichloro-3-fluorophenyl)-3-oxoprop-1-en-1-yl]benzonitrile ; _journal_coeditor_code CV5282 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1413 _journal_volume 68 _journal_year 2012 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 116.773 _cell_angle_gamma 90.000 _cell_length_a 13.2751 _cell_length_b 8.5002 _cell_length_c 13.9854 _exptl_crystal_F_000 648.00 _reflns_d_resolution_high 0.7493 _cod_data_source_file cv5282Isup3.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ba507_s in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 98.39 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2323.99 2408.03 16.28 o 3 0 0 0.95 0.72 0.29 o 4 0 0 152.67 147.68 1.30 o 5 0 0 1704.95 1843.70 12.40 o 6 0 0 46.22 35.59 0.84 o 7 0 0 1022.35 1147.33 10.37 o 8 0 0 622.10 611.74 5.96 o 9 0 0 1105.90 1103.50 10.22 o 10 0 0 1.31 0.56 0.79 o 11 0 0 291.61 294.23 8.69 o 12 0 0 9.71 5.92 1.10 o 13 0 0 19.80 13.55 1.33 o 14 0 0 110.59 112.26 2.78 o 15 0 0 27.60 34.87 3.13 o 1 1 0 253.47 254.05 1.62 o 2 1 0 902.55 895.40 4.59 o 3 1 0 38.99 32.56 0.43 o 5 1 0 5846.35 5852.20 29.41 o 6 1 0 37.93 42.78 0.66 o 7 1 0 132.49 112.12 1.17 o 8 1 0 8.33 7.68 0.47 o 9 1 0 427.44 401.77 3.06 o 10 1 0 315.50 299.58 2.99 o 11 1 0 69.76 54.90 1.35 o 12 1 0 67.14 74.97 1.54 o 13 1 0 64.03 68.39 1.63 o 14 1 0 21.93 21.14 1.33 o 15 1 0 14.37 14.97 1.29 o 0 2 0 242.60 265.58 2.15 o 1 2 0 5169.99 5268.89 45.74 o 2 2 0 59.24 43.44 0.59 o 3 2 0 3603.18 3573.89 19.22 o 4 2 0 491.30 541.74 5.71 o 5 2 0 2222.64 2298.49 13.35 o 6 2 0 1106.92 1103.61 6.43 o 7 2 0 9.45 11.38 0.47 o 8 2 0 1128.45 1131.18 7.32 o 9 2 0 640.39 657.81 4.90 o 10 2 0 142.75 137.95 1.69 o 11 2 0 70.00 55.06 1.34 o 12 2 0 100.96 95.01 2.05 o 13 2 0 2.13 1.69 0.96 o 14 2 0 22.52 22.81 1.36 o 15 2 0 4.11 3.99 1.14 o 2 3 0 1598.38 1535.06 9.07 o 3 3 0 1487.36 1628.22 9.39 o 4 3 0 1.06 1.17 0.24 o 5 3 0 662.18 731.35 4.74 o 6 3 0 5.48 5.75 0.41 o 7 3 0 648.90 639.63 4.31 o 8 3 0 163.30 177.95 1.47 o 9 3 0 5.47 1.85 0.45 o 10 3 0 164.06 151.59 1.68 o 11 3 0 35.87 32.43 1.46 o 12 3 0 25.98 29.11 