data_2240588 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 13.5860 _cell_length_b 15.5857 _cell_length_c 30.9389 _exptl_crystal_F_000 2848.00 _reflns_d_resolution_high 0.8078 _cod_data_source_file su5121IIIsup4.hkl _cod_data_source_block III _shelx_title ' KUM-12' _shelx_refln_list_code 4 _shelx_f_calc_maximum 641.38 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 6 0 0 15.97 3.84 9.97 o 8 0 0 54295.36 67178.15 3888.13 o 10 0 0 811.50 984.47 89.44 o 12 0 0 12270.97 14552.81 410.94 o 14 0 0 1491.42 1358.17 77.74 o 16 0 0 17285.82 20662.63 438.31 o 1 1 0 244.43 273.03 34.26 o 2 1 0 7593.09 8001.90 67.17 o 3 1 0 635.92 596.68 19.93 o 4 1 0 9763.15 10715.57 351.54 o 5 1 0 2188.63 2276.99 62.12 o 6 1 0 15593.14 17831.16 177.72 o 7 1 0 159.16 203.83 20.12 o 8 1 0 1588.99 1762.83 54.67 o 9 1 0 753.71 833.34 134.79 o 10 1 0 4008.21 4511.62 139.53 o 11 1 0 15.35 51.40 12.28 o 12 1 0 13.30 216.83 41.45 o 13 1 0 8.09 -4.27 12.58 o 14 1 0 358.64 462.83 33.39 o 15 1 0 135.55 194.02 26.91 o 16 1 0 6.61 135.32 28.53 o 0 2 0 58160.34 59650.70 2247.78 o 1 2 0 8892.77 7920.40 372.36 o 2 2 0 3204.73 2732.73 100.25 o 3 2 0 12118.60 12889.06 591.88 o 4 2 0 37151.28 40308.30 776.03 o 5 2 0 467.18 543.32 19.43 o 6 2 0 2898.18 2835.07 74.41 o 7 2 0 2321.25 2420.21 63.79 o 8 2 0 5948.70 7554.71 322.01 o 9 2 0 16.00 28.44 21.40 o 10 2 0 296.04 328.09 37.89 o 11 2 0 33.16 29.28 10.08 o 12 2 0 291.80 312.28 35.51 o 13 2 0 177.98 149.62 23.32 o 14 2 0 9.68 26.13 13.86 o 15 2 0 50.13 65.95 17.08 o 16 2 0 2129.44 2213.37 67.76 o 1 3 0 70.60 64.62 6.50 o 2 3 0 297.68 312.22 12.24 o 3 3 0 432.32 455.01 16.65 o 4 3 0 204.24 213.08 8.94 o 5 3 0 338.94 395.86 18.97 o 6 3 0 586.27 654.21 39.49 o 7 3 0 731.99 891.03 50.50 o 8 3 0 647.14 782.44 33.44 o 9 3 0 1233.66 1306.71 75.29 o 10 3 0 82.81 107.11 28.70 o 11 3 0 410.58 383.09 29.55 o 12 3 0 171.71 162.57 19.52 o 13 3 0 627.66 693.53 48.27 o 14 3 0 182.71 160.94 22.82 o 15 3 0 37.68 51.32 15.85 o 16 3 0 53.82 68.00 13.57 o 0 4 0 16325.98 15490.19 216.11 o 1 4 0 19750.11 21327.39 874.30 o 2 4 0 11912.45 11846.86 135.87 o 3 4 0 6512.18 6015.27 183.76 o 4 4 0 3815.46 3285.42 62.24 o 5 4 0 8241.76 7602.91 255.30 o 6 4 0 1321.13 1264.69 37.53 o 7 4 0 458.18 388.98 20.89 o 8 4 0 5.51 3.15 11.51 o 9 4 0 196.83 276.56 56.62 o 10 4 0 