#------------------------------------------------------------------------------ #$Date: 2016-11-11 03:50:57 +0200 (Fri, 11 Nov 2016) $ #$Revision: 188382 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/19/2241944.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2241944 _cell_angle_alpha 90.000 _cell_angle_beta 96.992 _cell_angle_gamma 90.000 _cell_length_a 4.8564 _cell_length_b 13.5188 _cell_length_c 6.7205 _exptl_crystal_F_000 278.00 _reflns_d_resolution_high 0.6499 _cod_data_source_file pj2038Isup2.hkl _cod_data_source_block I _shelx_title ' rkdd349_0m_a.res in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 178.87 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 501.42 416.12 3.24 o 2 0 0 3317.37 3129.75 19.07 o 3 0 0 1211.43 1178.92 17.22 o 4 0 0 1420.27 1424.99 14.52 o 5 0 0 123.30 130.91 3.97 o 6 0 0 984.05 946.72 11.94 o 7 0 0 273.71 270.47 17.31 o 1 1 0 7.46 11.23 0.36 o 2 1 0 61.21 85.66 0.82 o 3 1 0 27.12 25.27 0.56 o 4 1 0 93.81 98.83 2.04 o 5 1 0 217.14 217.03 3.10 o 6 1 0 2.68 2.11 0.88 o 7 1 0 83.35 86.00 3.42 o 0 2 0 7338.18 6457.95 171.10 o 1 2 0 495.21 557.98 3.11 o 2 2 0 46.18 27.32 0.55 o 3 2 0 2836.63 2863.07 13.42 o 4 2 0 1255.10 1255.87 8.54 o 5 2 0 155.64 159.36 2.59 o 6 2 0 599.13 585.47 6.90 o 7 2 0 314.94 307.62 5.15 o 1 3 0 30.72 30.44 0.43 o 2 3 0 229.13 255.09 1.70 o 3 3 0 224.00 241.08 2.04 o 4 3 0 282.65 288.31 2.80 o 5 3 0 3.34 3.76 0.87 o 6 3 0 0.46 1.20 0.90 o 7 3 0 7.90 11.74 1.86 o 0 4 0 2552.15 2592.19 24.06 o 1 4 0 246.54 213.36 1.34 o 2 4 0 1389.06 1322.55 6.50 o 3 4 0 1953.36 1958.78 10.04 o 4 4 0 3117.18 3089.26 17.38 o 5 4 0 31.89 37.20 1.74 o 6 4 0 403.71 391.67 5.46 o 7 4 0 163.57 164.88 3.83 o 1 5 0 1061.09 1153.17 5.34 o 2 5 0 192.05 189.82 1.40 o 3 5 0 9.98 13.45 0.57 o 4 5 0 0.03 0.56 0.51 o 5 5 0 284.73 281.12 4.14 o 6 5 0 10.54 9.23 1.27 o 7 5 0 0.00 2.00 1.06 o 0 6 0 9738.36 9130.85 92.16 o 1 6 0 1689.43 1674.44 8.52 o 2 6 0 2521.22 2486.12 11.62 o 3 6 0 625.66 624.50 5.51 o 4 6 0 2000.90 1988.33 12.91 o 5 6 0 184.17 182.12 3.32 o 6 6 0 319.91 313.60 4.86 o 7 6 0 226.63 230.00 4.48 o 1 7 0 1212.62 1322.32 6.12 o 2 7 0 8.27 11.57 0.45 o 3 7 0 232.14 232.30 2.60 o 4 7 0 14.94 16.57 0.97 o 5 7 0 0.00 0.92 1.20 o 6 7 0 2.21 4.68 1.33 o 0 8 0 2423.80 2379.79 15.01 o 1 8 0 1837.38 1851.91 9.31 o 2 