Crystallography Open Database

Information card for entry 2241952

2241951 << 2241952 >> 2241953

Preview

Coordinates	2241952.cif
Structure factors	2241952.hkl
Original paper (by DOI)	HTML

Structure parameters

Chemical name	Bis(μ-<i>N</i>^1^,<i>N</i>^2^-dicyclohexyl-3-cyclopropylpropynamidinato-κ^2^<i>N</i>^1^:<i>N</i>^2^)disilver(I) bis(μ-<i>N</i>^1^,<i>N</i>^2^-dicyclohexyl-3-cyclopropylpropynamidinato-κ^3^<i>N</i>^1^,<i>N</i>^2^:<i>N</i>^1^)bis(tetrahydrofuran- κ<i>O</i>)lithium(I) toluene monosolvate
Formula	C87 H132 Ag2 Li2 N8 O2
Calculated formula	C87 H132 Ag2 Li2 N8 O2
Title of publication	Crystal and molecular structures of two silver(I) amidinates, including an unexpected co-crystal with a lithium amidinate
Authors of publication	Wang, Sida; Harmgarth, Nicole; Liebing, Phil; Edelmann, Frank T.
Journal of publication	Acta Crystallographica Section E
Year of publication	2016
Journal volume	72
Journal issue	12
Pages of publication	1786 - 1790
a	10.588 ± 0.0003 Å
b	14.562 ± 0.0004 Å
c	14.983 ± 0.0005 Å
α	99.871 ± 0.002°
β	102.825 ± 0.002°
γ	106.538 ± 0.002°
Cell volume	2090.17 ± 0.12 Å³
Cell temperature	133 ± 2 K
Ambient diffraction temperature	133 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0335
Residual factor for significantly intense reflections	0.0282
Weighted residual factors for significantly intense reflections	0.0712
Weighted residual factors for all reflections included in the refinement	0.0731
Goodness-of-fit parameter for all reflections included in the refinement	1.028
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	Yes

Version history

Revision	Date	Message	Files
188496 (current)	2016-11-16	cif/ hkl/ Adding structures of 2241951, 2241952 via cif-deposit CGI script.	2241952.cif 2241952.hkl