#------------------------------------------------------------------------------ #$Date: 2016-11-11 03:50:47 +0200 (Fri, 11 Nov 2016) $ #$Revision: 188381 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/19/2241943.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2241943 _cell_angle_alpha 90.000 _cell_angle_beta 92.125 _cell_angle_gamma 90.000 _cell_length_a 22.5810 _cell_length_b 13.7701 _cell_length_c 18.5242 _exptl_crystal_F_000 2681.60 _reflns_d_resolution_high 0.7828 _cod_data_source_file rz5196Isup2.hkl _cod_data_source_block I _shelx_title ' exp_2196_5-CH3 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 563.96 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 5 0 0 191.87 168.51 81.11 o 6 0 0 165.17 341.06 180.91 o 7 0 0 551.22 924.87 219.16 o 8 0 0 39504.03 37646.21 974.55 o 9 0 0 819.44 1154.29 260.08 o 10 0 0 57579.36 57708.67 1347.57 o 11 0 0 8328.92 9030.79 596.66 o 12 0 0 33484.43 32586.26 1118.65 o 13 0 0 13412.12 14865.63 814.70 o 14 0 0 4886.71 5263.33 521.88 o 15 0 0 5818.73 5704.59 584.71 o 16 0 0 4692.23 4645.13 561.51 o 17 0 0 30656.11 31882.56 1358.91 o 18 0 0 6281.04 6732.49 691.20 o 19 0 0 87.11 500.43 301.40 o 20 0 0 4200.32 3753.24 577.88 o 21 0 0 379.73 491.49 381.58 o 22 0 0 10.97 90.95 319.63 o 23 0 0 3216.96 3181.08 615.19 o 24 0 0 460.36 339.57 304.89 o 25 0 0 384.07 172.48 306.50 o 26 0 0 1291.75 1046.82 401.79 o 27 0 0 427.78 786.19 444.66 o 28 0 0 851.79 655.94 408.08 o 5 1 0 843.36 620.91 77.18 o 6 1 0 1450.50 2010.55 136.62 o 7 1 0 1311.36 1703.48 176.83 o 8 1 0 12368.23 10979.72 387.38 o 9 1 0 1541.15 1566.17 189.75 o 10 1 0 24248.56 23600.17 614.73 o 11 1 0 6954.58 7650.15 388.56 o 12 1 0 34430.58 35173.68 1095.46 o 13 1 0 612.15 809.72 212.17 o 14 1 0 12222.09 11834.93 538.35 o 15 1 0 2976.14 3233.21 323.78 o 16 1 0 1640.13 1773.96 278.00 o 17 1 0 4043.17 4104.48 388.45 o 18 1 0 381.79 650.38 260.85 o 19 1 0 1044.12 689.91 273.40 o 20 1 0 5.33 86.91 262.40 o 21 1 0 93.14 220.38 227.32 o 22 1 0 1415.55 1143.73 299.24 o 23 1 0 397.42 130.07 169.10 o 24 1 0 889.76 445.95 253.88 o 25 1 0 6859.84 5721.70 521.75 o 26 1 0 332.86 323.06 246.83 o 27 1 0 3595.01 2697.19 425.52 o 28 1 0 6.37 -131.86 263.71 o 4 2 0 12613.98 14515.54 457.32 o 5 2 0 473.89 360.60 78.01 o 6 2 0 8207.31 9633.51 240.81 o 7 2 0 4318.31 5197.38 202.34 o 8 2 0 22732.52 25099.82 552.39 o 9 2 0 12152.55 14131.97 458.97 o 10 2 0 12299.80 11600.19 444.14 o 11 2 0 22105.96 22568.94 630.91 o 12 2 0 16932.73 17287.14 585.04 o 13 2 0 20724.56 21095.54 675.52 o 14 2 0 10695.94 10248.38 502.20 o 15 2 0 5639.16 5802.57 409.79 o 16 2 0 10.15 29.97 202.31 o 17 2 0 492.40 872.56 216.07 o 18 2 0 1973.19 1936.17 306.66 o 19 2 0 529.50 314.36 235.22 o 20 2 0 1876.34 2185.10 342.61 o 21 2 0 4257.90 4114.12 355.71 o 22 2 0 2564.02 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82.87 -178.15 356.30 o 27 3 0 1125.88 1056.11 461.74 o 28 3 0 7.18 -138.21 374.20 o 0 4 0 101553.10 105704.96 701.75 o 1 4 0 108809.47 113242.75 465.34 o 2 4 0 6227.09 6759.80 156.59 o 3 4 0 8151.12 9800.20 214.25 o 4 4 0 17458.18 19957.51 274.35 o 5 4 0 2369.68 2226.35 94.13 o 6 4 0 601.44 430.57 104.01 o 7 4 0 559.24 454.23 79.51 o 8 4 0 18813.48 19768.18 359.40 o 9 4 0 13384.18 12726.42 419.28 o 10 4 0 4035.34 3641.49 360.63 o 11 4 0 17001.60 16280.14 524.21 o 12 4 0 9375.68 8982.25 422.24 o 13 4 0 19779.57 18231.39 610.79 o 14 4 0 5219.82 5571.38 379.61 o 15 4 0 3345.93 3105.55 319.25 o 16 4 0 424.83 486.26 211.45 o 17 4 0 554.93 358.72 199.03 o 