#------------------------------------------------------------------------------ #$Date: 2016-11-19 03:59:14 +0200 (Sat, 19 Nov 2016) $ #$Revision: 188574 $ #$URL: file:///home/coder/svn-repositories/cod/cif/2/24/19/2241953.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2241953 loop_ _publ_author_name 'Suckert, Stefan' 'Jess, Inke' 'N\"ather, Christian' _publ_section_title ; Crystal structure of bis(3,5-dimethylpyridine-\kN)bis(methanol-\kO)bis(thiocyanato-\kN)cobalt(II) ; _journal_coeditor_code WM5338 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first 1824 _journal_page_last 1826 _journal_paper_doi 10.1107/S2056989016018326 _journal_volume 72 _journal_year 2016 _chemical_formula_iupac '[Co (N C S)2 (C7 H9 N)2 (C H4 O)2]' _chemical_formula_moiety 'C18 H26 Co N4 O2 S2' _chemical_formula_sum 'C18 H26 Co N4 O2 S2' _chemical_formula_weight 453.48 _chemical_name_systematic Bis(3,5-dimethylpyridine-\kN)bis(methanol-\kO)bis(thiocyanato-\kn)cobalt(II) _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _atom_sites_solution_hydrogens mixed _audit_creation_method SHELXL-2014/7 _cell_angle_alpha 87.403(5) _cell_angle_beta 81.419(5) _cell_angle_gamma 76.295(5) _cell_formula_units_Z 1 _cell_length_a 7.7027(5) _cell_length_b 7.8688(5) _cell_length_c 9.1970(5) _cell_measurement_reflns_used 6258 _cell_measurement_temperature 170(2) _cell_measurement_theta_max 27.439 _cell_measurement_theta_min 2.240 _cell_volume 535.48(6) _computing_cell_refinement ; X-AREA (Stoe & Cie, 2008) ; _computing_data_collection ; X-AREA (Stoe & Cie, 2008) ; _computing_data_reduction ; X-AREA (Stoe & Cie, 2008) ; _computing_molecular_graphics ; XP in SHELXTL (Sheldrick, 2008) and DIAMOND (Brandenburg, 1999) ; _computing_publication_material ; publCIF (Westrip, 2010) ; _computing_structure_refinement ; SHELXL2014 (Sheldrick, 2015) ; _computing_structure_solution ; SHELXS97 (Sheldrick, 2008) ; _diffrn_ambient_temperature 170(2) _diffrn_measured_fraction_theta_full 0.997 _diffrn_measured_fraction_theta_max 0.995 _diffrn_measurement_device_type 'Stoe IPDS-2' _diffrn_measurement_method 'omega scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0237 _diffrn_reflns_limit_h_max 9 _diffrn_reflns_limit_h_min -9 _diffrn_reflns_limit_k_max 10 _diffrn_reflns_limit_k_min -10 _diffrn_reflns_limit_l_max 11 _diffrn_reflns_limit_l_min -11 _diffrn_reflns_number 6258 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 27.439 _diffrn_reflns_theta_min 2.240 _exptl_absorpt_coefficient_mu 1.016 _exptl_absorpt_correction_T_max 0.923 _exptl_absorpt_correction_T_min 0.885 _exptl_absorpt_correction_type numerical _exptl_absorpt_process_details ; (X-SHAPE and X-RED32; Stoe & Cie, 2008) ; _exptl_crystal_colour blue _exptl_crystal_density_diffrn 1.406 _exptl_crystal_description block _exptl_crystal_F_000 237 _exptl_crystal_size_max 0.1495 _exptl_crystal_size_mid 0.0905 _exptl_crystal_size_min 0.0406 _refine_diff_density_max 0.366 _refine_diff_density_min -0.367 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.080 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 127 _refine_ls_number_reflns 2431 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.080 _refine_ls_R_factor_all 0.0430 _refine_ls_R_factor_gt 0.0344 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0503P)^2^+0.2412P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0868 _refine_ls_wR_factor_ref 0.0943 _reflns_number_gt 2052 _reflns_number_total 2431 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file wm5338sup1.cif _cod_data_source_block I _cod_database_code 2241953 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_hkl_file ; 2 0 0 6226.54 42.27 0 3 0 0 185.52 11.32 0 4 0 0 533.70 11.07 0 4 0 0 540.01 12.56 0 5 0 0 291.56 10.64 0 5 0 0 283.64 9.60 0 6 0 0 187.38 10.01 0 6 0 0 185.11 7.13 0 7 0 0 213.03 10.17 0 7 0 0 224.77 6.92 0 8 0 0 27.15 11.49 0 8 0 0 17.61 8.27 0 8 0 0 30.05 8.27 0 9 0 0 127.28 9.57 0 9 0 0 126.20 7.64 0 9 0 0 146.36 10.39 0 9 -1 0 32.38 6.97 0 9 -1 0 48.42 9.92 0 9 -1 0 24.56 6.70 0 8 -1 0 225.99 10.37 0 8 -1 0 264.21 9.72 0 8 -1 0 250.72 9.55 0 7 -1 0 186.08 9.47 0 7 -1 0 192.06 9.13 0 7 -1 0 208.92 8.79 0 6 -1 0 33.84 7.77 0 6 -1 0 42.59 8.99 0 6 -1 0 31.43 6.04 0 5 -1 0 99.23 6.22 0 5 -1 0 101.28 9.49 0 4 -1 0 353.24 10.39 0 4 -1 0 314.31 9.33 0 3 -1 0 22.08 8.16 0 3 -1 0 21.71 9.87 0 2 -1 0 5517.26 30.27 0 1 -1 0 8510.16 45.62 0 -1 1 0 8319.32 44.88 0 0 1 0 3700.33 40.67 0 0 -1 0 3721.93 40.72 0 -1 -1 0 930.76 22.23 0 1 1 0 944.41 22.10 0 2 1 0 53.09 20.55 0 -2 -1 0 55.22 14.51 0 2 1 0 106.23 15.64 0 3 1 0 104.66 13.71 0 3 1 0 98.56 8.42 0 4 1 0 59.11 9.04 0 4 1 0 54.59 12.02 0 5 1 0 1983.82 20.98 0 5 1 0 1939.47 14.25 0 6 1 0 70.88 9.58 0 6 1 0 86.80 8.98 0 7 1 0 41.94 5.80 0 7 1 0 39.18 8.33 0 8 1 0 624.88 9.34 0 8 1 0 641.75 13.59 0 9 1 0 56.51 8.96 0 9 1 0 80.63 9.59 0 8 -2 0 10.09 8.18 0 8 -2 0 -8.20 9.27 0 8 -2 0 -2.07 8.34 0 7 -2 0 -4.60 8.63 0 7 -2 0 8.60 7.91 0 6 -2 0 326.01 9.16 0 6 -2 0 329.44 10.47 0 5 -2 0 3.42 9.12 0 5 -2 0 5.52 7.65 0 4 -2 0 189.72 10.27 0 4 -2 0 189.27 8.76 0 3 -2 0 3540.51 20.64 0 3 -2 0 3790.85 22.10 0 2 -2 0 2816.71 19.56 0 -2 2 0 2847.16 20.29 0 1 -2 0 79.19 10.51 0 -1 2 0 85.33 10.39 0 0 2 0 234.61 14.45 0 0 -2 0 243.90 13.42 0 -1 -2 0 5242.84 35.53 0 1 2 0 5258.02 35.09 0 2 2 0 96.27 11.63 0 -2 -2 0 98.21 20.70 0 -2 -2 0 104.73 11.75 0 3 2 0 707.20 13.30 0 3 2 0 688.22 33.93 0 -3 -2 0 734.56 13.42 0 4 2 0 684.51 12.06 0 4 2 0 669.49 20.36 0 -4 -2 0 696.60 10.12 0 5 2 0 4.16 11.51 0 5 2 0 0.40 6.41 0 6 2 0 612.31 16.30 0 6 2 0 623.86 11.05 0 7 2 0 804.22 11.52 0 7 2 0 808.62 16.87 0 8 2 0 67.76 11.62 0 8 2 0 52.32 6.12 0 9 2 0 13.20 8.55 0 9 2 0 14.15 11.37 0 8 -3 0 6.35 6.32 0 8 -3 0 18.22 9.56 0 8 -3 0 6.86 6.15 0 7 -3 0 15.17 8.95 0 7 -3 0 -0.64 5.57 0 6 -3 0 73.23 8.03 0 6 -3 0 89.84 8.84 0 5 -3 0 454.89 9.81 0 5 -3 0 456.75 10.44 0 4 -3 0 960.72 12.59 0 4 -3 0 939.30 10.11 0 3 -3 0 93.47 6.95 0 3 -3 0 95.50 7.98 0 2 -3 0 196.47 8.61 0 -2 3 0 194.19 8.76 0 -1 3 0 2403.62 19.56 0 1 -3 0 2429.08 19.41 0 0 3 0 187.03 9.84 0 0 -3 0 177.94 10.11 0 -1 -3 0 178.67 10.53 0 1 3 0 173.53 10.17 0 2 3 0 6088.30 29.71 0 -2 -3 0 6088.81 30.13 0 3 3 0 637.34 11.89 0 -3 -3 0 635.15 12.12 0 -4 -3 0 14.49 8.66 0 4 3 0 25.43 6.02 0 5 3 0 376.60 10.24 0 -5 -3 0 387.99 8.29 0 6 3 0 920.90 12.17 0 7 3 0 10.08 14.62 0 7 3 0 9.50 7.99 0 8 3 0 69.78 15.33 0 8 3 0 60.87 8.37 0 9 3 0 159.84 20.11 0 9 3 0 141.67 9.40 0 7 -4 0 25.66 9.13 0 7 -4 0 22.68 8.25 0 6 -4 0 247.50 10.08 0 6 -4 0 245.84 9.05 0 5 -4 0 853.04 9.86 0 5 -4 0 896.81 12.11 0 4 -4 0 6.45 9.16 0 4 -4 0 7.72 7.35 0 3 -4 0 73.07 8.89 0 3 -4 0 80.65 7.79 0 2 -4 0 243.35 10.64 0 2 -4 0 249.42 8.73 0 -2 4 0 239.26 8.53 0 -1 4 0 253.83 8.34 0 1 -4 0 263.74 8.43 0 0 -4 0 2156.20 17.10 0 0 4 0 2156.52 17.11 0 -1 -4 0 2572.39 18.76 0 1 4 0 2545.81 18.76 0 -2 -4 0 13.34 7.79 0 2 4 0 3.29 7.73 0 -3 -4 0 222.06 15.10 0 3 4 0 207.85 8.79 0 -3 -4 0 220.53 9.11 0 4 4 0 1539.25 14.32 0 -4 -4 0 1610.89 14.84 0 -5 -4 0 581.03 10.90 0 5 4 0 552.12 8.85 0 -6 -4 0 -5.37 8.21 0 6 4 0 8.07 7.98 0 7 4 0 223.37 8.95 0 8 4 0 128.44 8.90 0 9 4 0 92.97 9.20 0 7 -5 0 26.71 6.49 0 7 -5 0 82.89 9.71 0 6 -5 0 20.45 8.18 0 6 -5 0 9.61 8.92 0 5 -5 0 5.50 5.96 0 5 -5 0 7.28 7.56 0 4 -5 0 576.60 10.13 0 4 -5 0 577.25 9.17 0 3 -5 0 397.10 8.47 0 3 -5 0 380.16 9.15 0 -3 5 0 380.22 9.26 0 2 -5 0 0.97 7.12 0 -2 5 0 5.77 7.36 0 2 -5 0 0.46 9.02 0 -1 5 0 626.80 10.51 0 1 -5 0 636.73 10.53 0 1 -5 0 631.58 11.81 0 0 5 0 1407.53 13.45 0 0 -5 0 1415.93 13.65 0 1 5 0 19.32 7.45 0 -1 -5 0 20.29 7.36 0 -2 -5 0 295.12 9.19 0 -2 -5 0 303.84 11.29 0 2 5 0 319.91 9.25 0 -3 -5 0 1136.96 12.94 0 -3 -5 0 1150.70 19.54 0 3 5 0 1088.52 12.59 0 -4 -5 0 2.99 17.22 0 -4 -5 0 3.37 16.00 0 4 5 0 5.13 7.68 0 -4 -5 0 5.30 8.33 0 5 5 0 184.95 8.88 0 -5 -5 0 208.31 9.16 0 6 5 0 487.97 10.12 0 -6 -5 0 507.22 10.69 0 7 5 0 66.39 8.01 0 8 5 0 103.86 8.77 0 9 5 0 293.67 11.16 0 6 -6 0 22.53 8.91 0 6 -6 0 2.34 8.81 0 5 -6 0 158.83 9.74 0 5 -6 0 145.72 8.65 0 4 -6 0 529.71 10.99 0 4 -6 0 544.22 10.34 0 3 -6 0 250.72 9.70 0 3 -6 0 251.52 8.76 0 -3 6 0 263.08 8.87 0 2 -6 0 203.55 8.49 0 -2 6 0 220.28 8.56 0 2 -6 0 228.44 7.61 0 1 -6 0 39.03 7.92 0 -1 6 0 49.43 7.50 0 1 -6 0 45.84 8.86 0 0 -6 0 51.03 8.11 0 0 -6 0 62.59 9.37 0 0 6 0 57.40 7.96 0 -1 -6 0 1983.09 15.51 0 1 6 0 1968.55 15.49 0 -1 -6 0 2023.40 17.61 0 -2 -6 0 364.87 9.71 0 -2 -6 0 354.53 12.97 0 2 6 0 359.68 9.54 0 3 6 0 120.10 8.49 0 -3 -6 0 117.25 12.11 0 -3 -6 0 118.93 8.66 0 -4 -6 0 120.86 9.20 0 4 6 0 108.32 8.10 0 -4 -6 0 112.35 13.29 0 -4 -6 0 118.33 12.77 0 5 6 0 958.94 11.91 0 -5 -6 0 909.07 12.34 0 6 6 0 152.08 8.92 0 -6 -6 0 169.23 9.07 0 -7 -6 0 222.05 9.21 0 7 6 0 215.03 9.02 0 8 6 0 223.02 9.66 0 9 6 0 7.39 9.56 0 5 -7 0 6.44 8.83 0 5 -7 0 20.90 8.78 0 4 -7 0 233.03 8.05 0 4 -7 0 234.24 9.43 0 3 -7 0 223.36 8.83 0 -3 7 0 237.56 8.82 0 3 -7 0 224.80 9.84 0 2 -7 0 17.86 7.40 0 -2 7 0 14.81 7.39 0 2 -7 0 23.49 8.62 0 1 -7 0 54.60 7.65 0 -1 7 0 52.05 8.06 0 1 -7 0 57.28 9.14 0 0 7 0 617.21 10.39 0 0 -7 0 623.24 11.81 0 0 -7 0 630.19 10.47 0 -1 -7 0 52.81 9.18 0 1 7 0 45.42 7.55 0 -1 -7 0 49.92 7.78 0 2 7 0 22.76 7.33 0 -2 -7 0 17.57 9.04 0 -2 -7 0 20.50 7.54 0 3 7 0 918.54 11.47 0 -3 -7 0 884.96 11.58 0 -3 -7 0 896.26 15.97 0 -4 -7 0 524.38 10.50 0 -4 -7 0 501.05 14.95 0 4 7 0 532.46 9.93 0 5 7 0 11.54 8.02 0 -5 -7 0 16.88 8.13 0 -6 -7 0 357.99 8.05 0 6 7 0 388.24 9.79 0 -7 -7 0 113.03 9.10 0 7 7 0 92.20 9.04 0 -8 -7 0 -2.19 6.11 0 8 7 0 9.47 8.79 0 4 -8 0 24.64 9.94 0 4 -8 0 29.72 9.34 0 3 -8 0 10.27 9.02 0 -3 8 0 3.00 8.16 0 3 -8 0 9.32 8.29 0 2 -8 0 78.03 9.83 0 2 -8 0 104.33 8.70 0 -2 8 0 118.39 8.38 0 1 -8 0 284.48 9.31 0 1 -8 0 265.82 10.03 0 -1 8 0 274.54 9.35 0 0 -8 0 21.67 7.96 0 0 -8 0 12.15 9.05 0 0 8 0 17.48 7.59 0 -1 -8 0 29.02 7.98 0 1 8 0 29.62 8.07 0 -1 -8 0 35.36 9.01 0 2 8 0 460.10 9.90 0 -2 -8 0 383.30 9.84 0 -2 -8 0 408.33 11.29 0 -3 -8 0 79.84 8.52 0 -3 -8 0 78.78 11.44 0 3 8 0 86.68 8.38 0 -4 -8 0 359.12 10.21 0 4 8 0 362.45 9.69 0 -4 -8 0 335.40 13.52 0 -5 -8 0 382.96 21.35 0 5 8 0 414.56 9.89 0 -5 -8 0 409.89 8.72 0 -5 -8 0 392.03 20.57 0 -6 -8 0 -0.51 8.78 0 6 8 0 8.84 8.12 0 -7 -8 0 11.67 8.89 0 7 8 0 2.94 5.95 0 2 -9 0 67.25 8.94 0 -2 9 0 61.73 9.01 0 2 -9 0 42.40 10.21 0 -1 9 0 4.86 8.37 0 1 -9 0 14.24 9.51 0 1 -9 0 7.76 8.70 0 0 -9 0 56.00 8.47 0 0 9 0 50.63 8.48 0 0 -9 0 57.24 9.63 0 -1 -9 0 56.44 9.81 0 1 9 0 70.94 8.19 0 -1 -9 0 70.05 8.54 0 2 9 0 30.15 8.02 0 -2 -9 0 14.99 9.45 0 -2 -9 0 35.43 8.13 0 -3 -9 0 325.33 9.97 0 3 9 0 336.66 9.69 0 -3 -9 0 326.76 11.32 0 -4 -9 0 477.56 15.20 0 4 9 0 508.76 10.71 0 -4 -9 0 508.75 11.25 0 -5 -9 0 1.84 8.74 0 -5 -9 0 4.37 14.45 0 5 9 0 6.55 8.50 0 -5 -9 0 0.48 13.61 0 6 9 0 0.10 8.70 0 -6 -9 0 4.94 9.21 0 1 10 0 71.10 9.09 0 -1 -10 0 48.51 10.76 0 -1 -10 0 71.55 9.30 0 -2 -10 0 404.19 12.74 0 2 10 0 299.90 11.32 0 -2 -10 0 429.47 11.35 0 -3 -10 0 23.84 12.25 0 3 10 0 31.12 8.79 0 -3 -10 0 21.92 9.09 0 -4 -10 0 28.21 12.42 0 -4 -10 0 18.20 9.46 0 -3 -10 1 -2.11 9.37 0 -3 -10 1 9.39 12.11 0 3 10 -1 2.65 8.83 0 -2 -10 1 31.06 10.61 0 -2 -10 1 45.06 9.59 0 2 10 -1 57.17 9.14 0 -1 -10 1 45.36 9.39 0 1 10 -1 43.49 11.25 0 -1 -10 1 66.84 10.97 0 6 9 -1 146.56 10.66 0 -6 -9 1 173.53 11.26 0 -5 -9 1 17.25 20.35 0 5 9 -1 16.36 8.46 0 -5 -9 1 17.59 9.15 0 -4 -9 1 95.14 9.41 0 -4 -9 1 82.40 11.96 0 4 9 -1 105.93 8.70 0 -3 -9 1 373.89 11.96 0 -3 -9 1 413.06 10.87 0 3 9 -1 395.34 10.26 0 2 9 -1 30.25 8.40 0 -2 -9 1 23.04 8.95 0 -2 -9 1 14.67 9.45 0 1 9 -1 20.84 8.06 0 -1 -9 1 7.99 9.33 0 -1 -9 1 12.77 8.32 0 0 -9 1 241.77 11.28 0 0 9 -1 270.97 10.03 0 0 -9 1 287.51 10.02 0 -1 9 -1 118.78 9.27 0 1 -9 1 130.17 10.13 0 1 -9 1 110.90 9.11 0 2 -9 1 -2.69 9.06 0 2 -9 1 -1.29 10.24 0 -2 9 -1 19.22 9.14 0 7 8 -1 123.05 9.79 0 -7 -8 1 108.82 9.83 0 -6 -8 1 6.61 9.06 0 6 8 -1 8.75 8.55 0 -5 -8 1 100.10 9.03 0 5 8 -1 75.72 8.51 0 -4 -8 1 785.99 18.50 0 4 8 -1 805.17 11.42 0 -4 -8 1 848.76 12.02 0 -3 -8 1 140.11 8.96 0 3 8 -1 152.68 8.39 0 -3 -8 1 134.92 11.71 0 -2 -8 1 77.74 8.30 0 -2 -8 1 79.42 11.79 0 2 8 -1 67.22 7.73 0 1 8 -1 95.49 8.29 0 -1 -8 1 94.35 9.53 0 -1 -8 1 99.76 8.46 0 0 -8 1 48.38 9.58 0 0 8 -1 33.09 7.72 0 0 -8 1 39.27 7.86 0 -1 8 -1 40.25 7.80 0 1 -8 1 35.86 9.34 0 1 -8 1 42.88 8.11 0 2 -8 1 387.46 10.70 0 2 -8 1 392.91 11.14 0 -2 8 -1 418.62 10.28 0 3 -8 1 101.27 8.98 0 3 -8 1 119.32 9.96 0 4 -8 1 12.71 8.56 0 4 -8 1 2.51 9.63 0 8 7 -1 5.20 9.16 0 -7 -7 1 -0.86 9.03 0 7 7 -1 -2.04 8.76 0 6 7 -1 1163.60 12.76 0 -6 -7 1 1138.01 13.46 0 -5 -7 1 614.49 11.27 0 5 7 -1 608.35 10.83 0 -4 -7 1 17.42 8.12 0 -4 -7 1 15.50 11.81 0 4 7 -1 16.90 7.48 0 3 7 -1 323.25 9.45 0 -3 -7 1 314.37 12.49 0 -3 -7 1 333.45 11.25 0 2 7 -1 423.70 9.85 0 -2 -7 1 415.10 11.11 0 -2 -7 1 434.18 9.91 0 -1 -7 1 42.49 8.98 0 1 7 -1 51.20 7.31 0 -1 -7 1 44.73 7.62 0 0 -7 1 18.65 7.46 0 0 7 -1 14.74 7.35 0 0 -7 1 14.60 9.18 0 -1 7 -1 543.14 11.67 0 1 -7 1 574.30 10.36 0 1 -7 1 553.22 11.58 0 2 -7 1 356.91 9.59 0 -2 7 -1 322.41 9.53 0 2 -7 1 342.34 10.62 0 3 -7 1 170.44 8.79 0 3 -7 1 159.85 9.86 0 4 -7 1 214.78 10.42 0 4 -7 1 213.21 9.41 0 5 -7 1 3.77 8.64 0 5 -7 1 0.39 8.97 0 8 6 -1 31.74 8.95 0 7 6 -1 586.70 10.99 0 -6 -6 1 287.29 9.61 0 6 6 -1 278.76 9.39 0 5 6 -1 104.97 8.14 0 -5 -6 1 113.41 8.40 0 4 6 -1 238.90 8.91 0 -4 -6 1 234.11 9.57 0 -4 -6 1 231.30 16.55 0 -3 -6 1 47.12 11.17 0 3 6 -1 55.05 8.01 0 -3 -6 1 61.95 8.30 0 -2 -6 1 2.47 7.61 0 2 6 -1 5.62 7.29 0 -2 -6 1 16.52 10.32 0 1 6 -1 656.24 11.01 0 -1 -6 1 650.34 12.24 0 -1 -6 1 655.55 12.58 0 0 -6 1 116.26 8.24 0 0 -6 1 123.13 10.22 0 0 6 -1 129.62 8.44 0 1 -6 1 6.70 9.17 0 -1 6 -1 6.98 7.10 0 1 -6 1 6.15 7.19 0 2 -6 1 1686.08 14.39 0 2 -6 1 1683.73 15.04 0 -2 6 -1 1727.63 14.51 0 3 -6 1 1087.79 12.38 0 3 -6 1 1027.45 12.73 0 4 -6 1 -3.15 8.66 0 4 -6 1 10.60 7.64 0 5 -6 1 29.12 9.20 0 5 -6 1 21.04 8.40 0 6 -6 1 8.54 8.89 0 6 -6 1 11.94 8.66 0 9 5 -1 102.84 7.58 0 8 5 -1 315.71 9.68 0 7 5 -1 25.58 8.23 0 6 5 -1 107.09 6.64 0 -6 -5 1 133.47 6.94 0 5 5 -1 900.56 12.19 0 -5 -5 1 946.24 12.67 0 -4 -5 1 41.03 8.54 0 4 5 -1 28.17 8.13 0 -3 -5 1 30.94 12.38 0 3 5 -1 42.61 7.89 0 -3 -5 1 27.32 8.20 0 -2 -5 1 1200.36 14.08 0 2 5 -1 1183.75 13.77 0 -2 -5 1 1202.30 16.50 0 -1 -5 1 363.47 9.86 0 1 5 -1 364.04 9.91 0 -1 -5 1 362.47 13.10 0 0 5 -1 373.92 10.96 0 0 -5 1 406.06 11.12 0 0 -5 1 392.93 9.86 0 -1 5 -1 1531.87 14.40 0 1 -5 1 1483.04 14.20 0 1 -5 1 1528.38 15.65 0 2 -5 1 627.04 12.12 0 2 -5 1 620.29 10.78 0 -2 5 -1 639.21 10.82 0 3 -5 1 2.04 7.57 0 3 -5 1 5.82 8.99 0 4 -5 1 25.66 8.30 0 4 -5 1 22.74 7.77 0 5 -5 1 111.53 8.17 0 5 -5 1 102.29 9.11 0 6 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539.50 17.24 0 7 3 1 548.42 10.23 0 8 3 1 10.87 8.14 0 8 3 1 12.14 11.40 0 9 3 1 27.37 12.82 0 9 3 1 16.98 8.67 0 7 -4 -1 7.83 9.42 0 7 -4 -1 1.13 5.81 0 6 -4 -1 7.13 8.63 0 6 -4 -1 11.23 7.48 0 5 -4 -1 682.25 10.26 0 5 -4 -1 634.44 10.94 0 4 -4 -1 220.49 8.45 0 -3 4 1 7.96 7.17 0 3 -4 -1 7.33 4.93 0 -2 4 1 628.46 10.66 0 2 -4 -1 632.04 10.54 0 -1 4 1 2009.34 14.61 0 1 -4 -1 2095.24 15.89 0 0 4 1 133.30 8.18 0 0 -4 -1 125.66 8.20 0 -1 -4 -1 118.07 6.47 0 1 4 1 119.00 6.28 0 2 4 1 152.31 8.59 0 -2 -4 -1 147.65 8.62 0 -3 -4 -1 145.71 10.39 0 3 4 1 161.13 8.74 0 -3 -4 -1 149.89 6.90 0 -4 -4 -1 2306.08 16.74 0 -4 -4 -1 2245.37 30.23 0 4 4 1 2187.22 15.01 0 5 4 1 1826.45 14.45 0 -5 -4 -1 1778.97 14.57 0 6 4 1 17.21 8.30 0 -6 -4 -1 21.26 8.39 0 7 4 1 30.90 5.70 0 8 4 1 419.78 10.04 0 9 4 1 50.18 8.59 0 7 -5 -1 -1.02 9.03 0 7 -5 -1 14.76 6.45 0 6 -5 -1 179.18 8.88 0 6 -5 -1 186.24 9.75 0 5 -5 -1 113.00 8.29 0 5 -5 -1 122.63 9.28 0 4 -5 -1 136.86 7.70 0 4 -5 -1 134.41 8.95 0 -3 5 1 635.21 9.97 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113.09 10.50 0 2 -9 2 8.54 10.91 0 2 -9 2 -1.89 10.25 0 7 8 -2 208.30 11.46 0 6 8 -2 102.87 9.23 0 -6 -8 2 112.10 9.53 0 5 8 -2 21.76 7.80 0 -5 -8 2 23.66 8.80 0 -4 -8 2 301.19 14.69 0 4 8 -2 310.18 9.81 0 -4 -8 2 324.02 12.27 0 -3 -8 2 374.48 10.71 0 3 8 -2 376.26 10.47 0 -3 -8 2 337.31 12.89 0 2 8 -2 3.49 9.76 0 -2 -8 2 1.76 10.83 0 -2 -8 2 2.53 9.61 0 1 8 -2 85.36 10.33 0 -1 -8 2 80.66 9.29 0 -1 -8 2 87.15 10.51 0 0 8 -2 169.74 8.80 0 0 -8 2 171.53 10.17 0 0 -8 2 182.68 9.41 0 1 -8 2 32.92 8.19 0 -1 8 -2 28.83 7.82 0 1 -8 2 28.68 9.37 0 2 -8 2 76.36 8.38 0 2 -8 2 79.34 9.64 0 3 -8 2 174.87 9.83 0 3 -8 2 176.47 10.50 0 4 -8 2 4.56 9.87 0 4 -8 2 14.11 9.25 0 8 7 -2 301.25 11.70 0 7 7 -2 51.20 8.98 0 -6 -7 2 13.43 8.74 0 6 7 -2 9.08 8.27 0 -5 -7 2 439.72 12.26 0 5 7 -2 421.16 9.86 0 4 7 -2 197.68 8.78 0 -4 -7 2 181.98 13.03 0 -4 -7 2 179.76 9.24 0 3 7 -2 20.21 9.20 