8 0 266.15 247.38 1.94 o 3 8 0 380.09 400.26 3.68 o 4 8 0 403.58 414.00 4.14 o 5 8 0 665.46 655.71 6.40 o 6 8 0 216.76 217.97 4.43 o 1 9 0 161.96 158.81 1.53 o 2 9 0 23.06 24.76 0.81 o 3 9 0 218.77 208.22 2.79 o 4 9 0 107.42 99.77 2.14 o 5 9 0 2.39 3.75 1.10 o 6 9 0 4.64 3.23 1.43 o 0 10 0 2098.79 2066.16 13.50 o 1 10 0 351.56 343.67 3.35 o 2 10 0 1571.89 1582.35 10.51 o 3 10 0 202.46 213.47 3.04 o 4 10 0 1457.22 1430.82 12.18 o 5 10 0 195.18 193.87 4.07 o 6 10 0 139.07 140.26 4.44 o 1 11 0 127.04 125.27 1.82 o 2 11 0 1.30 4.04 0.84 o 3 11 0 39.04 39.01 1.87 o 4 11 0 10.18 14.51 1.50 o 5 11 0 42.43 48.03 2.83 o 6 11 0 26.47 24.13 3.00 o 0 12 0 422.63 445.29 6.15 o 1 12 0 1420.64 1405.87 10.12 o 2 12 0 749.11 776.93 7.34 o 3 12 0 893.26 872.91 9.39 o 4 12 0 1381.21 1358.50 15.41 o 5 12 0 150.74 154.22 4.43 o 6 12 0 59.18 58.64 4.00 o 1 13 0 28.81 36.68 1.19 o 2 13 0 175.06 160.03 2.88 o 3 13 0 56.76 58.52 2.60 o 4 13 0 13.72 18.72 2.52 o 5 13 0 5.21 5.30 1.57 o 0 14 0 662.35 680.31 8.85 o 1 14 0 426.45 409.95 4.36 o 2 14 0 141.53 166.67 3.31 o 3 14 0 318.49 315.61 5.52 o 4 14 0 451.36 461.95 10.58 o 5 14 0 160.97 158.01 4.62 o 1 15 0 1.92 3.19 0.90 o 2 15 0 11.85 10.26 1.39 o 3 15 0 1.77 0.92 1.20 o 4 15 0 54.87 61.12 3.06 o 5 15 0 17.95 24.58 3.95 o 0 16 0 2327.17 2354.77 28.26 o 1 16 0 210.97 202.76 3.72 o 2 16 0 289.65 289.93 5.45 o 3 16 0 305.42 309.62 6.88 o 4 16 0 209.06 197.79 4.32 o 1 17 0 62.69 65.90 2.68 o 2 17 0 4.02 7.03 1.41 o 3 17 0 8.36 8.56 1.62 o 4 17 0 2.39 2.20 1.69 o 0 18 0 604.54 617.42 10.66 o 1 18 0 512.25 506.57 7.68 o 2 18 0 67.74 65.65 2.92 o 3 18 0 1029.07 1007.30 12.87 o 1 19 0 6.42 8.16 1.46 o 2 19 0 33.56 32.23 2.33 o 3 19 0 16.77 18.00 2.01 o 0 20 0 192.73 204.81 5.86 o 1 20 0 60.65 62.21 2.90 o 2 20 0 65.66 65.00 3.06 o -7 1 1 445.47 451.40 8.00 o -6 1 1 1149.54 1144.17 10.74 o -5 1 1 193.69 207.91 3.07 o -4 1 1 375.28 346.98 3.52 o -3 1 1 2239.79 2288.89 17.00 o -2 1 1 1118.26 1085.75 5.40 o -1 1 1 2529.01 2537.82 10.82 o 0 1 1 4765.20 4511.85 33.16 o 1 1 1 846.89 911.01 4.34 o 2 1 1 2091.85 2077.12 10.07 o 3 1 1 229.71 194.74 1.63 o 4 1 1 300.07 316.49 3.50 o 5 1 1 1388.15 1360.56 10.47 o 6 1 1 468.45 482.70 5.45 o 7 1 1 150.53 141.72 4.06 o -7 2 1 0.11 2.20 1.11 o -6 2 1 11.28 10.00 1.23 o -5 2 1 32.88 36.70 1.50 o -4 2 1 14.10 