#------------------------------------------------------------------------------ #$Date: 2017-07-25 12:33:55 +0300 (Tue, 25 Jul 2017) $ #$Revision: 199141 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/21/2242171.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2242171 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 10.3489 _cell_length_b 14.3664 _cell_length_c 21.4619 _exptl_crystal_F_000 1592.00 _reflns_d_resolution_high 0.6793 _cod_data_source_file hb7682Isup2.hkl _cod_data_source_block I _shelx_title ' AV_KO1001_2_A.RES IN P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 323.14 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 346.66 375.17 12.37 o 4 0 0 3408.92 3518.28 69.83 o 6 0 0 3763.34 3314.29 67.97 o 8 0 0 5626.26 5452.19 136.64 o 10 0 0 7745.64 7659.74 179.18 o 12 0 0 7.20 20.66 27.16 o 14 0 0 3.35 46.71 54.66 o 1 1 0 6122.89 6809.55 281.60 o 2 1 0 5956.19 6263.20 96.63 o 3 1 0 8288.84 8429.99 103.85 o 4 1 0 563.61 527.73 12.31 o 5 1 0 63.57 30.84 4.59 o 6 1 0 2016.68 1742.48 33.68 o 7 1 0 659.06 665.33 17.55 o 8 1 0 76.03 67.63 8.68 o 9 1 0 5769.87 5673.10 90.82 o 10 1 0 432.05 493.25 26.53 o 11 1 0 672.04 629.11 33.32 o 12 1 0 12.04 5.11 18.62 o 13 1 0 120.01 88.84 23.73 o 14 1 0 224.99 224.19 36.36 o 15 1 0 37.09 11.57 42.62 o 0 2 0 3801.69 3915.66 213.75 o 1 2 0 26279.23 28026.98 508.62 o 2 2 0 16.63 16.25 4.29 o 3 2 0 18.51 28.88 2.97 o 4 2 0 2454.84 2584.83 35.03 o 5 2 0 6764.44 6771.16 87.82 o 6 2 0 442.85 429.36 13.62 o 7 2 0 56.98 47.68 7.32 o 8 2 0 2306.25 2179.73 40.27 o 9 2 0 92.74 47.37 10.54 o 10 2 0 1301.22 1248.48 38.86 o 11 2 0 46.67 44.05 15.63 o 12 2 0 36.77 44.95 17.98 o 13 2 0 265.36 289.70 34.17 o 14 2 0 434.54 414.11 42.27 o 15 2 0 172.69 52.28 63.89 o 1 3 0 27573.02 29983.41 582.40 o 2 3 0 2343.32 2469.96 42.50 o 3 3 0 19417.20 20354.02 294.02 o 4 3 0 1594.53 1316.14 23.59 o 5 3 0 1171.40 1256.78 21.73 o 6 3 0 4669.92 4129.05 57.12 o 7 3 0 10829.33 10588.07 144.75 o 8 3 0 0.87 21.47 8.51 o 9 3 0 3626.21 3675.20 96.20 o 10 3 0 53.24 40.03 14.58 o 11 3 0 376.24 366.17 27.07 o 12 3 0 22.25 17.94 16.02 o 13 3 0 29.15 44.98 25.79 o 14 3 0 0.07 -7.03 25.04 o 1 4 0 45.64 40.27 4.27 o 2 4 0 6615.99 6675.99 103.45 o 3 4 0 29950.13 30735.72 502.46 o 4 4 0 427.31 493.46 13.98 o 5 4 0 89.24 52.04 5.41 o 6 4 0 244.50 266.64 11.64 o 7 4 0 1173.87 1085.19 26.53 o 8 4 0 4613.61 4679.50 80.73 o 9 4 0 3628.87 3365.28 64.33 o 10 4 0 1463.44 1352.78 41.84 o 11 4 0 62.64 74.23 22.26 o 12 4 0 272.78 306.39 29.11 o 13 4 0 