1.58 o 13 3 0 65.99 68.28 1.92 o 14 3 0 14.23 14.24 1.26 o 15 3 0 6.68 6.83 1.24 o 0 4 0 4917.48 5349.29 41.05 o 1 4 0 82.84 77.33 0.85 o 2 4 0 3490.42 3588.65 20.96 o 3 4 0 2381.14 2434.97 15.57 o 4 4 0 1985.35 2153.66 13.34 o 5 4 0 1858.61 1845.28 11.41 o 6 4 0 1975.78 1843.74 11.48 o 7 4 0 351.42 321.97 2.45 o 8 4 0 19.26 17.01 0.75 o 9 4 0 8.25 4.95 0.63 o 10 4 0 85.44 77.92 1.69 o 11 4 0 10.61 8.47 0.99 o 12 4 0 32.54 22.88 1.35 o 13 4 0 39.33 39.49 1.73 o 14 4 0 42.87 45.62 1.83 o 1 5 0 545.14 503.12 3.02 o 2 5 0 1432.47 1414.20 8.92 o 3 5 0 3.83 5.14 0.56 o 4 5 0 251.73 260.94 2.25 o 5 5 0 105.88 114.63 1.27 o 6 5 0 490.82 480.72 3.36 o 7 5 0 910.43 876.84 6.17 o 8 5 0 402.95 383.55 3.56 o 9 5 0 4.90 6.28 0.67 o 10 5 0 54.05 59.04 1.60 o 11 5 0 85.16 82.43 1.90 o 12 5 0 26.58 19.01 1.22 o 13 5 0 32.49 36.84 1.75 o 14 5 0 1.00 -1.00 1.00 o 0 6 0 1747.14 1858.21 14.20 o 1 6 0 1.94 3.87 0.94 o 2 6 0 775.56 757.88 5.57 o 3 6 0 653.36 614.95 5.73 o 4 6 0 159.47 142.10 1.47 o 5 6 0 5.67 3.62 0.37 o 6 6 0 101.45 96.70 1.03 o 7 6 0 6.84 6.32 0.53 o 8 6 0 53.85 52.07 1.54 o 9 6 0 111.88 116.44 3.18 o 10 6 0 11.04 11.01 0.96 o 11 6 0 125.53 131.75 3.20 o 12 6 0 65.37 77.72 2.02 o 13 6 0 8.91 6.42 1.10 o 1 7 0 126.14 113.96 3.38 o 2 7 0 140.99 126.03 1.43 o 3 7 0 48.33 36.56 0.85 o 4 7 0 548.42 564.43 4.32 o 5 7 0 356.91 357.34 3.29 o 6 7 0 12.80 15.73 1.17 o 7 7 0 126.40 124.35 1.80 o 8 7 0 63.97 62.76 1.62 o 9 7 0 31.35 24.09 1.76 o 10 7 0 8.94 7.93 1.10 o 11 7 0 3.69 2.64 1.10 o 12 7 0 32.83 31.21 2.02 o 0 8 0 1067.31 1104.78 12.32 o 1 8 0 300.73 292.18 2.68 o 2 8 0 1.45 1.37 0.59 o 3 8 0 130.02 121.66 2.02 o 4 8 0 0.22 9.08 1.37 o 5 8 0 2.72 3.22 1.27 o 6 8 0 0.63 0.71 0.60 o 7 8 0 35.74 32.42 2.69 o 8 8 0 227.34 222.19 5.47 o 9 8 0 62.09 60.75 3.32 o 10 8 0 4.42 0.78 1.86 o 11 8 0 18.29 18.85 2.44 o 1 9 0 42.95 45.95 1.42 o 2 9 0 9.48 8.55 1.37 o 3 9 0 136.79 124.33 3.42 o 4 9 0 255.49 259.11 5.37 o 5 9 0 136.32 135.66 3.91 o 6 9 0 0.62 0.59 1.56 o 7 9 0 28.81 25.49 2.54 o 8 9 0 2.51 3.61 1.66 o 9 9 0 2.69 1.66 1.76 o 0 10 0 41.53 