#------------------------------------------------------------------------------ #$Date: 2016-12-06 04:18:10 +0200 (Tue, 06 Dec 2016) $ #$Revision: 188961 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/19/2241970.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2241970 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 9.9100 _cell_length_b 8.3730 _cell_length_c 22.9990 _exptl_crystal_F_000 976.00 _reflns_d_resolution_high 0.7416 _cod_data_source_file wm5343Isup2.hkl _cod_data_source_block I _shelx_title ' S140 in Pbca (plate yellow)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 268.98 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 1394.62 1396.62 72.00 o 2 1 0 19918.80 19532.16 280.34 o 4 1 0 5249.85 6668.47 167.49 o 6 1 0 78.15 94.99 12.80 o 8 1 0 3381.00 3752.11 199.45 o 0 2 0 72350.65 90390.34 2516.36 o 2 2 0 25619.65 25870.79 362.78 o 4 2 0 649.90 564.90 16.66 o 6 2 0 3104.81 3383.29 90.19 o 8 2 0 2032.23 2740.00 153.14 o 10 2 0 2292.08 2072.37 115.01 o 2 3 0 282.65 314.80 12.36 o 4 3 0 13434.65 14419.55 206.62 o 6 3 0 4878.92 5227.39 160.21 o 8 3 0 1883.25 2475.82 146.87 o 10 3 0 946.60 1087.72 453.42 o 12 3 0 255.93 72.99 57.29 o 0 4 0 90.32 143.52 11.35 o 2 4 0 2715.63 2407.66 49.17 o 4 4 0 44.43 87.43 9.93 o 6 4 0 4584.58 5101.62 102.08 o 8 4 0 1487.01 1718.08 199.76 o 10 4 0 173.81 87.57 38.12 o 12 4 0 5.81 -14.98 35.78 o 2 5 0 1374.28 1189.22 34.81 o 4 5 0 396.65 405.02 16.75 o 6 5 0 1644.15 1702.08 55.25 o 8 5 0 75.94 72.63 18.75 o 10 5 0 2.49 37.73 76.76 o 2 6 0 456.56 431.05 32.27 o 4 6 0 0.02 5.02 15.60 o 6 6 0 178.70 203.58 17.80 o 8 6 0 408.33 442.84 50.09 o 10 6 0 148.81 87.42 43.71 o 2 7 0 97.50 98.71 23.15 o 4 7 0 210.27 249.14 29.47 o 6 7 0 57.72 121.16 65.06 o 8 7 0 27.90 5.14 29.17 o 10 7 0 5.93 -9.73 41.07 o 0 8 0 1898.82 2034.73 83.60 o 2 8 0 1595.55 1680.30 52.48 o 4 8 0 336.94 290.92 27.79 o 6 8 0 67.70 75.37 31.67 o 8 8 0 281.36 343.85 63.01 o 2 9 0 617.74 669.54 49.32 o 4 9 0 1647.24 1900.39 126.46 o 6 9 0 1049.09 1057.60 83.01 o 8 9 0 116.34 142.31 61.84 o 6 10 0 125.62 23.69 102.60 o 1 1 1 185.84 125.88 3.66 o 2 1 1 3893.06 2950.88 37.83 o 3 1 1 3344.39 2939.55 57.56 o 4 1 1 2790.14 2859.29 43.23 o 5 1 1 67.22 51.20 6.12 o 6 1 1 330.45 387.43 30.12 o 7 1 1 93.13 98.50 8.16 o 8 1 1 1.94 9.18 6.57 o 0 2 1 39234.77 40680.01 849.79 o 1 2 1 439.96 241.74 6.17 o 2 2 1 2871.12 2453.08 33.16 o 3 2 1 5433.17 5238.09 64.73 o 4 2 1 385.28 348.90 8.53 o 5 2 1 5455.35 5650.79 146.09 o 6 2 1 788.35 854.79 