31.78 17.99 14.27 o 11 4 0 1.07 2.38 12.13 o 12 4 0 1.08 -7.81 10.24 o 13 4 0 21.53 64.86 17.92 o 14 4 0 19.21 21.53 10.06 o 15 4 0 17.07 6.20 11.91 o 16 4 0 0.04 16.57 13.21 o 1 5 0 297.54 300.53 16.22 o 2 5 0 1474.38 1431.49 32.96 o 3 5 0 1831.72 1815.54 69.06 o 4 5 0 8298.48 8539.83 185.72 o 5 5 0 2279.97 2434.88 176.48 o 6 5 0 1790.78 1853.04 44.63 o 7 5 0 2983.02 3099.78 86.13 o 8 5 0 3722.17 3838.02 102.72 o 9 5 0 1278.17 1080.98 65.63 o 10 5 0 99.52 63.74 14.97 o 11 5 0 727.24 623.95 52.03 o 12 5 0 408.41 421.53 45.00 o 13 5 0 217.00 252.81 28.72 o 14 5 0 17.53 23.28 10.49 o 15 5 0 72.47 70.66 16.62 o 16 5 0 49.88 55.45 16.35 o 0 6 0 231.67 233.05 25.04 o 1 6 0 1912.66 2143.28 56.51 o 2 6 0 7205.47 8473.37 274.89 o 3 6 0 403.20 423.61 26.85 o 4 6 0 37.54 31.08 10.78 o 5 6 0 379.76 398.69 20.43 o 6 6 0 165.80 198.30 17.32 o 7 6 0 187.32 182.84 17.54 o 8 6 0 118.21 112.20 18.74 o 9 6 0 29.72 56.20 17.60 o 10 6 0 3.91 15.58 12.33 o 11 6 0 158.94 127.06 26.66 o 12 6 0 2.74 0.52 13.42 o 13 6 0 18.47 12.93 15.58 o 14 6 0 1.74 -5.40 12.47 o 15 6 0 16.18 19.73 12.22 o 1 7 0 17.86 32.37 8.34 o 2 7 0 306.77 346.22 26.16 o 3 7 0 380.18 422.39 46.45 o 4 7 0 2794.74 3200.41 101.40 o 5 7 0 1.64 18.81 7.79 o 6 7 0 78.32 128.89 16.87 o 7 7 0 704.42 747.91 35.89 o 8 7 0 856.32 853.17 46.76 o 9 7 0 25.86 15.82 11.30 o 10 7 0 51.14 52.97 20.70 o 11 7 0 44.09 36.25 17.62 o 12 7 0 54.63 99.31 23.86 o 13 7 0 0.55 -1.82 15.66 o 14 7 0 3.80 -1.65 11.13 o 15 7 0 10.15 11.02 8.39 o 0 8 0 0.83 9.46 21.10 o 1 8 0 22.98 9.64 14.47 o 2 8 0 42735.73 50497.98 3589.25 o 3 8 0 362.67 310.31 35.50 o 4 8 0 46.25 76.50 21.25 o 5 8 0 0.75 5.14 10.65 o 6 8 0 3893.75 4255.86 93.91 o 7 8 0 30.39 24.23 11.33 o 8 8 0 20.44 4.32 11.25 o 9 8 0 130.11 166.36 23.01 o 10 8 0 1.92 3.02 19.32 o 11 8 0 31.47 5.00 14.45 o 12 8 0 38.67 24.28 16.36 o 13 8 0 78.40 101.59 22.72 o 14 8 0 69.89 44.27 12.33 o 15 8 0 8.83 4.28 12.27 o 1 9 0 34.84 22.80 13.23 o 2 9 0 128.52 136.71 24.59 o 3 9 0 271.41 290.92 35.04 o 4 9 0 1057.55 1047.21 71.92 o 5 9 0 615.60 540.46 55.29 o 6 9 0 72.46 65.52 16.19 o 7 9 0 640.92 651.28 46.09 o 8 9 0 371.74 354.31 24.85 o 9 9 0 568.03 545.77 31.07 o 10 9 0 0.35 -6.11 11.30 o 11 9 0 23.44 21.52 16.40 o 12 9 0 13.90 12.00 16.91 o 13 9 0 35.78 25.86 10.96 o 14 9 0 14.28 11.65 