0 -3 -7 2 10.13 9.93 0 -3 -7 2 16.62 10.11 0 -2 -7 2 132.83 9.45 0 -2 -7 2 139.23 8.79 0 2 7 -2 146.12 10.20 0 1 7 -2 102.51 9.48 0 -1 -7 2 98.21 8.83 0 -1 -7 2 90.66 8.54 0 0 -7 2 3.00 7.82 0 0 -7 2 9.37 8.76 0 0 7 -2 -5.74 9.13 0 1 -7 2 586.79 12.09 0 1 -7 2 623.34 12.30 0 -1 7 -2 608.09 10.94 0 -2 7 -2 820.79 12.41 0 2 -7 2 811.41 13.04 0 2 -7 2 815.31 10.66 0 3 -7 2 12.33 7.94 0 3 -7 2 13.93 8.63 0 4 -7 2 0.69 9.32 0 4 -7 2 8.75 8.34 0 5 -7 2 3.83 9.26 0 5 -7 2 7.92 8.60 0 8 6 -2 4.36 8.88 0 7 6 -2 54.20 8.37 0 6 6 -2 407.37 10.20 0 -5 -6 2 193.94 8.92 0 5 6 -2 183.06 8.69 0 4 6 -2 180.27 10.37 0 -4 -6 2 186.50 11.04 0 -4 -6 2 177.57 15.78 0 3 6 -2 295.72 10.81 0 -3 -6 2 291.80 12.17 0 -3 -6 2 286.93 10.28 0 2 6 -2 345.56 11.14 0 -2 -6 2 333.97 11.91 0 -2 -6 2 339.87 12.59 0 -1 -6 2 8.41 9.89 0 1 6 -2 10.13 7.35 0 -1 -6 2 30.59 8.78 0 0 -6 2 3647.57 23.04 0 0 -6 2 3647.84 21.69 0 0 6 -2 3655.89 22.68 0 -1 6 -2 961.08 12.73 0 1 -6 2 977.69 12.75 0 1 -6 2 982.55 13.07 0 2 -6 2 17.45 8.79 0 2 -6 2 13.47 7.48 0 -2 6 -2 17.41 7.61 0 3 -6 2 25.02 7.62 0 3 -6 2 26.28 8.89 0 4 -6 2 117.22 9.19 0 4 -6 2 124.44 8.24 0 5 -6 2 3.78 7.69 0 5 -6 2 1.79 9.09 0 6 -6 2 11.88 8.68 0 6 -6 2 0.73 8.97 0 9 5 -2 12.69 9.08 0 8 5 -2 174.67 9.89 0 7 5 -2 246.90 9.77 0 6 5 -2 6.53 7.89 0 -5 -5 2 421.18 10.14 0 5 5 -2 385.77 9.90 0 4 5 -2 383.95 11.87 0 -4 -5 2 417.29 10.63 0 3 5 -2 168.69 10.06 0 -3 -5 2 164.69 11.39 0 -3 -5 2 170.46 9.14 0 2 5 -2 191.58 9.33 0 -2 -5 2 176.83 9.69 0 -2 -5 2 199.14 11.97 0 -1 -5 2 2501.48 20.09 0 -1 -5 2 2457.77 19.86 0 1 5 -2 2487.69 20.12 0 0 -5 2 1411.49 16.31 0 0 -5 2 1407.95 15.52 0 0 5 -2 1439.62 16.77 0 1 -5 2 148.68 8.31 0 1 -5 2 123.95 7.62 0 -1 5 -2 133.06 8.10 0 2 -5 2 93.89 9.31 0 2 -5 2 96.05 7.97 0 -2 5 -2 95.31 7.85 0 3 -5 2 23.82 7.31 0 3 -5 2 36.67 9.01 0 4 -5 2 69.11 6.47 0 4 -5 2 63.80 7.82 0 5 -5 2 341.89 9.60 0 5 -5 2 305.38 10.18 0 6 -5 2 -0.13 7.74 0 6 -5 2 6.72 9.15 0 7 -5 2 4.60 8.83 0 7 -5 2 5.96 8.94 0 9 4 -2 244.40 11.07 0 8 4 -2 53.46 8.81 0 7 4 -2 1.11 8.25 0 6 4 -2 184.99 7.28 0 5 4 -2 37.28 8.73 0 -4 -4 2 124.76 9.44 0 4 4 -2 118.16 9.06 0 -3 -4 2 2029.22 18.49 0 3 4 -2 1962.96 17.89 0 -3 -4 2 1917.62 27.67 0 2 4 -2 1375.60 17.48 0 -2 -4 2 1347.07 19.51 0 -2 -4 2 1385.65 18.28 0 -1 -4 2 210.52 10.13 0 -1 -4 2 215.42 10.78 0 1 4 -2 217.05 11.13 0 0 -4 2 910.22 13.66 0 0 4 -2 870.50 15.31 0 0 -4 2 892.13 15.29 0 1 -4 2 3686.38 20.81 0 -1 4 -2 3655.08 25.28 0 1 -4 2 3701.48 24.85 0 2 -4 2 24.76 9.07 0 2 -4 2 28.67 9.13 0 3 -4 2 4.51 6.29 0 3 -4 2 8.00 7.71 0 4 -4 2 172.58 9.72 0 4 -4 2 175.85 8.42 0 5 -4 2 34.00 8.68 0 5 -4 2 31.78 7.82 0 6 -4 2 70.71 6.76 0 6 -4 2 54.92 5.80 0 7 -4 2 118.70 6.80 0 7 -4 2 151.45 9.44 0 7 -4 2 135.99 10.03 0 9 3 -2 3.63 9.13 0 8 3 -2 42.80 8.45 0 7 3 -2 146.64 9.01 0 6 3 -2 21.70 8.35 0 5 3 -2 55.52 8.75 0 4 3 -2 1803.76 16.20 0 -3 -3 2 593.19 12.32 0 3 3 -2 557.68 12.16 0 3 3 -2 544.18 21.26 0 -2 -3 2 266.12 13.16 0 2 3 -2 238.22 14.12 0 2 3 -2 242.08 10.87 0 -2 -3 2 246.56 12.73 0 -1 -3 2 2359.74 25.96 0 1 3 -2 2297.01 22.60 0 1 3 -2 2342.87 25.29 0 -1 -3 2 2354.88 22.43 0 0 3 -2 121.17 10.95 0 0 -3 2 107.27 10.72 0 0 3 -2 121.92 10.77 0 0 -3 2 115.78 11.02 0 1 -3 2 595.03 12.73 0 -1 3 -2 607.97 13.00 0 1 -3 2 592.83 12.64 0 -1 3 -2 603.44 12.56 0 2 -3 2 2197.91 17.93 0 2 -3 2 2150.39 18.49 0 3 -3 2 130.27 7.87 0 3 -3 2 143.81 9.89 0 4 -3 2 207.20 7.02 0 4 -3 2 204.25 9.54 0 5 -3 2 99.87 9.40 0 5 -3 2 108.81 8.32 0 6 -3 2 853.93 11.63 0 6 -3 2 812.99 10.62 0 7 -3 2 21.20 8.90 0 7 -3 2 25.64 8.63 0 7 -3 2 30.60 8.79 0 8 -3 2 11.34 9.59 0 8 -3 2 10.53 8.72 0 8 -3 2 9.30 9.20 0 9 2 -2 77.55 9.83 0 9 2 -2 74.51 13.23 0 9 2 -2 98.10 9.29 0 8 2 -2 69.21 9.03 0 8 2 -2 60.32 13.25 0 7 2 -2 85.63 8.69 0 7 2 -2 77.16 13.27 0 6 2 -2 342.56 14.34 0 6 2 -2 341.81 8.19 0 5 2 -2 1367.83 20.52 0 5 2 -2 1308.13 14.34 0 5 2 -2 1310.36 22.58 0 4 2 -2 3.97 10.12 0 4 2 -2 20.03 8.67 0 3 2 -2 544.79 16.87 0 3 2 -2 564.45 12.47 0 -2 -2 2 3458.64 33.14 0 2 2 -2 3511.88 27.56 0 2 2 -2 3311.54 33.80 0 1 2 -2 988.88 21.25 0 -1 -2 2 1047.60 23.00 0 1 2 -2 978.65 18.31 0 -1 -2 2 1006.04 19.03 0 0 -2 2 33.16 13.90 0 0 -2 2 35.34 11.44 0 0 2 -2 34.43 12.91 0 0 2 -2 33.53 11.90 0 -1 2 -2 2128.14 19.02 0 1 -2 2 2159.44 25.19 0 1 -2 2 2188.84 20.70 0 2 -2 2 1092.76 16.05 0 -2 2 -2 1152.55 14.48 0 2 -2 2 1140.45 14.67 0 3 -2 2 90.53 8.02 0 -3 2 -2 85.67 9.59 0 3 -2 2 90.08 9.58 0 4 -2 2 519.15 10.29 0 4 -2 2 518.65 11.64 0 5 -2 2 328.08 8.20 0 5 -2 2 338.63 9.46 0 5 -2 2 348.04 10.32 0 6 -2 2 99.87 7.97 0 6 -2 2 93.47 9.36 0 6 -2 2 100.68 8.50 0 7 -2 2 204.80 8.97 0 7 -2 2 213.46 9.49 0 7 -2 2 204.78 9.44 0 8 -2 2 48.96 9.46 0 8 -2 2 54.58 9.28 0 8 -2 2 47.96 9.05 0 9 -2 2 2.10 9.86 0 9 -2 2 23.00 9.72 0 9 -2 2 16.60 9.60 0 9 1 -2 3.51 9.02 0 9 1 -2 -3.71 11.84 0 9 1 -2 -2.11 8.52 0 8 1 -2 2.27 8.45 0 8 1 -2 6.36 11.18 0 8 1 -2 10.26 8.23 0 7 1 -2 257.57 12.18 0 7 1 -2 276.40 9.59 0 6 1 -2 17.99 11.23 0 6 1 -2 -1.85 8.29 0 5 1 -2 11.73 5.93 0 4 1 -2 1436.44 14.91 0 2 1 -2 176.39 10.76 0 1 1 -2 2788.22 28.23 0 -1 -1 2 2852.64 27.94 0 0 -1 2 4106.45 30.96 0 0 1 -2 3982.93 31.18 0 1 -1 2 3796.74 38.96 0 1 -1 2 3765.59 28.35 0 -1 1 -2 3760.88 28.75 0 2 -1 2 91.73 13.01 0 2 -1 2 100.81 10.93 0 -2 1 -2 89.98 11.33 0 3 -1 2 3412.62 23.14 0 -3 1 -2 3456.89 22.62 0 3 -1 2 3442.69 22.64 0 4 -1 2 839.74 13.03 0 -4 1 -2 829.36 13.31 0 4 -1 2 805.05 12.65 0 5 -1 2 105.59 9.18 0 5 -1 2 98.09 9.13 0 6 -1 2 165.71 9.19 0 6 -1 2 192.44 10.05 0 7 -1 2 102.64 8.74 0 7 -1 2 101.18 9.00 0 8 -1 2 27.59 8.10 0 8 -1 2 25.70 9.11 0 8 -1 2 15.65 6.13 0 9 -1 2 142.20 10.22 0 9 -1 2 139.19 10.11 0 9 -1 2 161.23 12.40 0 9 0 -2 5.79 6.25 0 9 0 -2 30.20 9.98 0 9 0 -2 48.78 9.45 0 8 0 -2 304.98 8.16 0 8 0 -2 293.49 10.17 0 8 0 -2 314.27 11.48 0 7 0 -2 7.48 10.48 0 7 0 -2 4.98 7.92 0 7 0 -2 6.91 7.87 0 6 0 -2 402.60 9.65 0 6 0 -2 391.40 11.13 0 5 0 -2 927.53 10.35 0 4 0 -2 4804.11 22.63 0 3 0 -2 2129.33 17.15 0 2 0 -2 371.19 11.87 0 1 0 -2 3578.03 29.54 0 1 0 -2 3606.34 29.50 0 -1 0 2 3605.30 29.66 0 0 0 -2 6.63 14.12 0 0 0 2 6.32 12.73 0 0 0 2 5.25 11.81 0 0 0 -2 6.60 12.94 0 -1 0 -2 6067.57 37.37 0 1 0 2 6061.76 43.91 0 -1 0 -2 6183.40 44.88 0 1 0 2 6206.01 37.35 0 -2 0 -2 3151.23 27.12 0 2 0 2 3127.04 25.72 0 2 0 2 3199.43 27.21 0 -2 0 -2 3098.56 25.71 0 3 0 2 13.35 9.84 0 -3 0 -2 7.71 10.05 0 3 0 2 7.25 9.81 0 4 0 2 244.42 9.93 0 4 0 2 220.71 9.98 0 -4 0 -2 230.01 10.01 0 -5 0 -2 1932.18 17.02 0 5 0 2 1926.67 15.95 0 5 0 2 1912.89 17.33 0 6 0 2 58.30 9.07 0 6 0 2 49.72 8.94 0 7 0 2 41.27 8.09 0 7 0 2 44.54 9.43 0 8 0 2 222.25 9.16 0 8 0 2 205.13 10.06 0 9 0 2 3.32 8.72 0 9 0 2 11.62 9.18 0 8 -1 -2 7.24 5.91 0 8 -1 -2 11.70 8.41 0 8 -1 -2 7.53 9.21 0 7 -1 -2 80.60 11.10 0 7 -1 -2 84.59 6.13 0 6 -1 -2 332.49 7.32 0 6 -1 -2 333.21 10.14 0 5 -1 -2 82.78 8.10 0 4 -1 -2 2052.39 15.11 0 3 -1 -2 2122.32 16.29 0 -2 1 2 732.57 12.63 0 2 -1 -2 761.42 12.85 0 -1 1 2 1295.45 17.13 0 1 -1 -2 1296.46 15.78 0 0 -1 -2 8234.83 41.91 0 0 1 2 8443.99 41.87 0 1 1 2 6345.58 36.28 0 1 1 2 6434.08 37.25 0 -1 -1 -2 6372.68 37.72 0 -1 -1 -2 6365.82 37.27 0 2 1 2 1327.34 18.04 0 -2 -1 -2 1338.02 18.94 0 2 1 2 1300.67 18.70 0 -2 -1 -2 1341.46 16.62 0 -3 -1 -2 1125.59 15.31 0 3 1 2 1107.39 15.82 0 3 1 2 1114.29 15.39 0 -3 -1 -2 1092.44 17.54 0 -4 -1 -2 1515.87 15.16 0 4 1 2 1504.93 18.67 0 4 1 2 1590.22 15.53 0 -4 -1 -2 1461.15 17.85 0 5 1 2 456.72 11.55 0 -5 -1 -2 441.72 13.66 0 5 1 2 453.53 8.75 0 6 1 2 497.59 13.26 0 6 1 2 513.17 10.87 0 7 1 2 52.47 8.78 0 7 1 2 55.91 8.30 0 8 1 2 0.73 8.24 0 8 1 2 2.58 8.95 0 9 1 2 33.51 11.37 0 9 1 2 35.71 8.95 0 8 -2 -2 94.97 7.15 0 8 -2 -2 108.66 9.93 0 7 -2 -2 142.41 6.78 0 7 -2 -2 165.52 9.61 0 6 -2 -2 102.25 8.27 0 6 -2 -2 85.21 8.99 0 5 -2 -2 139.97 6.18 0 4 -2 -2 264.36 8.57 0 3 -2 -2 23.01 7.58 0 -2 2 2 1395.53 13.74 0 2 -2 -2 1406.93 13.69 0 -1 2 2 3926.63 22.36 0 1 -2 -2 3810.70 21.69 0 0 -2 -2 403.90 9.87 0 0 2 2 408.01 11.71 0 1 2 2 375.25 11.87 0 -1 -2 -2 374.26 12.69 0 -1 -2 -2 379.32 9.98 0 -2 -2 -2 3179.60 26.05 0 2 2 2 3158.93 25.30 0 2 2 2 3276.06 21.81 0 -2 -2 -2 3167.37 20.77 0 3 2 2 704.07 11.86 0 -3 -2 -2 697.30 10.45 0 -3 -2 -2 688.22 14.01 0 3 2 2 668.94 13.44 0 4 2 2 370.88 12.88 0 -4 -2 -2 392.39 10.51 0 4 2 2 388.57 10.57 0 -4 -2 -2 383.69 12.02 0 -5 -2 -2 682.03 