#------------------------------------------------------------------------------ #$Date: 2016-11-16 04:08:19 +0200 (Wed, 16 Nov 2016) $ #$Revision: 188490 $ #$URL: file:///home/coder/svn-repositories/cod/cif/2/24/19/2241945.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2241945 loop_ _publ_author_name 'Im, Hansu' 'Moon, Suk-Hee' 'Kim, Tae Ho' 'Park, Ki-Min' _publ_section_title ; Crystal structure of N,N'-dibenzylpyromellitic diimide ; _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first 1809 _journal_page_last 1811 _journal_paper_doi 10.1107/S2056989016017710 _journal_volume 72 _journal_year 2016 _chemical_formula_iupac 'C24 H16 N2 O4' _chemical_formula_moiety 'C24 H16 N2 O4' _chemical_formula_sum 'C24 H16 N2 O4' _chemical_formula_weight 396.39 _chemical_name_common ; N,N'-Dibenzylpyromellitic diimide ; _chemical_name_systematic ; 2,6-Dibenzylpyrrolo[3,4-f]isoindole-1,3,5,7(2H,6H)-\ tetraone ; _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2yn' _space_group_name_H-M_alt 'P 1 21/n 1' _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _atom_sites_solution_hydrogens geom _audit_creation_method SHELXL-2014/7 _cell_angle_alpha 90 _cell_angle_beta 90.461(3) _cell_angle_gamma 90 _cell_formula_units_Z 2 _cell_length_a 6.1500(5) _cell_length_b 4.7475(3) _cell_length_c 31.002(2) _cell_measurement_reflns_used 874 _cell_measurement_temperature 173(2) _cell_measurement_theta_max 24.82 _cell_measurement_theta_min 2.63 _cell_volume 905.14(11) _computing_cell_refinement ; SAINT (Bruker, 2013) ; _computing_data_collection ; APEX2 (Bruker, 2013) ; _computing_data_reduction ; SAINT (Bruker, 2013) ; _computing_molecular_graphics ; DIAMOND (Brandenburg, 2010) ; _computing_publication_material ; SHELXTL (Sheldrick, 2008) ; _computing_structure_refinement ; SHELXL2014 (Sheldrick, 2015) ; _computing_structure_solution ; SHELXS97 (Sheldrick 2008) ; _diffrn_ambient_temperature 173(2) _diffrn_measured_fraction_theta_full 0.984 _diffrn_measured_fraction_theta_max 0.978 _diffrn_measurement_device_type 'Bruker APEXII CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0343 _diffrn_reflns_limit_h_max 7 _diffrn_reflns_limit_h_min -6 _diffrn_reflns_limit_k_max 6 _diffrn_reflns_limit_k_min -2 _diffrn_reflns_limit_l_max 40 _diffrn_reflns_limit_l_min -38 _diffrn_reflns_number 4593 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 27.495 _diffrn_reflns_theta_min 1.314 _exptl_absorpt_coefficient_mu 0.101 _exptl_absorpt_correction_T_max 0.7456 _exptl_absorpt_correction_T_min 0.6611 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; (SADABS; Bruker 2013) ; _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 1.454 _exptl_crystal_description needle _exptl_crystal_F_000 412 _exptl_crystal_size_max 0.500 _exptl_crystal_size_mid 0.060 _exptl_crystal_size_min 0.020 _refine_diff_density_max 0.254 _refine_diff_density_min -0.215 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.042 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 136 _refine_ls_number_reflns 2016 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.042 _refine_ls_R_factor_all 0.0692 _refine_ls_R_factor_gt 0.0478 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0529P)^2^+0.0890P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1087 _refine_ls_wR_factor_ref 0.1194 _reflns_number_gt 1444 _reflns_number_total 2016 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file sj5513sup1.cif _cod_data_source_block I _cod_database_code 2241945 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.951 _shelx_estimated_absorpt_t_max 0.998 _shelx_hkl_file ; 0 0 -1 -1.30 0.40 0 0 1 -0.50 0.50 0 0 1 -0.20 0.40 0 0 -2 -0.50 1.00 0 0 2 -2.30 0.80 0 0 -3 0.00 1.40 0 0 3 0.50 1.30 0 0 4 280.47 10.80 0 0 -4 286.57 11.50 0 0 -5 -1.80 1.60 0 0 5 -2.20 1.30 0 0 6 -1.40 1.60 0 0 -6 1.60 2.30 0 0 -7 2.70 2.60 0 0 7 0.70 1.90 0 0 8 91.59 9.20 0 0 -8 97.99 10.10 0 0 -9 0.40 2.60 0 0 9 0.40 2.40 0 0 10 -3.90 2.00 0 0 11 -0.20 2.60 0 0 12 103.09 13.00 0 0 13 1.90 3.90 0 -1 0 -0.40 0.50 0 -1 0 -0.60 0.40 0 -1 -1 0.30 1.00 0 -1 -1 0.00 0.80 0 1 2 852.01 22.00 0 -1 -2 836.02 23.00 0 -1 2 871.41 20.70 0 -1 2 860.71 21.10 0 1 3 0.00 1.30 0 -1 -3 -0.40 1.50 0 -1 3 -0.90 1.00 0 -1 3 2.00 1.10 0 1 4 44.70 4.70 0 -1 4 50.69 4.80 0 -1 4 46.60 4.20 0 -1 -4 47.40 5.60 0 1 5 0.20 1.50 0 -1 5 0.50 0.80 0 -1 5 -0.90 1.20 0 -1 -5 0.00 1.90 0 1 6 30.30 5.10 0 -1 6 31.90 1.30 0 -1 -6 36.80 6.00 0 -1 6 29.90 4.80 0 -1 6 30.00 4.60 0 1 -7 -0.90 1.90 0 1 7 0.30 2.00 0 -1 7 -0.40 0.50 0 -1 7 -0.80 1.40 0 -1 -7 -1.30 2.10 0 1 8 25.00 5.30 0 -1 8 29.10 2.20 0 -1 -8 25.20 5.80 0 -1 8 22.00 4.80 0 1 9 -1.60 2.30 0 -1 -9 2.10 3.20 0 -1 9 -1.10 0.60 0 -1 9 2.50 2.80 0 1 10 2.60 3.10 0 -1 -10 4.10 3.80 0 -1 10 7.00 3.30 0 -1 11 1.10 2.80 0 -1 12 88.29 11.60 0 -1 13 3.30 4.00 0 -1 14 48.60 10.20 0 -1 15 2.30 4.40 0 -2 0 178.58 5.90 0 -2 0 171.88 5.50 0 -2 -1 0.00 0.90 0 -2 -1 -0.30 1.10 0 -2 -2 152.48 6.80 0 -2 2 144.59 4.70 0 -2 -2 149.79 7.40 0 -2 2 154.78 4.60 0 -2 3 -0.60 0.80 0 -2 -3 -1.40 1.10 0 -2 -3 0.80 1.80 0 -2 3 -0.70 0.80 0 -2 4 3.20 1.60 0 -2 -4 4.00 2.00 0 -2 4 6.20 1.70 0 -2 -4 6.10 2.60 0 2 5 -1.90 1.20 0 -2 5 0.30 1.20 0 -2 -5 -3.30 1.60 0 -2 5 0.00 1.30 0 2 6 29.80 4.90 0 -2 -6 30.60 6.00 0 -2 6 22.00 3.70 0 -2 6 24.20 4.20 0 -2 -7 2.20 2.80 0 -2 7 0.60 1.80 0 -2 7 0.50 1.70 0 -2 8 32.70 5.50 0 -2 -8 47.80 8.40 0 -2 9 -1.10 2.10 0 -2 -9 0.30 2.90 0 -2 -10 34.20 8.10 0 -2 10 30.40 6.10 0 -2 11 -1.90 2.10 0 -2 -11 -1.90 3.50 0 -2 12 40.40 8.10 0 -2 13 0.90 3.50 0 -2 14 28.60 8.00 0 -2 15 -2.20 4.40 0 -3 0 0.90 1.10 0 -3 0 -0.40 0.90 0 -3 1 0.40 0.80 0 -3 1 0.30 0.60 0 -3 -1 0.70 1.40 0 -3 -1 2.00 1.20 0 -3 -2 94.59 6.50 0 -3 2 88.09 3.50 0 -3 -2 87.09 5.50 0 -3 2 82.89 3.40 0 -3 3 0.30 0.80 0 -3 3 0.40 0.80 0 -3 -3 -2.50 1.50 0 -3 -3 -1.00 1.30 0 -3 -4 3.30 1.90 0 -3 4 2.10 1.30 0 -3 4 1.90 1.30 0 -3 -4 3.80 2.90 0 -3 5 0.80 1.30 0 -3 5 -0.70 1.10 0 -3 -5 3.00 2.70 0 -3 -6 59.09 8.70 0 -3 6 62.09 6.30 0 -3 6 56.99 5.50 0 -3 -7 0.80 2.90 0 -3 7 1.00 1.80 0 -3 -8 77.89 11.20 0 -3 8 82.69 8.00 0 -3 9 0.90 2.20 0 -3 -9 1.90 3.60 0 -3 -10 72.19 11.70 0 -3 10 65.09 8.50 0 -3 -11 2.10 4.50 0 -3 11 -1.50 2.60 0 -3 12 -2.20 2.70 0 -3 -12 8.40 6.10 0 -3 13 1.60 4.20 0 -4 0 0.00 1.30 0 -4 0 -0.50 1.10 0 -4 -1 0.40 1.40 0 -4 1 0.70 1.10 0 -4 1 -1.40 1.00 0 -4 -1 -1.60 1.40 0 -4 -2 193.18 10.50 0 -4 2 197.08 6.80 0 -4 2 195.38 6.60 0 -4 3 -0.50 0.90 0 -4 3 -0.40 0.70 0 -4 -3 3.40 2.50 0 -4 4 152.48 6.30 0 -4 -4 135.49 10.20 0 -4 4 143.89 6.10 0 -4 5 0.00 1.20 0 -4 -5 -3.30 1.90 0 -4 5 0.40 1.30 0 -4 6 34.00 4.30 0 -4 -6 55.79 9.00 0 -4 -7 1.10 3.20 0 -4 7 1.40 1.90 0 -4 -8 0.60 3.80 0 -4 8 1.90 2.00 0 -4 -9 2.30 4.30 0 -4 9 0.50 2.30 0 -4 -10 1.10 4.50 0 -4 10 0.50 2.40 0 -4 11 1.30 2.80 0 -4 -11 8.10 5.90 0 -4 12 13.80 5.00 0 -4 -12 13.80 7.50 0 -5 0 2.90 1.90 0 -5 -1 -0.30 1.70 0 -5 1 0.80 1.40 0 -5 -2 2.50 2.40 0 -5 2 3.40 1.30 0 -5 2 3.50 1.30 0 -5 3 0.40 0.90 0 -5 -3 -2.00 2.10 0 -5 3 -0.60 0.80 0 -5 4 1.10 0.90 0 -5 4 -0.50 1.00 0 -5 -4 -1.10 2.60 0 -5 -5 -3.20 2.30 0 -5 5 0.90 1.20 0 -5 6 76.19 5.00 0 -5 -6 78.79 11.30 0 -5 7 0.30 1.70 0 -5 -7 -0.40 3.90 0 -5 -8 32.60 8.30 0 -5 8 23.90 4.20 0 -5 9 0.80 2.20 0 -5 -9 -0.70 4.40 0 -6 0 82.49 6.10 0 -6 1 -1.00 1.50 0 -6 -1 0.90 2.10 0 -6 -2 16.10 4.30 0 -6 -3 3.10 3.00 -1 0 13 1.00 3.90 -1 0 12 -1.60 3.20 -1 0 11 -0.40 2.70 -1 0 10 89.39 10.70 1 0 -9 0.60 2.70 -1 0 9 2.20 2.90 -1 0 8 2.10 2.80 1 0 -8 -1.80 2.10 -1 0 7 -1.00 1.60 1 0 -7 -0.90 2.00 -1 0 6 1518.25 41.70 1 0 -6 1536.25 43.00 1 0 -5 -0.50 1.70 -1 0 5 -2.00 1.10 -1 0 4 -1.00 1.30 1 0 -4 1.10 2.00 1 0 -3 2.50 1.60 -1 0 3 1.00 1.30 1 0 -2 775.02 20.10 -1 0 2 759.82 19.60 -1 0 1 1.00 0.50 -1 0 1 -0.20 0.50 1 0 -1 0.00 0.60 1 0 0 -2.70 0.10 1 0 0 -2.60 0.10 -1 0 0 -2.70 0.10 -1 0 0 -2.80 0.10 1 0 1 -0.10 0.40 -1 0 -1 0.10 0.60 1 0 1 -0.50 0.50 -1 0 -2 110.49 5.00 1 0 2 106.59 4.60 -1 0 -3 0.40 1.50 1 0 3 -0.80 1.10 -1 0 -4 0.60 1.80 1 0 4 -0.30 1.40 1 0 5 0.20 1.60 -1 0 -5 1.00 2.00 1 0 6 -2.10 1.70 -1 0 -6 1.40 2.40 1 0 7 -0.30 1.70 -1 0 -7 1.20 2.20 1 0 8 -1.90 1.70 -1 0 -8 3.60 3.00 1 0 9 2.20 2.70 -1 0 -9 1.30 2.90 1 0 10 801.82 30.10 1 0 11 -0.40 2.50 1 0 12 -1.00 2.90 1 0 13 2.50 3.90 -1 -1 15 -2.00 4.30 -1 -1 14 13.50 6.10 -1 -1 13 0.30 3.60 -1 -1 12 17.00 5.60 -1 -1 11 4.20 3.40 -1 1 10 68.39 9.50 -1 -1 10 54.39 7.80 1 -1 -10 86.89 11.60 -1 1 9 0.80 2.80 1 -1 -9 0.70 2.90 -1 -1 9 -1.60 2.10 -1 -1 9 0.10 0.60 -1 1 8 -0.50 1.90 -1 -1 8 -0.90 1.90 -1 -1 8 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240.98 11.70 1 -1 6 245.08 11.00 1 -1 6 233.18 6.20 -1 1 -7 1.60 2.10 1 1 7 0.70 1.80 1 -1 7 0.10 0.60 1 -1 7 -0.90 1.50 -1 -1 -7 -1.60 2.00 1 1 8 7.50 3.30 1 -1 8 11.60 1.50 1 -1 8 12.00 3.60 -1 -1 -8 11.20 4.30 1 1 9 -0.30 2.30 1 -1 9 -1.10 1.80 -1 -1 -9 -0.60 2.70 1 1 10 271.97 16.10 1 -1 10 270.77 15.30 -1 -1 -10 278.47 17.50 1 -1 11 -1.30 2.40 1 -1 12 338.57 19.30 1 -1 13 2.20 4.00 1 -1 14 57.09 10.70 1 -1 15 7.90 5.60 -1 -2 15 -4.90 3.80 -1 -2 14 15.10 6.20 -1 -2 13 -3.90 2.60 -1 -2 12 13.60 5.60 -1 -2 11 -0.20 2.60 1 -2 -11 -2.60 2.80 1 -2 -10 10.80 5.20 -1 -2 10 19.10 5.20 -1 -2 9 -0.70 2.00 1 -2 -9 1.40 3.60 -1 -2 8 230.68 12.20 1 -2 -8 248.98 15.60 -1 -2 7 -0.80 1.70 -1 -2 7 -1.20 1.60 1 -2 -7 -2.60 2.00 -1 2 6 426.76 17.10 -1 -2 6 441.16 16.50 1 -2 -6 422.46 19.20 -1 -2 6 472.95 16.00 -1 2 5 3.10 1.90 -1 -2 5 0.20 1.20 1 -2 -5 2.90 2.40 -1 -2 5 -0.40 1.10 1 -2 -4 39.40 5.00 1 -2 -4 31.30 5.10 -1 -2 4 31.40 3.50 -1 -2 4 31.50 3.20 1 -2 -3 0.60 1.70 -1 -2 3 -0.10 0.70 -1 -2 3 -0.50 0.80 1 -2 -3 1.20 1.40 1 -2 -2 68.49 4.50 1 -2 -2 62.79 4.90 1 -2 -1 -1.00 0.80 1 -2 -1 0.20 1.20 1 -2 0 39.50 2.40 1 -2 0 45.70 2.90 -1 -2 0 47.00 2.50 -1 -2 0 40.40 2.10 -1 -2 0 39.80 2.10 1 -2 1 -0.20 0.60 -1 -2 -1 -1.10 0.90 -1 -2 -1 0.20 0.90 1 -2 1 -0.40 0.60 1 -2 2 143.79 5.00 -1 -2 -2 136.59 6.40 1 -2 2 155.38 5.00 -1 -2 -2 136.89 7.00 -1 -2 -3 -0.40 1.00 1 -2 3 0.00 0.80 1 -2 3 2.10 1.10 -1 -2 -3 1.70 1.80 -1 -2 -4 70.89 6.70 1 -2 4 75.49 4.50 -1 -2 -4 68.29 7.10 1 -2 4 88.59 5.30 1 2 5 0.00 1.40 1 -2 5 -1.10 1.10 1 -2 5 -0.10 1.40 -1 -2 -5 1.10 2.30 1 2 6 63.19 6.80 1 -2 6 56.09 5.60 1 -2 6 74.69 7.30 -1 -2 -6 75.59 8.70 -1 -2 -7 -1.80 2.20 1 -2 7 1.50 2.00 1 -2 7 0.00 1.60 1 -2 8 30.80 5.20 -1 -2 -8 47.60 8.30 -1 -2 -9 5.80 4.00 1 -2 9 -0.10 2.10 1 -2 10 55.99 8.20 -1 -2 -10 41.20 8.70 1 -2 11 2.50 3.30 -1 -2 -11 -3.90 3.70 1 -2 12 -2.40 2.70 1 -2 13 0.20 3.20 1 -2 14 68.99 11.30 1 -2 15 -3.10 4.00 -1 -3 13 -2.10 3.50 1 -3 -12 -1.40 4.10 -1 -3 12 0.90 3.20 1 -3 -11 -3.50 3.40 -1 -3 11 -2.90 2.40 -1 -3 10 1.00 2.50 1 -3 -10 1.80 3.60 -1 -3 9 0.60 2.20 1 -3 -9 0.30 3.40 -1 -3 8 17.20 4.00 1 -3 -8 19.30 5.80 -1 -3 7 -0.30 1.60 1 -3 -7 -0.50 2.70 -1 -3 6 52.79 5.30 1 -3 -6 55.19 8.50 -1 -3 6 53.29 5.80 -1 -3 5 0.30 1.20 1 -3 -5 -1.60 1.90 -1 -3 5 -0.50 1.10 -1 -3 4 3.90 1.50 1 -3 -4 4.50 2.30 -1 -3 4 5.20 1.50 1 -3 -4 0.80 2.50 -1 -3 3 -0.10 0.70 -1 -3 3 -0.10 0.70 1 -3 -3 -0.60 1.70 1 -3 -3 -1.20 1.20 1 -3 -2 9.30 2.50 1 -3 -2 11.30 2.90 1 -3 -1 0.30 1.10 1 -3 -1 -0.50 1.20 -1 -3 1 1.30 0.90 -1 -3 1 0.90 0.60 -1 -3 0 345.37 11.00 1 -3 0 344.37 10.80 1 -3 0 350.36 10.80 -1 -3 0 348.57 10.40 1 -3 0 346.97 11.40 1 -3 1 -1.20 0.70 -1 -3 -1 0.90 1.40 1 -3 1 0.10 0.80 -1 -3 -1 -1.30 0.80 1 -3 2 81.59 3.70 -1 -3 -2 72.89 6.60 1 -3 2 82.19 3.60 -1 -3 -2 83.09 5.30 1 -3 3 -0.70 0.80 -1 -3 -3 0.10 1.30 -1 -3 -3 -1.40 1.60 1 -3 3 1.10 0.90 -1 -3 -4 82.89 8.60 1 -3 4 92.59 5.20 1 -3 4 97.39 5.00 -1 -3 -4 99.49 7.00 -1 -3 -5 -1.90 2.00 1 -3 5 -0.10 1.30 1 -3 5 0.30 1.40 1 -3 6 0.90 1.70 1 -3 6 0.70 1.50 -1 -3 -6 -0.80 2.80 1 -3 7 0.90 1.70 -1 -3 -7 0.20 2.80 -1 -3 -8 2.00 3.90 1 -3 8 0.60 2.00 1 -3 9 -0.30 1.80 -1 -3 -9 -0.50 3.30 -1 -3 -10 27.70 7.90 1 -3 10 25.60 5.60 -1 -3 -11 6.80 4.90 1 -3 11 0.30 2.80 -1 -3 -12 5.70 5.10 1 -3 12 0.80 3.20 1 -3 13 -0.90 3.40 -1 -4 12 75.99 10.30 1 -4 -12 89.89 15.50 1 -4 -11 4.80 5.10 -1 -4 11 2.20 3.10 1 -4 -10 74.49 12.60 -1 -4 10 67.69 8.40 1 -4 -9 1.30 4.20 -1 -4 9 0.30 2.20 -1 -4 8 0.00 2.00 1 -4 -8 4.60 4.60 -1 -4 7 1.80 1.80 1 -4 -7 -2.90 2.70 -1 -4 6 200.98 8.90 1 -4 -6 182.98 13.80 1 -4 -5 -0.10 2.60 -1 -4 5 0.40 1.30 -1 -4 5 -0.20 1.00 -1 -4 4 20.20 2.30 -1 -4 4 20.20 2.50 1 -4 -4 29.80 5.90 -1 -4 3 -0.30 0.60 -1 -4 3 1.00 0.80 1 -4 -3 -0.40 2.00 1 -4 -2 10.60 3.30 -1 -4 2 12.00 1.60 -1 -4 2 7.20 1.30 1 -4 -1 1.30 1.40 -1 -4 1 0.80 0.90 -1 -4 1 -0.60 0.90 1 -4 -1 -0.50 1.50 1 -4 0 76.49 4.90 -1 -4 0 74.39 5.00 -1 -4 0 73.59 4.50 1 -4 0 82.29 5.40 1 -4 1 -0.80 1.20 -1 -4 -1 0.50 1.30 -1 -4 -1 -2.80 1.40 1 -4 1 0.00 1.00 1 -4 2 15.80 2.30 1 -4 2 13.10 2.00 -1 -4 -2 13.50 3.50 1 -4 3 0.60 1.10 -1 -4 -3 0.00 2.10 1 -4 3 0.10 1.00 1 -4 4 65.59 4.20 -1 -4 -4 65.19 8.30 1 -4 4 62.99 4.10 1 -4 5 2.50 1.60 1 -4 5 1.00 1.30 -1 -4 -5 2.60 3.00 1 -4 6 434.66 15.20 -1 -4 -6 456.35 22.10 -1 -4 -7 2.60 3.50 1 -4 7 0.00 1.70 1 -4 8 13.80 3.80 -1 -4 -8 6.00 4.80 1 -4 9 -3.30 1.80 -1 -4 -9 2.60 4.00 1 -4 10 18.00 4.70 -1 -4 -10 10.90 6.60 1 -4 11 1.10 2.80 -1 -4 -11 0.10 4.40 -1 -4 -12 16.50 7.70 1 -4 12 9.70 4.80 -1 -5 9 -0.10 2.20 1 -5 -9 -5.60 4.20 -1 -5 8 69.59 6.80 1 -5 -8 53.49 10.60 1 -5 -7 -2.10 3.20 -1 -5 7 0.20 1.60 -1 -5 6 11.90 2.40 1 -5 -6 12.30 5.20 -1 -5 5 2.20 1.20 1 -5 -5 -1.50 2.40 -1 -5 5 0.40 1.10 1 -5 -4 8.00 3.70 1 -5 -3 -1.90 2.10 1 -5 -2 6.90 3.30 -1 -5 2 9.30 1.50 -1 -5 2 11.30 1.70 1 -5 -1 -1.90 1.60 -1 -5 1 -0.10 1.00 -1 -5 1 -1.40 1.10 -1 -5 0 23.60 3.80 1 -5 0 32.20 4.50 -1 -5 -1 -2.10 1.40 1 -5 1 1.50 1.50 1 -5 2 194.38 7.60 1 -5 2 183.98 7.40 -1 -5 -2 204.08 11.30 1 -5 3 1.10 1.20 1 -5 3 0.10 1.10 1 -5 3 1.00 1.10 -1 -5 -3 -1.00 2.30 1 -5 4 114.99 5.90 -1 -5 -4 119.49 11.90 1 -5 4 121.99 5.40 1 -5 5 -0.50 1.20 -1 -5 -5 1.40 3.20 1 -5 6 7.60 2.30 -1 -5 -6 7.40 4.70 -1 -5 -7 -0.20 3.80 1 -5 7 -0.60 1.60 -1 -5 -8 60.99 11.00 1 -5 8 58.69 6.60 -1 -5 -9 8.50 5.70 1 -5 9 0.10 2.10 1 -6 -3 -0.90 2.60 1 -6 -2 50.09 7.00 1 -6 -1 -2.90 1.80 -1 -6 1 0.90 1.30 -1 -6 0 14.70 3.20 1 -6 0 17.70 3.60 1 -6 1 0.50 1.50 -1 -6 -1 -2.40 1.70 -1 -6 -2 2.80 2.90 -1 -6 -3 -1.40 2.50 -2 0 13 1.50 4.30 -2 0 12 7.40 4.70 -2 0 11 -0.50 2.70 -2 0 10 -1.40 2.40 -2 0 9 -2.40 2.10 2 0 -9 -2.50 2.10 2 0 -8 539.65 22.50 -2 0 8 583.34 22.20 2 0 -7 1.30 2.40 -2 0 7 3.00 2.30 -2 0 6 1.40 2.10 2 0 -6 -1.90 1.80 -2 0 5 6.10 2.10 2 0 -5 3.00 2.30 -2 0 4 81.09 5.30 2 0 -4 77.19 5.70 -2 0 3 -0.60 1.20 2 0 -3 -0.70 1.40 2 0 -2 -1.40 1.10 -2 0 2 -1.40 0.90 2 0 -1 -0.50 0.30 -2 0 1 0.20 0.60 2 0 -1 0.30 0.70 -2 0 1 1.20 0.70 -2 0 0 1802.52 40.80 2 0 0 1812.22 40.80 2 0 0 1788.92 40.70 -2 0 -1 -0.40 0.60 2 0 1 0.60 0.60 2 0 2 -0.30 1.00 -2 0 -2 -0.30 1.20 -2 0 -3 -1.30 1.40 -2 0 -4 548.15 17.60 2 0 4 530.75 16.80 2 0 5 -1.00 1.30 -2 0 -5 -0.40 1.60 -2 0 -6 -0.90 1.80 2 0 6 0.70 1.90 2 0 7 -0.10 1.70 -2 0 -7 -3.20 1.80 -2 0 -8 87.09 9.80 2 0 8 92.89 9.30 2 0 9 -1.30 1.80 -2 0 -9 -1.50 2.20 2 0 10 0.40 2.80 2 0 11 0.60 2.60 2 0 12 663.73 29.00 2 0 13 -2.00 3.40 -2 -1 15 0.90 4.80 -2 -1 14 2.70 4.90 -2 -1 13 3.60 4.30 -2 -1 12 91.89 12.00 -2 -1 11 1.80 2.70 -2 1 10 375.16 19.20 2 -1 -10 361.16 20.20 -2 -1 10 379.06 18.50 -2 1 9 4.50 3.30 -2 -1 9 -0.10 2.10 2 -1 -9 -0.40 2.90 -2 -1 9 -0.90 0.60 -2 1 8 5.10 3.10 2 -1 -8 2.50 3.20 -2 -1 8 6.40 1.00 -2 -1 8 0.60 2.10 -2 1 7 -1.10 1.90 2 -1 -7 4.20 2.90 -2 -1 7 -0.80 0.40 -2 -1 7 1.70 2.00 -2 1 6 83.59 8.10 -2 -1 6 103.09 7.40 -2 -1 6 105.99 7.00 2 -1 -6 94.89 9.50 -2 1 5 -1.80 1.30 -2 -1 5 -0.70 0.70 2 -1 -5 1.90 2.30 -2 -1 5 -1.10 1.20 -2 1 4 4.20 2.20 2 -1 -4 4.50 2.60 -2 -1 4 7.70 2.00 -2 -1 4 5.00 2.10 -2 1 3 2.40 1.50 -2 -1 3 0.20 1.10 -2 -1 3 -0.10 1.00 2 -1 -3 -1.30 1.60 -2 1 2 496.55 14.40 -2 -1 2 507.85 12.90 2 -1 -2 503.75 15.40 -2 -1 2 497.85 13.10 2 -1 -2 508.75 14.60 2 -1 -1 0.10 0.80 2 -1 -1 0.00 0.80 2 -1 -1 1.00 1.20 -2 -1 0 44.90 1.70 2 -1 0 40.80 2.50 2 -1 0 47.10 2.40 -2 -1 0 41.10 1.60 -2 -1 -1 -0.30 0.90 2 -1 1 -1.70 0.60 2 -1 1 0.10 0.70 -2 -1 -1 -0.50 0.70 2 1 2 71.39 4.00 -2 -1 -2 73.09 4.70 2 -1 2 67.89 3.50 2 -1 2 77.89 3.90 2 1 3 -1.20 1.10 -2 -1 -3 -2.10 1.40 2 -1 3 0.70 1.10 2 -1 3 -1.00 1.20 2 1 4 698.03 20.90 2 -1 4 597.84 20.30 2 -1 4 762.52 20.30 -2 -1 -4 746.53 22.50 2 1 5 1.80 1.60 2 -1 5 1.20 1.40 -2 -1 -5 4.10 2.60 2 -1 5 -1.20 1.20 -2 1 -6 40.90 7.00 2 1 6 30.40 5.00 2 -1 6 43.10 5.90 2 -1 6 34.80 1.60 -2 -1 -6 25.60 5.00 2 -1 6 31.80 1.70 2 -1 6 39.70 5.20 2 1 7 1.00 2.10 -2 1 -7 1.40 2.10 2 -1 7 1.10 0.70 -2 -1 -7 3.20 2.70 2 -1 7 -1.40 1.60 2 1 8 142.59 10.00 -2 -1 -8 159.98 11.70 2 -1 8 148.79 5.10 2 -1 8 139.39 9.60 2 1 9 -2.40 2.10 2 -1 9 2.10 2.30 -2 -1 -9 -3.60 2.50 2 1 10 -2.40 2.80 -2 -1 -10 8.20 4.30 2 -1 10 0.30 2.30 2 -1 11 -1.40 2.40 2 -1 12 12.60 4.80 2 -1 13 6.90 4.80 2 -1 14 -0.10 0.80 2 -1 14 2.80 4.10 2 -1 15 1.40 4.50 -2 -2 15 -8.40 3.30 -2 -2 14 5.50 4.40 -2 -2 13 -0.20 3.80 -2 -2 12 18.00 5.80 -2 -2 11 3.20 3.20 2 -2 -11 1.70 3.90 -2 -2 10 42.10 7.00 2 -2 -10 33.20 7.90 2 -2 -9 -2.00 2.80 -2 -2 9 -2.40 1.80 2 -2 -8 162.68 12.50 -2 -2 8 140.79 9.40 2 -2 -7 4.20 3.20 -2 -2 7 0.10 1.80 -2 -2 7 -0.40 1.70 -2 2 6 9.60 3.00 -2 -2 6 3.50 2.20 -2 -2 6 10.40 2.70 2 -2 -6 8.30 3.80 -2 2 5 1.00 1.80 -2 -2 5 -1.70 1.00 -2 -2 5 -0.80 1.20 2 -2 -5 -3.00 1.70 -2 -2 4 352.86 11.10 -2 -2 4 354.66 11.80 2 -2 -4 350.66 15.00 2 -2 -4 351.06 13.70 2 -2 -3 0.50 1.70 -2 -2 3 -0.50 0.70 2 -2 -3 -0.40 1.10 -2 -2 3 -0.50 0.80 2 -2 -2 33.70 4.30 2 -2 -2 47.20 4.40 2 -2 -1 1.00 1.20 2 -2 -1 0.00 0.90 -2 -2 0 355.56 9.40 2 -2 0 359.56 10.40 -2 -2 0 356.06 9.60 2 -2 0 374.36 11.00 2 -2 1 -0.20 0.70 -2 -2 -1 -1.10 0.90 2 -2 1 -0.90 0.70 -2 -2 -1 -0.10 0.80 2 -2 2 47.00 2.80 -2 -2 -2 50.39 5.00 2 -2 2 44.30 2.80 -2 -2 -2 43.10 4.00 -2 -2 -3 -0.50 1.10 -2 -2 -3 -0.10 1.40 2 -2 3 -0.80 0.90 2 -2 3 -0.70 0.80 2 -2 4 210.38 8.30 -2 -2 -4 230.88 11.30 2 -2 4 201.28 8.70 2 2 5 0.80 1.60 2 -2 5 -0.20 1.30 2 -2 5 0.30 1.40 -2 -2 -5 0.20 2.10 2 2 6 1.60 2.20 -2 -2 -6 1.90 2.90 2 -2 6 -0.40 1.60 2 -2 6 0.80 1.60 2 -2 7 -1.50 1.30 2 -2 7 1.40 2.00 -2 -2 -7 -2.90 2.20 2 -2 8 26.80 5.00 -2 -2 -8 38.00 7.30 -2 -2 -9 0.00 3.20 2 -2 9 -0.20 2.10 2 -2 10 69.89 9.00 -2 -2 -10 48.70 9.10 2 -2 11 0.10 2.70 -2 -2 -11 4.90 5.30 2 -2 12 11.50 4.90 2 -2 13 1.40 3.30 2 -2 14 10.90 5.50 2 -2 15 2.40 4.50 -2 -3 13 -0.30 3.80 2 -3 -12 17.00 7.60 -2 -3 12 15.20 5.70 -2 -3 11 -0.60 2.50 2 -3 -11 4.20 5.20 2 -3 -10 18.80 6.60 -2 -3 10 17.20 4.60 -2 -3 9 -0.50 2.20 2 -3 -9 6.70 4.30 2 -3 -8 316.17 18.60 -2 -3 8 274.17 13.30 2 -3 -7 2.10 3.30 -2 -3 7 -1.00 1.50 -2 -3 6 16.20 3.10 2 -3 -6 12.00 4.70 -2 -3 6 16.80 3.40 -2 -3 5 0.30 1.20 2 -3 -5 1.80 2.60 -2 -3 5 -0.80 1.10 2 -3 -4 189.68 11.20 2 -3 -4 187.48 11.40 -2 -3 4 174.68 7.00 -2 -3 4 174.78 6.60 2 -3 -3 0.00 1.50 -2 -3 3 -0.20 0.60 -2 -3 3 -0.30 0.60 2 -3 -3 0.70 1.90 2 -3 -2 -0.50 1.70 2 -3 -2 0.90 1.30 -2 -3 1 1.30 0.60 2 -3 -1 -1.00 1.20 2 -3 -1 -0.10 1.00 -2 -3 1 0.00 0.50 -2 -3 0 41.10 2.80 -2 -3 0 43.00 3.10 2 -3 0 44.80 3.30 2 -3 0 40.60 4.00 -2 -3 -1 -0.80 0.80 2 -3 1 1.10 1.00 -2 -3 -1 0.30 1.30 2 -3 1 -0.50 0.80 -2 -3 -2 13.10 2.60 2 -3 2 21.80 2.40 -2 -3 -2 20.80 3.80 2 -3 2 15.20 2.10 -2 -3 -3 0.00 1.30 2 -3 3 -0.20 0.90 -2 -3 -3 -0.70 1.50 2 -3 3 -0.50 0.90 -2 -3 -4 7.10 3.20 -2 -3 -4 8.50 2.80 2 -3 4 6.90 1.90 2 -3 4 3.40 1.60 2 -3 5 2.30 1.50 2 -3 5 1.10 1.50 -2 -3 -5 0.50 2.30 2 -3 6 107.09 7.20 -2 -3 -6 99.39 11.10 2 -3 6 114.39 7.00 2 -3 7 0.10 1.60 -2 -3 -7 1.90 3.20 2 -3 8 108.99 8.10 -2 -3 -8 111.59 13.10 2 -3 9 0.10 2.00 -2 -3 -9 1.60 3.40 2 -3 10 3.10 3.00 -2 -3 -10 10.90 6.00 -2 -3 -11 -0.60 3.50 2 -3 11 1.30 3.00 -2 -3 -12 6.60 5.20 2 -3 12 4.90 3.70 2 -3 13 -2.20 3.20 -2 -4 12 4.70 3.80 2 -4 -12 9.10 6.70 2 -4 -11 7.30 5.80 -2 -4 11 -1.50 2.50 2 -4 -10 2.70 4.90 -2 -4 10 2.80 2.80 2 -4 -9 -2.00 3.70 -2 -4 9 0.00 2.30 2 -4 -8 7.20 4.80 -2 -4 8 6.30 2.80 -2 -4 7 -1.00 1.50 2 -4 -7 -4.50 2.30 -2 -4 6 32.60 4.10 2 -4 -6 30.90 6.80 -2 -4 5 0.30 1.10 2 -4 -5 -0.90 2.70 -2 -4 5 -1.10 0.90 -2 -4 4 145.99 5.40 2 -4 -4 143.09 10.50 -2 -4 4 135.99 5.50 2 -4 -3 0.80 2.30 2 -4 -2 30.30 4.90 -2 -4 1 -1.20 0.90 2 -4 -1 1.10 1.40 2 -4 -1 1.30 1.80 -2 -4 1 -0.70 0.80 -2 -4 0 30.10 3.20 2 -4 0 29.30 4.10 -2 -4 0 27.00 3.40 2 -4 0 29.80 3.70 2 -4 1 -0.10 1.00 2 -4 1 -1.30 1.00 -2 -4 -1 0.50 1.10 2 -4 1 -0.20 1.20 -2 -4 -1 -1.30 1.40 -2 -4 -2 6.00 2.70 2 -4 2 3.00 1.50 2 -4 2 4.70 1.50 -2 -4 -3 -1.10 1.80 2 -4 3 -1.10 0.80 2 -4 3 0.30 1.10 2 -4 4 98.29 5.40 -2 -4 -4 102.39 10.60 2 -4 4 98.79 5.50 2 -4 5 -0.50 1.20 2 -4 5 -0.20 1.30 -2 -4 -5 2.70 3.20 2 -4 6 -0.90 1.80 -2 -4 -6 -0.90 3.10 2 -4 7 1.60 1.80 -2 -4 -7 0.60 3.30 2 -4 8 1.30 2.20 -2 -4 -8 3.10 4.60 -2 -4 -9 -4.00 3.00 2 -4 9 -2.30 1.90 -2 -4 -10 25.40 8.00 2 -4 10 33.50 6.40 2 -4 11 -0.20 2.80 -2 -4 -11 -2.80 4.00 -2 -4 -12 0.90 5.20 2 -4 12 6.50 4.00 2 -5 -9 1.80 5.00 -2 -5 9 -0.70 2.20 -2 -5 8 5.10 2.50 2 -5 -8 8.10 5.40 -2 -5 7 -1.90 1.50 2 -5 -7 0.70 3.90 2 -5 -6 4.90 4.10 -2 -5 6 17.80 2.70 2 -5 -5 4.60 3.40 2 -5 -4 121.49 12.20 2 -5 -3 0.20 2.40 2 -5 -2 170.98 10.60 2 -5 -1 -0.60 1.90 -2 -5 1 0.40 1.20 -2 -5 1 -0.30 1.00 2 -5 0 3.20 2.20 -2 -5 0 10.00 2.60 -2 -5 -1 2.60 2.00 2 -5 1 1.00 1.60 2 -5 2 115.59 5.90 -2 -5 -2 106.19 9.60 2 -5 3 0.30 1.20 -2 -5 -3 0.80 2.50 -2 -5 -4 30.50 6.40 2 -5 4 26.50 3.20 -2 -5 -5 1.80 3.30 2 -5 5 -0.20 1.40 2 -5 6 15.00 3.00 -2 -5 -6 18.00 6.10 -2 -5 -7 3.50 4.20 2 -5 7 -1.20 1.70 -2 -5 -8 8.80 5.20 2 -5 8 4.60 2.50 -2 -5 -9 -2.80 4.00 2 -5 9 2.00 2.20 2 -6 -3 0.20 2.90 2 -6 -2 93.89 9.70 2 -6 -1 -2.40 1.90 -2 -6 0 37.10 4.50 2 -6 0 30.60 4.60 -2 -6 -1 0.30 2.10 2 -6 1 0.20 1.60 -2 -6 -2 22.10 4.80 2 -6 2 22.50 3.00 -2 -6 -3 3.50 3.00 -3 0 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0 69.29 7.30 -4 -6 -1 2.30 2.30 4 -6 1 -1.60 1.60 4 -6 2 4.00 2.10 -4 -6 -2 6.70 3.40 -4 -6 -3 -1.60 2.40 4 -6 3 0.30 1.60 -5 0 13 0.30 3.40 -5 0 12 0.90 3.70 -5 0 11 2.10 3.40 -5 0 10 380.06 19.20 -5 0 9 -1.50 2.20 -5 0 8 -2.70 2.10 5 0 -8 -0.70 2.20 5 0 -7 -0.80 2.10 -5 0 7 -1.30 1.80 -5 0 6 55.59 6.70 5 0 -6 40.70 5.70 5 0 -5 0.80 1.90 -5 0 5 -1.50 1.50 -5 0 4 1.40 1.70 5 0 -4 -2.20 1.40 5 0 -3 -1.90 1.30 -5 0 3 0.60 1.40 -5 0 2 3197.38 73.59 5 0 -2 3126.29 73.89 -5 0 2 3147.49 73.39 5 0 -2 3154.58 71.29 5 0 -1 -0.50 0.50 -5 0 1 -0.10 0.90 5 0 -1 -1.30 0.90 5 0 0 4.00 1.10 5 0 0 3.30 0.70 -5 0 0 3.80 1.20 -5 0 -1 -0.50 1.10 5 0 1 -0.10 1.00 5 0 2 1292.97 32.40 -5 0 -2 1305.07 32.90 5 0 3 0.00 1.30 -5 0 -3 1.60 1.70 5 0 4 -0.30 1.40 -5 0 -4 -1.00 1.60 5 0 5 2.20 1.80 -5 0 -5 1.60 2.10 -5 0 -6 2.50 2.40 5 0 6 1.50 1.90 5 0 7 -1.30 1.50 -5 0 -7 -0.90 2.00 -5 0 -8 -1.30 1.90 5 0 8 1.40 2.50 -5 0 -9 -3.20 2.30 5 0 9 -1.50 2.40 5 0 10 196.78 13.40 5 0 11 1.80 3.20 5 0 12 -1.50 2.90 5 0 13 1.40 3.40 -5 -1 15 0.70 4.50 -5 -1 14 16.60 6.90 -5 -1 13 -0.60 3.70 -5 -1 12 -1.00 3.60 -5 -1 11 -1.00 2.90 -5 1 10 275.47 16.00 -5 -1 10 248.28 14.70 5 -1 -10 237.68 16.40 -5 1 9 -0.10 2.30 -5 -1 9 0.40 0.60 5 -1 -9 -1.90 2.70 -5 -1 9 2.20 2.50 -5 1 8 20.00 4.60 -5 -1 8 17.70 1.40 5 -1 -8 19.10 5.40 -5 -1 8 8.90 3.60 -5 1 7 1.40 2.20 -5 -1 7 -0.10 0.30 5 -1 -7 3.40 2.90 -5 -1 7 0.10 1.70 -5 1 6 2.20 2.10 5 -1 -6 -0.90 2.20 -5 -1 6 2.20 1.80 -5 -1 6 1.50 2.00 5 1 -5 -2.40 0.60 -5 1 5 -1.90 1.20 -5 -1 5 1.50 1.60 5 -1 -5 -0.80 1.90 -5 -1 5 0.30 1.00 -5 1 4 267.37 11.10 5 -1 -4 267.77 12.10 -5 -1 4 253.97 10.50 -5 -1 4 269.67 10.20 -5 1 3 1.80 1.50 -5 1 3 0.40 1.40 -5 -1 3 0.30 1.10 -5 -1 3 -1.10 1.00 5 -1 -3 0.10 1.60 -5 1 2 188.08 7.60 -5 -1 2 184.48 6.60 -5 -1 2 181.08 6.50 5 -1 -2 182.58 8.30 -5 1 1 -0.10 1.20 5 -1 -1 0.50 1.40 -5 -1 1 0.20 0.80 5 -1 -1 1.20 1.20 -5 -1 1 -0.20 0.80 5 -1 0 19.40 2.70 -5 -1 0 22.10 2.20 -5 -1 0 19.60 2.00 -5 -1 -1 0.90 1.20 5 -1 1 -0.40 1.00 -5 -1 -1 1.40 1.10 5 -1 1 -0.30 1.10 5 1 2 4839.42 107.79 -5 -1 -2 4273.27 107.99 5 -1 2 4404.46 108.09 5 -1 2 4903.51 107.79 -5 -1 -2 5135.09 109.19 5 1 3 -1.20 1.10 5 -1 3 0.00 1.10 5 -1 3 -0.20 0.50 -5 -1 -3 0.70 1.70 -5 1 -4 44.90 5.60 5 1 4 57.59 5.50 5 -1 4 43.50 1.80 -5 -1 -4 52.79 6.30 5 -1 4 51.49 5.00 5 -1 4 52.29 5.30 -5 1 -5 -0.60 1.60 5 1 5 1.60 1.80 5 -1 5 -0.30 0.50 5 -1 5 -0.20 1.60 5 -1 5 -0.50 1.40 -5 -1 -5 0.80 2.20 5 1 6 751.32 25.00 -5 1 -6 732.43 24.60 5 -1 6 797.22 24.60 5 -1 6 773.22 18.60 -5 -1 -6 799.52 27.00 -5 1 -7 2.80 2.40 5 1 7 -0.80 1.70 -5 -1 -7 -2.30 2.10 5 -1 7 0.20 1.80 5 1 8 82.69 9.10 5 -1 8 85.89 9.00 -5 -1 -8 114.69 11.70 5 1 9 4.00 2.70 5 -1 9 0.50 2.10 -5 -1 -9 1.60 3.40 5 1 10 375.16 22.40 5 -1 10 332.07 17.60 -5 -1 -10 340.07 19.80 5 -1 11 0.30 2.80 5 -1 12 -1.90 3.00 5 -1 13 -0.70 3.10 5 -1 14 46.90 2.80 5 -1 14 44.90 9.60 5 -1 15 -1.00 4.00 -5 -2 15 -1.40 4.40 -5 -2 14 28.40 8.00 -5 -2 13 -0.30 3.30 -5 -2 12 6.60 4.30 5 -2 -11 4.50 4.70 -5 -2 11 1.30 2.90 5 -2 -10 -2.20 3.10 -5 -2 10 -1.60 2.30 -5 -2 9 -0.50 2.40 5 -2 -9 -3.10 3.00 -5 -2 8 35.30 5.60 5 -2 -8 36.20 7.50 5 -2 -7 -4.20 1.80 -5 -2 7 -2.10 1.40 -5 -2 7 1.40 1.80 -5 2 6 274.07 13.00 -5 -2 6 276.17 11.50 -5 -2 6 236.18 11.60 5 -2 -6 256.07 14.50 -5 2 5 -1.00 1.50 -5 2 5 -0.90 1.50 -5 -2 5 0.40 1.30 -5 -2 5 1.30 1.40 5 -2 -5 1.60 2.30 -5 2 4 315.77 12.90 -5 -2 4 346.87 11.30 -5 -2 4 347.87 11.80 5 -2 -4 362.06 15.30 -5 -2 3 0.50 0.90 5 -2 -3 1.10 1.70 5 -2 -3 0.60 0.90 -5 -2 3 0.40 0.90 -5 -2 2 161.78 5.10 -5 -2 2 155.58 5.10 5 -2 -2 166.28 8.40 5 -2 -2 160.88 7.80 -5 -2 1 0.40 0.60 5 -2 -1 -0.60 1.40 5 -2 -1 0.00 1.00 -5 -2 1 0.20 0.50 5 -2 0 282.77 10.40 -5 -2 0 287.07 8.70 5 -2 0 275.47 9.80 -5 -2 0 286.67 8.40 5 -2 1 -1.20 0.90 5 -2 1 0.30 1.10 -5 -2 -1 0.10 1.00 -5 -2 -1 0.20 0.90 5 -2 2 345.17 11.40 -5 -2 -2 335.07 12.40 -5 -2 -2 356.06 11.80 5 -2 2 344.77 11.30 -5 -2 -3 0.70 1.70 5 -2 3 0.10 1.20 5 -2 3 -0.80 1.10 -5 -2 -3 -2.30 0.90 5 -2 4 75.99 5.10 -5 -2 -4 73.19 7.50 5 -2 4 68.99 6.20 5 2 5 -2.30 1.20 5 -2 5 0.00 1.50 5 -2 5 0.00 1.40 -5 -2 -5 1.80 2.40 5 2 6 1.40 2.20 -5 -2 -6 -1.40 2.10 5 -2 6 0.90 1.70 5 -2 6 -0.40 1.50 5 -2 7 -1.30 1.70 -5 -2 -7 -1.60 2.40 5 -2 8 6.90 3.20 -5 -2 -8 5.80 4.10 5 -2 9 -0.50 2.10 -5 -2 -9 -3.30 2.90 5 -2 10 53.49 7.90 -5 -2 -10 51.59 9.70 -5 -2 -11 -0.30 4.10 5 -2 11 -0.90 2.80 5 -2 12 -1.20 2.70 5 -2 13 2.90 4.30 5 -2 14 20.30 6.80 -5 -3 13 -3.40 3.20 5 -3 -12 12.80 6.50 -5 -3 12 4.70 3.90 -5 -3 11 -3.50 2.40 5 -3 -11 2.20 4.80 -5 -3 10 50.69 7.50 5 -3 -10 34.10 8.80 5 -3 -9 -3.60 2.60 -5 -3 9 2.80 2.40 -5 -3 8 162.28 9.90 5 -3 -8 161.68 15.70 -5 -3 7 -1.20 1.60 5 -3 -7 3.20 3.40 -5 -3 6 9.00 2.50 -5 -3 6 7.90 2.40 5 -3 -6 4.50 3.30 5 -3 -5 -0.70 2.20 -5 -3 5 -0.30 1.10 -5 -3 5 -0.70 1.00 -5 -3 4 0.40 1.00 5 -3 -4 -2.50 1.60 -5 -3 4 -0.30 1.00 5 -3 -3 1.00 1.50 -5 -3 3 -0.60 0.70 5 -3 -3 -1.10 1.60 -5 -3 3 0.50 0.80 5 -3 -2 235.28 11.20 5 -3 -2 218.78 10.20 5 -3 -1 0.30 1.10 5 -3 -1 -0.60 1.30 5 -3 -1 -0.50 1.20 -5 -3 1 0.90 0.70 -5 -3 1 0.40 0.70 5 -3 0 264.37 10.70 5 -3 0 240.78 9.80 -5 -3 0 250.47 8.20 -5 -3 0 270.37 8.90 5 -3 1 -0.80 1.20 -5 -3 -1 2.00 1.40 -5 -3 -1 -0.40 0.90 5 -3 1 -0.50 0.90 5 -3 2 207.68 8.60 -5 -3 -2 207.68 8.80 -5 -3 -2 218.68 10.10 5 -3 2 214.38 8.60 -5 -3 -3 -0.40 1.50 5 -3 3 2.10 1.40 5 -3 3 -0.30 1.10 -5 -3 -3 -0.10 2.00 -5 -3 -4 -0.90 1.80 5 -3 4 0.00 1.40 -5 -3 -4 -1.70 1.80 5 -3 4 0.20 1.40 5 -3 5 -1.20 1.30 -5 -3 -5 -0.70 2.20 5 -3 5 1.20 1.70 -5 -3 -6 0.80 2.80 5 -3 6 0.50 1.70 5 -3 7 -2.40 1.40 -5 -3 -7 -4.90 2.20 5 -3 8 56.09 7.20 -5 -3 -8 77.09 11.00 -5 -3 -9 -0.90 3.30 5 -3 9 2.90 2.60 5 -3 10 72.79 9.20 -5 -3 -10 70.99 11.90 -5 -3 -11 -2.50 4.10 5 -3 11 0.40 3.10 -5 -3 -12 18.90 7.30 5 -3 12 20.10 6.00 5 -3 13 0.60 3.80 5 -4 -12 5.20 6.00 -5 -4 12 4.50 3.90 -5 -4 11 1.20 2.80 5 -4 -11 4.10 5.50 5 -4 -10 10.00 6.20 -5 -4 10 2.50 3.10 -5 -4 9 0.80 2.20 5 -4 -9 4.70 4.50 5 -4 -8 47.20 9.30 -5 -4 8 46.90 6.20 -5 -4 7 0.50 1.70 5 -4 -7 4.20 4.20 -5 -4 6 17.70 3.10 5 -4 -6 11.70 4.90 -5 -4 5 1.60 1.20 -5 -4 5 -0.40 0.90 5 -4 -5 3.50 3.30 -5 -4 4 271.27 8.00 -5 -4 4 245.08 8.10 5 -4 -4 256.67 14.50 5 -4 -3 -2.70 1.80 5 -4 -2 1.10 2.10 5 -4 -1 -0.70 1.70 -5 -4 1 0.20 1.00 -5 -4 1 1.40 0.80 -5 -4 0 19.90 2.70 5 -4 0 17.00 3.20 5 -4 0 20.10 3.50 5 -4 0 13.60 3.30 -5 -4 0 23.30 3.30 -5 -4 -1 -1.40 1.10 5 -4 1 -1.60 1.30 5 -4 1 0.80 1.20 -5 -4 -1 -0.50 1.50 -5 -4 -2 126.79 8.40 5 -4 2 122.09 6.80 5 -4 2 126.19 6.70 5 -4 3 -2.00 1.00 5 -4 3 -1.20 1.20 -5 -4 -3 0.30 2.20 5 -4 4 3.40 2.10 -5 -4 -4 4.10 3.10 5 -4 5 2.10 1.90 -5 -4 -5 -0.20 2.80 -5 -4 -6 4.10 3.40 5 -4 6 1.60 2.00 5 -4 7 -0.30 1.80 -5 -4 -7 4.00 3.30 -5 -4 -8 7.40 5.20 5 -4 8 9.10 3.40 5 -4 9 -1.10 1.90 -5 -4 -9 1.70 4.50 5 -4 10 8.00 3.70 -5 -4 -10 7.90 5.50 -5 -4 -11 2.20 5.00 5 -4 11 4.10 3.50 -5 -5 9 2.90 2.40 5 -5 -9 -4.50 3.50 5 -5 -8 24.60 7.80 -5 -5 8 24.40 4.10 5 -5 -7 4.90 4.00 -5 -5 7 -0.30 1.50 -5 -5 6 38.50 3.40 5 -5 -6 45.50 8.40 5 -5 -5 -1.40 2.60 5 -5 -4 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3.40 4.50 -11 -3 9 -4.30 1.60 11 -3 -9 -0.40 3.80 -11 -3 8 169.78 10.60 11 -3 -8 175.98 16.70 -11 -3 7 -1.90 1.70 11 -3 -7 2.30 3.20 11 -3 -6 53.69 8.60 -11 -3 6 64.79 6.70 -11 -3 5 -0.40 1.50 -11 -3 5 -0.80 1.30 -11 -3 5 -0.70 1.30 11 -3 -5 -1.90 2.20 -11 -3 4 3.50 1.80 11 -3 -4 -1.50 2.40 -11 -3 4 5.30 2.00 11 -3 -3 1.10 2.30 -11 -3 3 -1.50 1.10 -11 -3 3 0.70 1.30 -11 -3 2 98.59 5.50 11 -3 -2 103.39 9.60 -11 -3 2 99.89 5.70 -11 -3 1 0.60 1.20 -11 -3 1 -0.50 1.00 11 -3 -1 -1.00 1.70 -11 -3 0 11.10 2.80 11 -3 0 7.90 2.80 -11 -3 0 7.70 2.10 11 -3 0 9.20 3.10 -11 -3 -1 -1.60 1.20 11 -3 1 -1.10 1.10 -11 -3 -1 0.30 1.70 11 -3 1 0.70 1.80 11 -3 2 9.20 3.00 -11 -3 -2 8.80 2.60 -11 -3 -2 8.80 2.90 11 -3 2 7.50 2.90 -11 -3 -3 -0.60 1.80 11 -3 3 1.00 1.80 -11 -3 -4 91.99 9.90 11 -3 4 98.19 7.40 11 -3 5 -2.20 1.60 -11 -3 -5 1.50 2.60 11 -3 6 27.20 5.30 -11 -3 -6 30.10 6.40 11 -3 7 -2.60 2.00 -11 -3 -7 -0.10 3.00 11 -3 8 -2.80 2.10 -11 -3 -8 2.10 3.90 -11 -3 -9 1.70 3.80 11 -3 9 0.50 2.60 -11 -3 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8 163.28 11.50 -12 0 7 3.20 2.80 12 0 -7 1.10 2.40 -12 0 6 -1.80 1.60 12 0 -6 -0.50 2.10 -12 0 6 0.30 1.90 -12 0 5 -1.50 1.50 12 0 -5 1.40 2.00 12 0 -5 -0.50 1.00 -12 0 5 0.00 2.00 12 0 -4 1213.28 34.70 -12 0 4 1188.88 34.40 12 0 -4 1193.48 30.30 12 0 -3 0.70 1.10 12 0 -3 -3.60 1.10 -12 0 3 -1.60 1.70 12 0 -2 0.30 1.70 -12 0 2 -1.20 1.50 12 0 -2 -0.80 0.90 12 0 -1 -0.80 0.70 12 0 -1 2.30 1.80 -12 0 1 -2.20 1.20 12 0 0 93.19 6.10 12 0 0 98.69 4.20 -12 0 0 97.79 6.30 12 0 1 -0.60 1.30 12 0 1 0.70 0.80 -12 0 -1 2.30 1.70 -12 0 -2 1.40 1.80 12 0 2 1.30 1.70 -12 0 -3 -0.80 1.60 12 0 3 0.60 1.70 -12 0 -4 1337.17 38.40 12 0 4 1331.27 37.20 12 0 5 0.20 1.80 -12 0 -5 3.20 2.30 12 0 6 -1.40 1.70 -12 0 -6 3.20 3.10 -12 0 -7 -1.60 2.20 12 0 7 0.90 2.10 -12 0 -8 118.59 12.30 12 0 8 101.39 10.40 12 0 9 -2.90 2.10 12 0 10 -2.50 2.20 12 0 11 4.80 3.60 -12 -1 15 -2.60 5.10 -12 -1 14 15.40 6.50 -12 -1 13 -0.70 3.40 -12 -1 12 5.70 4.10 -12 -1 11 0.40 3.20 -12 1 10 2.60 4.10 -12 -1 10 1.20 3.00 -12 1 9 -0.80 3.00 -12 1 9 -0.10 2.70 12 -1 -9 0.60 3.10 -12 -1 9 -1.80 2.30 -12 1 8 66.79 8.80 -12 1 8 56.19 8.30 -12 -1 8 72.29 8.90 12 -1 -8 80.19 10.50 -12 1 7 0.40 2.50 -12 1 7 -1.70 1.80 12 1 -7 -1.10 1.20 -12 -1 7 -4.30 1.70 12 -1 -7 -1.70 2.00 12 1 -6 467.75 14.10 -12 1 6 476.05 19.20 -12 1 6 452.45 18.80 12 -1 -6 461.45 20.20 -12 -1 6 445.16 18.10 12 1 -5 -0.30 0.90 -12 1 5 0.30 2.00 -12 -1 5 1.60 1.90 12 -1 -5 0.60 2.30 -12 -1 5 -0.70 1.60 -12 -1 5 -0.10 1.60 -12 1 4 86.29 8.10 12 1 -4 98.69 4.30 -12 -1 4 99.49 7.10 -12 -1 4 97.59 6.80 12 -1 -4 76.99 8.30 12 1 -3 -0.80 0.60 -12 1 3 -0.30 1.50 -12 -1 3 -2.00 1.10 12 -1 -3 -0.60 1.90 -12 -1 3 -0.30 1.00 -12 1 2 1464.65 39.50 -12 -1 2 1435.16 38.50 12 -1 -2 1461.75 40.50 -12 1 1 0.70 1.70 12 -1 -1 -1.70 1.60 -12 -1 1 -0.10 1.00 12 -1 -1 0.90 1.00 -12 -1 1 0.10 1.50 12 1 0 722.93 20.70 -12 1 0 706.73 21.90 12 -1 0 710.93 22.40 -12 -1 0 711.33 21.20 12 -1 0 713.93 18.50 -12 -1 0 705.43 21.60 12 1 1 -0.30 1.30 -12 1 -1 -0.70 1.50 12 -1 1 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2.70 20 -5 -2 1.10 3.90 20 -5 -1 2.70 3.50 -20 -5 1 -2.20 2.30 20 -5 0 -1.00 3.10 -20 -5 0 3.50 3.10 20 -5 1 0.30 3.20 -20 -5 -1 0.70 2.90 -20 -5 -2 0.10 3.10 20 -5 2 0.20 3.30 -20 -5 -3 -0.80 3.00 20 -5 3 1.00 3.10 -20 -5 -4 -1.90 3.50 20 -5 4 0.20 2.80 -21 0 11 -1.40 3.40 -21 0 10 134.99 15.00 -21 0 9 0.60 3.30 -21 0 8 -2.40 2.80 -21 0 7 1.00 3.00 21 0 -6 124.69 9.00 -21 0 6 102.99 11.30 21 0 -5 -1.80 1.30 -21 0 5 2.90 3.00 21 0 -4 -2.10 2.30 21 0 -4 2.30 1.70 -21 0 4 1.20 2.70 21 0 -3 0.70 2.20 -21 0 3 -2.70 2.10 21 0 -3 1.30 1.70 21 0 -2 265.77 13.80 -21 0 2 261.67 14.20 21 0 -2 263.27 10.10 21 0 -1 0.60 1.20 -21 0 1 2.20 2.40 21 0 -1 -1.90 1.60 21 0 0 3.80 1.50 21 0 0 1.90 2.70 -21 0 0 3.90 2.80 21 0 1 0.60 1.30 21 0 1 1.20 2.30 -21 0 -1 1.80 2.30 -21 0 -2 322.37 16.30 21 0 2 322.17 15.40 21 0 2 325.27 11.30 21 0 3 2.20 2.40 -21 0 -3 -0.80 2.60 21 0 3 0.80 1.20 -21 0 -4 -0.10 2.30 21 0 4 1.10 2.30 21 0 4 1.70 1.50 21 0 5 -0.60 1.20 -21 0 -5 0.10 2.60 21 0 5 3.20 2.90 -21 0 -6 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6.00 3.10 -21 -1 -3 1.10 2.80 21 -1 4 104.39 5.70 21 -1 4 80.29 9.20 -21 -1 -4 110.49 11.60 21 -1 5 1.00 1.30 21 -1 5 -3.40 1.70 -21 -1 -5 -3.30 2.20 21 -1 6 81.59 10.00 -21 -1 -6 83.19 10.90 21 -1 6 75.29 5.80 21 -1 7 0.10 2.70 21 -1 7 0.10 1.20 -21 -1 -7 -3.10 2.60 -21 -1 -8 83.79 12.10 21 -1 8 56.79 5.00 21 -1 8 58.29 9.10 21 -1 9 -1.10 1.30 21 -1 9 -4.00 2.60 21 -1 10 34.50 4.00 21 -1 10 18.90 6.20 21 -1 11 -1.90 1.20 21 -1 11 -3.80 3.60 21 -1 12 0.90 1.70 21 -1 13 1.90 1.70 -21 -2 12 1.80 3.90 -21 -2 11 -0.30 3.60 -21 -2 10 6.60 4.60 -21 -2 9 1.30 3.30 -21 -2 8 110.49 12.00 -21 -2 7 4.40 3.00 21 -2 -7 0.70 3.50 21 -2 -6 3.70 3.90 -21 -2 6 3.80 3.10 21 -2 -5 -1.20 3.30 -21 -2 5 -2.20 2.20 -21 -2 4 22.10 5.20 21 -2 -4 42.30 7.90 -21 -2 3 1.20 2.60 21 -2 -3 -3.20 2.30 -21 -2 2 -2.00 2.10 21 -2 -2 -2.20 2.30 -21 -2 1 -0.30 2.20 21 -2 -1 -1.10 2.30 21 -2 0 157.58 11.60 -21 -2 0 202.28 12.10 21 -2 1 -0.30 2.60 -21 -2 -1 -0.30 2.20 -21 -2 -2 157.48 11.50 21 -2 2 129.39 12.60 -21 -2 -3 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2.30 -21 -3 -4 -0.10 3.10 -21 -3 -5 -3.70 2.80 21 -3 5 -0.80 3.10 -21 -3 -6 86.89 12.40 21 -3 6 70.19 10.00 -21 -3 -7 -2.70 3.50 21 -3 7 -3.90 2.90 -21 -3 -8 201.88 20.60 21 -3 8 183.38 17.00 21 -3 9 -0.20 3.70 -21 -3 -9 1.40 5.10 21 -3 10 -1.10 3.80 -21 -3 -10 2.50 5.50 21 -3 11 0.20 3.80 -21 -3 -11 -3.60 4.40 21 -4 -8 10.40 6.40 -21 -4 8 14.40 4.90 -21 -4 7 -1.80 2.20 21 -4 -7 3.40 5.00 21 -4 -6 8.40 5.80 -21 -4 6 16.50 4.50 21 -4 -5 -3.90 3.00 -21 -4 5 0.70 2.40 21 -4 -4 61.69 10.20 -21 -4 4 58.19 7.70 -21 -4 3 -1.70 2.30 21 -4 -3 -0.90 3.60 21 -4 -2 20.00 6.50 -21 -4 2 20.60 5.00 -21 -4 1 -2.20 2.10 21 -4 -1 -2.40 2.90 -21 -4 0 26.50 5.70 21 -4 0 12.90 5.00 21 -4 1 -0.90 2.90 -21 -4 -1 2.20 2.90 21 -4 2 12.40 5.00 -21 -4 -2 6.80 3.90 -21 -4 -3 -0.90 2.80 21 -4 3 -3.30 2.50 21 -4 4 2.40 3.40 -21 -4 -4 5.60 3.70 21 -4 5 0.40 3.20 -21 -4 -5 -1.10 3.30 -21 -4 -6 10.20 5.80 21 -4 6 10.70 4.90 21 -4 7 -3.20 3.10 -21 -4 -7 3.40 4.80 -21 -4 -8 46.10 10.60 21 -4 8 52.09 9.30 -21 -5 4 9.20 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4 11.10 4.10 22 -2 4 17.60 2.50 -22 -2 -5 -0.50 2.80 22 -2 5 0.40 1.20 22 -2 5 3.70 3.10 22 -2 6 46.10 3.70 -22 -2 -6 52.39 9.30 22 -2 6 50.69 8.60 22 -2 7 2.10 3.50 -22 -2 -7 2.60 4.00 22 -2 7 -1.90 1.00 -22 -2 -8 74.59 12.00 22 -2 8 67.99 3.30 22 -2 8 76.49 10.90 22 -2 9 0.00 3.60 -22 -2 -9 0.30 3.90 -22 -2 -10 -3.20 5.40 22 -2 10 0.00 3.70 22 -2 11 1.60 4.10 22 -2 12 0.70 5.10 -22 -3 10 1.70 3.90 -22 -3 9 -1.20 2.80 -22 -3 8 2.00 3.30 22 -3 -8 2.70 4.40 -22 -3 7 -1.90 2.30 22 -3 -7 -3.80 3.30 -22 -3 6 0.70 2.70 22 -3 -6 -1.70 3.10 22 -3 -5 4.20 4.40 -22 -3 5 -1.60 2.10 -22 -3 4 223.58 13.70 22 -3 -4 245.28 16.60 22 -3 -3 3.80 3.50 -22 -3 3 0.20 2.50 -22 -3 2 22.10 5.20 22 -3 -2 21.90 6.40 22 -3 -1 -1.80 2.70 -22 -3 1 2.20 2.70 -22 -3 0 5.90 3.40 22 -3 0 14.60 4.90 -22 -3 -1 3.10 3.10 22 -3 1 -1.30 2.50 22 -3 2 4.80 3.30 -22 -3 -2 8.50 4.20 22 -3 3 0.90 3.00 -22 -3 -3 -0.10 2.60 -22 -3 -4 55.49 9.10 22 -3 4 41.60 7.90 -22 -3 -5 1.50 3.60 22 -3 5 -2.90 2.50 -22 -3 -6 16.70 6.20 22 -3 6 29.90 7.30 -22 -3 -7 1.60 4.10 22 -3 7 0.40 3.50 22 -3 8 6.10 4.40 -22 -3 -8 12.10 6.90 22 -3 9 2.60 3.90 -22 -3 -9 -7.10 3.50 -22 -3 -10 10.80 6.80 22 -3 10 8.00 5.10 -22 -4 8 32.30 6.60 22 -4 -8 23.60 8.00 -22 -4 7 -0.60 2.60 22 -4 -7 1.50 4.50 22 -4 -6 1.80 4.50 -22 -4 6 -0.90 2.40 -22 -4 5 3.40 2.90 22 -4 -5 1.10 4.00 -22 -4 4 26.70 5.50 22 -4 -4 37.10 8.70 22 -4 -3 -2.30 3.30 -22 -4 3 3.50 2.90 22 -4 -2 1.50 3.90 -22 -4 2 0.60 2.60 22 -4 -1 0.10 3.40 -22 -4 1 1.90 2.90 -22 -4 0 26.40 6.20 22 -4 0 25.50 6.60 22 -4 1 -2.00 2.60 -22 -4 -1 -1.10 2.60 -22 -4 -2 0.30 3.20 22 -4 2 -1.00 2.70 -22 -4 -3 -1.20 2.80 22 -4 3 2.70 3.70 22 -4 4 4.10 3.90 -22 -4 -4 4.00 3.80 22 -4 5 -0.50 3.60 -22 -4 -5 -3.00 3.30 -22 -4 -6 104.09 13.80 22 -4 6 96.69 12.50 -22 -4 -7 2.40 4.50 22 -4 7 1.20 3.80 22 -4 8 218.78 16.50 -22 -4 -8 204.68 21.40 22 -5 -3 -4.10 3.10 -22 -5 3 3.60 3.10 22 -5 -2 16.00 6.20 -22 -5 2 12.00 4.30 22 -5 -1 3.40 4.30 -22 -5 1 -1.70 2.60 -22 -5 0 35.40 7.20 22 -5 0 40.30 8.40 22 -5 1 0.10 3.50 -22 -5 -1 -0.60 2.80 -22 -5 -2 10.70 4.90 22 -5 2 25.30 7.00 22 -5 3 2.50 3.80 -22 -5 -3 -1.90 3.40 -23 0 11 1.00 4.20 -23 0 10 20.00 6.90 -23 0 9 -0.90 3.50 -23 0 8 -1.60 2.80 -23 0 7 -2.40 2.80 -23 0 6 223.38 15.10 23 0 -6 240.48 11.10 23 0 -5 -0.50 1.60 -23 0 5 1.80 3.10 -23 0 4 0.20 2.90 23 0 -4 -0.90 1.50 -23 0 3 1.10 2.70 23 0 -3 -1.20 1.40 -23 0 2 3.10 2.90 23 0 -2 0.20 1.50 23 0 -2 3.70 3.10 23 0 -1 -0.30 2.20 23 0 -1 2.20 1.80 -23 0 1 2.70 2.70 23 0 0 4.40 3.20 -23 0 0 2.80 3.10 23 0 0 3.90 1.80 23 0 1 0.00 1.30 23 0 1 0.50 2.30 -23 0 -1 0.90 2.50 23 0 2 336.37 16.60 -23 0 -2 355.56 17.70 23 0 2 335.07 12.00 23 0 3 -1.50 1.80 -23 0 -3 0.00 2.60 23 0 3 -0.40 1.30 23 0 4 -1.10 1.20 23 0 4 -1.00 2.00 -23 0 -4 -0.30 3.00 23 0 5 0.10 1.50 -23 0 -5 -0.30 3.10 23 0 5 -1.90 2.20 23 0 6 232.28 9.70 23 0 13 3.00 2.20 -23 -1 12 2.60 4.50 -23 -1 