15.84 0.75 o -3 2 1 1123.50 1196.62 5.95 o -2 2 1 130.28 132.93 1.15 o -1 2 1 2865.52 2856.66 18.63 o 0 2 1 670.74 751.49 4.95 o 1 2 1 46.84 42.12 0.50 o 2 2 1 1325.22 1476.57 7.14 o 3 2 1 72.03 80.53 1.14 o 4 2 1 59.62 57.24 1.42 o 5 2 1 6.47 7.80 0.84 o 6 2 1 6.41 5.15 1.03 o 7 2 1 9.16 11.95 1.41 o -7 3 1 297.67 290.88 5.06 o -6 3 1 198.43 197.94 3.78 o -5 3 1 485.24 496.66 5.74 o -4 3 1 790.30 783.31 5.26 o -3 3 1 3248.15 3231.83 15.05 o -2 3 1 2826.86 2793.59 20.78 o -1 3 1 1456.25 1338.10 6.25 o 0 3 1 2884.30 2640.51 14.78 o 1 3 1 6850.71 6333.36 32.00 o 2 3 1 5607.75 5550.44 26.09 o 3 3 1 1648.99 1632.81 12.02 o 4 3 1 1614.31 1596.07 10.37 o 5 3 1 494.89 500.85 5.23 o 6 3 1 595.22 579.32 10.79 o 7 3 1 4.22 8.73 1.97 o -7 4 1 24.68 25.71 1.93 o -6 4 1 10.46 9.69 1.28 o -5 4 1 48.05 48.51 1.82 o -4 4 1 96.71 101.79 1.52 o -3 4 1 38.73 37.38 0.76 o -2 4 1 9.84 12.25 0.44 o -1 4 1 2561.47 2692.87 13.09 o 0 4 1 640.45 769.66 3.90 o 1 4 1 214.75 234.06 1.56 o 2 4 1 1.49 1.46 0.22 o 3 4 1 32.50 36.52 0.79 o 4 4 1 86.29 86.70 1.57 o 5 4 1 24.43 24.15 1.45 o 6 4 1 77.81 83.00 2.56 o 7 4 1 38.04 40.91 2.82 o -7 5 1 209.79 221.34 4.44 o -6 5 1 661.17 650.42 8.34 o -5 5 1 397.46 401.62 4.69 o -4 5 1 1208.62 1207.28 7.99 o -3 5 1 1188.58 1153.40 6.18 o -2 5 1 3781.41 3898.37 23.75 o -1 5 1 11.87 8.75 0.40 o 0 5 1 78.66 64.81 0.79 o 1 5 1 3705.95 3810.95 22.76 o 2 5 1 858.82 815.30 4.39 o 3 5 1 942.54 942.32 7.31 o 4 5 1 611.64 621.39 5.61 o 5 5 1 643.93 625.26 6.77 o 6 5 1 143.84 148.91 4.87 o 7 5 1 111.13 103.23 3.13 o -7 6 1 0.98 3.96 1.41 o -6 6 1 4.81 4.53 1.11 o -5 6 1 349.31 335.89 5.50 o -4 6 1 240.07 245.71 2.77 o -3 6 1 289.53 307.01 2.84 o -2 6 1 524.72 571.93 3.37 o -1 6 1 79.40 86.20 0.93 o 0 6 1 136.17 146.34 1.15 o 1 6 1 1220.45 1344.00 7.13 o 2 6 1 432.58 468.11 2.92 o 3 6 1 462.80 459.15 3.96 o 4 6 1 520.06 502.80 5.20 o 5 6 1 9.91 9.04 1.05 o 6 6 1 4.87 7.30 1.15 o -7 7 1 297.05 305.44 6.80 o -6 7 1 555.14 554.44 7.74 o -5 7 1 723.65 720.70 6.79 o -4 7 1 14.09 17.03 0.93 o -3 7 1 1239.47 1211.12 7.71 o -2 7 1 2313.50 2323.16 14.18 o -1 7 1 1159.99 1152.08 6.01 o 0 7 1 1625.57 1608.10 7.69 o 1 7 1 3112.49 3161.10 14.33 o 2 7 1 1175.78 1107.94 5.92 o 3 7 1 5.71 6.21 0.57 o 4 7 1 1147.88 1132.17 8.84 o 5 7 1 711.84 718.15 7.51 o 6 7 1 315.69 310.47 4.91 