#------------------------------------------------------------------------------
#$Date: 2015-05-13 23:13:15 +0300 (Wed, 13 May 2015) $
#$Revision: 136384 $
#$URL: file:///home/coder/svn-repositories/cod/cif/2/24/05/2240592.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2240592
loop_
_publ_author_name
'Lee, Jeonghoo H.'
'Kang, Ji Hoon'
'Lim, Sung-Chul'
'Hong, Seung-Tae'
_publ_section_title
;
Crystal structure of barium perchlorate anhydrate, Ba(ClO~4~)~2~, from
laboratory X-ray powder data
;
_journal_coeditor_code CV5487
_journal_issue 6
_journal_name_full 'Acta Crystallographica Section E'
_journal_page_first 588
_journal_page_last 591
_journal_paper_doi 10.1107/S2056989015008828
_journal_volume 71
_journal_year 2015
_chemical_formula_analytical BaCl2O8
_chemical_formula_iupac 'Ba (ClO4)2'
_chemical_formula_moiety '2(Cl O4), Ba'
_chemical_formula_structural Ba(ClO4)2
_chemical_formula_sum 'Ba Cl2 O8'
_chemical_formula_weight 336.23
_chemical_name_common Barium_perchlorate_anhydrate
_chemical_name_systematic
;
Barium perchlorate anhydrate
;
_space_group_IT_number 70
_symmetry_cell_setting orthorhombic
_symmetry_space_group_name_Hall '-F 2uv 2vw'
_symmetry_space_group_name_H-M 'F d d d :2'
_audit_creation_method 'from EXP file using GSAS2CIF'
_cell_angle_alpha 90.0
_cell_angle_beta 90.0
_cell_angle_gamma 90.0
_cell_formula_units_Z 8
_cell_length_a 14.304(9)
_cell_length_b 11.688(7)
_cell_length_c 7.2857(4)
_cell_measurement_temperature 298
_cell_volume 1218.1(11)
_computing_cell_refinement
;
GSAS (Larson & Von Dreele, 2000)
;
_computing_data_collection
;
X'Pert Data Collector (PANalytical, 2011)
;
_computing_data_reduction
;
X'Pert HighScore-Plus (PANalytical, 2011)
;
_computing_molecular_graphics
;
ATOMS (Dowty, 2000)
;
_computing_publication_material
;
GSAS (Larson & Von Dreele, 2000)
;
_computing_structure_refinement
;
GSAS (Larson & Von Dreele, 2000)
;
_computing_structure_solution
;
SHELXS97 (Sheldrick, 2008) and CRYSTALS (Betteridge et al.,
2003)
;
_diffrn_ambient_temperature 298
_diffrn_measurement_device_type 'PANalytical Empyrean'
_diffrn_radiation_type 'Cu K\a~1~'
_diffrn_radiation_wavelength 1.54059
_exptl_absorpt_correction_T_max 1.00000
_exptl_absorpt_correction_T_min 1.00000
_exptl_absorpt_process_details
; GSAS Absorption/surface roughness correction: function number 0
No correction is applied.
;
_exptl_crystal_density_diffrn 3.667
_exptl_crystal_F_000 1232.0
_pd_block_id 2015-04-21T15:23|B5|SungChul_Lim|PANalytical
_pd_calc_method 'Rietveld Refinement'
_pd_char_colour white
_pd_instr_location
;
;
_pd_meas_2theta_range_inc 0.026
_pd_meas_2theta_range_max 129.96381
_pd_meas_2theta_range_min 14.9918
_pd_meas_number_of_points 4423
_pd_meas_scan_method step
_pd_phase_name 'Barium perchlorate anhydrate'
_pd_proc_2theta_range_inc 0.026
_pd_proc_2theta_range_max 129.96381
_pd_proc_2theta_range_min 14.9918
_pd_proc_info_datetime 2015-04-21T15:23:13
_pd_proc_info_excluded_regions
;
;
_pd_proc_ls_background_function
; GSAS Background function number 1 with 36 terms.
Shifted Chebyshev function of 1st kind
1: 567.648 2: -857.136 3: 662.653 4: -377.264
5: 131.512 6: 59.5938 7: -169.995 8: 206.701
9: -185.404 10: 133.783 11: -68.7256 12: 6.71856
13: 43.4515 14: -72.2732 15: 82.7653 16: -73.3661
17: 50.0183 18: -22.8495 19: -2.57480 20: 20.6662
21: -29.1651 22: 28.9267 23: -24.2542 24: 14.4066
25: -5.32227 26: -4.03875 27: 10.7050 28: -13.4416
29: 11.1646 30: -9.08855 31: 2.53787 32: -0.292410
33: -1.46976 34: 0.544854 35: -1.31862 36: 0.893355
;
_pd_proc_ls_peak_cutoff 0.00100
_pd_proc_ls_pref_orient_corr
; March-Dollase
AXIS 1 Ratio= 0.97385 h= 1.000 k= 0.000 l= 0.000
Prefered orientation correction range: Min= 0.96103, Max= 1.08275
;
_pd_proc_ls_profile_function
;
CW Profile function number 3 with 19 terms
Pseudovoigt profile coefficients as parameterized in
P. Thompson, D.E. Cox & J.B. Hastings (1987). J. Appl.
Cryst.,20,79-83.