1.09 -19.44 19.74 o 14 4 0 158.85 129.61 30.93 o 1 5 0 731.33 825.55 26.94 o 2 5 0 264.07 250.45 10.73 o 3 5 0 92.06 125.01 11.45 o 4 5 0 22.34 23.43 4.10 o 5 5 0 1609.51 1629.29 27.90 o 6 5 0 309.91 378.77 14.73 o 7 5 0 1887.68 1917.94 41.34 o 8 5 0 78.81 73.67 11.95 o 9 5 0 3146.00 2813.70 74.22 o 10 5 0 728.77 741.15 33.34 o 11 5 0 101.77 37.43 16.93 o 12 5 0 105.25 112.06 21.76 o 13 5 0 1.18 3.75 20.41 o 14 5 0 391.33 481.84 45.42 o 0 6 0 24427.64 24083.72 1274.24 o 1 6 0 1415.74 1550.40 36.57 o 2 6 0 4343.68 4367.30 77.07 o 3 6 0 13210.47 13338.57 188.47 o 4 6 0 1321.32 1431.51 27.53 o 5 6 0 636.97 574.45 14.73 o 6 6 0 960.94 1007.94 23.07 o 7 6 0 554.50 503.13 20.84 o 8 6 0 4200.59 4198.45 77.14 o 9 6 0 91.44 111.37 14.85 o 10 6 0 3.65 18.28 12.13 o 11 6 0 15.84 -1.16 14.19 o 12 6 0 3.43 13.70 16.18 o 13 6 0 384.59 410.02 37.39 o 14 6 0 6.10 15.31 30.74 o 1 7 0 1462.86 1258.42 31.48 o 2 7 0 21656.24 21631.33 356.44 o 3 7 0 941.03 926.16 19.92 o 4 7 0 4.39 8.14 4.37 o 5 7 0 2.52 6.08 4.74 o 6 7 0 1341.33 1342.73 27.89 o 7 7 0 3641.57 3472.06 62.42 o 8 7 0 2128.00 1863.61 43.65 o 9 7 0 4.55 13.31 10.48 o 10 7 0 170.81 161.76 19.12 o 11 7 0 1067.26 1009.91 44.76 o 12 7 0 412.35 506.53 40.55 o 13 7 0 61.75 22.30 22.85 o 14 7 0 179.30 228.82 47.64 o 0 8 0 3727.99 3604.33 239.30 o 1 8 0 4812.87 4872.84 103.66 o 2 8 0 480.11 522.08 13.78 o 3 8 0 19.04 21.99 4.91 o 4 8 0 838.86 790.99 19.96 o 5 8 0 1804.03 1724.39 34.85 o 6 8 0 31.02 32.71 7.35 o 7 8 0 75.45 58.81 10.16 o 8 8 0 561.44 590.34 26.79 o 9 8 0 180.35 175.57 17.87 o 10 8 0 502.70 528.36 30.85 o 11 8 0 655.56 726.20 36.47 o 12 8 0 173.46 99.83 25.65 o 13 8 0 30.75 13.02 23.67 o 14 8 0 145.19 80.04 55.76 o 1 9 0 1984.18 2054.66 48.80 o 2 9 0 881.80 1000.17 30.55 o 3 9 0 707.09 751.40 31.37 o 4 9 0 255.01 277.86 13.97 o 5 9 0 540.22 466.49 19.76 o 6 9 0 4.84 -3.26 6.82 o 7 9 0 1522.46 1434.39 39.84 o 8 9 0 689.60 734.10 30.10 o 9 9 0 49.32 35.78 12.09 o 10 9 0 350.31 422.33 28.03 o 11 9 0 257.82 239.86 24.22 o 12 9 0 43.25 20.92 21.46 o 13 9 0 93.37 67.38 63.89 o 0 10 0 80.02 85.96 41.82 o 1 10 0 659.58 648.11 33.15 o 2 10 0 2127.05 2324.94 43.55 o 3 10 0 1613.91 1579.75 35.77 o 4 10 0 30.71 27.13 6.75 o 5 10 0 551.81 532.13 21.23 o 6 10 0 374.86 492.59 20.88 o 7 10 0 1787.06 1885.84 51.21 o 8 10 0 694.75 641.06 33.79 o 9 10 0 59.83 41.11 18.18 o 10 10 0 264.30 307.64 26.70 o 11 10 0 742.93 763.44 42.63 o 12 10 0 365.54 394.21 46.87 o 13 10 0 128.43 78.99 69.70 o 1 11 0 78.22 65.65 21.75 o 2 11 0 62.41 