o -6 8 1 2.42 2.96 1.20 o -5 8 1 23.89 22.33 1.80 o -4 8 1 10.82 11.86 0.82 o -3 8 1 134.00 140.13 1.91 o -2 8 1 52.10 51.51 0.90 o -1 8 1 9.04 11.35 0.72 o 0 8 1 38.73 43.03 0.78 o 1 8 1 0.55 1.74 0.65 o 2 8 1 85.35 94.48 1.84 o 3 8 1 18.23 21.06 1.71 o 4 8 1 16.21 15.57 1.20 o 5 8 1 5.89 5.15 0.89 o 6 8 1 5.16 5.79 1.59 o -6 9 1 414.48 419.58 9.22 o -5 9 1 512.45 508.80 6.95 o -4 9 1 22.50 25.78 1.24 o -3 9 1 938.37 910.90 7.12 o -2 9 1 2396.60 2366.30 14.84 o -1 9 1 1039.52 1047.32 6.19 o 0 9 1 1740.75 1748.56 8.08 o 1 9 1 3908.55 3863.72 28.86 o 2 9 1 1514.30 1479.68 11.49 o 3 9 1 91.59 101.59 2.31 o 4 9 1 1261.91 1231.98 11.80 o 5 9 1 859.64 860.44 9.59 o 6 9 1 163.27 157.39 8.26 o -6 10 1 48.63 53.56 5.54 o -5 10 1 113.03 106.65 3.13 o -4 10 1 44.30 43.42 1.65 o -3 10 1 1.65 4.81 1.09 o -2 10 1 6.99 6.35 0.64 o -1 10 1 96.13 87.80 1.90 o 0 10 1 449.19 426.55 2.89 o 1 10 1 51.34 60.62 1.28 o 2 10 1 5.41 2.02 0.60 o 3 10 1 5.86 6.85 0.86 o 4 10 1 134.80 129.26 2.99 o 5 10 1 83.91 88.99 2.83 o 6 10 1 5.32 5.73 1.87 o -6 11 1 384.54 382.37 9.26 o -5 11 1 517.17 528.72 8.56 o -4 11 1 570.25 562.61 8.35 o -3 11 1 623.46 617.37 6.47 o -2 11 1 2056.25 2103.58 14.30 o -1 11 1 20.07 21.30 0.88 o 0 11 1 38.16 39.02 0.97 o 1 11 1 2004.37 2067.83 13.90 o 2 11 1 414.93 417.91 5.94 o 3 11 1 360.53 365.04 4.52 o 4 11 1 621.36 613.70 8.49 o 5 11 1 312.16 320.60 6.15 o 6 11 1 37.78 36.73 3.40 o -6 12 1 30.16 31.72 3.37 o -5 12 1 117.20 113.52 4.06 o -4 12 1 2.87 4.22 1.44 o -3 12 1 39.12 38.18 1.75 o -2 12 1 105.30 100.26 2.55 o -1 12 1 517.24 503.93 4.29 o 0 12 1 382.05 365.47 3.45 o 1 12 1 234.66 225.90 2.83 o 2 12 1 18.42 19.28 1.17 o 3 12 1 10.95 9.57 1.17 o 4 12 1 174.74 167.05 5.69 o 5 12 1 43.02 41.81 2.60 o -5 13 1 477.53 463.91 9.39 o -4 13 1 211.27 203.69 4.97 o -3 13 1 662.38 654.64 7.83 o -2 13 1 1114.87 1112.40 8.85 o -1 13 1 213.73 218.28 2.51 o 0 13 1 243.29 249.77 3.10 o 1 13 1 1500.45 1488.04 10.16 o 2 13 1 661.36 671.67 6.70 o 3 13 1 256.70 248.33 3.83 o 4 13 1 806.74 805.09 10.52 o 5 13 1 161.43 160.53 4.52 o -5 14 1 179.71 186.60 5.27 o -4 14 1 9.82 6.67 1.76 o -3 14 1 68.00 63.88 3.01 o -2 14 1 0.36 1.55 0.82 o -1 14 1 1.11 1.55 0.52 o 0 14 1 12.01 15.11 0.96 o 1 14 1 4.88 4.51 0.79 o 2 14 1 143.98 131.60 2.62 o 3 14 1 10.58 10.31 1.26 o 4 14 1 185.20 