11.25 0 -5 -2 -2 668.36 13.82 0 5 2 2 667.51 11.33 0 5 2 2 677.94 13.36 0 -6 -2 -2 228.78 12.42 0 6 2 2 227.74 7.59 0 6 2 2 219.50 10.13 0 7 2 2 9.84 7.79 0 7 2 2 -0.75 9.63 0 8 2 2 339.36 10.78 0 8 2 2 331.27 9.68 0 9 2 2 126.29 6.99 0 9 2 2 148.66 11.91 0 8 -3 -2 21.14 10.40 0 8 -3 -2 24.75 8.97 0 7 -3 -2 -1.54 6.02 0 7 -3 -2 9.74 8.05 0 6 -3 -2 336.33 10.03 0 6 -3 -2 315.04 9.28 0 5 -3 -2 24.46 7.29 0 4 -3 -2 77.38 5.78 0 -3 3 2 1645.35 13.54 0 3 -3 -2 1602.79 13.61 0 2 -3 -2 2693.20 16.81 0 -2 3 2 2734.74 16.82 0 1 -3 -2 324.20 7.72 0 -1 3 2 363.10 9.07 0 0 3 2 45.27 7.72 0 0 -3 -2 26.06 5.95 0 -1 -3 -2 45.48 7.96 0 1 3 2 49.97 7.95 0 2 3 2 13.08 7.37 0 -2 -3 -2 15.36 5.51 0 -2 -3 -2 17.70 7.46 0 -3 -3 -2 714.91 11.88 0 -3 -3 -2 736.24 14.02 0 3 3 2 739.29 11.70 0 4 3 2 3295.81 26.41 0 4 3 2 3403.92 18.81 0 -4 -3 -2 3454.15 19.26 0 -4 -3 -2 3395.92 27.23 0 5 3 2 64.00 8.52 0 -5 -3 -2 75.54 8.51 0 -5 -3 -2 62.65 11.23 0 5 3 2 58.66 10.04 0 -6 -3 -2 33.19 10.56 0 6 3 2 33.68 6.24 0 -6 -3 -2 35.21 8.59 0 6 3 2 31.23 9.65 0 7 3 2 721.99 15.66 0 7 3 2 692.04 10.76 0 8 3 2 84.30 8.34 0 8 3 2 82.19 11.14 0 9 3 2 4.46 8.42 0 9 3 2 3.31 12.29 0 7 -4 -2 17.30 8.92 0 7 -4 -2 16.77 6.90 0 6 -4 -2 39.37 5.81 0 6 -4 -2 44.07 8.52 0 5 -4 -2 103.11 8.18 0 4 -4 -2 1055.46 11.48 0 -3 4 2 646.85 10.20 0 3 -4 -2 674.21 10.32 0 2 -4 -2 73.09 7.50 0 -2 4 2 57.03 7.40 0 -1 4 2 203.53 8.16 0 1 -4 -2 195.04 8.35 0 0 -4 -2 12.26 7.35 0 0 4 2 11.75 7.32 0 -1 -4 -2 25.71 7.64 0 1 4 2 28.73 7.47 0 2 4 2 2722.10 17.35 0 -2 -4 -2 2623.33 17.26 0 3 4 2 1218.82 12.98 0 -3 -4 -2 1165.70 16.82 0 -3 -4 -2 1181.30 12.83 0 -4 -4 -2 18.90 7.90 0 4 4 2 7.74 8.08 0 -4 -4 -2 18.43 9.38 0 5 4 2 1508.68 13.29 0 -5 -4 -2 1469.34 12.35 0 -5 -4 -2 1459.85 22.15 0 -6 -4 -2 1171.48 12.51 0 -6 -4 -2 1113.68 21.26 0 6 4 2 1073.92 12.10 0 -7 -4 -2 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-2 72.49 7.60 0 -1 6 2 84.82 7.42 0 0 6 2 378.87 8.70 0 0 -6 -2 365.63 8.61 0 -1 -6 -2 187.22 6.22 0 1 6 2 189.16 7.97 0 2 6 2 811.88 10.55 0 -2 -6 -2 783.35 10.58 0 3 6 2 2324.01 15.32 0 -3 -6 -2 2220.36 15.48 0 4 6 2 27.44 5.43 0 -4 -6 -2 36.76 7.97 0 -4 -6 -2 30.41 5.80 0 5 6 2 33.64 5.44 0 -5 -6 -2 28.74 7.89 0 -5 -6 -2 29.63 10.71 0 -6 -6 -2 329.96 7.74 0 -6 -6 -2 310.33 20.97 0 6 6 2 291.42 9.16 0 -7 -6 -2 11.39 8.18 0 7 6 2 5.10 7.73 0 8 6 2 4.95 5.74 0 -8 -6 -2 1.47 8.35 0 9 6 2 7.17 8.40 0 5 -7 -2 1.28 6.51 0 5 -7 -2 19.36 8.80 0 4 -7 -2 16.74 9.06 0 4 -7 -2 17.13 8.43 0 -3 7 2 -2.10 7.47 0 3 -7 -2 8.19 7.72 0 -2 7 2 178.06 8.30 0 2 -7 -2 163.54 8.29 0 1 -7 -2 236.07 8.58 0 -1 7 2 231.85 8.09 0 0 -7 -2 46.06 7.73 0 0 7 2 39.14 7.31 0 -1 -7 -2 1011.70 11.31 0 1 7 2 1001.59 11.21 0 2 7 2 701.11 10.18 0 -2 -7 -2 711.15 10.50 0 3 7 2 11.92 5.33 0 -3 -7 -2 12.75 7.57 0 -4 -7 -2 58.71 7.75 0 4 7 2 61.67 7.83 0 -4 -7 -2 60.90 7.72 0 -5 -7 -2 179.26 12.53 0 5 7 2 196.04 8.29 0 -5 -7 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8.93 0 1 9 2 23.89 7.92 0 -1 -9 -2 12.81 7.96 0 -2 -9 -2 90.01 8.80 0 2 9 2 101.41 8.21 0 -3 -9 -2 6.33 9.18 0 -3 -9 -2 2.74 8.00 0 3 9 2 5.40 7.69 0 -4 -9 -2 53.17 10.46 0 -4 -9 -2 60.58 8.29 0 -4 -9 -2 52.57 9.40 0 4 9 2 44.07 5.93 0 5 9 2 706.96 11.86 0 -5 -9 -2 636.31 18.36 0 -5 -9 -2 728.76 12.26 0 -5 -9 -2 677.60 17.05 0 -6 -9 -2 52.41 16.60 0 -6 -9 -2 54.14 9.76 0 6 9 2 65.20 8.90 0 -6 -9 -2 50.35 16.98 0 2 10 2 40.08 6.38 0 -2 -10 -2 36.23 10.89 0 -2 -10 -2 48.97 8.86 0 -3 -10 -2 68.01 13.02 0 -3 -10 -2 98.89 9.19 0 3 10 2 83.96 9.24 0 -5 -9 3 28.99 9.68 0 5 9 -3 24.40 8.81 0 -4 -9 3 206.38 11.03 0 -4 -9 3 180.46 14.74 0 4 9 -3 179.29 12.20 0 3 9 -3 7.34 10.49 0 -3 -9 3 12.53 10.85 0 -3 -9 3 12.53 11.20 0 2 9 -3 70.82 10.57 0 -2 -9 3 77.87 11.27 0 -2 -9 3 66.50 11.87 0 1 9 -3 161.82 11.61 0 -1 -9 3 150.56 12.22 0 -1 -9 3 166.63 12.01 0 0 -9 3 22.73 11.97 0 0 9 -3 22.04 8.91 0 0 -9 3 11.91 10.76 0 1 -9 3 53.18 9.35 0 1 -9 3 45.40 10.04 0 6 8 -3 274.79 12.79 0 -5 -8 3 7.31 8.93 0 5 8 -3 4.67 10.17 0 -4 -8 3 53.19 11.14 0 4 8 -3 55.07 10.17 0 -4 -8 3 52.34 11.93 0 -3 -8 3 400.68 12.75 0 -3 -8 3 371.04 13.34 0 3 8 -3 385.91 9.93 0 2 8 -3 333.34 9.90 0 -2 -8 3 336.84 11.79 0 -2 -8 3 314.05 10.84 0 -1 -8 3 42.40 8.99 0 1 8 -3 41.01 7.90 0 -1 -8 3 40.42 9.75 0 0 -8 3 177.99 10.11 0 0 -8 3 173.13 9.11 0 0 8 -3 178.07 8.77 0 1 -8 3 172.73 9.35 0 1 -8 3 154.77 10.31 0 -1 8 -3 156.31 11.18 0 2 -8 3 -1.80 8.13 0 2 -8 3 -11.03 9.87 0 3 -8 3 55.54 9.65 0 3 -8 3 59.01 10.80 0 7 7 -3 117.16 9.91 0 6 7 -3 18.52 9.91 0 -5 -7 3 19.34 10.57 0 5 7 -3 19.94 8.02 0 4 7 -3 114.67 8.29 0 -4 -7 3 128.36 10.50 0 -4 -7 3 127.55 12.40 0 -3 -7 3 37.68 10.17 0 3 7 -3 35.89 8.00 0 -3 -7 3 36.15 10.06 0 2 7 -3 196.55 10.32 0 -2 -7 3 212.38 11.06 0 -2 -7 3 203.51 11.20 0 -1 -7 3 1150.05 13.98 0 1 7 -3 1196.17 14.76 0 -1 -7 3 1200.28 14.87 0 0 7 -3 109.81 8.14 0 0 -7 3 106.02 8.92 0 0 -7 3 99.87 8.62 0 1 -7 3 6.73 7.46 0 1 -7 3 9.36 8.77 0 -1 7 -3 13.40 7.68 0 2 -7 3 280.39 10.13 0 2 -7 3 306.92 9.67 0 3 -7 3 74.78 9.74 0 3 -7 3 81.95 8.94 0 4 -7 3 -1.13 9.49 0 4 -7 3 3.10 8.25 0 5 -7 3 3.58 8.96 0 5 -7 3 13.53 9.15 0 8 6 -3 13.11 9.73 0 7 6 -3 27.03 8.57 0 6 6 -3 334.62 9.95 0 5 6 -3 621.98 11.41 0 -4 -6 3 207.45 14.50 0 4 6 -3 189.64 10.48 0 -4 -6 3 220.65 10.03 0 3 6 -3 54.66 7.68 0 -3 -6 3 56.15 8.32 0 -3 -6 3 49.02 9.61 0 -2 -6 3 1929.24 17.97 0 -2 -6 3 1993.51 20.32 0 2 6 -3 1944.62 19.27 0 1 6 -3 530.82 13.07 0 -1 -6 3 517.29 12.05 0 -1 -6 3 545.75 11.33 0 0 6 -3 101.90 10.07 0 0 -6 3 110.39 9.55 0 0 -6 3 116.84 10.14 0 1 -6 3 87.90 9.33 0 1 -6 3 81.56 9.35 0 -1 6 -3 79.19 9.67 0 2 -6 3 1.28 7.87 0 2 -6 3 11.83 8.15 0 3 -6 3 16.91 7.49 0 3 -6 3 8.89 8.73 0 4 -6 3 278.03 9.94 0 4 -6 3 260.33 10.77 0 5 -6 3 100.51 9.13 0 5 -6 3 98.53 9.77 0 6 -6 3 1.91 8.73 0 6 -6 3 0.37 9.20 0 8 5 -3 7.00 8.90 0 7 5 -3 241.98 9.93 0 6 5 -3 43.42 8.43 0 5 5 -3 27.99 8.31 0 4 5 -3 913.09 14.86 0 3 5 -3 353.47 12.05 0 -3 -5 3 369.17 12.56 0 -3 -5 3 341.82 12.63 0 -2 -5 3 58.03 9.94 0 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8.88 0 -2 3 -3 0.37 8.96 0 3 -3 3 323.34 10.93 0 -3 3 -3 335.22 10.52 0 3 -3 3 323.29 10.67 0 4 -3 3 117.86 8.43 0 4 -3 3 118.47 9.14 0 5 -3 3 13.43 8.05 0 5 -3 3 8.99 6.12 0 5 -3 3 17.23 7.43 0 6 -3 3 600.62 10.95 0 6 -3 3 574.69 11.09 0 6 -3 3 590.61 10.80 0 7 -3 3 402.41 11.09 0 7 -3 3 391.30 10.45 0 7 -3 3 375.47 10.71 0 8 -3 3 0.09 9.34 0 8 -3 3 8.69 9.42 0 8 -3 3 5.65 8.71 0 9 2 -3 4.62 14.20 0 9 2 -3 2.43 9.59 0 9 2 -3 11.03 6.61 0 9 2 -3 2.97 13.24 0 8 2 -3 158.47 13.63 0 8 2 -3 119.93 9.35 0 8 2 -3 121.07 9.62 0 8 2 -3 134.94 14.47 0 7 2 -3 30.47 8.32 0 7 2 -3 23.32 11.04 0 7 2 -3 26.91 9.94 0 6 2 -3 12.50 8.16 0 6 2 -3 6.09 9.55 0 5 2 -3 850.66 16.33 0 5 2 -3 830.59 12.65 0 4 2 -3 313.42 10.13 0 4 2 -3 302.92 12.11 0 3 2 -3 4.53 8.35 0 3 2 -3 3.24 9.50 0 2 2 -3 1237.29 18.79 0 2 2 -3 1249.36 18.40 0 -2 -2 3 1242.45 17.07 0 1 2 -3 6893.44 34.94 0 -1 -2 3 7290.04 34.42 0 0 -2 3 882.65 14.71 0 0 2 -3 905.19 15.41 0 1 -2 3 363.94 11.49 0 1 -2 3 374.23 17.54 0 1 -2 3 359.68 15.64 0 -1 2 -3 348.23 12.09 0 2 -2 3 19.06 8.51 0 2 -2 3 13.39 11.05 0 -2 2 -3 16.41 9.05 0 2 -2 3 13.43 8.09 0 3 -2 3 18.59 8.46 0 -3 2 -3 15.89 9.02 0 3 -2 3 26.21 8.82 0 -4 2 -3 822.91 12.32 0 4 -2 3 782.63 12.39 0 4 -2 3 796.78 10.46 0 5 -2 3 1064.07 11.25 0 5 -2 3 1066.85 13.49 0 6 -2 3 96.95 6.68 0 6 -2 3 98.82 6.83 0 6 -2 3 90.85 8.62 0 7 -2 3 80.31 9.07 0 7 -2 3 88.38 8.44 0 7 -2 3 93.26 9.05 0 8 -2 3 122.21 10.13 0 8 -2 3 123.80 9.44 0 8 -2 3 144.60 7.32 0 9 1 -3 116.23 10.25 0 9 1 -3 58.57 13.10 0 9 1 -3 3.14 8.82 0 8 1 -3 49.84 9.46 0 8 1 -3 50.48 8.90 0 8 1 -3 47.62 8.62 0 7 1 -3 25.82 8.99 0 7 1 -3 30.72 8.04 0 7 1 -3 26.41 5.77 0 6 1 -3 561.01 10.73 0 6 1 -3 558.54 10.59 0 5 1 -3 1012.12 12.89 0 5 1 -3 982.40 12.31 0 4 1 -3 242.92 9.36 0 4 1 -3 226.75 8.86 0 3 1 -3 1671.81 18.03 0 3 1 -3 1600.39 15.73 0 2 1 -3 947.23 14.48 0 2 1 -3 961.29 15.65 0 -1 -1 3 47.27 9.02 0 1 1 -3 48.08 9.48 0 1 1 -3 46.79 10.98 0 0 1 -3 1926.78 20.02 0 0 1 -3 1889.72 40.64 0 0 -1 3 1952.82 40.09 0 0 -1 3 1966.44 19.52 0 1 -1 3 10.10 9.55 0 -1 1 -3 18.85 10.23 0 1 -1 3 11.10 13.10 0 2 -1 3 467.62 13.21 0 2 -1 3 473.71 11.38 0 -2 1 -3 439.18 11.31 0 3 -1 3 1491.84 15.31 0 3 -1 3 1582.31 17.29 0 -3 1 -3 1485.59 15.40 0 -4 1 -3 3554.76 20.74 0 4 -1 3 3528.82 21.55 0 4 -1 3 3593.22 