52.45 6.19 o 3 11 0 4575.68 4683.80 87.77 o 4 11 0 6055.05 6158.88 113.87 o 5 11 0 3627.22 3744.34 75.77 o 6 11 0 1641.34 1704.23 43.42 o 7 11 0 188.63 170.49 15.58 o 8 11 0 401.40 397.04 31.66 o 9 11 0 119.64 141.99 19.07 o 10 11 0 173.86 126.85 21.07 o 11 11 0 402.45 410.05 40.25 o 12 11 0 13.05 19.64 30.81 o 0 12 0 5661.47 5601.89 259.18 o 1 12 0 4946.66 4752.15 151.27 o 2 12 0 1146.70 1128.07 36.33 o 3 12 0 464.57 428.48 17.58 o 4 12 0 35.03 27.13 9.41 o 5 12 0 16.94 4.96 8.63 o 6 12 0 71.58 49.71 10.49 o 7 12 0 576.23 562.60 26.85 o 8 12 0 204.48 238.95 21.73 o 9 12 0 7.29 26.70 14.15 o 10 12 0 17.44 -1.19 14.83 o 11 12 0 214.08 197.09 31.35 o 12 12 0 109.77 105.80 43.31 o 1 13 0 549.16 550.43 35.45 o 2 13 0 2474.66 2460.42 56.89 o 3 13 0 1721.51 1791.16 43.50 o 4 13 0 48.44 54.73 10.57 o 5 13 0 4800.17 4846.21 113.28 o 6 13 0 54.30 54.61 11.71 o 7 13 0 272.65 223.24 19.13 o 8 13 0 3.85 6.61 12.51 o 9 13 0 90.41 104.45 18.49 o 10 13 0 620.71 527.09 42.60 o 11 13 0 76.52 51.88 30.78 o 12 13 0 10.05 3.74 43.99 o 0 14 0 30.69 32.43 30.80 o 1 14 0 89.34 118.68 31.68 o 2 14 0 2163.56 1932.34 58.15 o 3 14 0 55.96 60.98 9.34 o 4 14 0 5533.37 5727.16 120.88 o 5 14 0 2.79 11.43 10.71 o 6 14 0 754.68 725.51 29.84 o 7 14 0 103.27 114.70 18.30 o 8 14 0 105.33 84.02 17.77 o 9 14 0 58.78 58.63 21.00 o 10 14 0 11.04 18.57 20.40 o 11 14 0 0.29 -10.89 31.42 o 1 15 0 784.02 763.43 43.66 o 2 15 0 16.01 24.16 9.70 o 3 15 0 1569.00 1734.38 52.22 o 4 15 0 183.67 167.13 16.06 o 5 15 0 197.92 204.89 19.28 o 6 15 0 205.29 187.51 17.87 o 7 15 0 231.20 253.83 23.71 o 8 15 0 13.76 0.71 18.60 o 9 15 0 303.85 249.47 37.13 o 10 15 0 23.64 30.25 34.07 o 0 16 0 1513.08 1719.33 139.34 o 1 16 0 127.88 165.12 33.69 o 2 16 0 3.25 10.50 8.56 o 3 16 0 1.50 12.79 10.44 o 4 16 0 557.81 576.32 32.47 o 5 16 0 40.16 34.30 13.97 o 6 16 0 1016.72 1120.52 42.54 o 7 16 0 92.97 85.35 24.22 o 8 16 0 14.92 -4.33 20.14 o 9 16 0 75.25 85.07 42.01 o 1 17 0 22.75 48.73 31.06 o 2 17 0 116.02 116.15 13.37 o 3 17 0 1319.71 1333.84 50.72 o 4 17 0 2.08 26.47 14.22 o 5 17 0 1907.40 2027.67 72.55 o 6 17 0 6.24 1.36 16.48 o 7 17 0 304.83 278.66 34.83 o 8 17 0 0.23 -6.61 24.36 o 9 17 0 15.46 6.02 35.29 o 0 18 0 6.04 33.15 36.94 o 1 18 0 0.65 -9.02 23.60 o 2 18 0 95.66 127.84 17.42 o 3 18 0 144.59 163.46 18.57 o 4 18 0 175.77 162.44 46.47 o 5 18 0 45.20 47.45 26.46 o 6 18 0 586.07 603.95 67.47 o 7 18 0 31.30 1.42 30.80 o 8 18 0 38.27 38.34 51.11 o 1 19 0 21.08 -24.51 60.41 o 2 19 0 41.60 78.19 29.93 o 3 19 0 1347.08 