11 -2.80 3.40 -23 -1 10 3.70 4.30 -23 -1 9 -0.20 3.20 -23 -1 8 6.90 4.10 -23 -1 7 -2.70 2.80 -23 -1 6 104.39 11.90 -23 1 5 -3.80 2.20 -23 -1 5 -3.30 2.00 23 -1 -5 -2.40 2.50 -23 1 4 11.70 4.40 23 1 -4 15.40 3.10 -23 -1 4 7.60 4.00 23 -1 -4 11.60 4.50 -23 1 3 1.60 2.80 23 1 -3 0.10 1.40 -23 -1 3 0.50 2.70 23 -1 -3 -1.80 1.40 23 -1 -3 0.40 2.70 23 1 -2 63.89 5.50 -23 1 2 54.49 8.30 -23 -1 2 57.89 8.20 23 -1 -2 73.49 9.50 23 -1 -2 53.89 5.40 23 1 -1 0.90 1.30 -23 1 1 -1.20 2.00 23 -1 -1 -1.00 1.30 -23 -1 1 2.20 2.90 23 -1 -1 -0.60 2.40 23 1 0 30.60 3.70 -23 1 0 33.00 6.60 23 -1 0 28.40 3.80 -23 -1 0 27.60 6.10 23 -1 0 18.90 5.10 -23 1 -1 -0.70 2.50 23 -1 1 -1.40 2.30 23 -1 1 -0.40 1.30 -23 -1 -1 -0.90 2.20 23 -1 2 34.00 4.10 23 -1 2 35.30 6.40 -23 -1 -2 29.60 6.10 23 -1 3 -1.50 1.30 -23 -1 -3 1.30 2.90 23 -1 3 -1.00 2.20 -23 -1 -4 173.98 13.30 23 -1 4 191.68 12.90 23 -1 4 170.88 7.90 23 -1 5 1.30 1.50 23 -1 5 -2.80 2.00 -23 -1 -5 0.30 3.10 -23 -1 -6 1.90 3.80 23 -1 6 1.40 2.90 23 -1 6 -0.90 1.30 -23 -1 -7 -0.80 3.60 23 -1 7 -0.90 1.20 23 -1 7 1.10 2.90 -23 -1 -8 119.59 14.40 23 -1 8 99.49 5.90 23 -1 8 96.99 12.00 23 -1 9 -0.90 3.20 23 -1 9 -0.30 1.40 23 -1 10 5.90 4.60 23 -1 10 5.60 2.10 23 -1 11 -1.10 1.40 23 -1 12 3.90 2.00 -23 -2 12 0.80 3.70 -23 -2 11 -2.10 3.60 -23 -2 10 15.10 6.00 -23 -2 9 1.50 3.50 -23 -2 8 50.89 8.80 23 -2 -7 -2.90 3.30 -23 -2 7 3.50 3.10 -23 -2 6 34.60 6.80 23 -2 -6 43.80 8.70 -23 -2 5 0.10 2.40 23 -2 -5 0.20 2.90 -23 -2 4 4.00 3.10 23 -2 -4 5.40 4.30 -23 -2 3 0.80 2.70 23 -2 -3 -0.50 2.60 -23 -2 2 64.59 8.50 23 -2 -2 84.99 10.80 -23 -2 1 -2.40 2.20 23 -2 -1 2.10 3.30 23 -2 0 183.88 12.90 -23 -2 0 161.58 11.60 -23 -2 -1 -0.10 2.60 23 -2 1 3.20 3.40 -23 -2 -2 287.57 16.60 23 -2 2 270.37 16.20 23 -2 3 -0.90 1.20 23 -2 3 -1.20 2.70 -23 -2 -3 -0.50 2.70 23 -2 4 287.37 10.00 -23 -2 -4 295.07 17.90 23 -2 4 301.77 17.10 23 -2 5 -0.80 1.20 23 -2 5 1.40 2.90 -23 -2 -5 -1.20 3.10 -23 -2 -6 268.27 17.80 23 -2 6 259.77 9.00 23 -2 6 294.17 17.30 23 -2 7 -0.20 1.20 -23 -2 -7 -0.60 3.70 23 -2 7 -0.30 3.20 23 -2 8 28.40 6.90 -23 -2 -8 21.60 7.40 23 -2 8 30.10 2.80 -23 -2 -9 1.10 4.40 23 -2 9 -4.00 3.00 23 -2 10 27.80 7.60 23 -2 11 -3.10 3.60 -23 -3 10 15.70 5.90 -23 -3 9 1.30 3.60 23 -3 -8 1.20 4.70 -23 -3 8 3.20 3.60 23 -3 -7 3.10 4.20 -23 -3 7 -0.40 2.50 -23 -3 6 143.39 13.40 23 -3 -6 143.69 16.30 -23 -3 5 -2.30 2.00 23 -3 -5 -5.10 2.90 23 -3 -4 16.10 5.90 -23 -3 4 10.80 4.30 23 -3 -3 -0.70 3.40 -23 -3 3 0.70 2.70 23 -3 -2 16.20 5.80 -23 -3 2 17.40 5.10 23 -3 -1 4.20 4.10 -23 -3 1 -0.60 2.30 -23 -3 0 11.20 4.40 23 -3 0 8.50 4.40 23 -3 1 6.10 3.90 -23 -3 -1 -0.50 2.50 -23 -3 -2 1.60 3.00 23 -3 2 2.30 3.60 23 -3 3 1.00 3.00 -23 -3 -3 1.00 3.00 -23 -3 -4 3.90 3.80 23 -3 4 0.40 3.30 23 -3 5 1.20 3.10 -23 -3 -5 -1.10 3.10 23 -3 6 93.39 12.20 -23 -3 -6 55.69 10.30 23 -3 7 2.40 3.80 -23 -3 -7 1.10 4.80 -23 -3 -8 8.50 5.50 23 -3 8 11.10 5.30 23 -3 9 -1.80 3.10 -23 -3 -9 2.20 4.60 -23 -3 -10 7.60 7.00 23 -3 10 -0.70 4.00 -23 -4 8 47.80 7.90 23 -4 -8 58.59 12.30 23 -4 -7 -3.00 4.30 -23 -4 7 2.80 3.10 23 -4 -6 2.50 5.00 -23 -4 6 -0.40 2.50 23 -4 -5 -1.90 4.00 -23 -4 5 1.80 2.80 23 -4 -4 86.39 13.00 -23 -4 4 75.79 9.40 23 -4 -3 0.70 3.70 -23 -4 3 -4.00 2.00 23 -4 -2 5.60 4.80 -23 -4 2 7.00 3.90 -23 -4 1 -0.40 2.70 23 -4 -1 9.10 4.80 23 -4 0 31.10 7.40 -23 -4 0 40.50 7.60 23 -4 1 1.10 3.50 -23 -4 -1 6.40 3.90 23 -4 2 -0.70 2.90 -23 -4 -2 -1.50 2.60 -23 -4 -3 -0.70 3.00 23 -4 3 3.20 3.90 23 -4 4 6.40 4.40 -23 -4 -4 3.80 4.60 -23 -4 -5 3.50 3.90 23 -4 5 -0.50 3.50 -23 -4 -6 33.40 8.70 23 -4 6 31.00 7.40 -23 -4 -7 1.00 5.20 23 -4 7 -1.70 3.60 23 -5 -2 71.19 11.70 -23 -5 2 46.40 7.60 23 -5 -1 0.80 4.00 -23 -5 1 5.20 3.60 23 -5 0 54.99 9.50 -23 -5 0 53.19 8.40 23 -5 1 -0.30 3.70 -23 -5 -1 -2.00 3.00 -24 0 10 -0.90 3.90 -24 0 9 -0.80 3.60 -24 0 8 242.38 16.90 -24 0 7 6.10 3.90 24 0 -6 0.40 2.00 -24 0 6 -1.00 3.00 -24 0 5 -0.10 2.90 24 0 -5 -1.70 1.60 24 0 -4 385.86 14.40 -24 0 4 397.66 19.90 24 0 -3 1.10 1.80 -24 0 3 -2.10 2.60 24 0 -2 0.40 1.40 -24 0 2 1.00 2.50 -24 0 1 -3.10 2.10 24 0 -1 0.20 2.30 24 0 -1 0.50 1.40 24 0 0 7.30 2.20 24 0 0 12.10 4.00 -24 0 0 7.90 3.70 24 0 1 -1.30 2.10 24 0 1 -1.60 1.10 -24 0 -1 -2.70 2.30 24 0 2 1.00 2.50 24 0 2 3.00 1.80 -24 0 -2 -0.30 2.30 24 0 3 2.50 1.80 -24 0 -3 2.80 3.50 24 0 3 5.50 3.30 24 0 4 27.50 5.90 -24 0 -4 30.50 6.70 24 0 4 36.10 4.30 24 0 5 -1.50 1.30 -24 0 -5 3.20 3.90 24 0 6 -1.80 1.30 24 0 7 -0.10 1.50 24 0 8 20.50 3.60 24 0 9 -1.10 1.60 24 0 11 -0.80 1.70 24 0 12 41.00 5.20 -24 -1 12 48.40 10.20 -24 -1 11 2.20 3.70 -24 -1 10 2.90 3.50 -24 -1 9 -3.80 2.50 -24 -1 8 1.80 3.60 -24 -1 7 -0.90 2.80 -24 -1 6 152.38 14.60 -24 -1 5 5.20 3.90 24 1 -4 47.10 5.00 -24 1 4 56.19 8.90 24 -1 -4 65.39 9.80 -24 -1 4 44.20 7.70 -24 1 3 0.70 3.00 24 1 -3 0.10 1.50 24 -1 -3 0.50 3.10 -24 -1 3 -1.60 2.60 24 -1 -3 -0.10 1.80 -24 1 2 7.30 3.80 24 1 -2 8.80 2.20 24 -1 -2 7.00 2.50 24 -1 -2 2.80 3.50 -24 -1 2 7.20 3.60 24 1 -1 -1.00 1.10 -24 1 1 -0.30 2.50 24 -1 -1 0.80 2.40 24 -1 -1 0.20 1.50 -24 -1 1 3.10 2.70 -24 1 0 313.37 16.70 24 1 0 296.47 10.90 24 -1 0 315.87 16.80 -24 -1 0 286.17 16.20 24 -1 0 310.27 11.90 24 1 1 -1.00 1.10 24 -1 1 1.80 1.70 24 -1 1 -0.10 2.90 -24 -1 -1 -1.60 2.40 24 -1 2 118.39 6.70 -24 -1 -2 152.38 14.50 24 -1 2 131.69 12.60 -24 -1 -3 -0.20 2.90 24 -1 3 -0.30 2.60 24 -1 3 -2.10 1.10 24 -1 4 289.17 11.10 -24 -1 -4 297.17 17.60 24 -1 4 299.17 16.80 24 -1 5 6.00 3.60 -24 -1 -5 0.30 3.60 24 -1 5 -1.50 1.30 24 -1 6 62.59 5.50 24 -1 6 83.79 11.10 -24 -1 -6 61.09 10.30 24 -1 7 -0.20 1.50 24 -1 7 1.30 3.40 -24 -1 -7 -2.80 3.10 24 -1 8 1.20 1.60 24 -1 8 -1.80 2.70 24 -1 9 -1.00 1.40 24 -1 9 -1.10 3.00 24 -1 10 52.99 5.20 24 -1 11 3.00 1.90 24 -1 12 16.10 3.10 -24 -2 11 2.40 4.00 -24 -2 10 -1.80 3.10 -24 -2 9 0.00 3.20 -24 -2 8 -0.50 2.90 -24 -2 7 1.00 3.10 -24 -2 6 30.10 6.90 24 -2 -6 47.00 9.30 24 -2 -5 -1.20 3.10 -24 -2 5 1.00 3.10 -24 -2 4 156.48 12.00 24 -2 -4 157.08 15.30 24 -2 -3 -2.50 2.60 -24 -2 3 2.30 2.70 24 -2 -2 122.29 13.00 -24 -2 2 104.29 11.40 24 -2 -1 2.00 2.80 -24 -2 1 -0.50 2.30 -24 -2 0 118.59 11.80 24 -2 0 108.79 11.80 -24 -2 -1 1.40 2.80 24 -2 1 -2.60 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2.10 32 0 6 -0.30 2.10 32 0 7 0.20 2.10 32 0 8 59.59 6.90 32 0 9 -1.80 2.30 -32 -1 9 5.50 5.20 -32 -1 8 4.30 5.10 -32 -1 7 2.30 4.70 -32 -1 6 4.30 4.70 -32 -1 5 0.10 3.90 -32 -1 4 2.20 4.30 32 -1 -3 1.50 2.40 -32 -1 3 0.70 3.90 32 -1 -2 126.19 9.80 -32 -1 2 131.09 15.60 -32 -1 1 -2.60 3.50 32 -1 -1 1.50 2.30 32 1 0 144.99 8.30 32 -1 0 119.99 9.50 -32 -1 0 130.99 15.00 32 1 1 -1.00 2.00 -32 -1 -1 0.80 3.90 32 -1 1 0.30 1.70 32 1 2 60.19 6.60 -32 -1 -2 44.60 9.50 32 -1 2 41.80 5.50 32 1 3 -3.10 2.00 -32 -1 -3 1.50 4.00 32 -1 3 0.00 1.80 32 1 4 0.70 2.30 32 -1 4 1.80 2.20 -32 -1 -4 -2.90 3.80 32 1 5 -1.50 2.10 32 -1 5 -2.50 1.50 32 1 6 8.20 3.10 32 -1 6 1.30 2.20 32 1 7 0.60 2.30 32 -1 7 1.90 2.00 32 1 8 45.40 6.40 32 -1 8 38.10 5.10 32 1 9 -2.60 2.10 32 -1 9 -2.10 1.80 -32 -2 8 11.10 5.90 -32 -2 7 -4.70 2.90 -32 -2 6 10.00 5.50 -32 -2 5 -3.30 3.00 -32 -2 4 53.99 10.40 -32 -2 3 -0.40 3.70 -32 -2 2 10.70 5.00 -32 -2 1 -2.60 3.10 -32 -2 0 101.49 13.70 -32 -2 -1 2.50 4.80 32 -2 1 -2.10 3.50 32 -2 2 1.90 4.40 -32 -2 -2 0.30 3.50 -32 -2 -3 2.00 4.30 32 -2 3 1.40 2.00 32 -2 3 -3.20 2.70 32 -2 4 9.40 2.80 -32 -2 -4 10.10 5.70 32 -2 4 7.80 5.80 32 -2 5 -2.40 1.60 32 -2 5 -4.40 5.30 -32 -2 -5 8.00 5.90 32 -2 6 -1.30 1.70 -32 -2 -6 3.70 4.80 -32 -2 -7 -4.20 4.00 32 -2 7 2.40 2.10 32 -2 8 2.40 1.90 -32 -3 5 0.10 3.70 -32 -3 4 0.80 3.70 32 -3 -3 -1.50 4.00 -32 -3 3 -2.50 3.40 -32 -3 2 12.20 5.00 32 -3 -2 17.70 6.90 -32 -3 1 5.30 4.50 32 -3 -1 4.00 4.70 32 -3 0 55.59 10.70 -32 -3 0 42.00 9.00 32 -3 1 0.90 4.00 -32 -3 -1 -2.40 3.50 -32 -3 -2 20.10 7.20 32 -3 2 29.40 8.90 -32 -3 -3 0.30 4.10 32 -3 3 -4.30 3.20 32 -3 4 13.70 6.20 -32 -3 -4 20.70 7.50 32 -3 5 -2.00 4.10 -32 -3 -5 -2.80 3.70 33 0 -6 2.20 2.90 33 0 -5 -3.60 2.30 33 0 -4 -1.60 2.30 33 0 -3 0.80 2.40 33 0 -2 17.70 4.30 33 0 -1 2.00 2.30 33 0 0 2.10 2.50 33 0 1 0.50 2.10 33 0 3 -4.00 1.90 33 0 4 3.00 2.30 33 0 5 0.80 2.40 33 0 6 167.78 9.50 33 0 7 2.40 2.40 33 0 8 3.70 2.80 33 0 9 -1.50 2.20 -33 -1 8 36.30 9.40 -33 -1 7 -4.10 4.10 -33 -1 6 1.40 4.80 -33 -1 5 -0.70 3.50 -33 -1 4 2.10 4.30 33 -1 -3 -2.10 2.00 -33 -1 3 1.30 4.10 33 -1 -2 5.90 3.10 -33 -1 2 14.80 6.30 33 -1 -1 -2.30 1.90 -33 -1 1 0.00 4.00 33 1 0 4.10 2.50 33 -1 0 5.40 2.60 -33 -1 0 4.30 4.10 33 1 1 -2.00 2.00 33 -1 1 2.10 2.40 -33 -1 -1 -3.70 3.30 33 1 2 7.20 3.10 -33 -1 -2 12.50 5.80 33 -1 2 7.20 3.00 33 1 3 -1.70 2.00 33 -1 3 2.60 2.30 -33 -1 -3 -3.10 4.10 33 1 4 13.00 3.60 33 -1 4 6.40 2.70 33 1 5 0.80 2.30 33 -1 5 0.50 2.00 33 1 6 12.30 3.50 33 -1 6 7.20 2.90 33 1 7 -0.20 2.70 33 -1 7 0.60 2.10 33 1 8 2.10 2.80 33 -1 8 2.10 2.30 -33 -2 7 0.30 4.30 -33 -2 6 69.59 11.70 -33 -2 5 -1.40 3.90 -33 -2 4 1.40 4.50 -33 -2 3 -2.10 3.70 -33 -2 2 1.00 4.00 -33 -2 1 0.30 3.70 -33 -2 0 18.20 6.70 -33 -2 -1 -2.60 3.90 -33 -2 -2 -0.70 4.20 33 -2 3 2.30 2.20 -33 -2 -3 4.60 4.40 33 -2 4 8.90 2.90 -33 -2 -4 6.40 5.30 -33 -2 -5 3.90 5.00 33 -2 5 -1.00 1.90 33 -2 6 65.89 6.10 -33 -2 -6 58.59 12.00 33 -2 7 1.20 1.90 -33 -3 4 37.00 9.10 -33 -3 3 7.40 4.90 33 -3 -2 44.30 11.00 -33 -3 2 43.00 9.50 -33 -3 1 1.70 4.30 33 -3 -1 3.20 4.70 -33 -3 0 -0.30 3.70 33 -3 0 -2.20 4.00 -33 -3 -1 -2.90 3.60 33 -3 1 5.20 4.80 33 -3 2 3.80 4.70 -33 -3 -2 2.80 4.80 -33 -3 -3 1.10 4.60 33 -3 3 -2.60 4.10 33 -3 4 23.00 7.90 -33 -3 -4 21.10 7.50 34 0 -6 0.70 2.80 34 0 -5 1.80 2.80 34 0 -4 4.10 3.00 34 0 -3 2.80 2.90 34 0 -2 -1.60 2.00 34 0 -1 -3.20 1.70 34 0 0 1.90 2.40 34 0 1 -0.50 2.20 34 0 2 0.90 2.00 34 0 3 5.90 2.80 34 0 4 95.89 8.80 34 0 5 -0.80 2.00 34 0 6 1.70 2.40 34 0 7 0.30 2.60 34 0 8 76.29 7.60 -34 -1 8 13.90 6.80 -34 -1 7 -3.00 4.00 -34 -1 6 -0.50 4.30 -34 -1 5 1.70 4.30 -34 -1 4 59.49 11.30 34 -1 -3 3.60 2.70 -34 -1 3 1.70 4.60 34 -1 -2 6.20 3.10 -34 -1 2 -3.30 4.10 -34 -1 1 0.90 3.60 34 -1 -1 -1.50 2.00 34 1 0 17.10 4.40 -34 -1 0 14.70 6.20 34 -1 0 9.70 3.40 34 1 1 1.20 2.40 -34 -1 -1 -1.40 3.90 34 -1 1 -0.60 2.00 34 1 2 159.28 11.10 -34 -1 -2 77.79 12.90 34 -1 2 113.79 9.30 34 1 3 3.10 2.90 34 -1 3 2.60 2.30 -34 -1 -3 3.30 4.80 34 1 4 11.10 3.50 34 -1 4 3.70 2.40 34 1 5 4.20 3.00 34 -1 5 0.40 2.00 34 1 6 0.40 2.20 34 -1 6 5.90 2.60 34 1 7 -3.60 2.10 34 -1 7 1.80 2.30 34 1 8 0.00 2.20 34 -1 8 -0.90 1.90 -34 -2 6 2.20 4.50 -34 -2 5 -0.90 3.90 -34 -2 4 32.00 8.50 -34 -2 3 -0.80 4.30 -34 -2 2 35.50 8.90 -34 -2 1 -2.30 3.70 -34 -2 0 47.80 10.10 -34 -2 -1 -2.60 4.00 -34 -2 -2 -7.80 3.10 34 -2 3 1.90 2.20 -34 -2 -3 2.20 4.00 -34 -2 -4 30.80 9.10 34 -2 4 20.60 3.90 -34 -2 -5 2.80 5.00 34 -2 5 -2.30 1.70 34 -2 6 3.20 2.30 -34 -2 -6 14.00 7.10 -34 -3 3 -0.90 3.80 -34 -3 2 0.60 4.20 -34 -3 1 5.10 4.60 -34 -3 0 8.50 5.80 34 -3 0 17.20 7.10 -34 -3 -1 -4.50 3.90 34 -3 1 6.00 5.70 -34 -3 -2 -0.90 4.00 34 -3 2 -6.80 3.70 -34 -3 -3 -0.30 4.50 34 -3 3 -1.70 4.50 35 0 -6 5.10 3.40 35 0 -5 -1.70 2.50 35 0 -4 -0.10 2.60 35 0 -3 3.30 3.10 35 0 -2 9.50 3.70 35 0 -1 -0.70 2.20 35 0 0 3.10 2.60 35 0 1 0.90 2.30 35 0 2 115.99 9.80 35 0 3 1.20 2.70 35 0 4 0.00 2.50 35 0 5 -0.30 2.40 35 0 6 56.79 7.00 35 0 7 -0.90 2.30 -35 -1 7 -6.30 3.60 -35 -1 6 -2.70 3.50 -35 -1 5 2.40 4.70 -35 -1 4 -1.50 4.00 35 -1 -3 -2.10 2.10 -35 -1 3 6.50 5.70 -35 -1 2 4.40 5.50 35 -1 -2 5.40 3.10 35 -1 -1 2.70 3.00 -35 -1 1 3.30 4.50 35 -1 0 70.19 7.90 -35 -1 0 84.19 13.00 35 1 1 0.60 2.20 35 -1 1 2.30 2.50 -35 -1 -1 1.20 4.10 35 1 2 1.60 2.80 35 -1 2 3.60 2.50 -35 -1 -2 -2.70 3.70 35 1 3 3.40 2.90 35 -1 3 1.60 2.20 35 1 4 11.60 3.80 35 -1 4 16.10 4.00 35 1 5 4.20 2.90 35 -1 5 2.70 2.30 35 1 6 17.60 4.40 35 -1 6 22.60 4.40 35 1 7 -3.80 2.40 35 -1 7 1.60 2.30 -35 -2 6 -2.10 4.40 -35 -2 5 1.70 4.50 -35 -2 4 8.60 5.50 -35 -2 3 -1.70 3.90 -35 -2 2 13.20 6.40 -35 -2 1 -2.60 3.30 -35 -2 0 4.00 5.10 -35 -2 -1 0.70 4.60 -35 -2 -2 -1.40 4.70 -35 -2 -3 1.20 5.00 35 -2 4 -0.50 2.00 -35 -2 -4 -1.20 4.20 -35 -2 -5 -0.10 5.20 35 -2 5 1.00 2.10 -35 -3 1 -0.70 4.40 -35 -3 0 0.60 4.20 -35 -3 -1 -6.00 3.80 36 0 -6 -2.00 2.50 36 0 -5 -0.50 2.90 36 0 -4 -1.50 2.60 36 0 -3 -1.50 2.40 36 0 -2 -1.30 2.30 36 0 -1 -2.70 1.90 36 0 0 69.19 7.60 36 0 1 -0.70 2.30 36 0 2 2.20 2.60 36 0 3 2.30 2.50 36 0 4 -1.20 2.50 36 0 5 -1.80 2.40 36 0 6 2.60 2.50 36 0 7 0.60 2.40 -36 -1 6 3.60 5.70 -36 -1 5 4.80 5.30 -36 -1 4 3.10 5.30 -36 -1 3 -6.10 3.60 36 -1 -3 3.90 3.00 36 -1 -2 29.80 5.60 -36 -1 2 44.00 10.50 -36 -1 1 0.60 4.40 36 -1 -1 1.30 2.70 -36 -1 0 73.19 12.60 36 -1 0 56.79 6.90 36 1 1 2.90 2.60 36 -1 1 7.40 3.10 -36 -1 -1 -0.50 4.00 36 1 2 13.50 3.80 36 -1 2 2.90 2.60 36 1 3 -1.00 2.40 36 -1 3 1.60 2.30 36 1 4 66.49 7.40 36 -1 4 48.50 6.50 36 1 5 -0.30 2.70 36 -1 5 -1.20 2.10 36 1 6 -2.40 2.30 36 -1 6 1.40 2.20 -36 -2 5 -3.20 4.30 -36 -2 4 40.70 9.80 -36 -2 3 -0.90 3.90 -36 -2 2 36.10 8.90 -36 -2 1 -1.50 3.80 -36 -2 0 2.60 4.90 -36 -2 -1 -0.20 4.60 -36 -2 -2 6.50 5.70 -36 -2 -3 10.80 6.00 36 -2 4 25.90 4.30 -36 -2 -4 29.90 9.30 37 0 -6 51.79 7.90 37 0 -5 -1.50 2.70 37 0 -4 1.20 3.00 37 0 -3 -2.90 2.40 37 0 -2 12.70 4.20 37 0 -1 -0.60 2.30 37 0 0 -2.00 2.20 37 0 1 -0.90 2.20 37 0 2 84.89 8.40 37 0 3 0.80 2.60 37 0 4 3.60 2.90 37 0 5 0.80 2.70 37 0 6 0.50 2.60 -37 -1 5 3.20 5.70 -37 -1 4 30.10 8.60 -37 -1 3 -0.50 4.60 37 -1 -3 -0.40 2.50 37 -1 -2 23.10 5.10 -37 -1 2 20.90 7.80 -37 -1 1 -2.10 4.50 37 -1 -1 -2.50 2.10 -37 -1 0 3.40 5.70 37 -1 0 0.30 2.50 37 1 1 2.60 2.80 37 -1 1 0.40 2.40 37 1 2 117.19 9.80 37 -1 2 116.39 10.00 37 1 3 1.10 2.80 37 -1 3 -4.50 1.90 37 1 4 2.40 2.90 37 -1 4 1.80 2.50 37 1 5 -2.70 2.60 37 -1 5 -0.90 2.20 -37 -2 3 -4.30 4.30 -37 -2 2 20.90 7.60 -37 -2 1 -4.40 3.90 -37 -2 0 120.89 16.70 -37 -2 -1 1.20 4.70 -37 -2 -2 3.40 5.10 -37 -2 -3 -5.30 4.00 38 0 -5 -0.20 3.30 38 0 -4 19.40 4.70 38 0 -3 0.10 2.70 38 0 -2 3.70 2.90 38 0 -1 3.20 2.90 38 0 0 57.49 7.40 38 0 1 -2.30 2.20 38 0 2 4.10 2.90 38 0 3 -5.00 1.90 38 0 4 67.19 7.50 38 0 5 -2.30 2.00 -38 -1 4 49.20 11.90 -38 -1 3 -3.60 3.60 38 -1 -3 -3.70 2.20 38 -1 -2 5.00 3.30 -38 -1 2 -2.00 4.90 38 -1 -1 -3.00 2.30 38 -1 0 31.20 5.70 38 -1 1 -4.40 1.90 38 1 2 10.00 3.60 38 -1 2 2.30 2.70 38 1 3 1.40 2.70 38 -1 3 0.30 2.20 38 1 4 1.20 2.90 38 -1 4 2.80 2.90 -38 -2 1 -1.30 4.30 -38 -2 0 -2.30 4.30 39 0 -4 -2.70 2.90 39 0 -3 -3.50 2.50 39 0 -2 15.40 4.70 39 0 -1 -0.10 2.90 39 0 0 0.90 2.90 39 0 1 3.90 2.90 39 0 2 30.00 5.80 39 0 3 -4.20 2.20 39 -1 -3 -0.50 2.90 39 -1 -2 5.40 3.70 39 -1 -1 -1.60 2.90 39 -1 0 24.50 5.20 39 -1 1 0.80 2.60 39 1 2 2.70 3.20 39 -1 2 9.60 3.60 40 0 -1 -1.10 2.60 40 0 0 21.30 5.00 40 0 1 -1.30 2.50 _computing_structure_solution 'SHELXT 2014/4 (Sheldrick, 2014)' ; _shelx_hkl_checksum 28530 _shelx_res_file ; PMDI.res created by SHELXL-2014/7 TITL PMDI.res in P21/n CELL 0.71073 6.1500 4.7475 31.0020 90.000 90.461 90.000 ZERR 2 0.0005 0.0003 0.0020 0.000 0.003 0.000 LATT 1 SYMM 0.50000 - X , 0.50000 + Y , 0.50000 - Z SFAC C H N O UNIT 48 32 4 8 SIZE 0.020 0.060 0.500 TEMP -100 L.S. 5 ACTA BOND $H FMAP 2 PLAN 10 CONF WGHT 0.052900 0.089000 FVAR 0.79828 O1 4 0.914484 0.961741 0.097589 11.00000 0.03441 0.03054 = 0.02929 -0.00983 0.00228 -0.00604 O2 4 