18 4 0 2758.61 2555.57 437.85 o 19 4 0 1848.04 1813.88 244.99 o 20 4 0 707.52 532.80 213.89 o 21 4 0 8449.07 7842.73 553.76 o 22 4 0 3593.71 3225.08 385.36 o 23 4 0 4554.28 3911.23 406.42 o 24 4 0 307.27 -54.37 316.38 o 25 4 0 1262.06 1075.23 446.59 o 26 4 0 949.34 906.00 471.95 o 27 4 0 58.06 -239.02 478.04 o 1 5 0 111002.73 113806.79 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31.71 o 6 6 0 487.97 459.57 75.91 o 7 6 0 104.79 4.10 46.95 o 8 6 0 912.83 921.49 190.83 o 9 6 0 420.81 266.27 111.98 o 10 6 0 7346.38 6873.60 230.91 o 11 6 0 14923.29 14156.10 464.76 o 12 6 0 5830.23 5699.65 352.32 o 13 6 0 13323.06 13124.79 505.50 o 14 6 0 424.60 465.73 213.09 o 15 6 0 4040.48 4108.96 334.19 o 16 6 0 26.97 -92.25 203.83 o 17 6 0 3599.71 3608.19 335.77 o 18 6 0 1012.39 910.90 226.18 o 19 6 0 5383.77 5383.74 431.26 o 20 6 0 1684.24 1179.21 384.67 o 21 6 0 715.46 874.53 416.22 o 22 6 0 49.72 -192.80 385.59 o 23 6 0 562.27 239.72 361.47 o 24 6 0 1969.20 1390.32 508.16 o 25 6 0 1049.83 1018.54 539.04 o 26 6 0 2673.25 2922.38 694.40 o 1 7 0 22476.70 22612.48 305.69 o 2 7 0 16173.27 15970.02 249.03 o 3 7 0 6551.70 6349.76 153.97 o 4 7 0 35059.48 32578.34 399.86 o 5 7 0 2226.07 2009.76 203.48 o 6 7 0 13976.68 13369.19 499.63 o 7 7 0 5818.35 5403.01 139.31 o 8 7 0 21040.34 20172.29 293.06 o 9 7 0 1455.67 1485.45 150.95 o 10 7 0 2542.65 2910.71 292.66 o 11 7 0 2052.85 2069.04 153.03 o 12 7 0 5771.08 5997.72 317.25 o 13 7 0 209.10 80.71 258.44 o 14 7 0 3381.70 3393.92 283.80 o 15 7 0 170.36 78.92 266.78 o 16 7 0 846.22 841.07 205.63 o 17 7 0 1452.70 1308.85 454.74 o 18 7 0 730.41 242.39 337.36 o 19 7 0 1434.82 1601.24 463.52 o 20 7 0 159.39 82.58 401.31 o 21 7 0 793.05 439.25 362.82 o 22 7 0 142.12 -215.53 431.05 o 23 7 0 3733.44 4417.96 740.07 o 24 7 0 54.11 -0.59 328.25 o 25 7 0 5330.68 5671.51 909.58 o 0 8 0 912.21 743.37 148.07 o 1 8 0 54.59 26.31 71.92 o 2 8 0 2626.92 2512.53 118.33 o 3 8 0 264.29 231.61 105.69 o 4 8 0 2912.40 2723.98 144.02 o 5 8 0 890.84 883.60 201.87 o 6 8 0 1075.17 1635.65 240.32 o 7 8 0 3133.70 2750.66 418.64 o 8 8 0 263.74 12.82 122.55 o 9 8 0 3378.26 2938.18 149.17 o 10 8 0 392.91 463.74 94.40 o 11 8 0 3427.47 3096.93 314.26 o 12 8 0 350.37 287.80 141.76 o 13 8 0 4281.26 3489.72 522.34 o 14 8 0 293.84 78.65 284.94 o 15 8 0 2941.14 2281.86 503.78 o 16 8 0 368.26 305.08 319.61 o 17 8 0 430.76 173.53 390.78 o 18 8 0 12.87 -189.14 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2104.56 2111.11 162.86 o 2 10 0 6726.04 6576.06 202.66 o 3 10 0 2564.37 2613.62 144.05 o 4 10 0 1190.27 1026.20 115.35 o 5 10 0 2136.05 2171.98 234.11 o 6 10 0 142.53 325.89 297.39 o 7 10 0 1319.53 1530.82 278.32 o 8 10 0 3837.58 4720.67 396.35 o 9 10 0 19.31 290.26 212.74 o 10 10 0 2831.26 3593.07 383.89 o 11 10 0 515.44 824.70 348.91 o 12 10 0 1901.90 2309.97 510.26 o 13 10 0 580.64 537.17 341.70 o 14 10 0 157.02 394.40 344.27 o 15 10 0 1599.78 1206.06 371.93 o 16 10 0 415.47 180.36 318.72 o 17 10 0 526.55 523.33 349.74 o 18 10 0 675.94 760.57 395.73 o 19 10 0 141.97 90.75 345.54 o 20 10 0 568.28 268.33 411.21 o 21 10 0 231.51 89.77 390.43 o 22 10 0 827.01 1413.81 538.37 o 23 10 0 446.12 848.43 576.41 o 1 11 0 4891.35 4467.13 220.18 o 2 11 0 281.15 243.53 112.43 o 3 11 0 161.44 -86.50 173.00 o 4 11 0 5875.24 5289.53 422.80 o 5 11 0 5920.87 5514.93 333.67 o 6 11 0 13949.99 15095.52 651.71 o 7 11 0 32.55 146.49 196.07 o 8 11 0 183.22 398.15 223.91 o 9 11 0 244.31 497.52 245.82 o 10 11 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