#------------------------------------------------------------------------------ #$Date: 2016-04-06 17:01:17 +0300 (Wed, 06 Apr 2016) $ #$Revision: 181901 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/01/2240176.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2240176 _cell_angle_alpha 88.215 _cell_angle_beta 78.816 _cell_angle_gamma 83.072 _cell_length_a 8.4938 _cell_length_b 18.9062 _cell_length_c 19.9303 _exptl_crystal_F_000 1216.00 _reflns_d_resolution_high 0.8400 _cod_data_source_file vn2086Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 121230_s1_lkj in space group P -1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 365.03 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 27050.02 30096.34 196.14 o 3 0 0 28.09 39.33 8.76 o 4 0 0 6514.16 7171.39 149.29 o 5 0 0 5.53 -19.34 19.34 o 6 0 0 981.73 929.57 52.30 o 7 0 0 56.96 15.92 27.72 o 8 0 0 306.64 389.18 55.07 o 9 0 0 13.28 17.73 32.16 o -9 1 0 79.25 86.85 58.46 o -8 1 0 91.57 154.08 53.42 o -7 1 0 502.83 478.70 55.76 o -6 1 0 441.05 525.16 52.42 o -5 1 0 2384.72 2286.93 95.89 o -4 1 0 2634.85 2984.98 82.10 o -3 1 0 2509.76 2777.47 56.37 o -2 1 0 18009.33 19929.56 139.47 o 2 1 0 623.43 461.20 23.49 o 3 1 0 5244.59 5093.65 75.74 o 4 1 0 6901.92 7037.63 206.38 o 5 1 0 1947.43 1863.22 67.87 o 6 1 0 1138.18 1063.73 53.71 o 7 1 0 40.61 56.71 32.73 o 8 1 0 297.73 354.15 54.42 o 9 1 0 16.93 60.31 48.87 o -9 2 0 107.93 231.99 68.23 o -8 2 0 5.07 7.04 47.89 o -7 2 0 823.70 973.40 97.91 o -6 2 0 15.21 25.08 50.10 o -5 2 0 5048.64 5005.93 145.27 o -4 2 0 179.30 159.33 19.21 o -3 2 0 4467.14 5083.37 85.26 o -2 2 0 463.97 528.96 23.28 o -1 2 0 4392.08 4368.13 51.01 o 1 2 0 24669.82 23470.84 202.21 o 2 2 0 25170.65 27636.24 154.50 o 3 2 0 11843.07 11886.29 169.70 o 4 2 0 3319.79 3490.88 123.36 o 5 2 0 3873.52 3623.32 156.01 o 6 2 0 301.38 284.89 27.70 o 7 2 0 231.91 221.83 39.25 o 8 2 0 80.75 59.21 28.33 o 9 2 0 117.39 238.42 51.50 o -9 3 0 54.41 142.57 53.70 o -8 3 0 167.70 241.83 63.20 o -7 3 0 660.49 793.57 89.50 o -6 3 0 700.82 738.57 81.14 o -5 3 0 3962.71 4389.68 170.24 o -4 3 0 922.06 946.36 53.96 o -3 3 0 3992.70 4541.35 103.05 o -2 3 0 2496.70 2776.21 50.65 o -1 3 0 10945.22 12943.63 182.68 o 0 3 0 5113.17 5260.63 80.46 o 2 3 0 9588.77 9799.80 