0.473705 0.251351 0.049209 11.00000 0.02469 0.02849 = 0.03161 -0.00145 0.00297 -0.00557 N1 3 0.658932 0.617626 0.082166 11.00000 0.02302 0.02193 = 0.02043 -0.00079 0.00335 0.00007 C1 1 0.278342 0.327931 0.154452 11.00000 0.02638 0.02998 = 0.03456 -0.00406 0.00363 0.00024 AFIX 43 H1 2 0.161662 0.365866 0.135042 11.00000 -1.20000 AFIX 0 C2 1 0.250457 0.131143 0.187114 11.00000 0.04025 0.02866 = 0.04013 -0.00148 0.01694 -0.00232 AFIX 43 H2 2 0.115739 0.035447 0.190077 11.00000 -1.20000 AFIX 0 C3 1 0.420569 0.075989 0.215244 11.00000 0.05800 0.03072 = 0.03130 0.00347 0.01507 0.00422 AFIX 43 H3 2 0.402126 -0.056829 0.237841 11.00000 -1.20000 AFIX 0 C4 1 0.617546 0.212962 0.210706 11.00000 0.04598 0.03414 = 0.02672 0.00393 -0.00451 0.00385 AFIX 43 H4 2 0.734594 0.172400 0.229902 11.00000 -1.20000 AFIX 0 C5 1 0.643862 0.409392 0.178124 11.00000 0.03008 0.03151 = 0.02788 -0.00034 -0.00092 -0.00275 AFIX 43 H5 2 0.779188 0.503608 0.175141 11.00000 -1.20000 AFIX 0 C6 1 0.473902 0.469924 0.149733 11.00000 0.02585 0.02282 = 0.02143 -0.00456 0.00493 0.00093 C7 1 0.499373 0.689505 0.115233 11.00000 0.02476 0.02691 = 0.02397 -0.00093 0.00429 0.00255 AFIX 23 H7A 2 0.356503 0.720079 0.101054 11.00000 -1.20000 H7B 2 0.543210 0.869142 0.128992 11.00000 -1.20000 AFIX 0 C8 1 0.849936 0.768659 0.075478 11.00000 0.02272 0.01981 = 0.02140 0.00159 -0.00102 0.00109 C9 1 0.950668 0.645540 0.036182 11.00000 0.02115 0.01839 = 0.02016 0.00103 -0.00251 0.00106 C10 1 0.816836 0.428300 0.021687 11.00000 0.01870 0.01811 = 0.01901 0.00243 0.00007 0.00054 C11 1 0.627901 0.409294 0.051176 11.00000 0.02393 0.01944 = 0.01991 0.00275 -0.00207 0.00115 C12 1 1.138897 0.724860 0.015200 11.00000 0.02291 0.01815 = 0.01954 0.00050 -0.00192 -0.00140 AFIX 43 H12 2 1.230286 0.872494 0.025307 11.00000 -1.20000 AFIX 0 HKLF 4 1 0.0000 0.0000 0.5000 0.0000 -1.0000 0.0000 1.0000 0.0000 0.0000 REM PMDI.res in P21/n REM R1 = 0.0478 for 1444 Fo > 4sig(Fo) and 0.0692 for all 2016 data REM 136 parameters refined using 0 restraints END WGHT 0.0529 0.0890 REM Highest difference peak 0.254, deepest hole -0.215, 1-sigma level 0.051 Q1 1 0.9038 0.5219 0.0289 11.00000 0.05 0.25 Q2 1 0.2761 0.2185 0.1735 11.00000 0.05 0.22 Q3 1 0.4560 -0.0800 0.2484 11.00000 0.05 0.19 Q4 1 0.8673 0.3178 0.0137 11.00000 0.05 0.19 Q5 1 0.2855 0.1951 0.2092 11.00000 0.05 0.19 Q6 1 0.9160 0.6910 0.0536 11.00000 0.05 0.19 Q7 1 0.4842 0.5974 0.1369 11.00000 0.05 0.18 Q8 1 -0.0409 0.0836 0.1796 11.00000 0.05 0.18 Q9 1 0.7277 0.4195 0.0290 11.00000 0.05 0.17 Q10 1 0.5920 1.1512 0.1329 11.00000 0.05 0.17 ; _shelx_res_checksum 71708 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy O O1 0.9145(2) 0.9617(3) 0.09759(4) 0.0314(4) Uani d 1 O O2 0.4737(2) 0.2514(3) 0.04921(4) 0.0282(3) Uani d 1 N N1 0.6589(2) 0.6176(3) 0.08217(5) 0.0218(4) Uani d 1 C C1 0.2783(3) 0.3279(4) 0.15445(6) 0.0303(5) Uani d 1 H H1 0.1617 0.3659 0.1350 0.036 Uiso calc 1 C C2 0.2505(4) 0.1311(4) 0.18711(7) 0.0363(5) Uani d 1 H H2 0.1157 0.0354 0.1901 0.044 Uiso calc 1 C C3 0.4206(4) 0.0760(4) 0.21524(7) 0.0399(6) Uani d 1 H H3 0.4021 -0.0568 0.2378 0.048 Uiso calc 1 C C4 0.6175(4) 0.2130(4) 0.21071(6) 0.0356(5) Uani d 1 H H4 0.7346 0.1724 0.2299 0.043 Uiso calc 1 C C5 0.6439(3) 0.4094(4) 0.17812(6) 0.0298(5) Uani d 1 H H5 0.7792 0.5036 0.1751 0.036 Uiso calc 1 C C6 0.4739(3) 0.4699(4) 0.14973(6) 0.0233(4) Uani d 1 C C7 0.4994(3) 0.6895(4) 0.11523(6) 0.0252(4) Uani d 1 H H7A 0.3565 0.7201 0.1011 0.030 Uiso calc 1 H H7B 0.5432 0.8691 0.1290 0.030 Uiso calc 1 C C8 0.8499(3) 0.7687(3) 0.07548(6) 0.0213(4) Uani d 1 C C9 0.9507(3) 0.6455(3) 0.03618(5) 0.0199(4) Uani d 1 C C10 0.8168(3) 0.4283(3) 0.02169(5) 0.0186(4) Uani d 1 C C11 0.6279(3) 0.4093(3) 0.05118(5) 0.0211(4) Uani d 1 C C12 1.1389(3) 0.7249(3) 0.01520(5) 0.0202(4) Uani d 1 H H12 1.2303 0.8725 0.0253 0.024 Uiso calc 1 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 O1 0.0344(9) 0.0305(7) 0.0293(7) -0.0060(6) 0.0023(6) -0.0098(6) O2 0.0247(8) 0.0285(7) 0.0316(7) -0.0056(6) 0.0030(6) -0.0014(6) N1 0.0230(9) 0.0219(7) 0.0204(8) 0.0001(6) 0.0034(6) -0.0008(6) C1 0.0264(11) 0.0300(9) 0.0346(11) 0.0002(8) 0.0036(9) -0.0041(9) C2 0.0402(14) 0.0287(10) 0.0401(12) -0.0023(10) 0.0169(10) -0.0015(10) C3 0.0580(17) 0.0307(10) 0.0313(12) 0.0042(11) 0.0151(11) 0.0035(9) C4 0.0460(14) 0.0341(10) 0.0267(10) 0.0039(10) -0.0045(9) 0.0039(9) C5 0.0301(12) 0.0315(9) 0.0279(10) -0.0028(9) -0.0009(9) -0.0003(9) C6 0.0258(11) 0.0228(8) 0.0214(9) 0.0009(8) 0.0049(8) -0.0046(7) C7 0.0248(11) 0.0269(9) 0.0240(9) 0.0025(8) 0.0043(8) -0.0009(8) C8 0.0227(10) 0.0198(8) 0.0214(9) 0.0011(7) -0.0010(8) 0.0016(7) C9 0.0211(10) 0.0184(8) 0.0202(9) 0.0011(7) -0.0025(7) 0.0010(7) C10 0.0187(9) 0.0181(7) 0.0190(8) 0.0005(7) 0.0001(7) 0.0024(7) C11 0.0239(10) 0.0194(8) 0.0199(9) 0.0012(8) -0.0021(7) 0.0027(7) C12 0.0229(11) 0.0182(7) 0.0195(9) -0.0014(7) -0.0019(7) 0.0005(7) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle C11 N1 C8 . 111.98(15) C11 N1 C7 . 124.05(15) C8 N1 C7 . 123.68(14) C6 C1 C2 . 121.05(19) C6 C1 H1 . 119.5 C2 C1 H1 . 119.5 C3 C2 C1 . 119.4(2) C3 C2 H2 . 120.3 C1 C2 H2 . 120.3 C2 C3 C4 . 120.40(19) C2 C3 H3 . 119.8 C4 C3 H3 . 119.8 C3 C4 C5 . 119.9(2) C3 C4 H4 . 120.1 C5 C4 H4 . 120.1 C4 C5 C6 . 120.59(19) C4 C5 H5 . 119.7 C6 C5 H5 . 119.7 C1 C6 C5 . 118.72(17) C1 C6 C7 . 120.50(17) C5 C6 C7 . 120.77(17) N1 C7 C6 . 114.25(14) N1 C7 H7A . 108.7 C6 C7 H7A . 108.7 N1 C7 H7B . 108.7 C6 C7 H7B . 108.7 H7A C7 H7B . 107.6 O1 C8 N1 . 125.37(17) O1 C8 C9 . 128.58(17) N1 C8 C9 . 106.04(14) C12 C9 C10 . 122.98(16) C12 C9 C8 . 129.19(15) C10 C9 C8 . 107.81(16) C12 C10 C9 3_765 122.44(16) C12 C10 C11 3_765 129.49(16) C9 C10 C11 . 108.03(15) O2 C11 N1 . 125.35(18) O2 C11 C10 . 128.50(16) N1 C11 C10 . 106.14(15) C10 C12 C9 3_765 114.59(15) C10 C12 H12 3_765 122.7 C9 C12 H12 . 122.7 loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance O1 C8 . 1.210(2) O2 C11 . 1.210(2) N1 C11 . 1.391(2) N1 C8 . 1.393(2) N1 C7 . 1.465(2) C1 C6 . 1.387(3) C1 C2 . 1.389(3) C1 H1 . 0.9500 C2 C3 . 1.382(3) C2 H2 . 0.9500 C3 C4 . 1.383(3) C3 H3 . 0.9500 C4 C5 . 1.385(3) C4 H4 . 0.9500 C5 C6 . 1.391(2) C5 H5 . 0.9500 C6 C7 . 1.503(2) C7 H7A . 0.9900 C7 H7B . 0.9900 C8 C9 . 1.491(2) C9 C12 . 1.385(2) C9 C10 . 1.392(2) C10 C12 3_765 1.384(2) C10 C11 . 1.487(3) C12 C10 3_765 1.384(2) C12 H12 . 0.9500 loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_publ_flag C7 H7B O1 . 0.99 2.53 2.917(2) 103.2 y C12 H12 O2 1_665 0.95 2.45 3.401(2) 178.1 y C7 H7B Cg1 1_565 0.99 2.60 3.478(2) 148 y loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_4 _geom_torsion C6 C1 C2 C3 . . -0.1(3) C1 C2 C3 C4 . . -0.7(3) C2 C3 C4 C5 . . 0.8(3) C3 C4 C5 C6 . . -0.2(3) C2 C1 C6 C5 . . 0.7(3) C2 C1 C6 C7 . . -177.86(17) C4 C5 C6 C1 . . -0.6(3) C4 C5 C6 C7 . . 178.03(17) C11 N1 C7 C6 . . 71.0(2) C8 N1 C7 C6 . . -115.62(18) C1 C6 C7 N1 . . -115.50(19) C5 C6 C7 N1 . . 65.9(2) C11 N1 C8 O1 . . 179.57(16) C7 N1 C8 O1 . . 5.5(3) C11 N1 C8 C9 . . 0.27(18) C7 N1 C8 C9 . . -173.83(14) O1 C8 C9 C12 . . -1.3(3) N1 C8 C9 C12 . . 178.00(17) O1 C8 C9 C10 . . -179.63(17) N1 C8 C9 C10 . . -0.36(18) C12 C9 C10 C12 . 3_765 -0.4(3) C8 C9 C10 C12 . 3_765 178.05(15) C12 C9 C10 C11 . . -178.18(15) C8 C9 C10 C11 . . 0.31(18) C8 N1 C11 O2 . . -178.89(16) C7 N1 C11 O2 . . -4.8(3) C8 N1 C11 C10 . . -0.08(18) C7 N1 C11 C10 . . 173.99(14) C12 C10 C11 O2 3_765 . 1.1(3) C9 C10 C11 O2 . . 178.61(17) C12 C10 C11 N1 3_765 . -177.67(16) C9 C10 C11 N1 . . -0.15(18) C10 C9 C12 C10 . 3_765 0.4(3) C8 C9 C12 C10 . 3_765 -177.73(16) _cod_database_fobs_code 2241945