Asymmetry correction of L.W. Finger, D.E. Cox & A. P. Jephcoat (1994).
J. Appl. Cryst.,27,892-900.
Peak tails are ignored where the intensity is below 0.0010 times the peak
Aniso. broadening axis 0.0 0.0 1.0
;
_pd_proc_ls_prof_R_factor 0.0405
_pd_proc_ls_prof_wR_expected 0.0452
_pd_proc_ls_prof_wR_factor 0.0600
_pd_proc_number_of_points 4423
_pd_spec_mounting 'packed powder'
_pd_spec_mount_mode reflection
_pd_spec_shape flat_sheet
_pd_spec_size_axial 20
_pd_spec_size_equat 20
_pd_spec_size_thick 0
_refine_ls_goodness_of_fit_all 1.33
_refine_ls_matrix_type full
_refine_ls_number_parameters 25
_refine_ls_number_restraints 0
_refine_ls_shift/su_max 0.01
_refine_ls_shift/su_mean 0.00
_reflns_number_total 265
_cod_data_source_file cv5487sup1.cf
_cod_data_source_block I
_cod_cif_authors_sg_H-M 'F d d d'
_cod_cif_authors_sg_Hall -F_2uv_2vw
_cod_database_code 2240592
loop_
_symmetry_equiv_pos_site_id
_symmetry_equiv_pos_as_xyz
1 +x,+y,+z
2 -x,+y+1/4,+z+1/4
3 +x+1/4,-y,+z+1/4
4 -x+3/4,-y+1/4,+z+1/2
5 -x,-y,-z
6 +x,-y+3/4,-z+3/4
7 -x+3/4,+y,-z+3/4
8 +x+1/4,+y+3/4,-z+1/2
9 +x,+y+1/2,+z+1/2
10 -x,+y+3/4,+z+3/4
11 +x+1/4,-y+1/2,+z+3/4
12 -x+3/4,-y+3/4,+z
13 -x,-y+1/2,-z+1/2
14 +x,-y+1/4,-z+1/4
15 -x+3/4,+y+1/2,-z+1/4
16 +x+1/4,+y+1/4,-z
17 +x+1/2,+y,+z+1/2
18 -x+1/2,+y+1/4,+z+3/4
19 +x+3/4,-y,+z+3/4
20 -x+1/4,-y+1/4,+z
21 -x+1/2,-y,-z+1/2
22 +x+1/2,-y+3/4,-z+1/4
23 -x+1/4,+y,-z+1/4
24 +x+3/4,+y+3/4,-z
25 +x+1/2,+y+1/2,+z
26 -x+1/2,+y+3/4,+z+1/4
27 +x+3/4,-y+1/2,+z+1/4
28 -x+1/4,-y+3/4,+z+1/2
29 -x+1/2,-y+1/2,-z
30 +x+1/2,-y+1/4,-z+3/4
31 -x+1/4,+y+1/2,-z+3/4
32 +x+3/4,+y+1/4,-z+1/2
loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_thermal_displace_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
Ba Ba1 0.125 0.125 0.125 0.0139(2) Uiso 1.0 8
Cl Cl1 0.125 0.42875(18) 0.125 0.0160(7) Uiso 1.0 16
O O1 0.0471(3) 0.3533(3) 0.1575(5) 0.0162(11) Uiso 1.0 32
O O2 0.1412(3) 0.5016(4) 0.2807(4) 0.0170(12) Uiso 1.0 32
loop_
_atom_type_symbol
_atom_type_number_in_cell
_atom_type_scat_Cromer_Mann_a1
_atom_type_scat_Cromer_Mann_a2
_atom_type_scat_Cromer_Mann_a3
_atom_type_scat_Cromer_Mann_a4
_atom_type_scat_Cromer_Mann_b1
_atom_type_scat_Cromer_Mann_b2
_atom_type_scat_Cromer_Mann_b3
_atom_type_scat_Cromer_Mann_b4
_atom_type_scat_Cromer_Mann_c
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Ba 8.0 20.3361 3.21600 19.2970 0.27560 10.8880 20.2073 2.69590 167.202 2.77310
0.000 0.000 International_Tables_Vol_C
Cl 16.0 11.4604 0.01040 7.19640 1.16620 6.25560 18.5194 1.64550 47.7784 -9.5574
0.000 0.000 International_Tables_Vol_C
O 64.0 3.04850 13.2771 2.28680 5.70110 1.54630 0.32390 0.86700 32.9089 0.25080
0.000 0.000 International_Tables_Vol_C
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle
_geom_angle_publ_flag
O1 Ba1 O1 1_555 8_545 110.93(10) n
O1 Ba1 O1 1_555 10_544 78.56(7) n
O1 Ba1 O1 1_555 11_554 106.64(7) n
O1 Ba1 O1 1_555 13_555 63.56(12) n
O1 Ba1 O1 1_555 14_555 134.82(15) n
O1 Ba1 O1 1_555 20_555 170.64(14) n
O1 Ba1 O1 1_555 23_555 46.25(15) n
O1 Ba1 O2 1_555 6_555 60.21(10) n
O1 Ba1 O2 1_555 9_544 123.92(10) n
O1 Ba1 O2 1_555 28_554 65.35(10) n
O1 Ba1 O2 1_555 31_545 110.84(10) n
O1 Ba1 O1 8_545 10_544 170.09(14) n
O1 Ba1 O1 8_545 11_554 66.21(14) n
O1 Ba1 O1 8_545 13_555 114.73(14) n
O1 Ba1 O2 8_545 6_555 60.66(10) n
O1 Ba1 O2 8_545 9_544 110.87(10) n
O1 Ba1 O2 8_545 28_554 125.15(10) n
O1 Ba1 O2 8_545 31_545 63.76(10) n
O1 Ba1 O1 20_555 23_555 134.82(15) n
O2 Ba1 O2 6_567 9_544 170.85(15) n
O2 Ba1 O2 6_555 28_554 120.42(15) n
O2 Ba1 O2 6_555 31_545 60.43(15) n
O1 Cl1 O1 1_555 23_555 104.5(3) n
O1 Cl1 O2 1_555 1_555 110.96(19) n
O1 Cl1 O2 1_555 23_555 111.6(2) n
O2 Cl1 O2 1_555 23_555 107.3(3) n
Ba1 O1 Ba1 1_555 2_555 116.44(12) n
Ba1 O1 Cl1 1_555 1_555 104.6(2) n
Ba1 O1 Cl1 2_555 1_555 133.1(2) n
Ba1 O2 Cl1 6_555 1_555 164.5(2) n
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
Ba1 O1 1_555 2.901(4) y
Ba1 O1 8_545 2.939(4) y
Ba1 O1 10_544 2.939(4) ?