10.25 o 0 10 0 312.06 304.86 48.16 o 1 10 0 1331.13 1214.54 67.07 o 2 10 0 5450.96 5088.31 147.51 o 3 10 0 2107.14 1962.77 92.43 o 4 10 0 60.20 54.62 19.01 o 5 10 0 281.13 279.06 28.80 o 6 10 0 148.25 90.07 17.48 o 7 10 0 46.13 24.15 11.31 o 8 10 0 18.59 -12.84 12.84 o 9 10 0 554.29 468.86 33.31 o 10 10 0 50.14 26.93 12.07 o 11 10 0 270.66 267.99 103.00 o 12 10 0 154.80 146.44 43.82 o 13 10 0 587.00 607.01 38.33 o 14 10 0 39.14 16.83 17.44 o 1 11 0 40.89 60.67 23.55 o 2 11 0 9.31 15.35 14.83 o 3 11 0 700.16 844.05 115.82 o 4 11 0 84.19 69.25 28.64 o 5 11 0 187.66 204.25 28.70 o 6 11 0 8.04 2.67 16.84 o 7 11 0 1053.67 1063.19 51.19 o 8 11 0 4.27 -2.52 12.61 o 9 11 0 215.63 261.89 25.24 o 10 11 0 100.83 152.53 28.90 o 11 11 0 131.15 198.31 33.77 o 12 11 0 43.16 71.86 20.68 o 13 11 0 48.99 92.78 14.64 o 0 12 0 10948.77 10348.56 317.91 o 1 12 0 9870.88 9281.25 212.67 o 2 12 0 6378.33 5721.30 164.66 o 3 12 0 9971.74 9224.58 256.28 o 4 12 0 4785.42 4555.20 105.96 o 5 12 0 2292.00 2065.45 82.62 o 6 12 0 220.42 168.86 26.07 o 7 12 0 386.82 322.97 34.40 o 8 12 0 184.29 156.09 19.86 o 9 12 0 253.12 251.81 25.53 o 10 12 0 438.03 441.13 36.94 o 11 12 0 960.82 1170.40 90.90 o 12 12 0 69.09 95.91 15.74 o 13 12 0 9.26 40.33 13.04 o 1 13 0 54.54 43.55 12.08 o 2 13 0 3785.34 3610.05 93.06 o 3 13 0 2430.74 2560.09 92.69 o 4 13 0 1112.30 1058.47 56.59 o 5 13 0 2051.51 1952.91 69.69 o 6 13 0 13490.97 13615.57 200.16 o 7 13 0 2551.13 2539.48 88.80 o 8 13 0 614.52 606.69 37.47 o 9 13 0 2136.70 2142.78 58.53 o 10 13 0 6307.82 6629.78 150.88 o 11 13 0 1006.10 1008.31 53.75 o 12 13 0 54.88 48.62 13.33 o 0 14 0 26136.12 27987.54 435.48 o 1 14 0 1562.02 1542.04 71.12 o 2 14 0 35.49 47.21 15.53 o 3 14 0 3999.23 3914.82 114.80 o 4 14 0 12858.95 13271.48 194.43 o 5 14 0 18.96 11.77 12.26 o 6 14 0 0.57 1.24 11.63 o 7 14 0 791.97 855.53 43.34 o 8 14 0 1028.69 1209.95 48.43 o 9 14 0 6.80 8.06 10.88 o 10 14 0 7.00 -3.12 11.67 o 11 14 0 31.27 53.30 18.61 o 1 15 0 48.45 54.67 12.02 o 2 15 0 70.35 54.99 14.29 o 3 15 0 5.87 4.06 13.24 o 4 15 0 323.33 356.75 33.56 o 5 15 0 293.71 345.82 31.36 o 6 15 0 873.63 806.45 44.42 o 7 15 0 16.38 14.08 8.58 o 8 15 0 154.49 125.25 14.63 o 9 15 0 7.99 14.50 8.06 o 0 16 0 744.82 763.78 82.06 o 1 16 0 17.95 32.56 18.86 o 2 16 0 31.93 50.71 13.37 o 3 16 0 18.97 