1488.73 75.27 o 4 19 0 13.45 23.81 23.82 o 5 19 0 144.27 173.21 38.37 o 6 19 0 358.46 364.68 55.04 o 0 20 0 264.99 328.75 105.71 o 1 20 0 85.70 93.08 82.48 o 2 20 0 359.29 490.23 126.62 o 3 20 0 90.15 70.86 37.17 o 4 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21.59 o 5 1 1 205.61 228.02 9.34 o 6 1 1 955.09 979.60 20.75 o 7 1 1 9194.00 8673.30 111.28 o 8 1 1 1034.08 987.00 24.29 o 9 1 1 2626.09 2635.07 51.06 o 10 1 1 365.20 378.64 22.46 o 11 1 1 300.75 308.69 25.67 o 12 1 1 364.58 314.20 31.96 o 13 1 1 24.38 51.78 22.01 o 14 1 1 113.51 129.12 54.94 o 15 1 1 155.95 150.38 57.34 o -15 2 1 2.69 -51.11 51.11 o -14 2 1 7.58 42.10 23.87 o -13 2 1 322.62 365.94 38.10 o -12 2 1 20.39 20.54 15.45 o -11 2 1 1040.81 1172.52 47.97 o -10 2 1 2145.53 2075.71 52.48 o -9 2 1 656.91 652.10 26.89 o -8 2 1 6893.38 6665.56 102.40 o -7 2 1 2231.76 2321.29 41.17 o -6 2 1 2073.32 1852.14 30.67 o -5 2 1 678.51 758.86 16.10 o -4 2 1 1427.05 1575.37 24.88 o -3 2 1 2713.58 2726.31 37.97 o -2 2 1 11969.08 12521.05 206.93 o -1 2 1 11033.06 11496.06 210.58 o 0 2 1 33580.64 32730.46 1174.49 o 1 2 1 10335.70 11292.55 260.85 o 2 2 1 12532.94 12664.89 220.11 o 3 2 1 2568.23 2502.29 37.38 o 4 2 1 1460.69 1638.00 26.89 o 5 2 1 732.54 802.28 16.74 o 6 2 1 2179.57 1913.18 31.30 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3278.46 3203.15 73.26 o 11 3 1 41.30 36.73 15.25 o 12 3 1 399.79 430.73 33.78 o 13 3 1 16.49 16.12 21.27 o 14 3 1 145.11 69.65 29.21 o -14 4 1 56.20 63.72 26.32 o -13 4 1 181.41 171.26 27.26 o -12 4 1 53.50 60.16 21.10 o -11 4 1 368.99 282.92 27.04 o -10 4 1 287.59 315.22 23.20 o -9 4 1 511.84 456.90 29.91 o -8 4 1 5912.12 5695.81 94.63 o -7 4 1 678.84 640.30 20.02 o -6 4 1 591.15 631.94 18.22 o -5 4 1 3629.63 3672.21 51.51 o -4 4 1 2686.33 3168.91 50.74 o -3 4 1 1793.13 1823.24 30.88 o -2 4 1 24722.72 25983.40 388.06 o -1 4 1 10464.95 11011.65 203.97 o 0 4 1 19001.33 19660.17 721.81 o 1 4 1 10126.54 10824.07 254.61 o 2 4 1 25043.23 26619.32 434.89 o 3 4 1 1942.61 1973.53 35.10 o 4 4 1 2890.34 3240.54 50.26 o 5 4 1 3865.12 3890.70 54.17 o 6 4 1 590.48 625.19 16.50 o 7 4 1 623.35 610.57 20.02 o 8 4 1 5289.83 5122.16 96.52 o 9 4 1 576.40 575.49 24.43 o 10 4 1 305.65 293.45 22.32 o 11 4 1 327.49 332.88 28.67 o 12 4 1 38.70 23.70 18.62 o 13 4 1 171.03 230.35 33.10 o 14 4 1 59.89 117.25 28.52 o -14 5 1 456.70 502.78 47.01 o -13 5 1 130.29 135.75 24.64 o -12 5 1 594.53 562.73 38.03 o -11 5 1 220.61 187.37 26.04 o -10 5 1 966.77 947.45 37.81 o -9 5 1 1485.12 1594.92 54.70 