193.47 4.59 o 5 14 1 15.76 17.59 2.09 o -5 15 1 81.59 76.26 3.75 o -4 15 1 93.52 93.47 3.71 o -3 15 1 394.66 394.85 5.93 o -2 15 1 668.83 666.22 6.94 o -1 15 1 706.18 714.61 7.85 o 0 15 1 1024.80 1049.55 10.33 o 1 15 1 929.32 903.09 9.17 o 2 15 1 552.24 547.21 7.80 o 3 15 1 187.65 190.91 3.79 o 4 15 1 249.28 241.38 4.66 o -4 16 1 80.51 81.03 3.58 o -3 16 1 1.75 1.28 1.08 o -2 16 1 82.53 82.21 3.02 o -1 16 1 109.57 111.05 3.42 o 0 16 1 319.34 325.33 4.84 o 1 16 1 17.04 17.91 1.62 o 2 16 1 8.30 8.27 1.52 o 3 16 1 45.25 47.83 2.63 o 4 16 1 23.66 26.68 2.02 o -4 17 1 96.43 98.58 3.36 o -3 17 1 541.61 555.64 10.90 o -2 17 1 150.10 152.18 4.09 o -1 17 1 312.04 310.63 4.88 o 0 17 1 363.13 367.83 5.31 o 1 17 1 132.29 138.08 4.14 o 2 17 1 335.10 339.09 6.01 o 3 17 1 44.56 43.71 2.52 o 4 17 1 92.45 93.49 3.83 o -3 18 1 55.56 56.28 3.02 o -2 18 1 4.03 4.01 1.37 o -1 18 1 280.56 280.66 5.47 o 0 18 1 158.82 167.57 3.52 o 1 18 1 2.32 2.45 1.02 o 2 18 1 18.58 17.55 2.63 o 3 18 1 0.65 0.94 1.73 o -3 19 1 482.08 460.18 11.25 o -2 19 1 232.43 233.92 5.25 o -1 19 1 165.34 167.76 4.26 o 0 19 1 195.28 197.55 3.97 o 1 19 1 336.47 335.78 8.09 o 2 19 1 497.79 482.92 16.79 o -1 20 1 0.11 2.52 1.26 o 0 20 1 0.14 2.47 2.99 o 1 20 1 7.57 10.15 2.19 o -7 0 2 391.83 393.45 9.55 o -6 0 2 64.66 64.16 3.13 o -5 0 2 533.43 540.94 7.74 o -4 0 2 240.03 229.62 3.18 o -3 0 2 928.77 953.10 7.74 o -2 0 2 128.43 100.95 1.69 o -1 0 2 31993.42 25177.06 302.59 o 0 0 2 12.07 7.12 1.00 o 1 0 2 3938.31 3740.77 24.57 o 2 0 2 2387.22 2367.50 18.08 o 3 0 2 2090.09 2061.25 13.67 o 4 0 2 181.46 194.49 3.79 o 5 0 2 2136.61 2082.00 21.12 o 6 0 2 613.60 612.35 9.16 o 7 0 2 426.02 444.38 14.06 o -7 1 2 18.96 16.92 1.88 o -6 1 2 70.89 66.76 2.42 o -5 1 2 38.28 40.95 1.61 o -4 1 2 23.68 22.81 0.83 o -3 1 2 18.61 19.33 0.63 o -2 1 2 122.22 116.82 1.23 o -1 1 2 214.03 193.15 1.39 o 0 1 2 1323.67 1286.46 12.63 o 1 1 2 802.55 880.04 4.76 o 2 1 2 113.39 129.74 1.18 o 3 1 2 18.64 25.17 0.83 o 4 1 2 171.91 162.20 2.43 o 5 1 2 15.39 14.59 1.04 o 6 1 2 102.70 110.06 2.56 o 7 1 2 40.22 44.04 6.12 o -7 2 2 443.49 445.66 6.36 o -6 2 2 185.54 185.25 3.71 o -5 2 2 1099.72 1101.10 8.27 o -4 2 2 1467.15 1474.00 7.89 o -3 2 2 352.44 345.25 2.49 o -2 2 2 1621.83 1571.44 7.60 o -1 2 2 6143.38 6100.14 29.26 o 0 2 2 466.90 456.89 2.82 o 1 