Ba1 O1 11_554 2.939(4) ?
Ba1 O1 13_555 2.939(4) ?
Ba1 O1 14_555 2.901(4) y
Ba1 O1 20_555 2.901(4) ?
Ba1 O1 23_555 2.901(4) ?
Ba1 O2 6_555 2.903(4) y
Ba1 O2 9_544 2.903(4) ?
Ba1 O2 28_554 2.903(4) ?
Ba1 O2 31_545 2.903(4) ?
Cl1 O1 1_555 1.441(4) y
Cl1 O1 23_555 1.441(4) n
Cl1 O2 1_555 1.437(4) y
Cl1 O2 23_555 1.437(4) n
loop_
_pd_proc_ls_weight
_pd_proc_intensity_bkg_calc
_pd_calc_intensity_total
_pd_meas_counts_total
0.000486 2031.74194 2046.78674 2059.0
0.000479 2027.52161 2043.96497 2089.0
0.000490 2024.01160 2042.05774 2039.0
0.000496 2021.16577 2041.06042 2018.0
0.000486 2018.93884 2040.98120 2059.0
0.000502 2017.28857 2041.84534 1993.0
0.000505 2016.17456 2043.70068 1980.0
0.000500 2015.55835 2046.62585 2001.0
0.000487 2015.40344 2050.74023 2055.0
0.000490 2015.67542 2056.22363 2042.0
0.000482 2016.34180 2063.34106 2076.0
0.000490 2017.37146 2072.48560 2039.0
0.000480 2018.73535 2084.25244 2082.0
0.000484 2020.40588 2099.55444 2066.0
0.000467 2022.35754 2119.84668 2140.0
0.000475 2024.56592 2147.52686 2104.0
0.000449 2027.00781 2186.75195 2227.0
0.000443 2029.66248 2245.21899 2255.0
0.000408 2032.50891 2338.48999 2452.0
0.000372 2035.52991 2509.27173 2688.0
0.0002810 2038.70703 2985.80688 3559.0
0.0001921 2042.02417 4854.96094 5205.0
0.0001071 2045.46692 9678.92676 9336.0
0.0000796 2049.02100 13298.39453 12557.0
0.0001168 2052.67358 8877.30664 8559.0
0.0002279 2056.41333 4452.28271 4388.0
0.0003383 2060.22876 2898.22900 2956.0
0.000400 2064.11108 2506.02393 2501.0
0.000437 2068.05029 2358.43726 2287.0
0.000462 2072.03906 2278.27441 2164.0
0.000465 2076.07007 2229.80737 2152.0
0.000463 2080.13599 2199.01099 2161.0
0.000458 2084.23193 2178.82129 2183.0
0.000476 2088.35229 2165.37207 2102.0
0.000463 2092.49316 2156.40088 2160.0
0.000449 2096.65039 2150.51953 2229.0
0.000462 2100.82031 2146.83716 2164.0
0.000466 2105.00073 2144.76025 2148.0
0.000461 2109.18945 2143.88403 2167.0
0.000463 2113.38501 2143.92212 2159.0
0.000469 2117.58569 2144.66895 2131.0
0.000474 2121.79077 2145.97388 2109.0
0.000476 2126.00000 2147.72437 2099.0
0.000463 2130.21289 2149.83496 2158.0
0.000463 2134.42993 2152.24023 2162.0
0.000469 2138.65210 2154.89014 2133.0
0.000459 2142.87891 2157.74414 2180.0
0.000456 2147.11279 2160.77173 2191.0
0.000460 2151.35474 2163.94849 2172.0
0.000459 2155.60620 2167.25464 2181.0
0.000468 2159.86890 2170.67456 2139.0
0.000475 2164.14478 2164.14478 2106.0
0.000464 2168.43555 2168.43555 2155.0
0.000466 2172.74365 2172.74365 2146.0
0.000468 2177.07178 2177.07178 2139.0
0.000451 2181.42188 2181.42188 2217.0
0.000454 2185.79590 2185.79590 2203.0
0.000465 2190.19727 2190.19727 2151.0
0.000465 2194.62793 2194.62793 2149.0
0.000460 2199.09131 2199.09131 2172.0
0.000450 2203.58911 2203.58911 2221.0
0.000451 2208.12427 2208.12427 2216.0
0.000447 2212.69995 2212.69995 2238.0
0.000441 2217.31738 2217.31738 2267.0
0.000446 2221.98047 2221.98047 2240.0
0.000446 2226.69141 2226.69141 2243.0
0.000449 2231.45190 2231.45190 2226.0
0.000453 2236.26563 2236.26563 2209.0
0.000448 2241.13403 2241.13403 2231.0
0.000442 2246.05981 2246.05981 2263.0
0.000442 2251.04492 2251.04492 2265.0
0.000442 2256.09106 2256.09106 2260.0
0.000450 2261.20117 2261.20117 2223.0
0.000447 2266.37598 2266.37598 2238.0
0.000432 2271.61865 2271.61865 2317.0
0.000439 2276.92993 2276.92993 2276.0