105.40 o 3 3 0 10917.34 11738.20 104.30 o 4 3 0 2310.35 2209.62 78.75 o 5 3 0 2816.09 2765.84 157.29 o 6 3 0 40.66 22.38 12.88 o 7 3 0 318.19 334.15 44.74 o 8 3 0 1.48 -2.72 24.20 o 9 3 0 161.16 208.58 49.71 o -9 4 0 0.38 42.77 41.36 o -8 4 0 336.04 599.45 89.30 o -7 4 0 132.17 173.45 52.55 o -6 4 0 2352.04 2622.53 150.64 o -5 4 0 609.17 852.55 79.98 o -4 4 0 4793.81 4500.52 218.43 o -3 4 0 1099.14 1240.34 76.16 o -2 4 0 9597.39 9320.66 148.53 o -1 4 0 2663.53 3010.00 112.23 o 0 4 0 15085.88 16421.37 173.69 o 1 4 0 3380.61 3032.32 52.07 o 2 4 0 11351.43 11785.59 156.28 o 3 4 0 5263.67 5008.41 85.06 o 4 4 0 3635.75 3651.66 90.01 o 5 4 0 1056.29 1028.90 51.46 o 6 4 0 332.24 320.83 33.34 o 7 4 0 161.43 120.24 30.39 o 8 4 0 47.94 47.39 25.71 o 9 4 0 72.78 111.15 37.99 o -9 5 0 32.18 6.01 57.61 o -8 5 0 244.24 261.16 65.47 o -7 5 0 75.49 126.21 53.77 o -6 5 0 2134.16 2420.47 147.61 o -5 5 0 417.48 420.02 77.23 o -4 5 0 3103.50 3274.18 142.61 o -3 5 0 328.41 334.73 34.13 o -2 5 0 10487.26 10611.93 170.34 o -1 5 0 314.78 301.96 18.84 o 0 5 0 8958.03 8734.22 134.01 o 1 5 0 410.52 347.63 21.37 o 2 5 0 11241.87 12954.87 168.39 o 3 5 0 583.92 553.89 31.10 o 4 5 0 2772.23 2836.22 92.23 o 5 5 0 206.68 245.49 53.79 o 6 5 0 960.74 1019.02 90.33 o 7 5 0 8.54 8.95 23.58 o 8 5 0 203.72 215.78 40.45 o 9 5 0 5.18 -23.58 30.50 o -9 6 0 98.06 180.54 59.55 o -8 6 0 50.53 59.39 39.30 o -7 6 0 539.13 765.95 95.80 o -6 6 0 543.27 691.24 85.57 o -5 6 0 2270.87 2510.56 139.44 o -4 6 0 850.66 863.56 73.59 o -3 6 0 7069.59 6603.53 174.58 o -2 6 0 3343.70 3146.93 155.36 o -1 6 0 7389.61 6845.11 210.23 o 0 6 0 8139.46 8838.73 166.59 o 1 6 0 1831.77 1966.29 56.15 o 2 6 0 4151.48 3771.07 87.27 o 3 6 0 11300.47 12329.89 163.16 o 4 6 0 970.34 852.70 41.24 o 5 6 0 159.01 147.96 21.31 o 6 6 0 457.67 430.60 85.76 o 7 6 0 68.04 90.64 62.62 o 8 6 0 177.61 132.15 86.37 o 9 6 0 11.44 5.61 40.58 o -9 7 0 94.56 155.13 55.15 o -8 7 0 7.47 -12.98 34.11 o -7 7 0 521.15 496.55 114.11 o -6 7 0 18.82 90.00 30.92 o -5 7 0 2845.47 2659.19 112.24 o -4 7 0 3.70 1.77 25.18 o -3 7 0 8193.48 8136.78 185.72 o -2 7 0 87.48 86.74 10.85 o -1 7 0 10232.96 10013.33 334.67 o 0 7 0 1975.33 1919.66 70.73 o 1 7 0 9085.20 8176.90 318.13 o 2 7 0 188.74 220.51 19.69 o 3 7 0 12012.06 