21.96 10.94 o 4 16 0 297.79 317.68 29.90 o 5 16 0 125.68 130.70 18.93 o 6 16 0 0.11 1.58 9.45 o 7 16 0 102.90 114.83 16.33 o 8 16 0 35.16 28.04 7.80 o 1 17 0 7.34 17.58 13.16 o 2 17 0 76.68 70.19 15.33 o 3 17 0 16.26 20.28 11.15 o 4 17 0 7.23 7.64 11.66 o 5 17 0 180.26 210.58 25.37 o 6 17 0 168.89 163.13 20.54 o 7 17 0 64.69 73.55 14.40 o 0 18 0 936.35 1020.50 79.03 o 1 18 0 319.01 395.95 29.11 o 2 18 0 148.34 175.82 23.48 o 3 18 0 475.58 556.80 38.77 o 4 18 0 576.20 656.09 40.03 o 5 18 0 58.11 59.22 12.90 o 6 18 0 17.21 47.96 16.75 o 1 19 0 5.67 8.91 7.02 o 2 19 0 74.03 88.67 15.26 o 1 0 1 225.31 210.49 18.78 o 2 0 1 3.15 36.81 3.63 o 3 0 1 1940.46 1999.46 70.86 o 4 0 1 411366.84 399771.34 3163.70 o 5 0 1 6249.21 6601.23 72.25 o 6 0 1 958.85 786.66 26.26 o 7 0 1 2222.06 2494.66 93.02 o 8 0 1 168509.91 189053.28 2913.04 o 9 0 1 5945.65 6324.57 159.33 o 10 0 1 1918.72 1833.66 88.19 o 11 0 1 1007.49 1049.77 43.15 o 12 0 1 25264.39 25139.33 413.25 o 13 0 1 1847.38 1947.54 67.58 o 14 0 1 353.50 419.79 31.30 o 15 0 1 193.11 197.21 21.56 o 16 0 1 853.00 1255.01 67.80 o -16 1 1 1020.11 1177.21 61.35 o -15 1 1 2387.46 2250.10 66.69 o -14 1 1 679.15 691.00 56.49 o -13 1 1 116.58 133.62 20.22 o -12 1 1 13891.97 14786.53 294.26 o -11 1 1 4944.37 4529.62 102.70 o -10 1 1 854.73 960.01 125.35 o -9 1 1 1233.92 1267.24 68.43 o -8 1 1 65225.47 70391.78 1736.05 o -7 1 1 4749.60 4849.79 154.02 o -6 1 1 2916.28 3018.54 54.40 o -5 1 1 8277.18 8116.34 283.17 o -4 1 1 120305.98 126220.85 1186.52 o -3 1 1 722.71 784.45 44.28 o -2 1 1 35824.67 36832.86 1032.80 o -1 1 1 10000.54 7916.62 167.17 o 1 1 1 9956.93 9257.74 321.15 o 2 1 1 36021.67 36685.52 1009.64 o 3 1 1 537.04 442.39 12.69 o 4 1 1 121775.80 129796.96 922.26 o 5 1 1 8147.03 8246.34 280.06 o 6 1 1 2944.74 3088.76 75.66 o 7 1 1 4572.04 4991.92 78.42 o 8 1 1 66416.52 75595.70 687.89 o 9 1 1 1196.00 1235.30 67.51 o 10 1 1 788.37 852.39 59.46 o 11 1 1 4920.71 4855.73 100.45 o 12 1 1 13874.95 14818.16 291.08 o 13 1 1 118.56 104.02 20.36 o 14 1 1 658.85 648.96 38.54 o 15 1 1 2411.42 2586.67 82.60 o 16 1 1 975.64 1083.30 58.32 o -16 2 1 641.06 734.81 39.18 o -15 2 1 112.87 162.54 23.25 o -14 2 1 133.32 161.50 20.86 o -13 2 1 629.61 526.16 34.75 o -12 2 1 3237.14 3504.65 147.76 o -11 2 1 29.95 33.89 14.82 o -10 2 1 604.32 