#------------------------------------------------------------------------------ #$Date: 2017-07-20 08:48:32 +0300 (Thu, 20 Jul 2017) $ #$Revision: 198828 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/21/2242108.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2242108 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 15.3879 _cell_length_b 17.8733 _cell_length_c 22.2895 _exptl_crystal_F_000 2752.00 _reflns_d_resolution_high 0.7696 _cod_data_source_file zl2708k10131sup2.hkl _cod_data_source_block k10131 _shelx_title ' k10131 in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 425.07 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 12223.49 10676.15 944.39 o 4 0 0 105936.41 95212.20 2041.47 o 6 0 0 9093.83 8071.66 278.82 o 8 0 0 0.06 94.46 41.25 o 10 0 0 9828.32 9087.66 279.79 o 12 0 0 5734.92 5483.27 377.75 o 14 0 0 9867.19 9928.82 574.43 o 16 0 0 2004.23 2144.73 314.06 o 18 0 0 722.37 1035.84 274.73 o 2 1 0 20728.67 19362.22 341.11 o 3 1 0 15292.74 14424.79 201.05 o 4 1 0 297.08 213.73 16.22 o 5 1 0 4336.40 4069.78 84.40 o 6 1 0 2156.11 2315.79 83.98 o 7 1 0 19200.98 18229.29 309.86 o 8 1 0 2667.27 2497.50 64.09 o 9 1 0 12629.11 11686.78 257.22 o 10 1 0 1222.11 1024.65 64.59 o 11 1 0 328.92 336.75 59.14 o 12 1 0 55.82 52.89 54.79 o 13 1 0 405.86 583.00 87.28 o 14 1 0 81.93 121.67 161.09 o 15 1 0 554.22 435.62 120.36 o 16 1 0 827.11 712.99 141.41 o 17 1 0 1564.46 1743.11 183.22 o 18 1 0 15.50 88.43 119.32 o 19 1 0 1582.02 1557.69 235.36 o 1 2 0 39475.11 39861.66 701.25 o 2 2 0 3423.47 2990.53 59.46 o 3 2 0 3142.54 3343.50 62.04 o 4 2 0 1390.53 1350.82 30.48 o 5 2 0 1139.37 1244.13 35.40 o 6 2 0 5850.87 5276.17 101.81 o 7 2 0 337.13 389.93 26.78 o 8 2 0 5441.71 5426.06 143.60 o 9 2 0 170.11 170.13 18.86 o 10 2 0 295.36 254.71 69.03 o 11 2 0 4293.38 4106.04 197.64 o 12 2 0 3054.61 2920.28 132.19 o 13 2 0 702.62 725.34 103.91 o 14 2 0 1155.01 1004.64 96.01 o 15 2 0 5096.23 5168.81 512.61 o 16 2 0 1061.11 1159.26 395.23 o 17 2 0 253.50 137.11 126.28 o 18 2 0 7.27 32.25 231.33 o 19 2 0 207.85 259.36 135.64 o 1 3 0 86.84 61.07 26.32 o 2 3 0 27941.84 28472.75 519.18 o 3 3 0 805.27 865.82 28.64 o 4 3 0 10821.90 10598.12 206.14 o 5 3 0 9178.33 9222.39 164.25 o 6 3 0 8700.61 7920.38 152.33 o 7 3 0 6805.36 6758.73 111.45 o 8 3 0 6639.59 7085.48 128.40 o 9 3 0 3017.00 2821.00 72.46 o 10 3 0 3828.07 3764.73 136.60 o 11 3 0 13.68 35.11 20.70 o 12 3 0 4.01 42.32 52.21 o 13 3 0 2225.16 2048.15 131.85 o 14 3 0 647.29 560.22 98.64 o 15 3 0 11.21 -15.09 80.33 o 16 3 0 2222.94 2346.20 301.57 o 17 3 0 283.52 213.49 112.70 o 18 3 0 208.77 204.09 141.83 o 19 3 0 177.46 374.63 288.46 o 0 4 0 103282.38 102608.96 2495.29 o 1 4 0 360.60 293.91 21.68 o 2 4 0 18103.75 16281.87 326.55 o 3 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223.21 o 18 5 0 400.18 268.94 163.03 o 19 5 0 382.68 846.65 295.33 o 0 6 0 2419.70 2446.40 98.03 o 1 6 0 21879.35 21424.42 421.28 o 2 6 0 335.48 416.04 44.70 o 3 6 0 12263.63 12668.55 270.05 o 4 6 0 3864.73 3746.12 91.26 o 5 6 0 6594.85 6799.46 155.09 o 6 6 0 8743.96 9103.66 160.77 o 7 6 0 1916.29 1989.22 68.24 o 8 6 0 1892.48 1860.48 50.76 o 9 6 0 13660.38 14076.34 287.85 o 10 6 0 8574.41 9500.24 183.74 o 11 6 0 2794.40 2986.96 81.52 o 12 6 0 2121.21 2262.09 102.01 o 13 6 0 494.49 664.95 52.89 o 14 6 0 988.88 1118.84 83.74 o 15 6 0 246.66 125.26 91.13 o 16 6 0 0.77 13.41 78.55 o 17 6 0 0.15 114.74 118.61 o 18 6 0 0.04 -62.93 173.40 o 19 6 0 38.29 -7.49 193.56 o 1 7 0 2173.86 2097.34 74.44 o 2 7 0 25602.75 25797.40 519.18 o 3 7 0 176.14 35.54 26.69 o 4 7 0 1028.44 1156.97 46.81 o 5 7 0 1018.06 927.44 42.62 o 6 7 0 129.49 107.39 25.55 o 7 7 0 4890.29 4705.46 137.53 o 8 7 0 17732.85 18096.47 419.34 o 9 7 0 8116.66 8323.51 179.42 o 10 7 0 1864.22 2052.36 78.99 o 11 7 0 401.04 343.18 28.07 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7810.32 8162.77 337.23 o 5 11 0 337.68 372.06 51.57 o 6 11 0 9203.62 9931.69 243.18 o 7 11 0 3809.80 3829.80 113.68 o 8 11 0 3810.51 3802.68 105.52 o 9 11 0 587.18 767.24 53.88 o 10 11 0 2325.94 2419.23 89.64 o 11 11 0 284.55 354.74 56.27 o 12 11 0 138.34 144.88 43.17 o 13 11 0 103.76 106.81 39.31 o 14 11 0 607.74 882.42 134.55 o 15 11 0 224.98 142.96 114.20 o 16 11 0 92.52 59.76 120.81 o 17 11 0 297.28 85.40 203.02 o 0 12 0 199.34 96.48 66.45 o 1 12 0 16922.53 18280.19 407.16 o 2 12 0 33.95 -30.59 41.55 o 3 12 0 7089.26 7557.01 214.81 o 4 12 0 4333.47 4508.82 155.02 o 5 12 0 3447.97 3915.63 124.44 o 6 12 0 1792.63 1812.21 83.68 o 7 12 0 1651.62 1643.82 74.58 o 8 12 0 123.26 212.52 38.83 o 9 12 0 160.07 125.82 49.69 o 10 12 0 8.07 -27.22 34.99 o 11 12 0 7169.43 7818.61 215.02 o 12 12 0 35.36 82.42 54.13 o 13 12 0 2023.86 1904.71 140.78 o 14 12 0 49.22 6.24 80.42 o 15 12 0 824.21 770.27 192.15 o 16 12 0 7.58 57.47 235.70 o 17 12 0 776.08 771.10 220.40 o 1 13 0 99.95 72.81 49.84 o 2 13 0 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