12136.03 223.63 o 4 7 0 120.62 181.36 22.94 o 5 7 0 929.26 800.32 44.60 o 6 7 0 21.97 41.44 19.11 o 7 7 0 171.49 239.35 77.02 o 8 7 0 35.89 -1.70 30.20 o 9 7 0 37.98 24.74 65.39 o -8 8 0 130.13 205.66 59.62 o -7 8 0 170.32 88.95 39.71 o -6 8 0 380.00 411.10 55.56 o -5 8 0 1762.10 1757.95 157.99 o -4 8 0 611.09 669.95 47.18 o -3 8 0 5041.51 4731.87 261.01 o -2 8 0 5187.44 5148.03 264.02 o -1 8 0 11011.12 9916.69 935.35 o 0 8 0 365.35 282.67 36.15 o 1 8 0 3970.88 3780.10 152.35 o 2 8 0 990.12 1180.27 45.81 o 3 8 0 4787.93 4712.24 145.62 o 4 8 0 142.43 168.11 28.28 o 5 8 0 1248.25 1144.96 55.30 o 6 8 0 686.72 724.46 45.95 o 7 8 0 166.46 105.29 62.28 o 8 8 0 10.95 58.54 65.02 o 9 8 0 41.71 44.31 73.76 o -8 9 0 217.12 360.01 116.67 o -7 9 0 0.59 -13.45 42.33 o -6 9 0 435.07 429.37 71.57 o -5 9 0 84.44 47.15 20.47 o -4 9 0 1868.78 1921.51 80.99 o -3 9 0 226.27 255.65 25.48 o -2 9 0 5939.57 5420.34 418.44 o -1 9 0 937.63 1043.61 71.04 o 0 9 0 3444.63 3562.36 170.13 o 1 9 0 62.69 70.03 16.98 o 2 9 0 1560.92 1315.54 72.16 o 3 9 0 649.16 670.26 43.22 o 4 9 0 1320.75 1377.06 64.58 o 5 9 0 623.35 537.89 40.64 o 6 9 0 1008.84 1138.46 75.52 o 7 9 0 75.15 41.13 52.90 o 8 9 0 80.79 151.45 74.95 o 9 9 0 22.72 142.54 85.71 o -8 10 0 136.38 126.55 53.45 o -7 10 0 144.98 170.73 75.23 o -6 10 0 424.05 436.80 75.58 o -5 10 0 151.20 194.30 30.69 o -4 10 0 1368.36 1521.81 85.49 o -3 10 0 102.87 83.04 20.57 o -2 10 0 1079.98 977.78 63.28 o -1 10 0 203.04 302.49 76.31 o 0 10 0 2953.70 2674.45 119.12 o 1 10 0 658.93 667.41 51.81 o 2 10 0 1831.04 1632.25 126.53 o 3 10 0 1.63 6.47 19.20 o 4 10 0 1745.38 1864.19 162.73 o 5 10 0 66.34 30.65 24.67 o 6 10 0 564.87 495.57 52.63 o 7 10 0 14.75 40.38 55.20 o 8 10 0 112.99 134.55 77.70 o 9 10 0 2.72 74.18 69.67 o -8 11 0 17.62 69.18 52.34 o -7 11 0 350.42 324.05 74.34 o -6 11 0 136.49 231.07 61.61 o -5 11 0 763.55 697.29 88.36 o -4 11 0 129.58 131.94 31.05 o -3 11 0 1774.79 1512.36 185.41 o -2 11 0 240.68 229.48 33.82 o -1 11 0 8389.61 7088.60 827.13 o 0 11 0 2658.95 2941.38 207.58 o 1 11 0 4354.62 4126.93 132.23 o 2 11 0 2032.63 1880.01 136.11 o 3 11 0 498.72 512.51 41.94 o 4 11 0 825.88 856.32 119.51 o 5 11 0 46.25 32.89 23.33 o 6 11 0 112.25 39.92 52.37 o 7 11 0 13.26 65.44 58.76 o 8 11 0 67.69 86.63 