564.34 49.74 o -9 2 1 1430.41 1435.02 72.83 o -8 2 1 3204.43 3709.96 117.56 o -7 2 1 55.76 122.10 18.68 o -6 2 1 1309.09 1277.70 54.30 o -5 2 1 4810.02 5004.41 113.04 o -4 2 1 652.47 639.28 33.06 o -3 2 1 32.30 33.75 7.26 o -2 2 1 5633.96 5963.69 86.04 o -1 2 1 2700.89 2627.62 79.63 o 0 2 1 78.25 104.13 6.56 o 1 2 1 2734.03 3031.48 41.61 o 2 2 1 5495.04 5823.15 262.08 o 3 2 1 60.34 65.97 6.12 o 4 2 1 413.72 399.48 17.29 o 5 2 1 4971.24 5225.78 56.68 o 6 2 1 1265.85 1444.01 36.18 o 7 2 1 92.12 132.91 13.27 o 8 2 1 3086.22 3398.54 100.27 o 9 2 1 1408.30 1397.41 83.81 o 10 2 1 590.43 635.07 40.92 o 11 2 1 31.14 55.00 11.67 o 12 2 1 3264.19 3293.84 101.78 o 13 2 1 594.63 489.82 39.87 o 14 2 1 132.98 145.08 19.87 o 15 2 1 106.47 176.11 22.95 o 16 2 1 644.97 874.94 52.53 o -16 3 1 53.70 49.48 16.64 o -15 3 1 764.18 727.49 41.89 o -14 3 1 102.88 120.39 21.31 o -13 3 1 50.47 57.35 13.49 o -12 3 1 316.89 307.94 27.07 o -11 3 1 842.66 887.62 53.24 o -10 3 1 671.12 684.98 42.43 o -9 3 1 18.61 53.11 14.00 o -8 3 1 1054.14 1067.97 38.67 o -7 3 1 841.40 887.68 38.54 o -6 3 1 3170.49 3248.94 126.36 o -5 3 1 32.96 44.52 7.61 o -4 3 1 1093.29 1118.52 36.34 o -3 3 1 825.99 771.46 30.98 o -2 3 1 2142.77 2135.66 59.44 o -1 3 1 991.55 959.16 17.61 o 0 3 1 151.60 149.23 14.43 o 1 3 1 926.51 923.54 28.30 o 2 3 1 2455.30 2409.50 41.49 o 3 3 1 606.44 522.41 19.36 o 4 3 1 1098.27 1057.19 27.91 o 5 3 1 11.58 25.39 6.30 o 6 3 1 3200.79 3387.00 61.98 o 7 3 1 773.12 838.38 31.60 o 8 3 1 968.94 968.31 43.12 o 9 3 1 21.59 52.10 13.91 o 10 3 1 607.88 601.16 40.00 o 11 3 1 887.94 948.54 40.42 o 12 3 1 303.06 327.75 31.31 o 13 3 1 42.63 45.94 16.08 o 14 3 1 103.59 89.32 23.26 o 15 3 1 757.51 776.99 44.15 o 16 3 1 49.89 75.78 14.04 o -16 4 1 69.97 97.12 19.27 o -15 4 1 23.34 15.70 11.79 o -14 4 1 74.34 96.78 15.41 o -13 4 1 407.87 461.61 38.41 o -12 4 1 186.62 213.16 26.62 o -11 4 1 141.92 171.02 23.51 o -10 4 1 437.28 421.29 33.80 o -9 4 1 899.54 1007.37 67.81 o -8 4 1 7.62 18.23 11.27 o -7 4 1 2130.43 2139.56 48.91 o -6 4 1 2402.69 2259.71 47.35 o -5 4 1 1511.45 1422.74 34.78 o -4 4 1 3806.11 3451.98 91.87 o -3 4 1 11871.65 10979.46 195.74 o -2 4 1 8647.14 7753.12 119.63 o -1 4 1 14557.18 13838.49 321.28 o 0 4 1 10797.82 10607.17 380.60 o 1 4 1 14676.95 14868.29 767.53 o 2 4 1 8294.61 7697.67 