0.000442 2282.31152 2282.31152 2261.0
0.000446 2287.76489 2287.76489 2241.0
0.000437 2293.29126 2293.29126 2287.0
0.000436 2298.89233 2298.89233 2295.0
0.000438 2304.56860 2304.56860 2282.0
0.000444 2310.32080 2310.32080 2252.0
0.000432 2316.15039 2316.15039 2316.0
0.000430 2322.05664 2322.05664 2327.0
0.000425 2328.04224 2328.04224 2354.0
0.000424 2334.10596 2334.10596 2356.0
0.000410 2340.24829 2340.24829 2439.0
0.000418 2346.46973 2346.46973 2393.0
0.000411 2352.76953 2352.76953 2433.0
0.000417 2359.14795 2359.14795 2397.0
0.000426 2365.60498 2365.60498 2347.0
0.000417 2372.13843 2372.13843 2397.0
0.000416 2378.75000 2378.75000 2401.0
0.000418 2385.43750 2385.43750 2395.0
0.000416 2392.20068 2392.20068 2404.0
0.000414 2399.03833 2399.03833 2416.0
0.000404 2405.94849 2405.94849 2475.0
0.000419 2412.93115 2412.93115 2387.0
0.000414 2419.98389 2419.98389 2418.0
0.000402 2427.10571 2427.10571 2488.0
0.000407 2434.29468 2434.29468 2459.0
0.000398 2441.54810 2441.54810 2511.0
0.000414 2448.86597 2448.86597 2415.0
0.000404 2456.24463 2456.24463 2474.0
0.000395 2463.68311 2463.68311 2534.0
0.000399 2471.17871 2471.17871 2506.0
0.000411 2478.72827 2478.72827 2434.0
0.000395 2486.33032 2486.33032 2534.0
0.000409 2493.98071 2493.98071 2446.0
0.000401 2501.67920 2501.67920 2492.0
0.000398 2509.42188 2509.42188 2515.0
0.000383 2517.20508 2517.20508 2608.0
0.000403 2525.02710 2525.02710 2480.0
0.000393 2532.88379 2532.88379 2547.0
0.000394 2540.77295 2540.77295 2540.0
0.000407 2548.69116 2548.69116 2455.0
0.000397 2556.63428 2556.63428 2520.0
0.000384 2564.60059 2564.60059 2604.0
0.000390 2572.58447 2572.58447 2564.0
0.000397 2580.58472 2580.58472 2519.0
0.000382 2588.59741 2588.59741 2619.0
0.000389 2596.61743 2596.61743 2574.0
0.000383 2604.64307 2604.64307 2611.0
0.000373 2612.66895 2612.66895 2681.0
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0.000375 2628.71069 2628.71069 2666.0
0.000368 2636.71729 2636.71729 2717.0
0.000374 2644.71094 2644.71094 2671.0
0.000376 2652.68604 2652.68604 2662.0
0.000384 2660.64038 2660.64038 2605.0
0.000376 2668.56909 2668.56909 2663.0
0.000379 2676.46802 2676.46802 2641.0
0.000374 2684.33423 2684.33423 2673.0
0.000371 2692.16284 2692.16284 2695.0
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0.000374 2715.38647 2715.38647 2672.0
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0.000371 2730.61157 2730.61157 2693.0
0.000368 2738.13550 2738.13550 2717.0
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0.000376 2760.30444 2760.30444 2658.0
0.000363 2767.54712 2767.54712 2753.0
0.000365 2774.71045 2774.71045 2739.0
0.000370 2781.79028 2781.79028 2704.0
0.000365 2788.78174 2788.78174 2737.0
0.000359 2795.68359 2795.68359 2786.0
0.000353 2802.49023 2802.49023 2829.0
0.000358 2809.19922 2809.19922 2791.0
0.000359 2815.80664 2815.80664 2783.0
0.000359 2822.30835 2822.30835 2786.0
0.000359 2828.70190 2828.70190 2786.0
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0.0003447 2880.80420 2883.32080 2901.0
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0.0003464 2890.91602 2894.20972 2887.0
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0.0003473 2900.44556 2904.93945 2879.0
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0.0003419 2913.59888 2921.61768 2925.0