21.04 0 5 -1 3 220.73 10.02 0 5 -1 3 214.82 9.75 0 -5 1 -3 218.93 10.00 0 6 -1 3 -1.55 8.34 0 6 -1 3 -1.89 8.49 0 7 -1 3 435.10 8.45 0 7 -1 3 507.08 10.84 0 8 -1 3 114.60 7.19 0 8 -1 3 136.99 9.43 0 9 -1 3 1.13 8.91 0 9 -1 3 -0.60 9.16 0 9 -1 3 3.28 9.58 0 8 0 -3 0.38 8.65 0 8 0 -3 8.15 9.57 0 8 0 -3 8.87 8.47 0 7 0 -3 130.96 8.85 0 7 0 -3 140.23 11.41 0 7 0 -3 128.68 8.63 0 6 0 -3 204.01 8.25 0 5 0 -3 1383.06 12.08 0 4 0 -3 2273.38 16.67 0 3 0 -3 87.93 7.99 0 2 0 -3 52.66 7.83 0 2 0 -3 49.54 7.85 0 1 0 -3 406.06 12.00 0 1 0 -3 410.55 11.71 0 -1 0 3 423.42 12.29 0 0 0 3 176.16 11.04 0 0 0 3 181.96 10.98 0 0 0 -3 176.70 12.39 0 0 0 -3 169.09 11.32 0 -1 0 -3 217.37 11.46 0 -1 0 -3 216.76 14.17 0 1 0 3 204.47 10.98 0 1 0 3 218.83 13.06 0 2 0 3 3024.40 24.20 0 -2 0 -3 3103.84 24.78 0 -2 0 -3 2998.73 22.20 0 2 0 3 3074.72 22.00 0 3 0 3 2221.80 19.28 0 -3 0 -3 2219.35 19.04 0 3 0 3 2116.29 18.45 0 -3 0 -3 2105.67 18.50 0 -4 0 -3 71.03 8.85 0 4 0 3 73.87 9.35 0 4 0 3 87.41 8.78 0 -5 0 -3 1090.92 13.85 0 5 0 3 1090.71 13.64 0 5 0 3 1086.26 13.52 0 -6 0 -3 342.97 10.89 0 6 0 3 322.97 9.97 0 6 0 3 339.21 10.47 0 7 0 3 27.78 7.87 0 7 0 3 10.10 7.88 0 8 0 3 53.11 8.55 0 8 0 3 51.71 9.08 0 9 0 3 45.69 11.50 0 9 0 3 42.08 9.01 0 8 -1 -3 29.30 8.44 0 8 -1 -3 21.20 8.62 0 8 -1 -3 24.66 9.63 0 7 -1 -3 54.75 8.45 0 7 -1 -3 54.97 8.74 0 6 -1 -3 927.87 11.38 0 5 -1 -3 526.57 10.06 0 4 -1 -3 24.55 7.72 0 3 -1 -3 105.03 8.09 0 -2 1 3 1498.10 14.86 0 2 -1 -3 1429.49 14.59 0 1 -1 -3 392.55 11.16 0 -1 1 3 389.45 11.13 0 0 -1 -3 745.51 14.39 0 0 -1 -3 723.74 11.61 0 0 1 3 736.16 13.99 0 1 1 3 8799.63 38.28 0 -1 -1 -3 8724.22 38.75 0 1 1 3 8703.57 35.82 0 -1 -1 -3 8605.57 35.66 0 2 1 3 5342.59 28.80 0 -2 -1 -3 5398.52 29.29 0 -2 -1 -3 5299.44 28.36 0 2 1 3 5355.47 28.31 0 3 1 3 1315.91 15.16 0 -3 -1 -3 1297.31 15.41 0 -3 -1 -3 1290.08 15.59 0 3 1 3 1274.36 15.49 0 -4 -1 -3 369.32 12.97 0 -4 -1 -3 363.93 10.15 0 4 1 3 373.36 10.57 0 4 1 3 360.36 10.33 0 5 1 3 3.43 8.23 0 -5 -1 -3 12.66 11.04 0 5 1 3 -9.25 8.90 0 -6 -1 -3 21.15 9.04 0 6 1 3 24.96 8.79 0 6 1 3 27.36 7.95 0 7 1 3 235.69 8.98 0 7 1 3 243.20 9.82 0 8 1 3 184.75 8.97 0 8 1 3 165.58 11.41 0 9 1 3 5.69 8.40 0 9 1 3 -5.39 11.05 0 8 -2 -3 19.27 9.66 0 8 -2 -3 16.54 8.93 0 7 -2 -3 190.32 9.88 0 7 -2 -3 206.30 9.08 0 6 -2 -3 257.42 9.11 0 5 -2 -3 42.42 7.58 0 4 -2 -3 330.41 8.91 0 3 -2 -3 52.26 7.74 0 -3 2 3 57.34 7.91 0 2 -2 -3 93.91 7.62 0 -2 2 3 89.57 7.69 0 1 -2 -3 2548.89 17.96 0 -1 2 3 2601.96 17.89 0 0 -2 -3 2132.19 16.99 0 0 2 3 2112.35 16.78 0 -1 -2 -3 232.81 10.30 0 1 2 3 225.15 7.87 0 -1 -2 -3 220.47 8.03 0 2 2 3 2645.06 20.73 0 -2 -2 -3 2653.44 18.46 0 -2 -2 -3 2617.01 20.68 0 2 2 3 2678.25 19.55 0 3 2 3 2517.96 20.07 0 -3 -2 -3 2534.14 17.12 0 -3 -2 -3 2470.39 20.80 0 3 2 3 2566.32 18.20 0 -4 -2 -3 44.61 8.44 0 -4 -2 -3 49.89 8.77 0 4 2 3 48.20 8.29 0 4 2 3 50.04 8.48 0 -5 -2 -3 131.74 8.65 0 5 2 3 126.61 6.67 0 -5 -2 -3 136.29 9.47 0 5 2 3 129.36 8.72 0 -6 -2 -3 1103.10 11.05 0 6 2 3 1096.30 11.25 0 -6 -2 -3 1099.13 14.76 0 6 2 3 1104.81 14.19 0 -7 -2 -3 234.11 10.00 0 7 2 3 232.14 8.93 0 7 2 3 235.41 9.80 0 8 2 3 16.26 5.93 0 8 2 3 23.79 8.66 0 9 2 3 197.08 10.42 0 9 2 3 169.57 9.72 0 7 -3 -3 9.53 8.95 0 7 -3 -3 5.52 5.55 0 6 -3 -3 58.01 7.95 0 5 -3 -3 597.88 10.04 0 4 -3 -3 21.98 7.58 0 -3 3 3 -0.50 7.14 0 3 -3 -3 -5.26 7.02 0 -2 3 3 1009.37 11.34 0 2 -3 -3 941.67 10.52 0 1 -3 -3 1466.67 12.33 0 -1 3 3 1504.71 13.54 0 0 -3 -3 123.01 8.18 0 0 3 3 121.96 8.05 0 -1 -3 -3 293.49 9.21 0 1 3 3 335.45 9.13 0 2 3 3 1214.11 12.97 0 -2 -3 -3 1149.21 13.90 0 -2 -3 -3 1147.89 13.13 0 -3 -3 -3 190.00 8.86 0 -3 -3 -3 170.89 9.18 0 3 3 3 173.39 8.68 0 4 3 3 1236.32 15.25 0 -4 -3 -3 1258.12 13.45 0 -4 -3 -3 1240.40 15.58 0 4 3 3 1260.43 11.94 0 5 3 3 323.48 11.78 0 -5 -3 -3 343.88 9.98 0 -5 -3 -3 320.95 10.77 0 5 3 3 339.68 9.85 0 -6 -3 -3 19.03 6.03 0 6 3 3 30.93 8.36 0 -6 -3 -3 23.84 10.84 0 6 3 3 20.29 7.89 0 -7 -3 -3 391.50 9.39 0 -7 -3 -3 393.10 12.97 0 7 3 3 365.45 9.70 0 7 3 3 382.52 12.48 0 8 3 3 466.97 10.11 0 8 3 3 479.61 13.63 0 9 3 3 24.01 10.68 0 9 3 3 22.59 8.53 0 7 -4 -3 35.53 8.93 0 7 -4 -3 15.70 9.47 0 6 -4 -3 38.12 8.08 0 5 -4 -3 62.57 7.87 0 4 -4 -3 453.62 9.21 0 3 -4 -3 555.17 10.01 0 -3 4 3 600.97 10.01 0 -2 4 3 166.28 6.02 0 2 -4 -3 167.07 7.77 0 -1 4 3 24.79 7.53 0 1 -4 -3 18.77 7.59 0 0 4 3 3964.08 19.40 0 0 -4 -3 3987.75 19.39 0 -1 -4 -3 245.44 9.01 0 1 4 3 237.66 8.55 0 -2 -4 -3 89.88 8.12 0 2 4 3 83.27 5.76 0 -2 -4 -3 84.61 8.12 0 3 4 3 1586.49 13.51 0 -3 -4 -3 1565.94 13.79 0 -3 -4 -3 1544.15 16.71 0 -4 -4 -3 1401.38 16.67 0 -4 -4 -3 1422.45 13.29 0 4 4 3 1474.99 13.21 0 -5 -4 -3 137.89 9.19 0 5 4 3 134.09 8.74 0 -5 -4 -3 128.47 9.04 0 -6 -4 -3 84.33 8.38 0 -6 -4 -3 81.61 10.65 0 6 4 3 78.48 6.17 0 -7 -4 -3 147.53 11.63 0 7 4 3 167.31 10.91 0 -7 -4 -3 162.65 8.88 0 7 4 3 146.09 6.43 0 8 4 3 -0.71 12.06 0 8 4 3 5.15 5.98 0 9 4 3 71.94 13.51 0 9 4 3 63.83 6.70 0 6 -5 -3 -4.86 8.29 0 6 -5 -3 -1.16 6.37 0 5 -5 -3 138.17 8.53 0 4 -5 -3 296.34 8.87 0 -3 5 3 2.43 7.00 0 3 -5 -3 4.94 5.09 0 2 -5 -3 182.69 8.21 0 -2 5 3 173.25 8.11 0 -1 5 3 259.52 8.79 0 1 -5 -3 273.94 8.95 0 0 5 3 43.20 7.17 0 0 -5 -3 36.39 5.44 0 -1 -5 -3 652.12 10.24 0 1 5 3 644.46 9.95 0 2 5 3 1461.36 12.77 0 -2 -5 -3 1455.23 13.14 0 -3 -5 -3 474.51 10.55 0 3 5 3 463.38 7.77 0 -3 -5 -3 474.74 9.59 0 4 5 3 312.07 9.05 0 -4 -5 -3 314.76 9.90 0 -4 -5 -3 310.06 7.61 0 -5 -5 -3 688.19 14.37 0 -5 -5 -3 691.54 10.82 0 5 5 3 723.41 10.60 0 -6 -5 -3 90.68 8.22 0 -6 -5 -3 96.02 12.28 0 6 5 3 83.41 7.91 0 -7 -5 -3 87.31 8.26 0 -7 -5 -3 80.75 12.74 0 7 5 3 93.41 8.13 0 -8 -5 -3 570.91 10.75 0 8 5 3 520.61 10.72 0 9 5 3 74.24 8.73 0 5 -6 -3 17.02 8.32 0 4 -6 -3 8.47 7.96 0 -4 6 3 6.54 5.54 0 -3 6 3 201.20 8.23 0 3 -6 -3 184.91 8.33 0 -2 6 3 131.60 7.58 0 2 -6 -3 136.89 5.99 0 1 -6 -3 -4.90 7.25 0 -1 6 3 4.92 7.02 0 0 -6 -3 494.75 9.50 0 0 6 3 461.92 9.17 0 -1 -6 -3 1318.29 12.34 0 1 6 3 1322.51 12.15 0 -2 -6 -3 84.99 5.89 0 2 6 3 92.90 7.81 0 -3 -6 -3 471.40 10.32 0 3 6 3 489.18 9.42 0 -3 -6 -3 462.77 9.76 0 4 6 3 460.71 9.59 0 -4 -6 -3 458.85 9.92 0 -4 -6 -3 452.09 11.83 0 5 6 3 117.81 7.90 0 -5 -6 -3 108.14 8.30 0 -5 -6 -3 111.72 8.40 0 -6 -6 -3 4.61 5.88 0 6 6 3 -3.10 7.81 0 -6 -6 -3 8.66 9.75 0 -7 -6 -3 419.12 9.72 0 -7 -6 -3 395.39 18.30 0 7 6 3 417.65 9.73 0 -8 -6 -3 196.73 9.40 0 8 6 3 187.20 9.16 0 -9 -6 -3 34.84 6.54 0 9 6 3 6.75 8.44 0 4 -7 -3 12.76 8.46 0 3 -7 -3 12.31 5.18 0 -3 7 3 -4.19 7.81 0 -2 7 3 169.15 7.97 0 2 -7 -3 201.57 8.22 0 1 -7 -3 1137.11 10.68 0 -1 7 3 1169.85 11.79 0 0 -7 -3 16.04 7.25 0 0 7 3 4.77 6.96 0 -1 -7 -3 31.61 7.24 0 1 7 3 25.94 7.21 0 2 7 3 942.11 10.87 0 -2 -7 -3 999.35 10.98 0 3 7 3 593.16 9.31 0 -3 -7 -3 574.77 9.76 0 -4 -7 -3 8.52 5.29 0 4 7 3 3.47 5.03 0 -4 -7 -3 7.14 7.64 0 5 7 3 11.85 7.54 0 -5 -7 -3 17.55 8.06 0 -5 -7 -3 19.30 7.80 0 6 7 3 161.86 8.27 0 -6 -7 -3 189.59 8.82 0 -6 -7 -3 163.71 13.52 0 7 7 3 24.32 6.14 0 -7 -7 -3 24.86 18.24 0 -7 -7 -3 26.15 8.50 0 -8 -7 -3 201.49 9.86 0 8 7 3 18.29 8.42 0 -3 8 3 1.50 8.34 0 3 -8 -3 56.15 9.06 0 2 -8 -3 207.38 9.35 0 -2 8 3 258.61 9.14 0 -1 8 3 34.17 7.86 0 1 -8 -3 40.61 8.36 0 0 8 3 72.46 8.25 0 0 -8 -3 73.81 8.07 0 1 8 3 282.06 8.46 0 -1 -8 -3 259.00 8.90 0 -2 -8 -3 41.76 7.57 0 2 8 3 49.75 7.56 0 -3 -8 -3 2.15 7.51 0 3 8 3 8.23 5.53 0 -4 -8 -3 412.10 10.43 0 4 8 3 436.81 10.03 0 -4 -8 -3 444.71 9.89 0 5 8 3 74.72 5.79 0 -5 -8 -3 80.45 8.22 0 -5 -8 -3 89.23 10.19 0 6 8 3 15.39 8.27 0 -6 -8 -3 -4.30 7.93 0 -6 -8 -3 5.19 11.99 0 7 8 3 203.25 9.30 0 -7 -8 -3 181.16 7.67 0 1 -9 -3 150.81 9.22 0 -1 9 3 113.51 9.17 0 0 -9 -3 251.42 9.75 0 0 9 3 297.53 9.73 0 -1 -9 -3 5.73 8.34 0 1 9 3 18.41 7.89 0 2 9 3 19.67 7.75 0 -2 -9 -3 31.29 7.66 0 -3 -9 -3 282.04 9.13 0 3 9 3 300.14 9.44 0 -4 -9 -3 43.22 10.49 0 4 9 3 21.52 8.13 0 -4 -9 -3 28.08 8.32 0 5 9 3 76.63 6.33 0 -5 -9 -3 74.17 8.90 0 -5 -9 -3 72.57 11.20 0 -6 -9 -3 83.55 13.70 0 6 9 3 102.94 9.41 0 -6 -9 -3 103.75 7.58 0 -6 -9 -3 99.56 12.81 0 -4 -9 4 251.04 13.97 0 -4 -9 4 227.37 14.96 0 4 9 -4 278.41 12.85 0 3 9 -4 45.80 11.47 0 -3 -9 4 58.00 12.40 0 -3 -9 4 27.05 11.58 0 2 9 -4 7.63 12.00 0 -2 -9 4 9.86 9.20 0 -2 -9 4 14.15 12.13 0 1 9 -4 53.06 13.03 0 -1 -9 4 59.13 11.87 0 -1 -9 4 60.70 9.82 0 0 -9 4 94.97 10.62 0 0 -9 4 105.49 12.66 0 1 -9 4 72.10 10.30 0 1 -9 4 52.92 