191.57 o 3 4 1 12108.01 11269.22 278.08 o 4 4 1 3464.09 3083.71 52.76 o 5 4 1 1773.51 1693.28 53.13 o 6 4 1 2208.66 2669.52 63.29 o 7 4 1 2225.52 2328.39 60.76 o 8 4 1 10.03 26.72 10.07 o 9 4 1 918.16 1031.54 54.02 o 10 4 1 425.24 445.67 34.37 o 11 4 1 166.79 160.54 19.31 o 12 4 1 180.50 223.95 23.38 o 13 4 1 411.75 487.13 39.71 o 14 4 1 75.18 80.87 13.33 o 15 4 1 28.32 10.24 11.59 o 16 4 1 64.64 73.72 17.90 o -16 5 1 11.65 -0.04 10.61 o -15 5 1 54.09 46.66 13.93 o -14 5 1 29.00 24.00 11.53 o -13 5 1 96.96 119.23 21.31 o -12 5 1 11.10 28.70 12.14 o -11 5 1 200.01 217.92 26.42 o -10 5 1 264.39 259.50 27.57 o -9 5 1 1341.29 1441.81 62.12 o -8 5 1 405.17 433.83 28.31 o -7 5 1 105.82 99.41 12.48 o -6 5 1 645.54 702.33 27.40 o -5 5 1 3657.28 3980.60 70.66 o -4 5 1 434.26 417.69 30.15 o -3 5 1 292.70 308.13 12.94 o -2 5 1 245.97 316.43 15.81 o -1 5 1 1745.38 2068.15 45.08 o 0 5 1 2817.20 3157.74 53.61 o 1 5 1 1775.62 2064.49 46.33 o 2 5 1 262.17 334.58 18.94 o 3 5 1 401.27 392.95 15.74 o 4 5 1 356.30 397.58 20.65 o 5 5 1 3714.52 4041.53 90.83 o 6 5 1 700.02 797.54 28.68 o 7 5 1 63.30 73.03 13.11 o 8 5 1 426.53 462.58 28.82 o 9 5 1 1350.01 1480.07 75.91 o 10 5 1 293.49 274.89 24.53 o 11 5 1 195.81 225.05 33.77 o 12 5 1 13.73 26.69 15.73 o 13 5 1 99.50 81.42 20.39 o 14 5 1 26.70 16.74 9.73 o 15 5 1 64.22 68.43 12.55 o 16 5 1 9.85 11.16 10.46 o -15 6 1 21.84 28.12 14.19 o -14 6 1 19.05 1.47 12.80 o -13 6 1 13.44 13.31 11.25 o -12 6 1 83.72 87.49 23.02 o -11 6 1 32.96 24.18 26.89 o -10 6 1 74.11 60.35 16.70 o -9 6 1 148.81 173.89 27.84 o -8 6 1 128.54 200.31 23.14 o -7 6 1 211.42 196.56 22.19 o -6 6 1 67.08 88.08 16.98 o -5 6 1 339.29 339.57 18.85 o -4 6 1 110.15 114.92 10.81 o -3 6 1 56.14 89.54 11.70 o -2 6 1 272.97 301.76 17.79 o -1 6 1 73.46 76.60 11.19 o 0 6 1 220.85 166.78 12.94 o 1 6 1 69.26 56.30 12.84 o 2 6 1 278.16 338.25 21.23 o 3 6 1 47.46 73.68 10.32 o 4 6 1 155.85 153.10 15.90 o 5 6 1 354.13 337.59 25.34 o 6 6 1 63.95 83.64 12.44 o 7 6 1 280.45 304.22 29.71 o 8 6 1 116.82 158.48 20.91 o 9 6 1 150.32 211.24 49.49 o 10 6 1 56.27 39.70 35.55 o 11 6 1 51.49 61.04 18.46 o 12 6 1 88.38 92.35 22.67 o 13 6 1 8.27 11.86 13.62 o 14 6 1 16.23 25.65 13.90 o 15 6 1 21.93 31.02 11.63 o -15 7 1 18.73 6.31 9.63 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