43.17 2.25 o 1 10 0 32.94 30.02 4.30 o 2 10 0 0.62 1.56 1.37 o 3 10 0 52.25 63.29 2.93 o 4 10 0 4.85 5.96 1.56 o 5 10 0 37.70 39.26 2.73 o 6 10 0 53.76 57.53 3.22 o 7 10 0 9.43 6.74 1.76 o 1 11 0 70.37 74.52 2.83 o 2 11 0 29.88 36.63 2.54 o 3 11 0 0.01 2.64 1.56 o -16 1 1 8.36 9.00 1.55 o -15 1 1 11.15 7.16 1.13 o -14 1 1 7.83 8.13 1.07 o -13 1 1 20.40 21.33 1.11 o -12 1 1 37.92 34.16 1.21 o -11 1 1 1.64 -0.63 0.63 o -10 1 1 38.65 34.22 1.06 o -9 1 1 129.43 130.80 1.44 o -8 1 1 149.52 156.12 1.48 o -7 1 1 25.88 18.55 0.59 o -6 1 1 3.69 10.07 0.39 o -5 1 1 0.61 2.44 0.23 o -4 1 1 270.22 246.50 1.38 o -3 1 1 683.51 645.31 3.54 o -2 1 1 110.92 97.47 0.65 o -1 1 1 159.74 179.73 1.25 o 0 1 1 2527.26 2503.85 16.17 o 1 1 1 2736.50 2850.79 14.45 o 2 1 1 9680.67 9648.94 158.32 o 3 1 1 1948.29 1939.76 10.57 o 4 1 1 1847.78 1956.99 9.48 o 5 1 1 3013.42 3337.92 18.47 o 6 1 1 0.32 2.02 0.33 o 7 1 1 529.18 520.78 3.63 o 8 1 1 15.46 11.12 0.55 o 9 1 1 146.27 125.88 1.55 o 10 1 1 0.93 -0.59 0.59 o 11 1 1 61.43 56.18 1.35 o 12 1 1 33.81 31.26 1.24 o 13 1 1 6.98 8.02 1.11 o 14 1 1 4.71 6.92 1.12 o 15 1 1 8.53 8.35 1.55 o -15 2 1 19.16 16.72 1.31 o -14 2 1 6.58 4.17 1.05 o -13 2 1 30.83 29.73 1.54 o -12 2 1 1.76 0.71 0.67 o -11 2 1 386.55 362.35 4.96 o -10 2 1 401.36 391.63 3.25 o -9 2 1 590.13 571.40 4.33 o -8 2 1 427.71 429.37 2.84 o -7 2 1 202.40 223.73 1.75 o -6 2 1 0.16 -0.28 0.28 o -5 2 1 231.97 283.10 1.83 o -4 2 1 825.82 837.08 11.96 o -3 2 1 5700.34 5659.06 34.30 o -2 2 1 1972.73 1966.44 13.44 o -1 2 1 2446.34 2449.80 18.75 o 2 2 1 8895.66 8922.55 54.80 o 3 2 1 1658.68 1567.27 15.40 o 4 2 1 413.91 398.31 2.30 o 6 2 1 1553.77 1701.16 9.25 o 7 2 1 12.29 9.94 0.44 o 8 2 1 64.88 67.71 1.06 o 9 2 1 201.64 191.35 1.95 o 10 2 1 135.11 118.13 1.74 o 11 2 1 24.17 25.60 1.19 o 12 2 1 126.36 114.58 2.26 o 13 2 1 15.79 11.87 1.16 o 14 2 1 3.90 0.23 1.03 o 15 2 1 2.58 3.55 1.92 o -15 3 1 3.99 4.47 1.16 o -14 3 1 1.91 0.09 0.98 o -13 3 1 22.47 17.15 1.15 o -12 3 1 25.35 22.27 2.14 o -11 3 1 0.88 -0.10 0.81 o -10 3 1 31.02 26.07 0.89 o -9 3 1 6.61 3.65 0.46 o -8 3 1 46.05 42.31 1.79 o -7 3 1 92.06 99.97 1.20 o -6 3 1 593.99 645.07 4.59 o -5 3 1 524.17 534.44 3.81 o -4 3 1 1572.63 1699.27 10.34 o -3 3 1 247.55 270.60 2.06 o -2 3 1 1446.67 1500.09 8.80 o -1 3 1 37.90 30.41 0.82 o 0 3 1 1274.13 1283.22 7.00 o 1 3 1 3669.83 3676.73 20.98 o 2 3 1 37.48 40.92 0.61 o 3 3 1 3.63 5.28 0.36 o 4 3 1 69.89 94.97 0.97 o 5 3 1 1.78 0.63 0.32 o 6 3 1 47.61 45.08 0.76 o 7 3 1 27.25 24.13 0.77 o 8 3 1 11.68 13.71 0.65 o 9 3 1 9.88 6.48 0.53 o 10 3 1 48.91 43.81 1.28 o 11 3 1 15.93 15.17 1.09 o 12 3 1 8.43 4.70 0.99 o 13 3 1 3.89 3.23 1.05 o 14 3 1 43.83 59.40 1.98 o -15 4 1 52.06 70.78 2.15 o -14 4 1 1.10 -0.33 1.07 o -13 4 1 36.53 35.37 1.78 o -12 4 1 4.92 2.63 0.93 o -11 4 1 0.19 -0.79 0.79 o -10 4 1 16.34 12.10 0.77 o -9 4 1 8.05 4.32 0.72 o -8 4 1 72.10 69.21 1.22 o -7 4 1 2.04 4.73 0.46 o -6 4 1 24.83 23.07 0.82 o -5 4 1 17.86 19.24 0.59 o -4 4 1 175.92 186.79 1.90 o -3 4 1 81.15 79.67 1.10 o -2 4 1 184.07 188.96 1.30 o -1 4 1 85.12 104.35 0.74 o 0 4 1 532.75 578.47 3.22 o 1 4 1 3244.51 3504.45 18.78 o 2 4 1 426.85 462.48 4.37 o 3 4 1 168.87 161.53 1.20 o 4 4 1 9.94 11.94 0.89 o 5 4 1 0.01 3.18 0.53 o 6 4 1 160.11 164.13 1.41 o 7 4 1 25.68 18.82 0.90 o 8 4 1 59.80 44.42 0.96 o 9 4 1 1.98 3.16 0.63 o 10 4 1 14.59 17.27 0.98 o 11 4 1 0.64 -0.11 1.18 o 12 4 1 24.85 20.25 1.26 o 13 4 1 0.14 -0.18 0.99 o 14 4 1 22.16 25.18 2.41 o -14 5 1 13.83 15.61 1.29 o -13 5 1 6.75 4.92 1.10 o -12 5 1 7.04 5.34 1.00 o -11 5 1 28.36 24.07 1.34 o -10 5 1 5.48 1.19 0.69 o -9 5 1 2.28 -1.05 1.73 o -8 5 1 174.44 144.93 1.73 o -7 5 1 71.78 68.03 1.05 o -6 5 1 30.87 28.00 0.69 o -5 5 1 20.67 20.78 0.53 o -4 5 1 220.09 206.90 1.82 o -3 5 1 730.51 767.18 5.02 o -2 5 1 498.92 476.12 3.19 o -1 5 1 4.96 5.17 0.38 o 0 5 1 61.38 79.16 1.30 o 1 5 1 195.08 161.39 1.21 o 2 5 1 948.50 900.54 4.83 o 3 5 1 0.03 0.65 0.32 o 4 5 1 9.74 12.72 0.64 o 5 5 1 768.09 793.99 5.30 o 6 5 1 164.00 158.59 1.39 o 7 5 1 0.90 2.14 0.49 o 8 5 1 2.37 1.10 0.60 o 9 5 1 41.40 29.02 1.15 o 10 5 1 11.43 7.79 0.96 o 11 5 1 2.40 1.47 0.93 o 12 5 1 2.46 -0.16 