27.44 o 7 2 1 1406.03 1503.51 35.88 o 8 2 1 41.93 72.04 11.23 o 9 2 1 326.61 278.31 41.56 o 10 2 1 88.77 58.28 24.78 o 1 3 1 140.58 40.37 5.51 o 2 3 1 1309.51 1063.66 17.56 o 3 3 1 201.42 171.09 6.76 o 4 3 1 1472.13 1302.14 21.28 o 5 3 1 23.81 30.94 5.19 o 6 3 1 283.71 293.61 14.96 o 7 3 1 854.24 805.61 55.39 o 8 3 1 15.33 13.76 12.01 o 9 3 1 1185.42 1586.95 104.88 o 10 3 1 1.44 10.25 16.83 o 11 3 1 122.01 78.87 35.51 o 12 3 1 183.35 59.50 26.17 o 0 4 1 4.86 22.79 8.55 o 1 4 1 1848.88 1781.35 32.15 o 2 4 1 2295.97 2186.13 33.27 o 3 4 1 6884.25 7029.76 80.92 o 4 4 1 435.18 536.42 12.48 o 5 4 1 14628.99 16595.16 203.23 o 6 4 1 296.81 320.80 12.89 o 7 4 1 7925.86 9519.53 234.20 o 8 4 1 30.21 29.68 9.03 o 9 4 1 139.61 139.46 36.70 o 10 4 1 132.34 83.59 53.61 o 11 4 1 97.13 65.15 23.11 o 12 4 1 71.31 71.53 29.74 o 1 5 1 3303.21 3097.43 60.51 o 2 5 1 14.50 35.02 7.90 o 3 5 1 2028.39 1738.76 36.82 o 4 5 1 2671.64 2889.34 45.46 o 5 5 1 93.10 89.95 8.64 o 6 5 1 1377.29 1621.08 39.24 o 7 5 1 2661.05 2932.57 195.06 o 8 5 1 40.04 46.10 12.56 o 9 5 1 1510.17 1402.20 267.63 o 10 5 1 0.61 12.17 35.02 o 11 5 1 136.08 168.11 31.02 o 0 6 1 514.31 461.05 33.00 o 1 6 1 6.94 7.04 12.71 o 2 6 1 1216.99 1168.30 41.30 o 4 6 1 774.11 827.92 24.69 o 5 6 1 5041.09 5528.20 123.43 o 6 6 1 346.67 347.87 15.61 o 7 6 1 1290.71 1697.17 86.74 o 8 6 1 1228.80 1324.37 124.99 o 9 6 1 14.11 17.25 17.44 o 10 6 1 252.24 198.14 52.00 o 11 6 1 58.50 60.82 45.24 o 1 7 1 6334.13 5652.16 160.82 o 2 7 1 3.10 12.05 14.76 o 3 7 1 4410.89 4365.17 130.43 o 4 7 1 355.09 355.16 21.95 o 5 7 1 12.91 8.67 14.79 o 6 7 1 863.61 981.86 50.23 o 7 7 1 1559.12 1819.23 146.62 o 8 7 1 20.64 27.86 19.25 o 9 7 1 953.56 1195.29 62.99 o 10 7 1 35.76 27.10 23.07 o 0 8 1 111.21 217.79 65.07 o 1 8 1 3.68 8.94 17.03 o 2 8 1 168.79 210.30 20.85 o 3 8 1 654.04 663.51 43.57 o 4 8 1 85.08 92.31 16.54 o 5 8 1 1071.54 1172.72 183.92 o 6 8 1 160.48 142.45 32.13 o 7 8 1 156.30 136.66 27.94 o 8 8 1 470.14 547.00 38.64 o 9 8 1 68.91 41.17 28.56 o 1 9 1 1887.38 1901.79 67.48 o 2 9 1 45.49 9.11 38.17 o 4 9 1 326.25 507.04 51.23 o 5 9 1 133.92 122.50 49.08 o 6 9 1 283.72 355.05 44.53 o 7 9 1 218.50 179.12 39.07 o 8 9 1 74.04 16.37 36.45 o 4 10 1 0.16 25.25 45.68 o 5 10 1 14.55 49.65 56.73 o 6 10 1 10.00 52.89 35.11 o 2 11 1 12.56 305.35 58.93 o 1 0 2 10.20 17.40 2.66 o 2 0 2 5712.20 4772.32 76.93 o 3 0 2 23548.45 23470.08 592.06 o 4 0 2 6.19 2.01 3.00 o 5 0 2 9521.48 9242.57 240.49 o 6 0 2 643.88 678.61 26.34 o 7 0 2 506.56 