65.96 o 9 11 0 1.83 53.81 55.35 o -7 12 0 279.81 308.44 72.55 o -6 12 0 22.17 51.92 42.23 o -5 12 0 722.18 742.31 97.26 o -4 12 0 483.27 485.60 93.90 o -3 12 0 2011.83 2327.92 226.21 o -2 12 0 126.10 114.52 25.95 o -1 12 0 3016.04 2733.90 312.88 o 0 12 0 1.77 -22.09 44.49 o 1 12 0 1408.57 1304.07 77.95 o 2 12 0 4.23 -2.50 23.96 o 3 12 0 915.60 908.17 56.20 o 4 12 0 2.34 35.24 47.39 o 5 12 0 267.58 237.05 80.99 o 6 12 0 0.82 -26.70 27.54 o 7 12 0 84.14 144.12 75.10 o 8 12 0 10.23 38.29 60.83 o -7 13 0 88.88 87.85 50.48 o -6 13 0 312.50 338.63 75.72 o -5 13 0 160.26 145.03 49.10 o -4 13 0 987.37 1020.95 157.62 o -3 13 0 614.18 578.34 115.27 o -2 13 0 835.54 698.69 111.67 o -1 13 0 1169.91 1119.26 144.59 o 0 13 0 1889.12 1834.67 173.81 o 1 13 0 1618.21 1387.75 82.76 o 2 13 0 429.30 375.61 75.80 o 3 13 0 1588.17 1703.02 178.43 o 4 13 0 220.13 492.81 102.35 o 5 13 0 311.43 408.20 55.50 o 6 13 0 49.98 83.79 32.95 o 7 13 0 67.64 1.82 54.10 o 8 13 0 8.37 43.46 68.25 o -6 14 0 404.04 548.57 93.65 o -5 14 0 1.98 13.50 34.92 o -4 14 0 605.96 648.17 138.80 o -3 14 0 125.57 88.65 68.36 o -2 14 0 1939.72 2060.22 210.78 o -1 14 0 56.23 143.84 68.67 o 0 14 0 1561.60 1618.31 101.40 o 1 14 0 84.45 62.60 25.83 o 2 14 0 1334.52 1190.46 131.33 o 3 14 0 113.92 90.67 35.00 o 4 14 0 489.75 715.31 120.71 o 5 14 0 30.48 -14.69 29.10 o 6 14 0 188.72 292.59 49.13 o 7 14 0 19.77 41.92 59.35 o 8 14 0 38.24 98.19 73.35 o -6 15 0 175.99 163.22 58.94 o -5 15 0 69.63 -19.97 39.67 o -4 15 0 409.07 631.64 135.05 o -3 15 0 7.26 89.25 61.12 o -2 15 0 1495.62 1559.95 199.14 o -1 15 0 52.36 68.45 54.79 o 0 15 0 1251.74 1215.71 117.41 o 1 15 0 366.90 418.64 52.28 o 2 15 0 941.52 791.30 116.08 o 3 15 0 21.46 38.27 31.82 o 4 15 0 210.74 190.37 69.79 o 5 15 0 0.51 -30.00 30.00 o 6 15 0 121.87 118.87 63.39 o 7 15 0 1.43 -5.87 46.24 o 8 15 0 25.23 95.13 75.81 o -6 16 0 7.06 77.11 49.38 o -5 16 0 166.47 157.00 58.08 o -4 16 0 42.05 -42.66 51.72 o -3 16 0 354.10 337.97 108.54 o -2 16 0 133.81 204.15 89.06 o -1 16 0 275.45 262.34 85.99 o 0 16 0 413.16 397.25 56.85 o 1 16 0 337.04 264.99 44.49 o 2 16 0 366.57 320.99 79.36 o 3 16 0 288.31 262.72 56.31 o 4 16 0 91.22 49.22 50.69 o 5 16 0 81.83 203.07 80.64 o 6 16 0 41.39 80.01 73.13 o 7 16 0 6.96 10.44 47.96 o -5 17 