11.80 0 6 8 -4 16.79 9.35 0 5 8 -4 139.10 10.03 0 -4 -8 4 4.94 10.71 0 4 8 -4 -2.45 8.14 0 -4 -8 4 4.28 12.03 0 3 8 -4 26.86 9.94 0 -3 -8 4 25.45 10.79 0 -3 -8 4 24.69 10.28 0 -2 -8 4 467.77 13.58 0 -2 -8 4 546.31 16.47 0 2 8 -4 532.47 14.43 0 -1 -8 4 189.24 10.06 0 -1 -8 4 182.31 12.41 0 1 8 -4 160.23 11.44 0 0 -8 4 -1.44 9.34 0 0 -8 4 -0.08 10.11 0 0 8 -4 -1.50 9.95 0 1 -8 4 265.17 10.49 0 1 -8 4 235.37 12.28 0 2 -8 4 119.28 11.32 0 2 -8 4 116.77 10.33 0 3 -8 4 12.44 8.66 0 3 -8 4 23.10 10.00 0 7 7 -4 98.63 9.68 0 6 7 -4 43.42 8.73 0 5 7 -4 71.23 10.39 0 4 7 -4 75.17 10.32 0 -4 -7 4 64.20 10.33 0 -3 -7 4 1006.41 16.76 0 3 7 -4 969.83 15.77 0 -3 -7 4 926.60 15.62 0 2 7 -4 245.57 11.51 0 -2 -7 4 256.90 13.86 0 -2 -7 4 242.72 9.68 0 1 7 -4 313.62 12.40 0 -1 -7 4 312.08 12.49 0 -1 -7 4 318.05 10.21 0 0 -7 4 261.76 11.78 0 0 7 -4 257.55 11.94 0 0 -7 4 266.38 10.03 0 1 -7 4 63.78 9.85 0 1 -7 4 73.74 9.02 0 2 -7 4 12.73 8.43 0 2 -7 4 -0.89 9.40 0 3 -7 4 194.34 9.52 0 3 -7 4 173.68 7.79 0 4 -7 4 66.22 7.10 0 4 -7 4 54.17 10.50 0 7 6 -4 2.66 8.63 0 6 6 -4 262.61 10.11 0 5 6 -4 217.16 9.30 0 4 6 -4 1010.92 15.08 0 -4 -6 4 999.59 19.36 0 -3 -6 4 629.35 15.00 0 3 6 -4 605.21 14.00 0 -3 -6 4 595.22 13.24 0 -2 -6 4 682.03 17.20 0 -2 -6 4 644.47 12.02 0 2 6 -4 663.24 14.97 0 -1 -6 4 53.10 10.65 0 -1 -6 4 54.11 8.45 0 1 6 -4 55.35 11.22 0 0 -6 4 97.88 9.00 0 0 -6 4 106.21 11.87 0 0 6 -4 99.66 11.60 0 1 -6 4 3.98 6.23 0 1 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9.16 0 8 4 -4 118.62 10.47 0 7 4 -4 341.64 11.14 0 6 4 -4 50.07 10.52 0 5 4 -4 82.56 15.96 0 5 4 -4 93.97 9.14 0 4 4 -4 779.91 13.00 0 4 4 -4 720.88 18.36 0 -3 -4 4 27.05 9.73 0 3 4 -4 36.81 10.59 0 3 4 -4 30.94 9.77 0 2 4 -4 149.85 12.26 0 2 4 -4 132.16 11.58 0 -2 -4 4 142.93 8.88 0 1 4 -4 854.67 25.60 0 -1 -4 4 840.95 12.45 0 1 4 -4 816.88 15.24 0 0 4 -4 62.44 9.36 0 0 -4 4 54.24 17.50 0 0 -4 4 47.39 8.53 0 1 -4 4 182.05 12.54 0 -1 4 -4 174.34 10.03 0 1 -4 4 188.20 9.73 0 2 -4 4 644.93 12.82 0 -2 4 -4 642.09 9.77 0 2 -4 4 640.48 11.44 0 3 -4 4 228.21 10.06 0 3 -4 4 220.66 10.69 0 -3 4 -4 235.10 7.89 0 4 -4 4 78.63 10.66 0 4 -4 4 79.90 8.01 0 4 -4 4 84.57 8.82 0 5 -4 4 292.44 9.52 0 5 -4 4 244.99 11.67 0 5 -4 4 289.87 9.68 0 6 -4 4 78.16 8.74 0 6 -4 4 63.42 8.97 0 6 -4 4 66.52 8.87 0 7 -4 4 10.28 9.01 0 7 -4 4 25.50 9.19 0 7 -4 4 21.42 8.98 0 8 3 -4 109.65 22.55 0 8 3 -4 107.08 9.62 0 8 3 -4 91.67 9.50 0 8 3 -4 105.93 23.39 0 7 3 -4 29.22 8.88 0 7 3 -4 28.52 13.59 0 7 3 -4 24.55 15.71 0 7 3 -4 22.16 8.87 0 6 3 -4 641.63 11.33 0 6 3 -4 611.16 17.75 0 5 3 -4 73.21 8.94 0 5 3 -4 65.67 12.09 0 4 3 -4 245.56 10.13 0 4 3 -4 240.10 12.56 0 3 3 -4 936.71 16.26 0 3 3 -4 970.02 14.88 0 2 3 -4 2852.07 23.57 0 2 3 -4 2981.90 29.28 0 -2 -3 4 2938.16 21.89 0 1 3 -4 79.92 9.11 0 -1 -3 4 71.07 8.07 0 0 -3 4 44.10 8.57 0 0 3 -4 44.44 8.93 0 -1 3 -4 1061.85 13.66 0 1 -3 4 1140.17 25.64 0 1 -3 4 1118.36 13.80 0 1 -3 4 1090.31 23.21 0 2 -3 4 418.60 10.60 0 2 -3 4 412.85 13.71 0 -2 3 -4 414.70 11.11 0 2 -3 4 399.90 12.16 0 3 -3 4 76.21 8.73 0 -3 3 -4 91.92 8.96 0 3 -3 4 73.64 7.99 0 3 -3 4 90.81 8.67 0 4 -3 4 537.01 10.95 0 4 -3 4 545.87 11.82 0 -4 3 -4 529.71 9.08 0 4 -3 4 531.83 11.08 0 5 -3 4 55.82 8.49 0 5 -3 4 49.15 7.69 0 5 -3 4 52.57 6.18 0 6 -3 4 78.50 8.43 0 6 -3 4 80.05 8.79 0 6 -3 4 68.09 8.29 0 7 -3 4 219.02 9.60 0 7 -3 4 199.75 7.87 0 7 -3 4 192.84 9.88 0 8 -3 4 25.84 9.16 0 8 -3 4 29.81 9.49 0 8 -3 4 38.59 9.57 0 8 2 -4 60.87 11.98 0 8 2 -4 41.99 9.22 0 8 2 -4 62.22 8.98 0 8 2 -4 67.34 13.06 0 7 2 -4 240.87 9.77 0 7 2 -4 240.17 12.77 0 7 2 -4 251.20 9.59 0 7 2 -4 257.96 12.69 0 6 2 -4 7.05 8.73 0 6 2 -4 18.91 7.70 0 6 2 -4 15.28 9.39 0 5 2 -4 9.37 8.90 0 5 2 -4 8.57 7.73 0 5 2 -4 10.09 9.88 0 4 2 -4 582.51 11.84 0 4 2 -4 538.59 10.94 0 4 2 -4 579.17 13.70 0 3 2 -4 940.59 15.66 0 3 2 -4 906.91 13.98 0 3 2 -4 915.16 14.43 0 2 2 -4 441.36 12.84 0 -2 -2 4 452.76 11.03 0 2 2 -4 423.67 13.04 0 2 2 -4 435.50 14.37 0 1 2 -4 1699.78 30.70 0 1 2 -4 1751.47 32.96 0 1 2 -4 1650.13 16.99 0 -1 -2 4 1737.62 16.63 0 0 -2 4 26.47 5.99 0 0 2 -4 27.00 6.48 0 -1 2 -4 388.19 10.97 0 1 -2 4 406.96 10.52 0 1 -2 4 396.88 20.02 0 1 -2 4 396.59 19.29 0 2 -2 4 1723.21 15.47 0 2 -2 4 1785.49 22.86 0 -2 2 -4 1682.28 15.47 0 3 -2 4 1315.47 16.41 0 3 -2 4 1266.80 13.50 0 -3 2 -4 1271.24 14.21 0 4 -2 4 6.12 8.54 0 -4 2 -4 6.04 8.63 0 4 -2 4 8.94 8.45 0 5 -2 4 193.88 9.65 0 -5 2 -4 196.41 9.80 0 5 -2 4 219.82 9.53 0 6 -2 4 771.69 11.88 0 6 -2 4 801.51 11.59 0 7 -2 4 129.84 9.27 0 7 -2 4 126.48 8.83 0 7 -2 4 143.00 9.16 0 8 -2 4 19.33 8.83 0 8 -2 4 23.87 9.28 0 8 -2 4 15.47 8.92 0 8 1 -4 71.54 9.40 0 8 1 -4 69.03 11.63 0 8 1 -4 53.57 6.92 0 8 1 -4 89.02 11.27 0 7 1 -4 1.61 7.93 0 7 1 -4 4.10 8.39 0 7 1 -4 8.46 8.16 0 6 1 -4 76.08 8.38 0 6 1 -4 90.66 10.17 0 6 1 -4 79.38 8.66 0 5 1 -4 1334.20 12.43 0 5 1 -4 1497.48 17.10 0 4 1 -4 181.56 10.04 0 4 1 -4 170.86 8.50 0 3 1 -4 19.48 7.28 0 3 1 -4 8.93 7.62 0 2 1 -4 1024.91 14.70 0 2 1 -4 1025.01 13.82 0 -1 -1 4 181.51 8.95 0 1 1 -4 173.02 11.22 0 1 1 -4 168.67 9.16 0 0 -1 4 343.60 15.94 0 0 -1 4 316.62 10.46 0 0 1 -4 342.62 16.07 0 0 1 -4 332.68 10.65 0 1 -1 4 1095.42 21.45 0 -1 1 -4 1088.17 22.63 0 -1 1 -4 1079.56 13.97 0 1 -1 4 1087.17 13.64 0 2 -1 4 265.04 12.77 0 -2 1 -4 240.31 10.27 0 2 -1 4 265.46 10.02 0 3 -1 4 -0.61 8.71 0 -3 1 -4 3.81 8.80 0 3 -1 4 4.10 8.31 0 -4 1 -4 1121.74 13.55 0 4 -1 4 1159.88 14.24 0 4 -1 4 1171.92 13.62 0 -5 1 -4 2152.63 14.91 0 5 -1 4 2250.13 18.11 0 5 -1 4 2169.23 16.21 0 6 -1 4 96.01 8.79 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0 6 -4 5 198.61 9.69 0 7 -4 5 -1.54 8.88 0 7 -4 5 30.38 8.90 0 7 -4 5 27.85 9.37 0 8 3 -5 73.02 10.21 0 8 3 -5 77.50 10.70 0 8 3 -5 100.30 18.35 0 8 3 -5 102.16 18.93 0 7 3 -5 31.06 12.78 0 7 3 -5 26.52 9.11 0 7 3 -5 20.45 8.86 0 6 3 -5 88.49 9.12 0 6 3 -5 81.86 12.50 0 6 3 -5 82.40 10.29 0 5 3 -5 650.78 12.20 0 5 3 -5 595.21 11.64 0 5 3 -5 672.26 16.56 0 4 3 -5 114.25 10.91 0 4 3 -5 107.70 9.37 0 4 3 -5 99.16 10.24 0 3 3 -5 5.35 9.62 0 3 3 -5 0.15 10.83 0 3 3 -5 8.31 10.09 0 -2 -3 5 472.39 10.27 0 2 3 -5 453.78 16.41 0 2 3 -5 474.80 16.34 0 2 3 -5 450.93 12.72 0 1 3 -5 628.87 11.76 0 -1 -3 5 645.91 11.02 0 0 3 -5 40.69 9.04 0 0 -3 5 34.11 8.22 0 -1 3 -5 316.59 10.81 0 1 -3 5 314.19 9.65 0 -2 3 -5 1710.32 14.81 0 2 -3 5 1693.37 14.57 0 2 -3 5 1725.63 23.45 0 2 -3 5 1749.88 24.29 0 3 -3 5 319.81 12.84 0 -3 3 -5 306.49 10.34 0 3 -3 5 300.94 10.16 0 3 -3 5 301.20 9.84 0 4 -3 5 240.33 10.74 0 4 -3 5 268.49 10.58 0 -4 3 -5 245.49 7.53 0 4 -3 5 278.53 9.49 0 -5 3 -5 78.84 8.87 0 5 -3 5 74.02 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489.68 8.21 0 -2 -4 -9 460.14 9.97 0 -2 -4 -9 462.95 9.86 0 2 4 9 496.77 9.80 0 -3 -4 -9 28.48 8.03 0 3 4 9 25.63 7.77 0 -3 -4 -9 15.28 7.89 0 4 4 9 33.34 7.72 0 -4 -4 -9 36.60 8.49 0 -4 -4 -9 27.50 8.30 0 5 4 9 199.23 9.46 0 -5 -4 -9 179.35 9.75 0 -5 -4 -9 195.04 9.50 0 6 4 9 62.61 8.94 0 -6 -4 -9 43.39 8.74 0 -6 -4 -9 38.43 8.93 0 7 4 9 -0.41 9.00 0 -7 -4 -9 3.26 9.51 0 -7 -4 -9 8.51 9.21 0 2 -5 -9 30.61 8.89 0 2 -5 -9 26.69 9.16 0 -2 5 9 30.98 9.07 0 1 -5 -9 15.29 8.71 0 1 -5 -9 1.88 8.24 0 -1 5 9 2.20 8.40 0 0 -5 -9 131.82 9.43 0 0 5 9 162.73 7.19 0 0 -5 -9 166.39 8.93 0 1 5 9 214.76 8.77 0 -1 -5 -9 175.01 8.73 0 -1 -5 -9 192.48 8.87 0 2 5 9 73.04 8.09 0 -2 -5 -9 72.24 8.49 0 -2 -5 -9 83.85 8.40 0 -3 -5 -9 197.71 9.05 0 3 5 9 208.55 8.59 0 -3 -5 -9 201.81 9.11 0 4 5 9 56.90 7.97 0 -4 -5 -9 56.33 8.58 0 -4 -5 -9 49.46 8.39 0 5 5 9 30.65 8.16 0 -5 -5 -9 21.29 8.76 0 -5 -5 -9 37.75 8.80 0 6 5 9 85.20 9.42 0 -6 -5 -9 96.75 9.64 0 -6 -5 -9 90.05 9.86 0 0 -6 -9 30.16 6.16 0 0 -6 -9 52.12 8.63 0 0 6 9 36.21 6.21 0 1 6 9 84.08 6.31 0 -1 -6 -9 77.58 8.69 0 -1 -6 -9 80.40 6.37 0 2 6 9 165.03 7.00 0 -2 -6 -9 168.77 9.28 0 -2 -6 -9 174.00 9.36 0 -3 -6 -9 8.52 8.32 0 3 6 9 5.14 8.23 0 -3 -6 -9 15.43 8.63 0 -4 -6 -9 1.01 8.38 0 4 6 9 -0.04 8.07 0 -4 -6 -9 0.55 8.59 0 5 6 9 205.14 9.52 0 -5 -6 -9 193.79 10.25 0 -5 -6 -9 208.90 10.19 0 -3 -7 -9 15.62 8.69 0 3 7 9 9.18 8.65 0 -1 -5 10 115.31 9.49 0 1 5 -10 81.61 10.44 0 0 5 -10 14.13 10.54 0 0 -5 10 22.91 9.62 0 -1 5 -10 58.87 10.29 0 1 -5 10 75.11 9.53 0 -2 -4 10 83.99 9.41 0 2 4 -10 84.87 10.30 0 -1 -4 10 43.74 9.01 0 1 4 -10 34.40 9.87 0 0 -4 10 273.92 9.98 0 0 4 -10 258.17 10.83 0 -1 4 -10 74.20 9.42 0 1 -4 