390.13 23.91 o 1 1 2 1317.69 1249.39 21.24 o 2 1 2 3652.73 2820.78 34.55 o 3 1 2 3911.35 3300.73 39.89 o 4 1 2 784.74 581.40 12.21 o 5 1 2 10.61 21.12 4.44 o 6 1 2 2789.55 3051.49 72.19 o 7 1 2 441.59 424.95 22.29 o 8 1 2 1447.08 1300.05 187.41 o 0 2 2 16423.67 13192.38 220.01 o 1 2 2 16042.44 14677.63 174.31 o 2 2 2 3962.97 3005.93 38.56 o 3 2 2 19133.28 20076.42 196.08 o 4 2 2 2.30 -0.20 3.49 o 5 2 2 7271.08 7460.37 165.90 o 6 2 2 457.96 477.50 27.79 o 7 2 2 3952.62 4565.24 184.57 o 8 2 2 1358.88 1564.00 69.45 o 9 2 2 99.19 82.73 12.94 o 10 2 2 787.85 679.52 60.77 o 11 2 2 169.03 125.29 24.95 o 1 3 2 931.54 736.26 14.23 o 2 3 2 726.33 649.01 14.15 o 3 3 2 434.51 662.33 13.78 o 4 3 2 4094.66 3972.21 52.40 o 5 3 2 404.37 338.51 9.83 o 6 3 2 1363.04 1446.55 44.74 o 7 3 2 4.43 7.58 5.37 o 8 3 2 294.71 301.34 31.01 o 9 3 2 634.66 756.99 34.92 o 10 3 2 18.79 26.30 16.93 o 11 3 2 235.37 129.48 65.97 o 12 3 2 239.08 43.98 41.77 o 0 4 2 25.18 7.40 9.40 o 1 4 2 3371.06 2975.05 53.84 o 2 4 2 3088.96 2736.96 41.29 o 3 4 2 4171.34 4174.10 57.89 o 4 4 2 300.80 334.76 10.78 o 5 4 2 966.57 1053.27 22.69 o 6 4 2 467.49 480.35 14.51 o 7 4 2 137.81 168.10 11.98 o 8 4 2 52.71 46.77 8.74 o 9 4 2 75.78 54.43 13.71 o 10 4 2 12.23 25.19 21.12 o 11 4 2 120.01 125.62 43.71 o 12 4 2 101.87 51.56 28.19 o 1 5 2 978.88 954.71 29.56 o 2 5 2 117.15 132.14 7.51 o 3 5 2 1066.22 1039.27 23.84 o 4 5 2 1605.55 1691.71 35.28 o 5 5 2 161.29 156.67 11.16 o 6 5 2 142.65 146.70 10.53 o 7 5 2 226.12 199.46 13.43 o 8 5 2 30.79 32.56 10.82 o 9 5 2 12.61 18.77 11.97 o 10 5 2 7.11 -5.89 27.08 o 11 5 2 391.63 609.30 42.13 o 0 6 2 556.91 533.99 26.77 o 1 6 2 22.70 27.80 8.83 o 2 6 2 43.04 39.91 10.74 o 3 6 2 264.86 230.67 17.46 o 4 6 2 31.31 33.81 9.55 o 5 6 2 4.92 23.33 10.35 o 6 6 2 1.02 3.25 9.85 o 7 6 2 731.64 858.48 51.08 o 8 6 2 41.98 26.83 17.33 o 9 6 2 98.75 75.65 19.13 o 10 6 2 132.06 114.94 28.86 o 11 6 2 92.64 117.73 36.18 o 1 7 2 964.28 975.23 106.99 o 2 7 2 14.27 5.45 20.05 o 3 7 2 23.76 47.11 12.50 o 4 7 2 92.18 77.39 15.83 o 5 7 2 10.65 13.56 13.16 o 6 7 2 71.68 84.72 22.13 o 7 7 2 383.09 423.18 24.83 o 8 7 2 5.05 17.39 16.73 o 9 7 2 349.69 329.37 62.64 o 10 7 2 49.48 26.43 25.36 o 0 8 2 544.47 491.85 33.50 o 1 8 2 17.09 13.34 22.16 o 2 8 2 1389.83 1409.47 56.33 o 3 8 2 68.94 56.25 21.31 o 4 8 2 199.71 199.42 15.44 o 5 8 2 54.19 131.37 36.24 o 6 8 2 183.91 191.13 28.04 o 7 8 2 99.70 149.29 21.00 o 8 8 2 35.00 32.06 24.75 o 9 8 2 76.38 45.76 28.15 o 2 9 2 77.89 82.86 45.12 o 3 9 2 