0 120.00 164.55 87.74 o -4 17 0 57.51 143.77 85.06 o -3 17 0 488.59 557.90 134.15 o -2 17 0 189.62 264.74 91.90 o -1 17 0 85.98 91.54 62.08 o 0 17 0 59.15 10.20 24.26 o 1 17 0 498.54 395.44 55.63 o 2 17 0 5.19 60.57 53.94 o 3 17 0 323.79 297.65 57.03 o 4 17 0 5.15 -65.61 65.61 o 5 17 0 90.97 139.40 71.82 o 6 17 0 0.11 155.41 78.73 o 7 17 0 11.33 117.57 69.42 o -4 18 0 191.48 351.13 116.46 o -3 18 0 206.77 193.13 90.76 o -2 18 0 412.65 480.80 121.96 o -1 18 0 18.16 -32.47 59.21 o 0 18 0 58.15 53.11 29.17 o 1 18 0 225.88 218.30 45.49 o 2 18 0 119.00 141.95 72.04 o 3 18 0 99.26 61.90 42.24 o 4 18 0 4.09 6.77 49.87 o 5 18 0 40.12 65.03 65.80 o 6 18 0 5.51 125.46 72.81 o -4 19 0 197.71 273.34 117.41 o -3 19 0 3.83 -57.87 57.87 o -2 19 0 336.73 577.88 136.42 o -1 19 0 0.07 -61.39 64.71 o 0 19 0 160.32 185.11 48.84 o 1 19 0 14.69 -8.76 41.82 o 2 19 0 185.98 222.43 87.83 o 3 19 0 0.62 8.65 31.27 o 4 19 0 24.13 -37.55 60.89 o 5 19 0 1.90 31.36 46.60 o 6 19 0 16.27 150.80 80.39 o -3 20 0 49.24 82.94 82.55 o -2 20 0 77.81 186.48 107.93 o -1 20 0 35.18 97.32 69.08 o 0 20 0 102.36 256.48 91.02 o 1 20 0 34.63 72.29 60.40 o 2 20 0 55.34 135.98 71.84 o 3 20 0 6.36 8.88 33.90 o 4 20 0 23.78 40.98 53.59 o 5 20 0 4.30 17.21 49.66 o -2 21 0 1.35 -59.44 59.44 o -1 21 0 62.07 131.21 84.58 o 0 21 0 13.70 12.77 52.23 o 1 21 0 77.21 107.37 84.68 o 2 21 0 4.96 64.39 39.55 o 3 21 0 24.75 40.39 32.21 o 4 21 0 7.62 78.25 51.93 o 0 22 0 8.00 5.80 58.18 o 1 22 0 75.51 281.07 101.03 o 2 22 0 2.32 10.36 44.40 o 3 22 0 30.02 81.72 44.51 o -3 -22 1 14.01 -33.79 44.57 o -2 -22 1 19.43 25.54 37.78 o -1 -22 1 14.45 34.49 72.36 o 0 -22 1 44.05 125.92 75.56 o -4 -21 1 0.44 -60.79 60.79 o -3 -21 1 45.44 -16.89 32.43 o -2 -21 1 3.09 3.01 34.94 o -1 -21 1 77.17 100.47 64.93 o 0 -21 1 17.01 81.13 72.10 o 1 -21 1 117.23 144.13 87.17 o 2 -21 1 18.80 137.97 92.49 o -5 -20 1 17.07 58.53 59.63 o -4 -20 1 10.24 -59.95 59.95 o -3 -20 1 40.06 -2.90 33.16 o -2 -20 1 4.05 28.99 41.04 o -1 -20 1 110.14 172.61 83.36 o 0 -20 1 6.93 99.08 72.44 o 1 -20 1 158.94 250.93 61.23 o 2 -20 1 0.72 81.81 50.81 o 3 -20 1 114.93 318.18 113.45 o -6 -19 1 11.69 50.27 64.57 o -5 -19 1 3.18 -8.01 81.07 o -4 -19 1 56.24 108.58 66.03 o -3 -19 1 18.73 34.08 26.61 o -2 -19 1 63.25 208.13 74.69 