#------------------------------------------------------------------------------ #$Date: 2017-07-25 12:34:50 +0300 (Tue, 25 Jul 2017) $ #$Revision: 199144 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/21/2242174.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2242174 _cell_angle_alpha 90.000 _cell_angle_beta 93.331 _cell_angle_gamma 90.000 _cell_length_a 17.2445 _cell_length_b 14.1398 _cell_length_c 19.6452 _exptl_crystal_F_000 2044.00 _reflns_d_resolution_high 0.7781 _cod_data_source_file qm2115Isup2.hkl _cod_data_source_block I _shelx_title ' 20150327_CoT18C6PPCN in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 262.74 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 6 0 0 1071.04 1257.13 37.79 o 8 0 0 5755.78 5722.54 157.07 o 10 0 0 461.96 471.77 28.16 o 12 0 0 440.00 613.08 35.24 o 14 0 0 2208.99 2308.68 79.78 o 16 0 0 632.68 733.69 47.94 o 18 0 0 2378.71 2398.95 92.12 o 20 0 0 473.09 648.18 80.07 o 22 0 0 1729.52 1919.31 124.13 o 2 1 0 2277.51 2186.74 67.51 o 3 1 0 1544.78 1806.57 30.87 o 4 1 0 6256.56 5896.83 95.48 o 5 1 0 6882.02 6133.25 115.75 o 6 1 0 40.61 66.51 7.45 o 7 1 0 4653.25 4511.83 87.79 o 8 1 0 29.36 11.66 6.49 o 9 1 0 3224.44 3168.89 65.16 o 10 1 0 13142.31 13306.30 231.04 o 11 1 0 2020.85 2049.64 43.04 o 12 1 0 7658.98 7464.46 146.88 o 13 1 0 37.18 28.18 12.72 o 14 1 0 355.84 431.01 24.13 o 15 1 0 621.84 586.50 33.87 o 16 1 0 90.33 104.10 18.31 o 17 1 0 6.72 16.84 17.39 o 18 1 0 213.87 234.84 24.13 o 19 1 0 309.81 283.08 26.83 o 20 1 0 65.02 101.74 45.55 o 21 1 0 5.26 42.93 28.10 o 22 1 0 895.39 1007.69 58.30 o 1 2 0 20740.68 18644.49 374.19 o 2 2 0 3652.57 4029.13 65.72 o 3 2 0 3800.86 3915.05 60.77 o 4 2 0 8542.06 8778.42 133.53 o 5 2 0 6.20 44.47 4.68 o 6 2 0 13.60 15.50 3.65 o 7 2 0 8401.93 8542.29 161.64 o 8 2 0 1003.28 1122.92 28.52 o 9 2 0 562.11 775.60 23.36 o 10 2 0 2682.44 2820.07 60.56 o 11 2 0 8.50 15.52 8.84 o 12 2 0 2129.14 2086.05 45.55 o 13 2 0 96.75 95.72 10.94 o 14 2 0 7.03 11.30 8.88 o 15 2 0 449.51 440.88 26.83 o 16 2 0 252.32 303.49 23.05 o 17 2 0 1966.42 1971.07 57.24 o 18 2 0 1038.72 960.52 42.58 o 19 2 0 343.46 377.13 39.20 o 20 2 0 623.36 617.37 45.40 o 21 2 0 391.25 453.93 44.70 o 2 3 0 60263.41 56691.71 2534.33 o 3 3 0 5238.50 4561.55 76.01 o 4 3 0 376.26 571.53 14.94 o 5 3 0 2359.85 1982.81 32.24 o 6 3 0 27.42 56.33 6.28 