191.76 242.95 22.56 o 4 9 2 621.34 593.57 49.13 o 5 9 2 37.81 49.42 29.39 o 6 9 2 337.68 260.18 32.60 o 7 9 2 103.05 85.40 35.61 o 8 9 2 26.06 -6.24 33.32 o 0 10 2 494.56 475.52 73.41 o 1 10 2 265.18 235.59 56.21 o 2 10 2 176.75 177.29 31.12 o 3 10 2 977.56 929.20 97.88 o 4 10 2 63.86 81.30 45.70 o 5 10 2 492.31 600.22 59.76 o 6 10 2 18.87 8.91 27.63 o 1 11 2 927.12 888.14 44.58 o 2 11 2 404.99 334.53 40.78 o 1 1 3 3261.09 2433.44 36.21 o 2 1 3 1164.34 812.02 13.75 o 3 1 3 3550.43 3585.23 43.96 o 4 1 3 16.96 13.89 2.89 o 5 1 3 9.02 1.92 3.93 o 6 1 3 561.31 637.93 18.61 o 7 1 3 609.69 575.09 37.26 o 8 1 3 0.45 1.44 6.81 o 9 1 3 23.35 27.98 11.95 o 0 2 3 6722.34 5616.35 147.17 o 1 2 3 7717.34 7268.30 86.86 o 2 2 3 526.20 502.87 10.63 o 3 2 3 3167.07 3054.91 41.14 o 4 2 3 1102.86 1026.56 17.17 o 5 2 3 403.41 495.17 9.80 o 6 2 3 7.32 17.88 4.23 o 7 2 3 260.80 268.23 16.02 o 8 2 3 1789.85 2013.07 98.79 o 9 2 3 296.27 285.48 20.93 o 10 2 3 489.53 397.37 32.09 o 11 2 3 138.75 56.23 70.07 o 1 3 3 3992.29 3426.18 43.99 o 2 3 3 8828.31 8152.32 91.00 o 3 3 3 504.41 502.50 11.96 o 4 3 3 9958.27 10360.90 114.06 o 5 3 3 68.85 70.52 6.02 o 6 3 3 7260.68 8397.49 181.58 o 7 3 3 785.38 770.55 21.29 o 8 3 3 728.43 834.89 44.85 o 9 3 3 0.25 3.26 12.67 o 10 3 3 104.67 149.63 21.62 o 11 3 3 231.55 210.60 39.97 o 12 3 3 176.84 60.43 20.57 o 0 4 3 876.13 572.72 17.32 o 1 4 3 438.30 410.25 10.67 o 2 4 3 2605.94 2165.73 30.14 o 3 4 3 1840.78 1770.00 27.19 o 4 4 3 561.65 608.89 13.84 o 5 4 3 36.89 23.25 6.56 o 6 4 3 214.70 190.85 9.33 o 7 4 3 0.37 9.02 7.54 o 8 4 3 583.68 657.78 34.76 o 9 4 3 173.31 154.40 24.71 o 10 4 3 883.75 1284.91 82.88 o 11 4 3 63.15 57.85 22.92 o 12 4 3 449.36 339.07 53.19 o 1 5 3 1149.83 1113.08 24.08 o 2 5 3 3249.66 3227.50 47.10 o 3 5 3 124.46 156.87 11.02 o 4 5 3 12709.76 14142.99 181.78 o 5 5 3 18.66 11.62 7.77 o 6 5 3 3450.10 3974.50 62.71 o 7 5 3 68.83 85.71 10.45 o 8 5 3 239.13 290.10 29.93 o 9 5 3 57.70 61.96 13.43 o 10 5 3 6.65 11.90 15.64 o 11 5 3 53.26 91.72 34.79 o 0 6 3 4995.09 4625.42 83.54 o 1 6 3 61.30 52.80 9.16 o 2 6 3 9640.90 9424.36 125.81 o 3 6 3 57.98 58.95 9.20 o 4 6 3 2517.21 2738.72 63.98 o 5 6 3 379.20 388.45 15.40 o 6 6 3 397.85 379.71 15.77 o 7 6 3 290.10 314.91 23.64 o 8 6 3 887.49 1041.42 95.17 o 9 6 3 0.18 -9.10 17.31 o 10 6 3 1683.02 2227.39 464.81 o 11 6 3 11.45 5.75 36.09 o 1 7 3 381.10 373.71 16.90 o 2 7 3 527.92 552.44 20.35 o 3 7 3 101.21 93.79 9.65 o 4 7 3 3426.94 3781.15 65.27 o 5 7 3 19.97 29.82 16.19 o 6 7 3 