o -1 -19 1 41.22 34.23 63.62 o 0 -19 1 104.63 28.41 31.36 o 1 -19 1 98.88 137.38 45.37 o 2 -19 1 76.52 191.65 87.39 o 3 -19 1 80.64 199.55 100.98 o 4 -19 1 55.22 106.94 85.43 o -6 -18 1 27.81 78.29 61.23 o -5 -18 1 7.00 64.12 34.54 o -4 -18 1 107.38 129.70 71.85 o -3 -18 1 3.00 -28.54 31.34 o -2 -18 1 140.18 120.42 60.14 o -1 -18 1 3.28 21.67 54.68 o 0 -18 1 298.14 316.68 55.74 o 1 -18 1 0.06 -51.45 51.45 o 2 -18 1 241.89 440.91 119.32 o 3 -18 1 6.59 57.55 66.84 o 4 -18 1 196.01 268.27 116.61 o 5 -18 1 9.96 -86.51 86.51 o -7 -17 1 15.85 16.52 49.27 o -6 -17 1 25.56 191.61 87.74 o -5 -17 1 71.65 65.82 37.15 o -4 -17 1 73.77 -12.53 59.55 o -3 -17 1 177.79 212.09 83.10 o -2 -17 1 206.87 287.82 80.00 o -1 -17 1 314.23 249.66 57.05 o 0 -17 1 139.27 118.81 36.91 o 1 -17 1 160.53 78.66 57.74 o 2 -17 1 350.71 361.76 101.82 o 3 -17 1 260.19 229.30 100.26 o 4 -17 1 186.70 260.06 106.72 o 5 -17 1 25.36 -18.00 54.94 o -7 -16 1 19.48 34.93 53.27 o -6 -16 1 6.18 91.23 69.26 o -5 -16 1 84.80 144.91 44.48 o -4 -16 1 30.10 11.95 42.19 o -3 -16 1 371.62 431.10 66.51 o -2 -16 1 45.31 132.71 65.09 o -1 -16 1 596.92 585.78 129.54 o 0 -16 1 1.46 -42.25 45.88 o 1 -16 1 728.41 769.65 139.30 o 2 -16 1 198.39 146.47 70.62 o 3 -16 1 796.88 995.91 170.72 o 4 -16 1 41.91 62.15 72.52 o 5 -16 1 172.50 176.22 107.21 o 6 -16 1 35.67 66.00 108.15 o -8 -15 1 3.77 -40.65 67.23 o -7 -15 1 21.50 82.04 66.32 o -6 -15 1 27.99 54.56 31.82 o -5 -15 1 68.19 113.30 37.67 o -4 -15 1 36.57 43.66 53.62 o -3 -15 1 397.86 393.37 61.79 o -2 -15 1 203.10 129.21 45.96 o -1 -15 1 905.97 822.81 74.49 o 0 -15 1 155.16 135.69 37.39 o 1 -15 1 957.57 1109.96 155.46 o 2 -15 1 41.56 122.71 64.25 o 3 -15 1 1023.37 1072.63 174.78 o 4 -15 1 117.92 76.87 67.39 o 5 -15 1 262.72 421.49 117.17 o 6 -15 1 17.28 -40.43 42.60 o -8 -14 1 15.51 60.35 63.71 o -7 -14 1 1.44 2.64 49.18 o -6 -14 1 117.76 150.12 38.71 o -5 -14 1 6.81 28.44 33.61 o -4 -14 1 226.18 252.41 85.63 o -3 -14 1 3.16 37.34 25.46 o -2 -14 1 1010.86 1006.35 124.56 o -1 -14 1 261.72 412.16 52.62 o 0 -14 1 594.59 593.21 71.80 o 1 -14 1 568.81 612.03 113.43 o 2 -14 1 984.44 891.34 141.70 o 3 -14 1 294.78 270.84 89.67 o 4 -14 1 682.53 828.92 149.29 o 5 -14 1 113.68 183.27 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