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0.0003388 2921.58032 2934.85327 2952.0
0.0003349 2925.32690 2943.37256 2986.0
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0.0003307 2932.32349 2973.12744 3024.0
0.0003211 2935.56885 3023.34692 3114.0
0.0003063 2938.64355 3237.14771 3265.0
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0.00538 111.34499 173.86064 186.0
0.00592 111.45406 178.68829 169.0
0.00671 111.57913 178.38287 149.0
0.00649 111.72066 172.31946 154.0
0.00694 111.87909 162.88356 144.0
0.00694 112.05480 153.02594 144.0
0.00645 112.24816 144.35181 155.0
0.00680 112.45952 137.50104 147.0
0.00775 112.68907 132.47276 129.0
0.00794 112.93703 129.00116 126.0
0.00893 113.20352 126.72369 112.0
0.00893 113.48861 125.30039 112.0
0.00813 113.79204 124.45950 123.0
0.00758 114.11423 124.01433 132.0
0.00781 114.45425 123.84886 128.0
0.00787 114.81254 123.89832 127.0
0.00781 115.18784 124.12981 128.0
0.00800 115.58022 124.53214 125.0
0.00826 115.98878 125.10645 121.0
0.00855 116.41267 125.86197 117.0
0.00741 116.85097 126.78557 135.0
0.00714 117.30249 127.94783 140.0
0.00870 117.76592 129.33235 115.0
0.00901 118.23982 130.93919 111.0
0.00769 118.72246 132.76015 130.0
0.00730 119.21194 134.83664 137.0
0.00714 119.70621 137.34752 140.0
0.00685 120.20255 140.62225 146.0
0.00654 120.69932 145.04852 153.0
0.00658 121.19247 150.97240 152.0
0.00680 121.68005 158.62344 147.0
0.00625 122.15746 168.05356 160.0
0.00538 122.62186 178.85362 186.0
0.00493 123.06889 189.71651 203.0
0.00469 123.49418 198.13739 213.0
0.00448 123.89293 201.16350 223.0
0.00472 124.26002 197.61719 212.0
0.00552 124.58991 189.28288 181.0
0.00578 124.87662 179.15598 173.0
0.00578 125.11372 169.45836 173.0
0.00565 125.29434 161.22932 177.0
0.00617 125.41113 154.76639 162.0
0.00694 125.45618 149.98190 144.0
0.00741 125.42106 146.62984 135.0
0.00658 125.29690 144.42706 152.0
0.00658 125.07377 143.12059 152.0
0.00685 124.74202 142.54298 146.0
0.00730 124.29031 142.63454 137.0
0.00775 123.70722 143.46422 129.0
0.00680 122.98056 145.23444 147.0
0.00662 122.09726 148.27922 151.0
0.00637 121.04362 153.02196 157.0
0.00654 119.80499 159.90607 153.0
0.00581 118.36597 169.26117 172.0
0.00575 116.71021 181.06589 174.0
. . . 188.0
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_observed_status
_refln_F_squared_meas
_refln_F_squared_calc
_refln_phase_calc
_refln_d_spacing
1 1 1 o 36571.45 37199.02 180.00 5.67539
2 2 0 o 10274.317 9798.892 180.00 4.52542
3 1 1 o 23911.348 25974.445 180.00 3.77576
4 0 0 o 534255.8 502843.1 180.00 3.57608
1 3 1 o 168204.27 174351.36 180.00 3.34063
2 0 2 o 363998.5 370369.6 180.00 3.24606
0 2 2 o 7283.241 1112.444 180.00 3.09143
0 4 0 o 134378.44 141771.78 180.00 2.92200
2 2 2 o 3368.635 2610.601 0.00 2.83769
3 3 1 o 121153.67 130983.16 0.00 2.78742
5 1 1 o 15155.415 15935.301 0.00 2.59639
1 1 3 o 76583.51 65754.38 180.00 2.34560
4 2 2 o 71515.14 62092.79 0.00 2.33870
4 4 0 o 27165.822 28631.314 0.00 2.26271
1 5 1 o 51484.68 52822.82 0.00 2.19937
5 3 1 o 191550.17 197276.45 0.00 2.19846
6 2 0 o 108095.73 116874.07 0.00 2.20744
2 4 2 o 236157.34 231905.53 0.00 2.17173
3 1 3 o 110818.75 98979.16 0.00 2.12788
1 3 3 o 39032.72 37046.65 0.00 2.03989
3 5 1 o 13447.838 14949.688 0.00 2.01690
6 0 2 o 87484.34 87298.80 0.00 1.99483
7 1 1 o 31251.803 32445.676 0.00 1.94025