1669.91 1896.02 81.57 o 7 7 3 481.22 538.38 21.98 o 8 7 3 7.52 19.91 19.42 o 9 7 3 150.29 127.16 21.54 o 10 7 3 122.55 84.36 26.40 o 0 8 3 1143.73 1185.40 56.63 o 1 8 3 89.25 73.20 18.04 o 2 8 3 1102.46 1069.51 32.05 o 3 8 3 0.32 8.52 17.39 o 4 8 3 750.34 788.48 22.64 o 5 8 3 103.55 98.50 17.10 o 6 8 3 118.01 122.72 19.75 o 7 8 3 5.05 -14.83 20.94 o 8 8 3 1414.19 1768.21 127.63 o 9 8 3 37.27 39.68 25.20 o 1 9 3 190.69 190.60 24.68 o 2 9 3 639.84 613.87 25.96 o 3 9 3 221.58 201.86 19.27 o 4 9 3 1235.21 1249.97 45.15 o 5 9 3 135.33 138.59 26.40 o 6 9 3 1918.42 2186.33 79.94 o 7 9 3 138.79 148.34 26.88 o 0 10 3 12.01 23.83 40.12 o 1 10 3 9.35 -7.78 23.94 o 2 10 3 1.66 5.54 26.67 o 3 10 3 5.42 -1.39 27.75 o 4 10 3 21.78 26.21 42.67 o 5 10 3 7.11 2.68 25.36 o 6 10 3 11.20 -12.60 33.65 o 1 11 3 40.63 16.96 31.49 o 2 11 3 53.24 25.23 54.65 o 0 0 4 9010.20 7660.26 248.06 o 1 0 4 3768.59 2929.20 55.21 o 2 0 4 1720.40 1498.55 32.53 o 3 0 4 8992.26 7334.79 120.08 o 4 0 4 11.00 18.54 5.15 o 5 0 4 1900.69 1408.78 38.23 o 6 0 4 153.56 153.36 8.09 o 7 0 4 991.90 1013.20 92.62 o 8 0 4 6.89 4.49 7.65 o 1 1 4 44535.07 54397.86 934.61 o 2 1 4 840.21 724.99 12.77 o 3 1 4 10251.28 9646.33 105.94 o 4 1 4 518.49 485.62 9.66 o 5 1 4 7.78 14.35 3.53 o 6 1 4 6.24 6.73 4.73 o 7 1 4 1791.68 1812.71 142.09 o 8 1 4 14.48 5.43 6.37 o 9 1 4 5019.14 4690.60 180.92 o 10 1 4 50.89 26.34 17.13 o 0 2 4 2741.39 1995.38 37.41 o 1 2 4 1614.74 1144.76 17.30 o 2 2 4 27.14 15.60 4.58 o 3 2 4 11418.30 10547.60 114.70 o 4 2 4 1615.12 1604.52 23.38 o 5 2 4 8509.69 8421.05 126.05 o 6 2 4 6.96 6.14 4.77 o 7 2 4 2224.50 2391.25 115.00 o 8 2 4 201.62 157.52 16.89 o 9 2 4 262.52 299.85 52.42 o 10 2 4 29.26 30.34 12.72 o 11 2 4 74.62 19.11 22.77 o 1 3 4 2443.56 2039.99 31.21 o 2 3 4 3529.89 3428.45 45.60 o 3 3 4 1124.92 987.33 18.26 o 4 3 4 101.15 105.11 6.56 o 5 3 4 15.09 18.64 5.67 o 6 3 4 24.62 31.65 5.56 o 7 3 4 1510.55 1660.62 61.95 o 8 3 4 612.16 613.68 57.42 o 9 3 4 1450.46 1762.63 56.22 o 10 3 4 136.73 98.91 22.43 o 11 3 4 478.36 294.06 99.51 o 12 3 4 145.11 23.67 23.54 o 0 4 4 6201.95 5345.81 99.49 o 1 4 4 1104.17 926.41 19.47 o 2 4 4 210.84 183.40 8.18 o 3 4 4 1754.63 1588.67 24.97 o 4 4 4 350.37 355.93 11.34 o 5 4 4 3112.47 3363.91 46.14 o 6 4 4 144.20 150.10 8.99 o 7 4 4 1200.11 1395.01 66.21 o 8 4 4 3.16 11.03 9.15 o 9 4 4 51.52 29.26 11.48 o 10 4 4 170.02 182.94 27.68 o 11 4 4 4.26 6.42 24.06 o 12 4 4 2.99 -17.10 26.56 o 1 5 4 143.75 149.97 8.92 o 2 5 4 31.02 19.29 7.36 o 3 5 4 67.22 