0.97 o 13 5 1 19.29 17.04 1.25 o -13 6 1 11.22 9.17 1.14 o -12 6 1 0.24 -0.87 0.87 o -11 6 1 75.27 63.42 1.72 o -10 6 1 10.02 6.21 0.87 o -9 6 1 163.24 150.27 2.21 o -8 6 1 154.74 154.40 2.14 o -7 6 1 110.78 102.62 1.58 o -6 6 1 29.54 24.92 0.76 o -5 6 1 77.46 73.58 1.25 o -4 6 1 338.57 321.29 2.95 o -3 6 1 2648.19 2642.49 17.89 o -2 6 1 625.31 608.98 4.54 o -1 6 1 72.38 62.98 1.60 o 0 6 1 343.33 337.59 2.38 o 1 6 1 935.39 968.63 5.69 o 2 6 1 602.94 607.77 3.97 o 3 6 1 30.49 26.79 2.09 o 4 6 1 261.23 238.96 2.07 o 5 6 1 51.02 44.59 0.64 o 6 6 1 47.74 42.58 0.75 o 7 6 1 1.47 2.09 0.50 o 8 6 1 1.23 0.37 0.72 o 9 6 1 27.83 24.92 1.41 o 10 6 1 0.02 -0.84 0.84 o 11 6 1 0.63 -0.90 0.90 o 12 6 1 0.30 0.16 0.99 o -12 7 1 0.04 -1.47 1.66 o -11 7 1 2.21 3.60 1.06 o -10 7 1 46.20 37.38 3.03 o -9 7 1 39.76 45.36 2.22 o -8 7 1 17.40 21.12 1.11 o -7 7 1 53.51 56.02 1.05 o -6 7 1 48.71 51.51 0.93 o -5 7 1 99.45 92.23 1.95 o -4 7 1 597.97 603.64 6.05 o -3 7 1 149.08 143.27 1.74 o -2 7 1 185.54 171.32 2.37 o -1 7 1 8.18 4.81 0.33 o 0 7 1 146.60 136.69 1.22 o 1 7 1 999.22 989.25 6.27 o 2 7 1 72.11 61.14 0.83 o 3 7 1 142.08 122.46 1.25 o 4 7 1 66.07 63.45 0.92 o 5 7 1 57.78 54.21 1.44 o 6 7 1 0.13 -0.52 0.52 o 7 7 1 19.59 17.99 1.04 o 8 7 1 45.40 41.30 1.59 o 9 7 1 1.03 2.28 0.96 o 10 7 1 17.92 19.23 2.10 o 11 7 1 6.53 3.93 1.20 o -11 8 1 0.19 4.30 1.95 o -10 8 1 0.93 -1.37 1.66 o -9 8 1 2.04 -0.59 1.47 o -8 8 1 22.73 22.17 2.54 o -7 8 1 19.95 23.15 2.34 o -6 8 1 0.01 0.29 1.27 o -5 8 1 1.14 0.08 0.86 o -4 8 1 33.57 30.29 2.20 o -3 8 1 8.81 7.59 1.05 o -2 8 1 108.28 103.75 2.40 o -1 8 1 5.72 4.27 1.04 o 0 8 1 5.83 3.48 2.10 o 1 8 1 11.96 10.51 1.23 o 2 8 1 191.29 173.29 1.91 o 3 8 1 19.07 14.34 0.99 o 4 8 1 5.50 6.85 0.56 o 5 8 1 2.51 2.43 1.03 o 6 8 1 1.61 0.77 0.74 o 7 8 1 4.38 2.54 0.83 o 8 8 1 5.00 3.95 0.94 o 9 8 1 18.72 16.90 2.05 o 10 8 1 20.21 20.61 2.34 o -9 9 1 0.10 -0.20 1.66 o -8 9 1 0.93 0.29 1.56 o -7 9 1 0.38 -1.56 1.56 o -6 9 1 12.58 9.96 1.76 o -5 9 1 50.66 50.40 2.64 o -4 9 1 43.32 35.16 2.54 o -3 9 1 0.08 -0.98 1.27 o -2 9 1 115.44 