o -8 5 1 35.56 48.80 10.59 o -7 5 1 895.14 887.13 24.27 o -6 5 1 1443.43 1520.26 31.01 o -5 5 1 1736.86 1822.55 30.52 o -4 5 1 1790.43 1659.07 28.67 o -3 5 1 6762.66 7815.82 117.28 o -2 5 1 16799.64 17015.02 256.07 o -1 5 1 13478.35 14218.72 262.96 o 0 5 1 22551.75 22896.80 689.70 o 1 5 1 14777.54 15407.12 360.62 o 2 5 1 16666.41 16668.89 275.57 o 3 5 1 6950.81 8033.76 115.97 o 4 5 1 1818.43 1669.74 28.65 o 5 5 1 1807.81 1988.00 33.34 o 6 5 1 1329.97 1367.74 28.83 o 7 5 1 956.23 965.92 28.58 o 8 5 1 42.54 27.24 9.17 o 9 5 1 1593.64 1567.97 44.34 o 10 5 1 1109.52 1045.36 36.60 o 11 5 1 254.68 270.07 25.98 o 12 5 1 565.95 603.81 41.43 o 13 5 1 143.62 112.03 25.94 o 14 5 1 491.76 530.28 48.51 o -14 6 1 217.74 125.57 34.51 o -13 6 1 28.88 1.42 18.76 o -12 6 1 6.19 -4.19 16.16 o -11 6 1 930.92 969.10 41.18 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234.87 45.98 o 2 4 28 162.61 120.02 34.66 o 3 4 28 237.61 239.74 42.50 o 4 4 28 366.20 335.57 48.19 o 5 4 28 71.29 119.59 40.15 o 6 4 28 397.97 432.63 67.26 o -5 5 28 65.92 114.97 45.92 o -4 5 28 104.29 68.43 42.46 o -3 5 28 16.39 9.47 31.30 o -2 5 28 35.64 47.18 33.91 o -1 5 28 101.16 130.43 39.07 o 0 5 28 47.72 27.36 31.05 o 1 5 28 85.16 198.45 41.51 o 2 5 28 32.47 26.06 32.22 o 3 5 28 23.04 43.28 37.31 o 4 5 28 94.16 155.95 49.05 o 5 5 28 55.79 72.44 37.45 o -5 6 28 2.35 90.61 107.45 o -4 6 28 118.76 100.89 49.40 o -3 6 28 89.54 170.83 51.33 o -2 6 28 5.47 32.19 32.67 o -1 6 28 457.12 621.77 88.50 o 0 6 28 3.41 58.85 33.94 o 1 6 28 400.72 400.51 54.50 o 2 6 28 11.81 48.53 33.56 o 3 6 28 80.55 108.69 46.53 o 4 6 28 104.64 134.40 68.58 o 5 6 28 2.05 11.48 40.41 o -4 7 28 200.48 305.70 136.50 o -3 7 28 292.07 340.87 61.89 o -2 7 28 292.00 235.79 55.16 o -1 7 28 160.16 151.19 50.08 o 0 7 28 511.26 570.52 77.10 o 1 7 28 166.90 183.92 115.91 o 2 7 28 277.25 209.50 56.77 o 3 7 28 286.04 386.79 73.10 o 4 7 28 185.07 267.66 57.76 o -3 8 28 35.63 -23.81 50.93 o -2 8 28 6.97 31.24 52.86 o -1 8 28 26.21 34.90 51.33 o 0 8 28 9.55 80.16 77.83 o 1 8 28 28.92 139.70 134.75 o 2 8 28 11.41 219.44 210.26 o 3 8 28 47.93 62.52 53.24 o -2 9 28 1.12 45.31 70.86 o -1 9 28 94.46 120.81 85.96 o 0 9 28 187.37 204.45 94.10 o 1 9 28 113.22 96.42 84.80 o 2 9 28 3.94 132.43 78.99 o 1 0 29 0.86 90.64 54.49 o 2 0 29 26.12 100.19 50.47 o 3 0 29 4.94 24.30 31.89 o 4 0 29 67.75 6.77 36.61 o 5 0 29 76.31 49.33 37.69 o -5 1 29 101.97 -12.20 70.78 o -4 1 29 223.80 217.76 47.95 o -3 1 29 284.96 211.68 71.84 o -2 1 29 210.28 230.75 48.19 o -1 1 29 