10 70.42 9.12 0 -2 4 -10 14.24 6.79 0 2 -4 10 5.59 6.47 0 -3 4 -10 22.49 9.80 0 3 -4 10 23.94 9.46 0 3 3 -10 -1.70 9.50 0 2 3 -10 66.62 9.94 0 -1 -3 10 291.88 10.17 0 1 3 -10 303.11 10.52 0 0 -3 10 63.53 8.62 0 0 3 -10 66.39 8.95 0 -1 3 -10 -1.44 8.77 0 1 -3 10 13.10 8.32 0 -2 3 -10 33.76 9.24 0 2 -3 10 39.28 8.79 0 -3 3 -10 71.23 9.51 0 3 -3 10 73.15 8.92 0 -4 3 -10 89.95 9.91 0 4 -3 10 53.13 7.16 0 4 2 -10 12.20 11.37 0 3 2 -10 45.85 12.98 0 3 2 -10 45.75 14.13 0 3 2 -10 61.39 9.72 0 2 2 -10 119.90 17.91 0 2 2 -10 117.06 9.91 0 2 2 -10 114.51 16.87 0 -1 -2 10 15.52 7.93 0 1 2 -10 26.15 8.89 0 0 -2 10 21.82 8.34 0 0 2 -10 25.61 8.91 0 1 -2 10 341.02 9.66 0 -1 2 -10 319.46 7.77 0 -2 2 -10 44.89 9.06 0 2 -2 10 37.82 8.23 0 -3 2 -10 66.32 9.32 0 3 -2 10 49.95 8.69 0 -4 2 -10 224.12 10.35 0 4 -2 10 237.13 15.28 0 4 -2 10 226.26 9.91 0 5 -2 10 96.87 13.66 0 -5 2 -10 80.38 9.93 0 5 -2 10 1.03 8.69 0 4 1 -10 137.63 10.55 0 4 1 -10 188.94 10.56 0 3 1 -10 9.89 10.28 0 3 1 -10 21.69 8.99 0 2 1 -10 121.03 11.36 0 2 1 -10 122.98 9.18 0 1 1 -10 188.22 9.34 0 1 1 -10 186.70 11.92 0 0 -1 10 476.09 10.19 0 0 1 -10 480.51 16.97 0 0 1 -10 483.76 10.33 0 1 -1 10 111.40 8.28 0 -1 1 -10 123.36 15.36 0 -1 1 -10 102.34 6.32 0 1 -1 10 120.92 12.93 0 2 -1 10 100.56 8.62 0 -2 1 -10 105.68 13.44 0 -2 1 -10 96.61 8.85 0 2 -1 10 108.14 12.18 0 -3 1 -10 198.82 9.37 0 3 -1 10 216.27 13.22 0 3 -1 10 201.25 9.13 0 4 -1 10 24.55 10.23 0 -4 1 -10 24.11 8.97 0 4 -1 10 18.46 6.10 0 5 -1 10 41.13 10.73 0 -5 1 -10 44.20 9.79 0 5 -1 10 34.84 8.64 0 4 0 -10 22.45 9.07 0 4 0 -10 23.07 9.39 0 3 0 -10 42.16 10.89 0 3 0 -10 60.68 8.78 0 2 0 -10 212.82 10.04 0 2 0 -10 207.88 9.57 0 1 0 -10 384.87 9.99 0 1 0 -10 378.54 11.25 0 0 0 10 14.29 9.28 0 0 0 -10 12.16 8.17 0 0 0 -10 11.92 8.10 0 1 0 10 157.28 11.20 0 1 0 10 157.15 8.60 0 -1 0 -10 160.81 11.72 0 -1 0 -10 148.53 9.04 0 2 0 10 313.97 9.50 0 2 0 10 342.62 10.90 0 -2 0 -10 343.16 11.86 0 -2 0 -10 337.49 9.87 0 3 0 10 112.64 8.60 0 -3 0 -10 105.33 12.10 0 -3 0 -10 104.72 9.09 0 3 0 10 108.12 10.30 0 4 0 10 94.63 6.83 0 -4 0 -10 106.85 11.56 0 4 0 10 97.58 8.81 0 -4 0 -10 90.91 8.77 0 5 0 10 7.35 10.21 0 -5 0 -10 3.90 8.40 0 5 0 10 3.41 8.07 0 6 0 10 1.61 11.17 0 -6 0 -10 8.30 6.95 0 6 0 10 -2.63 8.25 0 3 -1 -10 78.21 11.36 0 3 -1 -10 108.28 9.44 0 2 -1 -10 8.03 10.27 0 2 -1 -10 1.32 8.68 0 1 -1 -10 95.52 8.85 0 1 -1 -10 88.42 8.78 0 -1 1 10 80.14 10.34 0 0 1 10 396.55 10.07 0 0 -1 -10 361.00 7.47 0 0 -1 -10 386.74 10.27 0 1 1 10 46.95 9.81 0 -1 -1 -10 63.93 10.28 0 -1 -1 -10 37.60 8.25 0 2 1 10 164.90 8.66 0 2 1 10 163.40 10.45 0 -2 -1 -10 161.61 11.09 0 -2 -1 -10 154.18 6.82 0 3 1 10 408.35 9.78 0 -3 -1 -10 412.32 13.07 0 -3 -1 -10 389.50 10.16 0 3 1 10 397.45 11.80 0 4 1 10 8.72 8.13 0 -4 -1 -10 -2.62 8.58 0 4 1 10 0.29 8.14 0 -4 -1 -10 3.97 6.15 0 5 1 10 87.62 8.99 0 -5 -1 -10 103.26 9.65 0 5 1 10 93.06 10.85 0 -5 -1 -10 84.76 6.99 0 6 1 10 95.71 9.44 0 -6 -1 -10 79.61 9.93 0 6 1 10 86.26 9.49 0 -6 -1 -10 82.07 7.29 0 3 -2 -10 5.47 8.69 0 3 -2 -10 11.60 9.05 0 -2 2 10 39.46 8.37 0 2 -2 -10 31.28 10.16 0 2 -2 -10 26.15 6.26 0 1 -2 -10 150.07 9.46 0 1 -2 -10 142.57 6.62 0 -1 2 10 178.04 9.37 0 0 2 10 134.02 8.58 0 0 -2 -10 144.02 8.61 0 0 -2 -10 140.88 8.88 0 1 2 10 179.86 9.04 0 -1 -2 -10 181.74 9.46 0 -1 -2 -10 180.99 8.74 0 2 2 10 258.70 9.43 0 -2 -2 -10 263.05 9.93 0 -2 -2 -10 223.17 8.93 0 -3 -2 -10 12.04 10.48 0 -3 -2 -10 8.30 8.35 0 3 2 10 12.38 8.05 0 4 2 10 2.96 8.28 0 -4 -2 -10 21.87 10.81 0 4 2 10 12.45 7.80 0 -4 -2 -10 10.19 8.61 0 5 2 10 145.33 9.47 0 -5 -2 -10 137.58 9.85 0 5 2 10 147.25 9.21 0 -5 -2 -10 149.88 9.64 0 6 2 10 29.40 8.95 0 6 2 10 18.55 9.05 0 -6 -2 -10 28.84 9.36 0 -6 -2 -10 19.31 9.41 0 -2 3 10 -2.80 8.74 0 2 -3 -10 10.33 8.51 0 2 -3 -10 16.92 8.61 0 1 -3 -10 13.35 8.42 0 -1 3 10 5.99 8.26 0 1 -3 -10 13.20 8.30 0 0 -3 -10 562.20 10.92 0 0 3 10 626.87 11.41 0 0 -3 -10 594.20 11.63 0 1 3 10 453.56 10.73 0 -1 -3 -10 437.48 10.92 0 -1 -3 -10 418.00 8.28 0 2 3 10 76.09 7.98 0 -2 -3 -10 67.15 9.03 0 -2 -3 -10 61.18 8.78 0 -3 -3 -10 8.25 8.44 0 -3 -3 -10 11.50 5.96 0 3 3 10 8.35 8.19 0 -4 -3 -10 307.45 10.48 0 4 3 10 293.13 9.88 0 -4 -3 -10 254.33 9.65 0 5 3 10 79.91 8.88 0 -5 -3 -10 78.07 9.22 0 -5 -3 -10 79.47 6.71 0 6 3 10 -6.44 8.53 0 6 3 10 0.29 9.04 0 -6 -3 -10 -0.67 9.55 0 -6 -3 -10 12.00 9.25 0 1 -4 -10 194.07 10.21 0 -1 4 10 256.49 9.95 0 1 -4 -10 208.97 7.93 0 0 4 10 21.20 8.72 0 0 -4 -10 24.69 6.33 0 0 -4 -10 28.45 8.62 0 1 4 10 12.02 8.57 0 -1 -4 -10 11.26 8.77 0 -1 -4 -10 11.67 8.25 0 2 4 10 114.10 8.89 0 -2 -4 -10 107.19 9.05 0 -2 -4 -10 115.18 8.86 0 -3 -4 -10 104.28 9.24 0 -3 -4 -10 82.38 9.00 0 3 4 10 90.28 8.90 0 -4 -4 -10 33.63 8.84 0 4 4 10 27.75 8.66 0 -4 -4 -10 31.79 8.80 0 -5 -4 -10 58.48 9.75 0 5 4 10 78.18 9.19 0 -5 -4 -10 72.22 9.14 0 -6 -4 -10 16.23 9.52 0 0 5 10 0.57 8.66 0 0 -5 -10 -0.31 6.18 0 0 -5 -10 4.56 8.83 0 1 5 10 195.88 9.70 0 -1 -5 -10 182.08 9.63 0 -1 -5 -10 202.01 9.77 0 2 5 10 71.20 8.93 0 -2 -5 -10 60.21 6.53 0 -2 -5 -10 76.19 9.00 0 -3 -5 -10 6.92 6.21 0 -3 -5 -10 1.57 6.30 0 3 5 10 12.95 8.53 0 -4 -5 -10 78.83 9.32 0 4 5 10 82.22 8.96 0 -4 -5 -10 97.67 9.35 0 -5 -5 -10 5.80 9.57 0 5 5 10 -1.41 9.26 0 -5 -5 -10 4.19 9.28 0 -1 -3 11 72.47 10.11 0 1 3 -11 76.33 10.12 0 0 -3 11 117.16 9.10 0 0 3 -11 107.74 9.77 0 1 -3 11 6.60 9.24 0 -1 3 -11 3.21 9.79 0 -2 3 -11 32.18 10.26 0 2 -3 11 22.29 9.55 0 2 2 -11 82.95 7.91 0 1 2 -11 126.60 9.91 0 0 -2 11 20.15 8.80 0 0 2 -11 9.96 9.13 0 1 -2 11 88.15 9.08 0 -1 2 -11 79.82 7.13 0 2 -2 11 153.89 7.25 0 -2 2 -11 164.30 10.04 0 -3 2 -11 27.94 6.89 0 3 -2 11 30.22 9.17 0 2 1 -11 65.66 9.62 0 2 1 -11 74.26 13.74 0 1 1 -11 9.71 14.28 0 1 1 -11 15.75 8.95 0 0 1 -11 156.78 17.19 0 0 1 -11 138.78 9.83 0 1 -1 11 155.57 7.01 0 -1 1 -11 164.41 19.58 0 -1 1 -11 179.16 9.56 0 2 -1 11 -4.00 8.38 0 2 -1 11 2.58 15.09 0 -2 1 -11 6.90 8.85 0 3 -1 11 35.78 8.70 0 3 -1 11 38.76 12.68 0 -3 1 -11 42.58 6.70 0 4 -1 11 -0.48 8.58 0 -4 1 -11 73.71 9.99 0 4 -1 11 61.76 11.94 0 2 0 -11 59.38 11.49 0 2 0 -11 67.12 9.44 0 1 0 -11 120.55 9.61 0 1 0 -11 109.94 11.92 0 0 0 -11 17.95 10.98 0 0 0 11 11.94 10.73 0 0 0 -11 9.81 8.44 0 -1 0 -11 66.42 11.73 0 1 0 11 64.24 11.02 0 -1 0 -11 71.40 8.91 0 2 0 11 191.83 9.36 0 -2 0 -11 222.82 15.29 0 -2 0 -11 190.70 9.76 0 2 0 11 206.27 12.20 0 3 0 11 12.64 8.53 0 3 0 11 3.00 10.34 0 -3 0 -11 7.62 11.14 0 -3 0 -11 10.72 9.06 0 4 0 11 4.70 8.61 0 -4 0 -11 1.71 8.81 0 -4 0 -11 3.32 9.53 0 4 0 11 0.02 10.57 0 2 -1 -11 108.92 11.94 0 2 -1 -11 114.03 7.99 0 -1 1 11 4.57 8.59 0 1 -1 -11 11.84 8.61 0 1 -1 -11 9.81 8.70 0 0 -1 -11 55.98 11.36 0 0 -1 -11 68.87 6.60 0 0 1 11 79.35 9.43 0 1 1 11 167.55 11.85 0 -1 -1 -11 167.15 11.79 0 -1 -1 -11 171.45 9.47 0 2 1 11 18.97 10.03 0 -2 -1 -11 21.18 8.91 0 -2 -1 -11 21.58 8.75 0 3 1 11 1.84 8.76 0 3 1 11 5.79 8.43 0 -3 -1 -11 11.10 11.09 0 -3 -1 -11 1.25 8.77 0 4 1 11 -3.52 5.90 0 -4 -1 -11 145.18 10.41 0 -4 -1 -11 134.23 7.48 0 4 1 11 146.06 11.53 0 5 1 11 4.90 8.79 0 -5 -1 -11 38.83 9.66 0 5 1 11 40.14 11.31 0 -5 -1 -11 49.95 9.71 0 -1 2 11 146.36 10.27 0 1 -2 -11 135.12 10.04 0 1 -2 -11 120.77 10.16 0 0 2 11 166.13 9.94 0 0 -2 -11 163.45 7.12 0 0 -2 -11 154.09 11.73 0 -1 -2 -11 13.45 8.67 0 1 2 11 11.37 8.50 0 -1 -2 -11 22.98 8.80 0 2 2 11 114.50 9.26 0 -2 -2 -11 126.12 9.57 0 -2 -2 -11 96.50 6.97 0 -3 -2 -11 98.39 9.44 0 -3 -2 -11 80.44 9.11 0 3 2 11 99.18 9.24 0 4 2 11 -5.82 8.67 0 -4 -2 -11 7.21 11.72 0 -4 -2 -11 4.13 6.52 0 4 2 11 19.19 8.78 0 5 2 11 -1.65 8.46 0 -5 -2 -11 37.58 9.84 0 5 2 11 28.58 11.45 0 -5 -2 -11 41.51 9.16 0 0 3 11 42.98 9.28 0 0 -3 -11 48.19 9.13 0 0 -3 -11 44.92 9.30 0 1 3 11 155.87 9.89 0 -1 -3 -11 166.45 10.23 0 -1 -3 -11 144.53 9.50 0 2 3 11 15.23 8.61 0 -2 -3 -11 13.82 8.97 0 -2 -3 -11 20.08 8.73 0 -3 -3 -11 1.63 9.07 0 -3 -3 -11 5.44 8.83 0 3 3 11 8.04 8.64 0 -4 -3 -11 21.73 9.40 0 -4 -3 -11 32.37 9.20 0 4 3 11 22.53 8.91 0 1 4 11 -1.89 9.30 0 -1 -4 -11 -0.70 9.27 0 -1 -4 -11 14.77 9.27 0 2 4 11 -3.83 9.15 0 -2 -4 -11 19.84 9.05 0 -2 -4 -11 7.34 9.10 0 3 4 11 116.87 9.96 0 -3 -4 -11 78.16 10.09 0 -3 -4 -11 80.08 9.57 0 ; _shelx_hkl_checksum 94884 _shelx_res_file ; ss1605f.res created by SHELXL-2014/7 TITL Co(NCS)2(MeOH)2(3,5-Dimethylpyridine) in P-1 at 170K CELL 0.71073 7.7027 7.8688 9.1970 87.403 81.419 76.295 ZERR 1.00 