61.29 7.87 o 4 5 4 1117.82 1110.57 22.31 o 5 5 4 205.08 213.67 10.08 o 6 5 4 95.46 98.09 10.57 o 7 5 4 177.14 187.74 12.16 o 8 5 4 28.27 14.29 11.79 o 9 5 4 221.56 223.43 32.78 o 10 5 4 37.89 9.90 18.39 o 11 5 4 14.10 1.70 29.24 o 0 6 4 68.25 73.46 11.89 o 1 6 4 0.62 2.16 9.39 o 2 6 4 56.13 52.37 8.35 o 3 6 4 113.45 118.71 9.47 o 4 6 4 116.72 116.77 10.28 o 5 6 4 11.79 17.98 9.42 o 6 6 4 57.73 59.97 10.72 o 7 6 4 67.79 68.40 12.55 o 8 6 4 479.11 568.20 61.02 o 9 6 4 19.02 25.57 17.58 o 10 6 4 10.35 11.82 18.25 o 11 6 4 2.43 -34.76 26.81 o 1 7 4 1408.91 1409.97 29.64 o 2 7 4 869.48 828.82 20.26 o 3 7 4 62.86 71.76 10.31 o 4 7 4 24.76 23.10 12.28 o 5 7 4 90.54 97.88 12.55 o 6 7 4 406.90 436.06 18.69 o 7 7 4 354.44 382.95 22.51 o 8 7 4 1.38 -0.75 19.72 o 9 7 4 421.02 420.22 43.27 o 10 7 4 3.04 -12.27 26.70 o 0 8 4 2383.32 2463.80 65.62 o 1 8 4 220.13 222.18 13.98 o 2 8 4 135.83 122.43 12.60 o 3 8 4 110.78 117.88 13.81 o 4 8 4 36.70 21.52 12.32 o 5 8 4 369.56 394.98 17.59 o 6 8 4 348.83 356.67 25.08 o 7 8 4 638.88 757.81 47.56 o 8 8 4 73.13 15.09 22.72 o 9 8 4 3.69 -14.77 28.65 o 1 9 4 1106.88 1091.80 28.73 o 2 9 4 328.50 304.29 18.26 o 3 9 4 490.92 437.43 21.89 o 4 9 4 13.51 8.36 15.61 o 5 9 4 9.62 -3.33 16.77 o 6 9 4 38.57 28.52 20.27 o 7 9 4 387.05 371.58 28.44 o 0 10 4 29.80 22.69 25.90 o 1 10 4 23.33 33.74 17.40 o 2 10 4 0.13 15.65 23.69 o 3 10 4 1510.29 1512.65 68.47 o 4 10 4 9.00 11.87 21.05 o 5 10 4 1945.03 1992.40 170.40 o 1 11 4 626.48 484.51 28.29 o 2 11 4 3.89 -8.18 31.96 o 1 1 5 4212.42 3576.74 47.41 o 2 1 5 5994.35 5312.04 64.85 o 3 1 5 4704.91 4802.30 57.93 o 4 1 5 330.27 274.10 7.59 o 5 1 5 73.87 84.59 4.73 o 6 1 5 370.35 403.09 16.55 o 7 1 5 595.29 636.57 27.07 o 8 1 5 320.16 262.99 19.07 o 9 1 5 209.11 236.58 18.55 o 10 1 5 6.09 14.99 14.89 o 0 2 5 11544.88 10150.35 176.94 o 1 2 5 3374.65 2911.48 39.11 o 2 2 5 18.78 26.39 4.76 o 3 2 5 367.04 455.11 10.61 o 4 2 5 172.00 190.32 6.80 o 5 2 5 1525.78 1513.09 25.70 o 6 2 5 778.75 840.87 26.75 o 7 2 5 7.96 4.81 6.33 o 8 2 5 136.18 150.17 13.65 o 9 2 5 47.97 34.55 10.69 o 10 2 5 388.78 267.58 30.59 o 11 2 5 2.04 0.36 20.28 o 1 3 5 162.43 88.39 6.12 o 2 3 5 15267.51 15698.81 196.71 o 3 3 5 4584.99 4875.31 63.92 o 4 3 5 4106.80 4488.22 60.78 o 5 3 5 160.45 161.77 7.94 o 6 3 5 4071.87 4774.36 120.66 o 7 3 5 2524.21 2997.35 147.85 o 8 3 5 1472.54 1698.87 72.47 o 9 3 5 325.52 312.69 37.25 o 10 3 5 117.17 158.01 35.22 o 11 3 5 36.32 19.81 20.07 o 12 3 5 230.47 112.83 44.09 o 0 4 5 3039.97 2351.68 