68.15 84.12 48.63 o 0 1 29 266.01 234.82 49.10 o 1 1 29 52.26 139.96 40.24 o 2 1 29 215.78 191.04 52.83 o 3 1 29 278.52 407.05 61.37 o 4 1 29 232.55 306.04 54.78 o 5 1 29 101.12 2.65 90.28 o -5 2 29 258.27 319.98 79.56 o -4 2 29 356.62 429.12 63.94 o -3 2 29 20.98 40.00 39.84 o -2 2 29 205.19 215.53 49.14 o -1 2 29 172.43 178.52 42.61 o 0 2 29 57.24 53.71 35.62 o 1 2 29 176.18 123.78 52.33 o 2 2 29 168.32 188.56 85.46 o 3 2 29 25.76 38.82 39.86 o 4 2 29 354.81 455.37 65.73 o 5 2 29 263.42 266.87 79.22 o -5 3 29 5.94 -50.49 79.57 o -4 3 29 57.76 41.32 47.32 o -3 3 29 250.36 254.02 43.89 o -2 3 29 144.77 161.61 37.86 o -1 3 29 77.83 107.93 35.10 o 0 3 29 90.67 128.59 35.89 o 1 3 29 85.54 84.14 35.26 o 2 3 29 147.20 114.53 41.85 o 3 3 29 288.94 258.84 45.93 o 4 3 29 50.12 -1.05 31.99 o 5 3 29 8.55 44.14 70.86 o -5 4 29 46.18 -74.35 74.35 o -4 4 29 254.43 223.78 48.70 o -3 4 29 22.88 49.19 32.80 o -2 4 29 68.90 91.77 36.71 o -1 4 29 36.66 41.01 31.20 o 0 4 29 2.44 11.57 28.63 o 1 4 29 29.50 30.74 33.42 o 2 4 29 61.47 49.19 40.85 o 3 4 29 29.09 100.56 34.77 o 4 4 29 258.05 324.88 52.09 o 5 4 29 41.26 -26.72 61.57 o -4 5 29 4.73 29.78 46.05 o -3 5 29 537.40 598.55 78.79 o -2 5 29 50.76 61.77 39.79 o -1 5 29 65.20 102.59 36.64 o 0 5 29 194.26 163.26 75.12 o 1 5 29 71.48 98.66 50.13 o 2 5 29 53.53 58.12 51.26 o 3 5 29 467.59 672.05 152.38 o 4 5 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2 30 151.61 190.72 48.83 o 0 2 30 4.25 -35.04 35.04 o 1 2 30 140.55 198.66 71.43 o 2 2 30 57.05 -20.14 67.18 o 3 2 30 318.05 396.26 63.01 o 4 2 30 158.42 138.24 99.90 o -3 3 30 291.66 249.91 80.16 o -2 3 30 139.08 106.34 42.35 o -1 3 30 267.68 270.65 44.58 o 0 3 30 21.18 90.93 37.11 o 1 3 30 249.68 322.39 48.36 o 2 3 30 133.08 114.68 48.20 o 3 3 30 289.86 339.59 226.53 o -3 4 30 123.02 223.20 105.13 o -2 4 30 194.06 170.86 55.38 o -1 4 30 47.52 49.38 35.98 o 0 4 30 305.97 292.69 52.87 o 1 4 30 60.22 52.99 38.28 o 2 4 30 159.89 75.52 51.07 o 3 4 30 112.94 622.54 141.72 o -2 5 30 48.58 117.33 85.96 o -1 5 30 177.58 171.98 80.74 o 0 5 30 7.39 98.74 72.02 o 1 5 30 170.94 208.30 68.65 o 2 5 30 55.01 39.50 72.02 o -1 6 30 139.42 109.20 80.16 o 0 6 30 22.72 59.25 74.35 o 1 6 30 139.76 110.36 80.16 o 1 0 31 122.66 180.06 89.45 o -1 1 31 142.43 -84.80 84.80 o 0 1 31 80.25 74.35 82.48 o 1 1 31 135.22 160.31 90.61 o -1 2 31 95.91 -98.74 98.74 o 0 2 31 9.20 135.92 91.77 o 1 2 31 81.84 220.72 116.17 o -1 3 31 301.17 521.59 130.11 o 0 3 31 245.71 583.04 138.24 o 1 3 31 299.43 105.71 92.93 o