4 4 2 o 803.499 578.364 0.00 1.92210
3 3 3 o 91947.43 86273.18 0.00 1.89180
6 2 2 o 5896.500 5442.959 180.00 1.88788
2 6 0 o 100803.49 94395.87 0.00 1.87953
5 1 3 o 36407.70 38111.16 0.00 1.82864
0 0 4 o 199726.39 191475.61 180.00 1.82143
8 0 0 o 202848.88 186836.19 0.00 1.78804
5 5 1 o 15490.927 15972.938 180.00 1.75676
7 3 1 o 98030.63 101032.35 180.00 1.75629
0 6 2 o 76188.41 74764.53 0.00 1.71782
2 2 4 o 19009.031 16610.348 0.00 1.68970
1 5 3 o 4018.392 3796.689 0.00 1.67262
5 3 3 o 50552.21 47977.52 180.00 1.67222
2 6 2 o 43.901 40.878 180.00 1.67031
6 4 2 o 60322.81 64566.43 180.00 1.64751
4 0 4 o 98536.48 93536.29 0.00 1.62303
1 7 1 o 31241.045 30550.789 0.00 1.61709
3 5 3 o 10346.699 7710.109 180.00 1.58803
4 2 4 o 32.795 98.521 0.00 1.56384
0 4 4 o 249557.75 186834.44 0.00 1.54572
7 1 3 o 27820.211 29234.373 180.00 1.54979
4 6 2 o 127791.89 123109.09 180.00 1.54843
8 2 2 o 58674.60 54209.20 180.00 1.54779
3 7 1 o 49652.91 50553.98 180.00 1.54027
9 1 1 o 7577.635 7820.552 180.00 1.53932
8 4 0 o 26358.318 24672.090 180.00 1.52515
2 4 4 o 1316.221 1082.554 0.00 1.51084
6 6 0 o 154577.19 145424.80 180.00 1.50847
7 5 1 o 2726.622 2852.075 180.00 1.50530
0 8 0 o 78182.84 83021.50 0.00 1.46100
5 5 3 o 8.676 0.094 0.00 1.45136
7 3 3 o 55863.34 56080.61 180.00 1.45110
1 1 5 o 30687.873 31841.543 0.00 1.43862
9 3 1 o 77967.72 88012.09 180.00 1.44249
4 4 4 o 107133.92 101050.39 180.00 1.41885
5 7 1 o 59952.92 58027.87 180.00 1.41463
6 2 4 o 45067.48 46503.68 180.00 1.40491
8 4 2 o 276.479 254.529 0.00 1.40683
3 1 5 o 4886.631 5192.448 0.00 1.38373
6 6 2 o 1343.104 1853.229 180.00 1.39371
10 2 0 o 15239.739 19661.238 180.00 1.38942
1 7 3 o 53689.90 50282.31 180.00 1.36958
1 3 5 o 67783.45 65261.02 0.00 1.35864
4 8 0 o 35437.06 41156.43 180.00 1.35248
2 8 2 o 16325.763 15802.482 180.00 1.33228
10 0 2 o 131307.34 122398.30 180.00 1.33146
3 7 3 o 75123.60 74831.75 180.00 1.32196
9 1 3 o 41534.85 41892.89 180.00 1.32136
3 3 5 o 44354.63 42459.59 180.00 1.31212
2 6 4 o 73556.59 70940.28 180.00 1.30801
7 5 3 o 238.018 613.673 0.00 1.29966
10 2 2 o 3020.255 3147.019 0.00 1.29820
6 4 4 o 59.172 58.818 180.00 1.29697
5 1 5 o 31028.656 32503.018 180.00 1.29049
9 5 1 o 11526.564 11705.305 0.00 1.29347
8 0 4 o 64237.88 68099.08 180.00 1.27598
1 9 1 o 29860.887 31092.193 180.00 1.27344
7 7 1 o 68439.62 72907.48 0.00 1.27308
11 1 1 o 26608.457 29178.416 180.00 1.27255
4 8 2 o 505.876 809.023 180.00 1.26792
9 3 3 o 56217.44 53114.07 0.00 1.25859
4 6 4 o 2657.789 3566.996 0.00 1.24694
8 2 4 o 1917.584 2483.209 180.00 1.24661
5 7 3 o 72228.16 69194.90 0.00 1.23995
8 6 2 o 95483.88 94731.16 0.00 1.23876
1 5 5 o 14074.330 14510.315 180.00 1.23198
5 3 5 o 57961.17 59823.48 180.00 1.23182
3 9 1 o 21127.615 19393.520 180.00 1.23489
11 3 1 o 34083.840 37803.95 0.00 1.21619
10 4 2 o 70953.49 72302.41 0.00 1.21161
2 0 6 o 154864.97 160130.56 0.00 1.19716
3 5 5 o 4454.489 4442.686 180.00 1.19697
0 2 6 o 13732.412 13279.898 0.00 1.18889
12 0 0 o 147665.66 169362.02 180.00 1.19203
7 1 5 o 13662.980 12127.591 180.00 1.18034
2 2 6 o 133.935 84.723 180.00 1.17280
6 8 2 o 5477.629 5276.186 0.00 1.17869
8 4 4 o 58846.45 57949.18 0.00 1.16935
5 9 1 o 8103.752 6340.542 0.00 1.16726
6 6 4 o 84972.87 84713.66 0.00 1.16178
9 5 3 o 3692.902 4415.134 0.00 1.15592
2 10 0 o 91426.55 93924.98 180.00 1.15350