117.38 2.34 o -1 9 1 8.28 8.42 0.75 o 0 9 1 0.72 0.52 1.17 o 1 9 1 70.43 67.18 1.73 o 2 9 1 164.53 161.36 4.65 o 3 9 1 26.04 19.04 2.00 o 4 9 1 0.03 -1.03 1.03 o 5 9 1 5.83 5.47 1.56 o 6 9 1 33.26 31.25 2.54 o 7 9 1 4.04 2.73 1.66 o 8 9 1 6.07 8.69 1.86 o 9 9 1 0.61 0.88 1.76 o -7 10 1 0.83 0.39 1.66 o -6 10 1 18.95 16.02 2.05 o -5 10 1 1.64 1.66 1.56 o -4 10 1 27.43 26.57 2.54 o -3 10 1 86.69 87.61 3.22 o -2 10 1 89.98 99.82 3.13 o -1 10 1 134.79 144.92 3.52 o 0 10 1 64.49 69.46 1.80 o 1 10 1 5.63 5.76 1.37 o 2 10 1 24.52 25.59 2.15 o 3 10 1 38.07 41.90 2.64 o 4 10 1 2.52 2.83 1.56 o 5 10 1 5.30 5.08 1.66 o 6 10 1 20.94 16.80 2.05 o -4 11 1 20.69 23.73 2.73 o -3 11 1 15.22 17.48 1.86 o -2 11 1 2.93 3.32 1.47 o 1 11 1 39.02 39.26 2.54 o 2 11 1 16.79 21.98 2.34 o 3 11 1 92.48 106.36 3.71 o -16 0 2 27.28 32.33 3.13 o -15 0 2 8.82 6.84 1.95 o -14 0 2 107.30 108.55 2.64 o -13 0 2 29.75 27.77 1.62 o -12 0 2 6.62 5.68 1.03 o -11 0 2 125.92 116.47 3.37 o -10 0 2 238.73 221.57 2.85 o -9 0 2 6.44 4.97 0.76 o -8 0 2 324.31 354.42 4.38 o -7 0 2 680.13 667.89 7.35 o -6 0 2 707.04 705.24 6.22 o -5 0 2 920.40 931.99 6.90 o -4 0 2 11.32 9.81 0.42 o -3 0 2 4657.65 4688.94 34.26 o -1 0 2 1331.10 1298.24 9.73 o 0 0 2 540.33 524.51 5.53 o 2 0 2 1974.32 2058.08 14.46 o 3 0 2 1264.90 1283.70 8.82 o 4 0 2 69.02 55.68 0.83 o 5 0 2 1307.18 1342.91 10.56 o 6 0 2 3.75 2.15 0.47 o 7 0 2 235.51 274.22 3.12 o 8 0 2 410.09 405.75 4.33 o 9 0 2 608.31 638.39 7.56 o 10 0 2 23.93 21.37 1.95 o 11 0 2 3.21 5.60 1.56 o 12 0 2 244.46 238.80 6.69 o 13 0 2 10.00 5.66 1.24 o 14 0 2 8.75 10.16 2.15 o -16 1 2 4.02 2.19 1.35 o -15 1 2 37.79 42.95 1.82 o -14 1 2 20.74 18.94 1.23 o -13 1 2 0.05 -0.13 0.68 o -12 1 2 302.84 308.55 3.12 o -11 1 2 16.18 11.30 0.81 o -10 1 2 147.53 140.22 1.93 o -9 1 2 435.22 413.73 3.30 o -8 1 2 124.03 116.92 1.32 o -7 1 2 978.71 948.06 5.97 o -6 1 2 638.56 609.32 3.83 o -5 1 2 0.02 -0.22 0.22 o -4 1 2 1911.97 1916.46 10.13 o -3 1 2 694.47 697.70 3.66 o -2 1 2 1086.33 1161.69 6.58 o -1 1 2 41.36 52.22 0.45 o 0 1 2 69.73 60.04 0.42 o 1 1 2 595.91 620.57 