45.30 o 1 4 5 559.59 515.80 15.99 o 2 4 5 750.86 582.96 13.02 o 3 4 5 739.93 673.11 14.31 o 4 4 5 141.58 142.20 8.11 o 5 4 5 7069.36 7608.66 91.50 o 6 4 5 0.62 -3.60 7.39 o 7 4 5 2266.35 2561.47 81.49 o 8 4 5 853.79 983.34 75.33 o 9 4 5 213.11 231.37 35.07 o 10 4 5 833.91 1158.56 69.61 o 11 4 5 19.33 21.13 26.44 o 12 4 5 186.20 91.51 29.69 o 1 5 5 1647.30 1551.52 32.09 o 2 5 5 2852.41 2981.00 40.11 o 3 5 5 745.56 771.52 15.74 o 4 5 5 8598.65 9862.01 106.70 o 5 5 5 21.04 32.33 7.85 o 6 5 5 3412.90 3997.42 86.96 o 7 5 5 1934.62 2257.50 79.51 o 8 5 5 466.67 576.60 38.86 o 9 5 5 1071.22 1214.43 153.13 o 10 5 5 0.20 3.21 18.44 o 11 5 5 30.78 40.78 27.93 o 0 6 5 976.22 908.42 23.33 o 1 6 5 136.49 120.51 9.66 o 2 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8 267.69 283.43 16.98 o 3 8 8 23.23 10.03 13.21 o 4 8 8 104.95 134.38 14.70 o 5 8 8 132.99 96.00 15.78 o 6 8 8 27.84 27.68 15.97 o 7 8 8 30.92 27.50 21.55 o 8 8 8 178.75 178.20 24.47 o 1 9 8 538.23 471.34 20.36 o 2 9 8 517.39 479.78 20.45 o 3 9 8 3.04 12.10 16.48 o 4 9 8 984.97 952.37 41.21 o 5 9 8 15.17 16.28 18.28 o 6 9 8 937.19 998.84 43.33 o 7 9 8 3.62 3.79 23.02 o 0 10 8 1435.43 1140.50 58.78 o 1 10 8 17.61 15.45 20.22 o 2 10 8 676.03 572.15 45.05 o 3 10 8 118.89 123.56 22.47 o 4 10 8 173.43 165.90 19.91 o 5 10 8 79.90 59.23 23.48 o 1 1 9 244.86 225.09 7.92 o 2 1 9 375.65 535.26 12.66 o 3 1 9 1171.52 1230.33 21.68 o 4 1 9 56.64 39.97 5.85 o 5 1 9 677.58 748.24 15.02 o 6 1 9 208.84 268.10 10.04 o 7 1 9 118.07 119.19 8.31 o 8 1 9 46.68 40.61 7.85 o 9 1 9 164.31 112.83 15.78 o 10 1 9 10.68 9.74 11.08 o 11 1 9 297.84 179.81 27.03 o 12 1 9 37.44 33.80 28.49 o 0 2 9 656.59 618.61 28.35 o 1 2 9 66.72 67.01 6.77 o 2 2 9 1759.65 1780.02 29.90 o 3 2 9 5975.72 6646.07 79.70 o 4 2 9 1046.75 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11 2954.19 3092.60 44.71 o 3 5 11 13.17 12.92 9.08 o 4 5 11 4779.65 5625.92 76.96 o 5 5 11 25.66 26.43 10.25 o 6 5 11 1400.88 1688.23 46.84 o 7 5 11 35.38 51.96 13.56 o 8 5 11 828.68 981.40 57.59 o 9 5 11 1.94 2.47 16.44 o 10 5 11 13.79 6.03 20.08 o 11 5 11 2.81 -3.26 30.10 o 0 6 11 5610.02 5745.00 112.04 o 1 6 11 136.09 133.02 11.29 o 2 6 11 1569.31 1642.30 28.71 o 3 6 11 0.16 4.48 10.53 o 4 6 11 2.15 -1.08 10.75 o 5 6 11 105.85 118.19 13.22 o 6 6 11 29.40 32.84 14.56 o 7 6 11 3.45 11.40 17.82 o 8 6 11 670.94 939.31 68.47 o 9 6 11 0.68 -5.46 20.99 o 10 6 11 1756.82 1844.02 236.06 o 1 7 11 15.31 7.79 12.55 o 2 7 11 4286.54 4365.34 82.81 o 3 7 11 33.20 23.72 