10 6 0 o 57978.50 59575.43 0.00 1.15297
1 9 3 o 40080.86 42091.91 180.00 1.14156
7 7 3 o 55179.30 58097.75 0.00 1.14130
11 1 3 o 12639.021 13260.373 0.00 1.14092
0 8 4 o 9408.811 8797.576 180.00 1.13967
5 5 5 o 5703.210 5919.646 0.00 1.13508
7 3 5 o 60754.34 63454.41 0.00 1.13495
9 7 1 o 30380.787 28284.176 0.00 1.13710
4 2 6 o 17305.557 19724.895 180.00 1.12818
2 8 4 o 1018.232 1212.595 180.00 1.12547
8 8 0 o 18311.508 20311.947 0.00 1.13135
11 5 1 o 8739.234 7522.834 0.00 1.12282
3 9 3 o 35734.00 32673.900 0.00 1.11354
0 10 2 o 85442.82 79816.80 180.00 1.11292
12 2 2 o 6565.442 5845.658 0.00 1.11221
2 4 6 o 31559.248 31447.018 180.00 1.10779
10 2 4 o 13225.680 14467.084 0.00 1.10470
12 4 0 o 57443.75 63396.47 0.00 1.10372
11 3 3 o 25324.924 27091.303 0.00 1.09977
2 10 2 o 972.091 1042.815 0.00 1.09969
10 6 2 o 4151.529 4577.235 0.00 1.09923
1 7 5 o 31512.883 32541.434 180.00 1.09465
4 8 4 o 4831.715 4456.888 0.00 1.08586
6 0 6 o 102455.35 100313.65 180.00 1.08202
7 9 1 o 12602.968 9353.651 0.00 1.08386
13 1 1 o 11326.714 9319.218 0.00 1.08331
8 8 2 o 169.905 143.349 180.00 1.08045
4 4 6 o 692.542 779.258 180.00 1.06995
3 7 5 o 19332.316 21639.736 0.00 1.06988
9 1 5 o 9523.844 10290.144 0.00 1.06956
8 6 4 o 33.275 58.750 180.00 1.06738
6 2 6 o 110.434 113.140 180.00 1.06394
5 9 3 o 18163.672 17146.623 0.00 1.06319
4 10 2 o 90012.16 81632.17 0.00 1.06265
7 5 5 o 7058.521 8081.563 0.00 1.05795
12 4 2 o 45.337 47.905 180.00 1.05630
10 4 4 o 408.854 422.701 180.00 1.04986
1 11 1 o 6322.387 6822.070 180.00 1.04859
13 3 1 o 35898.57 40779.28 0.00 1.04790
6 10 0 o 87368.35 87819.24 0.00 1.04946
9 7 3 o 51087.63 48816.54 180.00 1.04025
9 3 5 o 20310.959 19463.260 0.00 1.03544
1 1 7 o 7174.642 5237.249 0.00 1.03400
0 6 6 o 45089.89 44484.53 180.00 1.03048
11 5 3 o 4070.662 3891.701 180.00 1.02928
6 8 4 o 33.187 32.240 0.00 1.02823
5 7 5 o 44443.48 44946.16 0.00 1.02499
3 11 1 o 10695.993 9976.511 0.00 1.02676
2 6 6 o 1319.848 1332.835 0.00 1.01995
3 1 7 o 13588.866 14935.034 180.00 1.01305
6 4 6 o 23658.463 21685.375 0.00 1.01469
11 7 1 o 28714.137 30236.193 180.00 1.01593
6 10 2 o 967.405 1088.979 180.00 1.00845
1 3 7 o 33375.164 33370.797 180.00 1.00308
14 2 0 o 3694.026 5196.312 0.00 1.00647
12 0 4 o 81455.25 82736.50 0.00 0.99742
7 9 3 o 11874.277 12168.771 180.00 0.99902
13 1 3 o 15190.097 15095.536 0.00 0.99859
4 6 6 o 49514.77 48088.63 0.00 0.99019
8 2 6 o 16885.156 16219.134 0.00 0.99002
9 9 1 o 7281.329 6961.020 180.00 0.99620
3 3 7 o 51871.88 55126.81 180.00 0.98391
12 2 4 o 1583.626 1447.293 0.00 0.98320
5 11 1 o 20689.266 21329.129 0.00 0.98688
13 5 1 o 13061.097 13222.932 180.00 0.98639
10 8 2 o 9114.186 9382.664 180.00 0.98410
14 0 2 o 87218.09 90266.82 0.00 0.98377
5 1 7 o 4913.394 4842.260 180.00 0.97469
12 6 2 o 34231.887 34127.449 180.00 0.97934
9 5 5 o 645.503 577.378 180.00 0.97597
2 10 4 o 63617.29 62341.12 0.00 0.97452
10 6 4 o 45710.40 44049.39 180.00 0.97420
1 11 3 o 1929.953 1887.736 0.00 0.97121
13 3 3 o 20735.760 22315.033 180.00 0.97066
1 9 5 o 18357.238 18520.076 0.00 0.96728
0 12 0 o 5486.070 5168.611 180.00 0.97400
7 7 5 o 26223.395 26907.053 180.00 0.96713
11 1 5 o 10754.206 11258.856 0.00 0.96690
14 2 2 o 2100.550 2439.659 180.00 0.97013
8 8 4 o 3951.052 4129.845 180.00 0.96105
3 11 3 o 5354.519 5003.514 0.00 0.95378
