#------------------------------------------------------------------------------ #$Date: 2017-07-25 12:31:11 +0300 (Tue, 25 Jul 2017) $ #$Revision: 199134 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/21/2242163.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2242163 _cell_angle_alpha 79.628 _cell_angle_beta 81.255 _cell_angle_gamma 89.348 _cell_length_a 13.2227 _cell_length_b 17.7311 _cell_length_c 24.0242 _exptl_crystal_F_000 2376.00 _reflns_d_resolution_high 0.7777 _cod_data_source_file wm5402Isup2.hkl _cod_data_source_block I _shelx_title ' ' _shelx_refln_list_code 4 _shelx_f_calc_maximum 545.56 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 15.43 33.24 3.79 o 2 0 0 60315.04 62439.16 527.77 o 3 0 0 185.21 149.01 13.43 o 4 0 0 822.75 984.39 47.32 o 5 0 0 129.73 175.26 24.36 o 6 0 0 5168.40 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3246.45 98.04 o 11 5 0 1612.32 1461.11 71.92 o 12 5 0 970.01 1002.69 82.70 o 13 5 0 42.31 12.98 129.84 o 14 5 0 5.16 106.61 63.95 o 15 5 0 2.75 22.03 68.63 o 16 5 0 122.14 127.89 79.45 o -16 6 0 22.06 39.25 87.28 o -15 6 0 1100.06 1151.52 121.72 o -14 6 0 1187.69 1174.27 107.88 o -13 6 0 460.49 318.29 74.57 o -12 6 0 1644.23 1821.28 112.40 o -11 6 0 96.28 108.17 40.05 o -10 6 0 3.86 68.67 35.76 o -9 6 0 1911.77 1901.99 63.76 o -8 6 0 2231.96 2202.75 50.85 o -7 6 0 111.86 115.04 22.02 o -6 6 0 36304.82 38699.19 327.06 o -5 6 0 613.02 649.06 17.65 o -4 6 0 30866.20 32837.40 310.59 o -3 6 0 2006.76 1776.77 51.13 o -2 6 0 74536.66 77359.90 689.88 o -1 6 0 257.65 242.02 14.60 o 0 6 0 21.33 121.04 17.37 o 1 6 0 14.94 25.50 15.35 o 2 6 0 23857.97 26374.59 289.14 o 3 6 0 2034.83 2022.82 41.46 o 4 6 0 6590.17 6351.96 121.07 o 5 6 0 1620.72 1439.73 47.77 o 6 6 0 2197.91 2460.88 62.90 o 7 6 0 1725.53 1768.45 45.97 o 8 6 0 2518.04 2587.32 57.65 o 9 6 0 718.36 735.46 37.92 o 10 6 0 160.95 165.06 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282.40 113.61 o 2 3 29 26.33 12.98 94.13 o 3 3 29 1785.25 2061.20 194.76 o 4 3 29 4356.23 4417.79 256.43 o 5 3 29 558.39 792.02 142.82 o 6 3 29 38.44 71.41 103.87 o 7 3 29 32.80 -35.71 110.36 o 8 3 29 178.85 256.43 120.10 o -3 4 29 982.62 1021.16 112.47 o -2 4 29 64.99 107.73 94.13 o -1 4 29 785.92 699.94 94.02 o 0 4 29 92.60 -16.89 108.74 o 1 4 29 134.49 155.81 103.87 o 2 4 29 30.20 12.98 84.40 o 3 4 29 17.10 126.59 100.63 o 4 4 29 22.30 19.48 97.38 o 5 4 29 650.91 714.12 139.58 o 6 4 29 7.04 -84.40 100.63 o 7 4 29 882.44 1223.74 168.79 o 8 4 29 351.97 340.83 126.59 o -3 5 29 1485.46 1824.04 135.36 o -2 5 29 357.12 450.96 97.38 o -1 5 29 1047.80 1001.25 170.41 o 0 5 29 952.72 1208.38 111.30 o 1 5 29 517.57 581.03 120.10 o 2 5 29 134.98 246.70 103.87 o 3 5 29 711.56 973.80 139.58 o 4 5 29 17.64 -81.15 84.40 o 5 5 29 1.13 0.00 90.89 o 6 5 29 9.34 -12.98 103.87 o 7 5 29 1295.24 1304.89 172.04 o 8 5 29 393.68 396.01 126.59 o -3 6 29 1489.42 1667.84 131.60 o -2 6 29 66.19 -61.89 67.45 o -1 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