12.35 o 4 7 11 2117.64 2486.81 38.34 o 5 7 11 27.83 37.59 13.77 o 6 7 11 1301.52 1637.87 55.56 o 7 7 11 32.62 28.89 18.53 o 8 7 11 772.19 949.47 51.36 o 9 7 11 1.05 6.49 23.40 o 0 8 11 3142.54 3004.85 59.19 o 1 8 11 46.64 36.21 13.08 o 2 8 11 586.61 563.53 22.20 o 3 8 11 132.44 119.52 13.28 o 4 8 11 14.08 8.92 17.44 o 5 8 11 175.23 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9.60 o 5 4 12 8.41 11.03 9.37 o 6 4 12 221.53 245.08 12.51 o 7 4 12 408.60 453.55 20.88 o 8 4 12 297.79 346.28 17.54 o 9 4 12 4.88 7.98 14.84 o 10 4 12 119.79 100.75 19.42 o 11 4 12 85.47 59.60 26.23 o 1 5 12 598.19 599.72 16.71 o 2 5 12 11.89 17.10 9.70 o 3 5 12 185.59 190.42 9.69 o 4 5 12 828.24 850.08 19.22 o 5 5 12 25.09 28.57 10.57 o 6 5 12 196.81 199.98 12.83 o 7 5 12 3.39 -1.94 13.08 o 8 5 12 0.06 2.56 14.71 o 9 5 12 192.18 212.04 24.28 o 10 5 12 1.42 10.41 19.91 o 0 6 12 2818.80 2728.95 81.89 o 1 6 12 12.09 16.45 10.17 o 2 6 12 357.67 352.53 14.13 o 3 6 12 0.57 -0.12 10.46 o 4 6 12 22.48 9.66 11.50 o 5 6 12 4.60 2.35 11.67 o 6 6 12 2.43 -3.88 13.69 o 7 6 12 0.08 12.68 16.12 o 8 6 12 27.32 37.90 19.27 o 9 6 12 9.28 -4.70 20.59 o 10 6 12 17.47 12.99 24.12 o 1 7 12 393.39 416.88 17.42 o 2 7 12 45.41 36.87 12.03 o 3 7 12 69.12 70.99 13.12 o 4 7 12 382.66 394.83 18.42 o 5 7 12 28.95 38.36 14.41 o 6 7 12 521.03 624.63 22.44 o 7 7 12 2.21 3.42 18.22 o 8 7 12 18.37 3.27 20.93 o 9 7 12 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13 15.97 30.22 18.17 o 5 9 13 48.77 37.88 22.08 o 0 10 13 16.37 12.43 24.24 o 1 10 13 11.63 10.74 20.27 o 2 10 13 4.85 4.18 20.37 o 0 0 14 1331.18 1197.20 49.43 o 1 0 14 0.79 -7.02 11.68 o 2 0 14 1660.31 1655.47 49.45 o 3 0 14 591.64 554.02 21.06 o 4 0 14 340.22 356.87 15.69 o 5 0 14 920.83 1008.32 39.86 o 6 0 14 803.41 891.06 72.74 o 7 0 14 211.53 233.46 20.56 o 8 0 14 1131.24 1234.73 104.22 o 9 0 14 163.15 151.55 23.39 o 10 0 14 353.41 255.23 31.65 o 11 0 14 8.79 -12.46 19.65 o 1 1 14 60.21 59.19 7.73 o 2 1 14 2790.94 2817.40 43.85 o 3 1 14 43.09 37.06 8.01 o 4 1 14 9112.67 10022.15 118.06 o 5 1 14 191.86 209.00 10.39 o 6 1 14 7144.20 8150.31 128.55 o 7 1 14 48.62 69.13 10.70 o 8 1 14 995.57 1001.84 47.75 o 9 1 14 1.97 10.97 14.14 o 10 1 14 12.01 6.05 14.72 o 11 1 14 4.91 -1.38 19.96 o 0 2 14 4691.24 4324.22 132.86 o 1 2 14 3.29 9.46 8.01 o 2 2 14 3434.65 3441.56 53.36 o 3 2 14 43.44 31.70 9.76 o 4 2 14 600.68 627.47 17.24 o 5 2 14 39.44 36.25 9.52 o 6 2 14 347.03 378.99 14.06 o 7 2 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