0.0005 0.0005 0.0005 0.005 0.005 0.005 LATT 1 SFAC C H N S CO O UNIT 18 26 4 2 1 2 TEMP -103 BOND $H L.S. 10 ACTA HTAB EQIV $1 x, y-1, z HTAB O1 S1_$1 HTAB C15 N1 WGHT 0.050300 0.241200 FVAR 1.40573 CO1 5 0.000000 0.500000 0.500000 10.50000 0.03238 0.02301 = 0.02244 -0.00096 -0.00600 -0.01104 N1 3 0.134279 0.668817 0.371936 11.00000 0.04187 0.03146 = 0.02636 0.00066 -0.00564 -0.01604 C1 1 0.206362 0.778230 0.325290 11.00000 0.03300 0.02986 = 0.02259 -0.00339 -0.00618 -0.00703 S1 4 0.308077 0.930601 0.256992 11.00000 0.04560 0.03036 = 0.03578 -0.00176 -0.00037 -0.01838 O1 6 0.226252 0.283439 0.458083 11.00000 0.03285 0.03026 = 0.04275 -0.01025 -0.00540 -0.00886 AFIX 3 H1 2 0.241612 0.191669 0.409803 11.00000 -1.20000 AFIX 0 C2 1 0.411482 0.296143 0.438034 11.00000 0.03081 0.04274 = 0.05121 -0.00556 -0.00917 -0.01139 AFIX 137 H2A 2 0.445467 0.333966 0.336963 11.00000 -1.50000 H2B 2 0.489148 0.181605 0.456602 11.00000 -1.50000 H2C 2 0.426091 0.381518 0.506871 11.00000 -1.50000 AFIX 0 N11 3 0.111844 0.567804 0.685214 11.00000 0.03338 0.02552 = 0.02402 -0.00181 -0.00641 -0.01013 C11 1 0.160708 0.449226 0.789925 11.00000 0.03665 0.02260 = 0.02781 -0.00141 -0.00705 -0.01040 AFIX 43 H11 2 0.151417 0.332673 0.777452 11.00000 -1.20000 AFIX 0 C12 1 0.224151 0.487069 0.915625 11.00000 0.03036 0.02995 = 0.02516 -0.00143 -0.00374 -0.00892 C13 1 0.235770 0.658448 0.931266 11.00000 0.03198 0.03135 = 0.02608 -0.00591 -0.00509 -0.00978 AFIX 43 H13 2 0.277989 0.689995 1.015767 11.00000 -1.20000 AFIX 0 C14 1 0.186527 0.784117 0.825099 11.00000 0.03224 0.02597 = 0.02923 -0.00448 -0.00265 -0.00958 C15 1 0.126288 0.731911 0.703336 11.00000 0.03229 0.02488 = 0.02609 -0.00076 -0.00505 -0.00914 AFIX 43 H15 2 0.093664 0.816503 0.629149 11.00000 -1.20000 AFIX 0 C16 1 0.277960 0.347620 1.028052 11.00000 0.04181 0.03390 = 0.02987 0.00274 -0.01137 -0.01095 AFIX 137 H16A 2 0.388234 0.264035 0.986674 11.00000 -1.50000 H16B 2 0.180703 0.286391 1.055391 11.00000 -1.50000 H16C 2 0.300064 0.401418 1.115468 11.00000 -1.50000 AFIX 0 C17 1 0.198300 0.970999 0.837467 11.00000 0.04796 0.02834 = 0.04097 -0.00502 -0.00965 -0.01613 AFIX 137 H17A 2 0.217947 1.021803 0.738837 11.00000 -1.50000 H17B 2 0.299138 0.974728 0.889886 11.00000 -1.50000 H17C 2 0.085481 1.038157 0.891733 11.00000 -1.50000 AFIX 0 HKLF 4 REM Co(NCS)2(MeOH)2(3,5-Dimethylpyridine) in P-1 at 170K REM R1 = 0.0344 for 2052 Fo > 4sig(Fo) and 0.0430 for all 2431 data REM 127 parameters refined using 0 restraints END WGHT 0.0503 0.2412 REM Instructions for potential hydrogen bonds HTAB O1 S1_$1 HTAB C15 N1 REM Highest difference peak 0.366, deepest hole -0.367, 1-sigma level 0.065 Q1 1 0.1399 0.5668 0.4767 11.00000 0.05 0.37 Q2 1 0.1431 0.3644 0.4855 11.00000 0.05 0.34 Q3 1 0.1791 1.0083 0.9669 11.00000 0.05 0.34 Q4 1 0.1369 0.3785 0.4470 11.00000 0.05 0.32 Q5 1 0.3253 0.9938 0.7803 11.00000 0.05 0.31 Q6 1 0.1129 0.5968 0.4477 11.00000 0.05 0.31 Q7 1 0.1458 0.5183 0.5674 11.00000 0.05 0.30 Q8 1 0.0242 0.5966 0.3873 11.00000 0.05 0.30 Q9 1 -0.0092 0.5540 0.6340 11.00000 0.05 0.29 Q10 1 0.0527 0.3582 0.4248 11.00000 0.05 0.28 Q11 1 0.1190 0.3732 0.5691 11.00000 0.05 0.27 Q12 1 0.0766 0.4400 0.6156 11.00000 0.05 0.25 Q13 1 0.2216 0.3857 1.1327 11.00000 0.05 0.25 Q14 1 0.1464 0.7634 0.7770 11.00000 0.05 0.24 Q15 1 0.2260 0.4799 0.8440 11.00000 0.05 0.24 Q16 1 0.4384 0.4199 0.4214 11.00000 0.05 0.23 Q17 1 0.4813 0.2396 0.3439 11.00000 0.05 0.23 Q18 1 0.4925 0.2020 0.3602 11.00000 0.05 0.23 Q19 1 0.0841 1.0482 0.8001 11.00000 0.05 0.23 Q20 1 0.2553 0.5613 0.9071 11.00000 0.05 0.22 ; _shelx_res_checksum 9896 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy Co Co1 0.0000 0.5000 0.5000 0.02492(13) Uani d 1 N N1 0.1343(3) 0.6688(3) 0.3719(2) 0.0319(4) Uani d 1 C C1 0.2064(3) 0.7782(3) 0.3253(2) 0.0282(4) Uani d 1 S S1 0.30808(9) 0.93060(7) 0.25699(6) 0.03616(16) Uani d 1 O O1 0.2263(2) 0.2834(2) 0.45808(19) 0.0347(4) Uani d 1 H H1 0.2416 0.1917 0.4098 0.042 Uiso d 1 C C2 0.4115(3) 0.2961(4) 0.4380(3) 0.0406(6) Uani d 1 H H2A 0.4455 0.3340 0.3370 0.061 Uiso calc 1 H H2B 0.4891 0.1816 0.4566 0.061 Uiso calc 1 H H2C 0.4261 0.3815 0.5069 0.061 Uiso calc 1 N N11 0.1118(3) 0.5678(2) 0.68521(19) 0.0268(4) Uani d 1 C C11 0.1607(3) 0.4492(3) 0.7899(2) 0.0281(4) Uani d 1 H H11 0.1514 0.3327 0.7775 0.034 Uiso calc 1 C C12 0.2242(3) 0.4871(3) 0.9156(2) 0.0282(4) Uani d 1 C C13 0.2358(3) 0.6584(3) 0.9313(2) 0.0291(4) Uani d 1 H H13 0.2780 0.6900 1.0158 0.035 Uiso calc 1 C C14 0.1865(3) 0.7841(3) 0.8251(2) 0.0287(4) Uani d 1 C C15 0.1263(3) 0.7319(3) 0.7033(2) 0.0272(4) Uani d 1 H H15 0.0937 0.8165 0.6291 0.033 Uiso calc 1 C C16 0.2780(3) 0.3476(3) 1.0281(2) 0.0343(5) Uani d 1 H H16A 0.3882 0.2640 0.9867 0.051 Uiso calc 1 H H16B 0.1807 0.2864 1.0554 0.051 Uiso calc 1 H H16C 0.3001 0.4014 1.1155 0.051 Uiso calc 1 C C17 0.1983(4) 0.9710(3) 0.8375(3) 0.0374(5) Uani d 1 H H17A 0.2179 1.0218 0.7388 0.056 Uiso calc 1 H H17B 0.2991 0.9747 0.8899 0.056 Uiso calc 1 H H17C 0.0855 1.0382 0.8917 0.056 Uiso calc 1 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Co1 0.0324(2) 0.0230(2) 0.0224(2) -0.01104(16) -0.00600(15) -0.00096(14) N1 0.0419(11) 0.0315(9) 0.0264(9) -0.0160(8) -0.0056(8) 0.0007(7) C1 0.0330(11) 0.0299(10) 0.0226(9) -0.0070(9) -0.0062(8) -0.0034(8) S1 0.0456(4) 0.0304(3) 0.0358(3) -0.0184(3) -0.0004(3) -0.0018(2) O1 0.0328(9) 0.0303(8) 0.0428(9) -0.0089(7) -0.0054(7) -0.0103(7) C2 0.0308(12) 0.0427(13) 0.0512(14) -0.0114(10) -0.0092(10) -0.0056(11) N11 0.0334(10) 0.0255(9) 0.0240(8) -0.0101(7) -0.0064(7) -0.0018(7) C11 0.0367(12) 0.0226(10) 0.0278(10) -0.0104(9) -0.0071(8) -0.0014(8) C12 0.0304(11) 0.0300(11) 0.0252(10) -0.0089(9) -0.0037(8) -0.0014(8) C13 0.0320(11) 0.0314(11) 0.0261(10) -0.0098(9) -0.0051(8) -0.0059(8) C14 0.0322(11) 0.0260(10) 0.0292(10) -0.0096(9) -0.0027(8) -0.0045(8) C15 0.0323(11) 0.0249(10) 0.0261(10) -0.0091(8) -0.0051(8) -0.0008(8) C16 0.0418(13) 0.0339(12) 0.0299(11) -0.0110(10) -0.0114(9) 0.0027(9) C17 0.0480(14) 0.0283(11) 0.0410(13) -0.0161(10) -0.0097(11) -0.0050(9) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Co Co 0.3494 0.9721 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle N1 Co1 N1 . 2_566 180.0 N1 Co1 O1 . 2_566 87.76(7) N1 Co1 O1 2_566 2_566 92.24(7) N1 Co1 O1 . . 92.24(7) N1 Co1 O1 2_566 . 87.76(7) O1 Co1 O1 2_566 . 180.0 N1 Co1 N11 . 2_566 92.30(7) N1 Co1 N11 2_566 2_566 87.70(7) O1 Co1 N11 2_566 2_566 89.25(6) O1 Co1 N11 . 2_566 90.75(6) N1 Co1 N11 . . 87.70(7) N1 Co1 N11 2_566 . 92.30(7) O1 Co1 N11 2_566 . 90.75(6) O1 Co1 N11 . . 89.25(6) N11 Co1 N11 2_566 . 180.0 C1 N1 Co1 . . 167.28(17) N1 C1 S1 . . 179.04(19) C2 O1 Co1 . . 124.49(14) C2 O1 H1 . . 97.4 Co1 O1 H1 . . 131.5 O1 C2 H2A . . 109.5 O1 C2 H2B . . 109.5 H2A C2 H2B . . 109.5 O1 C2 H2C . . 109.5 H2A C2 H2C . . 109.5 H2B C2 H2C . . 109.5 C11 N11 C15 . . 117.71(17) C11 N11 Co1 . . 121.05(13) C15 N11 Co1 . . 121.16(14) N11 C11 C12 . . 123.78(19) N11 C11 H11 . . 118.1 C12 C11 H11 . . 118.1 C13 C12 C11 . . 116.89(19) C13 C12 C16 . . 122.06(19) C11 C12 C16 . . 121.05(19) C14 C13 C12 . . 120.79(19) C14 C13 H13 . . 119.6 C12 C13 H13 . . 119.6 C13 C14 C15 . . 117.59(19) C13 C14 C17 . . 122.42(19) C15 C14 C17 . . 120.0(2) N11 C15 C14 . . 123.23(19) N11 C15 H15 . . 118.4 C14 C15 H15 . . 118.4 C12 C16 H16A . . 109.5 C12 C16 H16B . . 109.5 H16A C16 H16B . . 109.5 C12 C16 H16C . . 109.5 H16A C16 H16C . . 109.5 H16B C16 H16C . . 109.5 C14 C17 H17A . . 109.5 C14 C17 H17B . . 109.5 H17A C17 H17B . . 109.5 C14 C17 H17C . . 109.5 H17A C17 H17C . . 109.5 H17B C17 H17C . . 109.5 loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance Co1 N1 . 2.0898(19) Co1 N1 2_566 2.0898(19) Co1 O1 2_566 2.1311(16) Co1 O1 . 2.1311(16) Co1 N11 2_566 2.1602(17) Co1 N11 . 2.1602(17) N1 C1 . 1.164(3) C1 S1 . 1.636(2) O1 C2 . 1.438(3) O1 H1 . 0.8399 C2 H2A . 0.9800 C2 H2B . 0.9800 C2 H2C . 0.9800 N11 C11 . 1.342(3) N11 C15 . 1.342(3) C11 C12 . 1.390(3) C11 H11 . 0.9500 C12 C13 . 1.388(3) C12 C16 . 1.502(3) C13 C14 . 1.386(3) C13 H13 . 0.9500 C14 C15 . 1.388(3) C14 C17 . 1.505(3) C15 H15 . 0.9500 C16 H16A . 0.9800 C16 H16B . 0.9800 C16 H16C . 0.9800 C17 H17A . 0.9800 C17 H17B . 0.9800 C17 H17C . 0.9800 loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA O1 H1 S1 1_545 0.84 2.45 3.2885(17) 175.3 _cod_database_fobs_code 2241953