1 5 7 o 5379.846 5629.343 180.00 0.94873
5 3 7 o 24883.578 25984.834 0.00 0.94866
3 9 5 o 8833.922 9250.003 0.00 0.95006
8 4 6 o 256.112 268.501 180.00 0.94997
4 10 4 o 363.036 374.321 180.00 0.94846
6 6 6 o 324.790 324.829 180.00 0.94590
12 4 4 o 53018.13 50938.86 180.00 0.94394
11 7 3 o 20501.787 19969.801 180.00 0.94508
8 10 2 o 66589.23 64130.41 180.00 0.94485
11 3 5 o 41956.52 43207.81 180.00 0.94147
15 1 1 o 13145.541 13621.247 0.00 0.94248
4 12 0 o 8726.006 6111.583 0.00 0.93977
3 5 7 o 12127.798 12807.583 0.00 0.93247
7 11 1 o 12169.022 13329.697 180.00 0.93493
2 12 2 o 17782.338 18258.547 0.00 0.93291
14 4 2 o 46348.33 47915.06 180.00 0.93235
2 8 6 o 18971.059 20003.324 0.00 0.92599
10 0 6 o 68995.49 72382.80 0.00 0.92572
9 9 3 o 19343.293 16719.166 180.00 0.92914
7 1 7 o 4031.835 4367.090 0.00 0.92454
5 11 3 o 7692.066 7577.368 180.00 0.92156
13 5 3 o 4829.925 4635.033 180.00 0.92116
5 9 5 o 11194.988 12156.405 180.00 0.91821
12 8 0 o 16134.284 17214.928 180.00 0.92361
15 3 1 o 16325.379 17352.596 180.00 0.91888
10 2 6 o 762.827 738.157 0.00 0.91432
0 0 8 o 59026.92 56204.30 0.00 0.91072
11 9 1 o 21338.963 19432.465 180.00 0.91168
13 7 1 o 12153.742 10990.472 180.00 0.91155
6 10 4 o 62876.17 57464.73 180.00 0.90933
4 12 2 o 253.655 221.926 0.00 0.90997
5 5 7 o 3060.511 2970.815 0.00 0.90230
7 3 7 o 31498.471 30246.297 0.00 0.90223
4 8 6 o 1143.565 1193.360 0.00 0.90355
9 7 5 o 23263.553 24461.836 180.00 0.90331
10 10 0 o 53818.51 55328.54 180.00 0.90508
14 6 0 o 27435.672 28134.943 180.00 0.90483
2 2 8 o 10528.000 10397.028 180.00 0.89282
11 5 5 o 9260.922 10669.261 180.00 0.89610
8 6 6 o 39367.68 38660.55 180.00 0.89282
12 8 2 o 9.933 10.289 0.00 0.89528
10 8 4 o 930.686 915.073 0.00 0.89135
16 0 0 o 52548.05 53482.96 0.00 0.89402
12 6 4 o 395.643 356.731 0.00 0.88781
1 13 1 o 43109.59 40841.95 0.00 0.89058
4 0 8 o 55463.73 53330.32 180.00 0.88255
15 1 3 o 10947.021 11473.827 180.00 0.88509
10 4 6 o 24427.529 23565.355 180.00 0.88249
1 7 7 o 14767.894 14245.879 0.00 0.88159
14 2 4 o 5753.821 5547.030 180.00 0.88093
7 11 3 o 9002.069 8951.951 180.00 0.87883
7 9 5 o 6570.637 5870.612 180.00 0.87592
13 1 5 o 14352.102 13289.775 180.00 0.87563
10 10 2 o 279.424 278.598 0.00 0.87838
14 6 2 o 1019.315 1020.526 180.00 0.87815
4 2 8 o 143.793 738.119 0.00 0.87265
3 13 1 o 29741.510 28912.924 0.00 0.87708
9 11 1 o 13053.276 12480.315 180.00 0.87691
15 5 1 o 2469.160 2248.707 180.00 0.87656
6 12 2 o 16195.385 15696.051 180.00 0.87524
6 8 6 o 12720.979 12676.887 180.00 0.86952
0 4 8 o 26410.406 27148.027 180.00 0.86946
3 7 7 o 22523.799 19815.936 0.00 0.86849
9 1 7 o 15495.757 13632.159 0.00 0.86832
2 4 8 o 182.321 311.941 180.00 0.86311
15 3 3 o 28359.105 26325.766 180.00 0.86546
7 5 7 o 2269.868 4718.736 180.00 0.86207
8 10 4 o 967.075 1715.718 180.00 0.86187
0 12 4 o 18700.910 17982.959 0.00 0.85891
1 11 5 o 5052.041 4520.604 0.00 0.85699
13 3 5 o 17557.844 15486.847 180.00 0.85661
11 9 3 o 14397.600 13645.686 0.00 0.85944
13 7 3 o 17593.840 16778.961 0.00 0.85933
16 2 2 o 9420.729 8936.280 180.00 0.85883
2 12 4 o 577.297 644.628 0.00 0.85278
8 12 0 o 6389.239 6545.203 180.00 0.85533
14 4 4 o 89.700 89.483 180.00 0.85235
16 4 0 o 24838.307 27986.473 180.00 0.85490
5 13 1 o 23036.086 21664.896 180.00 0.85184
_cod_database_fobs_code 2240592