2 2 71.19 46.00 0.63 o 2 2 2 3946.75 3981.78 22.78 o 3 2 2 956.32 915.85 5.94 o 4 2 2 94.89 107.21 1.97 o 5 2 2 675.50 661.78 6.32 o 6 2 2 382.54 399.11 6.16 o 7 2 2 176.47 173.79 7.46 o -7 3 2 0.00 0.00 1.15 o -6 3 2 2.19 4.06 1.14 o -5 3 2 163.94 166.81 3.51 o -4 3 2 106.23 110.07 1.51 o -3 3 2 97.72 97.80 1.23 o -2 3 2 23.56 27.29 0.64 o -1 3 2 10.70 11.98 0.62 o 0 3 2 0.00 1.82 0.29 o 1 3 2 161.12 186.20 1.42 o 2 3 2 202.86 221.19 1.94 o 3 3 2 421.12 435.40 3.47 o 4 3 2 0.35 1.84 0.89 o 5 3 2 0.32 0.23 0.59 o 6 3 2 9.34 10.23 2.23 o 7 3 2 26.39 27.26 2.45 o -7 4 2 283.68 274.46 5.63 o -6 4 2 50.01 55.54 2.28 o -5 4 2 2055.95 2062.58 13.70 o -4 4 2 1015.73 1002.44 6.93 o -3 4 2 1055.57 1045.03 5.41 o -2 4 2 948.94 926.69 4.62 o -1 4 2 2284.77 2249.69 13.56 o 0 4 2 87.97 70.47 1.02 o 1 4 2 1787.23 1774.57 11.45 o 2 4 2 2549.56 2623.91 13.50 o 3 4 2 3398.42 3344.33 19.75 o 4 4 2 12.92 19.82 0.93 o 5 4 2 509.11 506.66 5.95 o 6 4 2 207.57 201.29 4.85 o -7 5 2 0.00 1.61 1.31 o -6 5 2 107.16 104.83 3.34 o -5 5 2 0.33 -0.14 0.66 o -4 5 2 0.78 1.60 0.56 o -3 5 2 125.94 132.49 1.49 o -2 5 2 336.57 360.17 2.21 o -1 5 2 84.33 89.92 0.96 o 0 5 2 2013.93 2088.47 16.23 o 1 5 2 0.50 1.58 0.33 o 2 5 2 15.50 13.50 0.52 o 3 5 2 47.28 51.19 1.06 o 4 5 2 304.92 294.13 3.75 o 5 5 2 4.97 3.86 1.00 o 6 5 2 0.06 1.94 1.69 o -7 6 2 109.70 111.95 3.80 o -6 6 2 74.13 76.06 3.03 o -5 6 2 927.90 924.21 8.14 o -4 6 2 106.37 110.47 1.89 o -3 6 2 889.83 876.74 5.97 o -2 6 2 872.82 858.75 4.45 o -1 6 2 4727.53 4706.84 26.83 o 0 6 2 676.19 643.10 3.53 o 1 6 2 3248.03 3219.16 16.26 o 2 6 2 1266.64 1281.32 7.06 o 3 6 2 2744.63 2748.50 17.83 o 4 6 2 349.82 353.80 4.78 o 5 6 2 805.43 790.60 10.26 o 6 6 2 520.37 501.31 8.20 o -7 7 2 4.49 6.88 1.65 o -6 7 2 2.91 2.54 1.30 o -5 7 2 0.37 1.22 0.74 o -4 7 2 165.85 173.69 2.61 o -3 7 2 8.73 10.19 0.75 o -2 7 2 1058.38 1119.54 5.96 o -1 7 2 72.97 78.41 1.02 o 0 7 2 198.40 228.82 1.51 o 1 7 2 218.93 234.70 1.88 o 2 7 2 15.20 15.97 0.76 o 3 7 2 0.35 1.36 0.55 o 4 7 2 36.85 34.04 3.04 o 5 7 2 0.19 0.02 1.11 o 6 7 2 53.52 49.83 2.98 o -6 8 2 638.27 627.93 8.49 o -5 8 2 548.81 551.25 5.91 o -4 8 2 269.50 286.28 3.41 o -3 8 2 515.25 494.98 4.39 o -2 8 2 2157.43 2145.42 12.19 o -1 8 2 2429.03 2435.16 12.09 o 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