2.88 o 2 1 2 2391.98 2362.58 11.74 o 3 1 2 0.11 0.09 0.23 o 4 1 2 945.58 894.00 4.72 o 5 1 2 3119.88 3213.77 17.57 o 6 1 2 304.54 311.44 2.22 o 7 1 2 264.09 267.07 2.04 o 8 1 2 90.97 80.79 1.15 o 9 1 2 1.82 -0.52 0.52 o 10 1 2 238.62 222.94 2.51 o 11 1 2 8.97 5.13 0.75 o 12 1 2 13.77 17.04 1.33 o 13 1 2 72.17 83.58 2.12 o 14 1 2 0.03 -0.08 1.05 o -16 2 2 29.36 33.14 1.80 o -15 2 2 1.89 2.67 1.07 o -14 2 2 56.40 49.77 1.72 o -13 2 2 230.14 224.63 5.46 o -12 2 2 12.50 8.14 0.78 o -11 2 2 2.56 -0.31 0.65 o -10 2 2 98.25 96.18 1.74 o -9 2 2 70.80 75.15 1.17 o -8 2 2 380.17 376.95 2.69 o -7 2 2 218.02 242.19 1.84 o -6 2 2 602.62 589.44 3.49 o -5 2 2 1428.69 1387.53 7.27 o -4 2 2 222.08 221.80 1.34 o -3 2 2 77.18 73.50 0.66 o -2 2 2 1044.19 1063.24 6.56 o -1 2 2 244.16 239.93 1.28 o 0 2 2 2748.22 2762.57 12.57 o 1 2 2 76.21 72.60 0.46 o 2 2 2 1043.34 1029.04 4.95 o 3 2 2 1306.79 1235.46 5.94 o 4 2 2 438.00 425.58 2.52 o 5 2 2 0.04 -0.28 0.28 o 6 2 2 1172.75 1218.40 6.75 o 7 2 2 130.65 99.62 1.15 o 8 2 2 78.45 81.47 1.25 o 9 2 2 75.74 61.18 1.16 o 10 2 2 34.51 26.23 1.32 o 11 2 2 190.85 179.04 2.76 o 12 2 2 18.77 14.79 1.16 o 13 2 2 2.19 -0.88 0.98 o 14 2 2 18.79 16.11 1.31 o -16 3 2 27.81 36.95 2.34 o -15 3 2 22.67 22.28 1.44 o -14 3 2 0.71 -0.54 0.97 o -13 3 2 23.39 29.68 1.57 o -12 3 2 22.36 25.27 1.48 o -11 3 2 2.52 0.80 0.79 o -10 3 2 51.02 47.45 1.44 o -9 3 2 340.88 332.82 2.65 o -8 3 2 436.28 419.96 3.30 o -7 3 2 3.56 1.79 0.40 o -6 3 2 145.97 140.48 1.37 o -5 3 2 5.86 5.97 0.33 o -4 3 2 483.44 514.48 3.27 o -3 3 2 358.54 376.08 2.44 o -2 3 2 1698.44 1668.89 8.87 o -1 3 2 7275.49 7211.39 44.04 o 0 3 2 265.14 252.17 1.55 o 1 3 2 30.97 33.14 0.44 o 2 3 2 2929.52 3106.88 15.84 o 3 3 2 11.25 5.50 0.29 o 4 3 2 126.65 123.54 0.92 o 5 3 2 482.32 542.06 3.54 o 6 3 2 0.15 0.29 0.29 o 7 3 2 459.15 428.45 3.11 o 8 3 2 338.97 325.60 2.57 o 9 3 2 123.86 126.94 1.52 o 10 3 2 34.16 47.24 1.56 o 11 3 2 156.50 155.02 2.53 o 12 3 2 9.91 8.17 1.05 o 13 3 2 53.65 55.98 2.03 o 14 3 2 7.61 8.46 1.23 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