o 7 3 0 11447.81 11400.10 197.43 o 8 3 0 405.38 350.29 14.50 o 9 3 0 554.07 619.10 24.15 o 10 3 0 434.80 375.65 21.09 o 11 3 0 1830.47 1747.17 47.57 o 12 3 0 6702.78 6904.83 150.07 o 13 3 0 2332.02 2385.64 63.33 o 14 3 0 569.94 634.52 27.84 o 15 3 0 7.57 21.33 12.74 o 16 3 0 1105.20 1033.76 45.05 o 17 3 0 21.99 9.89 52.03 o 18 3 0 157.87 100.87 25.66 o 19 3 0 675.39 707.18 70.97 o 20 3 0 232.94 306.71 39.32 o 21 3 0 483.06 635.62 54.64 o 1 4 0 57904.81 54602.46 1222.50 o 2 4 0 1372.25 1552.93 29.48 o 3 4 0 19192.25 17593.19 281.03 o 4 4 0 3.60 18.72 4.79 o 5 4 0 8.24 47.90 8.39 o 6 4 0 545.28 501.25 13.80 o 7 4 0 8508.62 8752.14 143.72 o 8 4 0 3269.40 3708.24 70.00 o 9 4 0 1516.61 1512.23 37.06 o 10 4 0 0.32 19.28 11.51 o 11 4 0 1353.47 1392.03 42.39 o 12 4 0 406.02 495.19 27.67 o 13 4 0 45.48 19.46 16.61 o 14 4 0 149.70 110.53 16.80 o 15 4 0 58.21 20.24 14.89 o 16 4 0 307.08 314.06 23.73 o 17 4 0 19.15 10.74 16.16 o 18 4 0 201.32 214.81 28.56 o 19 4 0 622.26 615.94 43.35 o 20 4 0 42.45 27.12 30.02 o 21 4 0 1478.59 1534.33 70.23 o 1 5 0 1796.31 1462.38 25.77 o 2 5 0 11570.18 11893.29 182.48 o 3 5 0 1289.42 1453.90 28.93 o 4 5 0 396.51 369.75 12.17 o 5 5 0 11.51 27.14 5.96 o 6 5 0 11556.07 11599.19 189.48 o 7 5 0 34.37 36.37 7.09 o 8 5 0 247.64 270.98 12.98 o 9 5 0 1923.18 1837.52 43.10 o 10 5 0 166.32 239.00 15.72 o 11 5 0 1210.69 1173.14 32.22 o 12 5 0 127.49 137.11 15.00 o 13 5 0 932.02 992.17 39.46 o 14 5 0 370.74 402.17 27.06 o 15 5 0 4628.99 4725.24 103.89 o 16 5 0 273.60 258.94 29.23 o 17 5 0 318.14 311.73 26.17 o 18 5 0 20.63 15.83 22.50 o 19 5 0 30.71 12.57 22.22 o 20 5 0 340.95 262.65 34.95 o 21 5 0 34.38 84.97 38.69 o 0 6 0 1005.62 1443.93 36.98 o 1 6 0 11682.00 10878.82 167.91 o 2 6 0 56.47 116.09 9.17 o 3 6 0 2609.72 2949.09 50.91 o 4 6 0 33.48 57.57 6.79 o 5 6 0 919.81 791.93 20.85 o 6 6 0 8853.59 9551.06 158.54 o 7 6 0 999.20 932.01 23.87 o 8 6 0 18.42 5.52 7.39 o 9 6 0 84.48 64.41 10.52 o 10 6 0 1231.55 1243.22 34.82 o 11 6 0 1214.84 1216.99 34.98 o 12 6 0 614.93 607.91 29.98 o 13 6 0 9.80 -2.38 16.07 o 14 6 0 275.76 209.40 22.30 o 15 6 0 782.62 846.84 36.82 o 16 6 0 341.88 294.21 23.61 o 17 6 0 130.02 87.41 21.61 o 18 6 0 230.79 241.61 25.27 o 19 6 0 329.49 305.80 28.60 o 20 6 0 19.65 -26.35 26.35 o 1 7 0 3158.60 3242.39 55.70 o 2 7 0 2854.34 3018.77 49.96 o 3 7 0 12162.34 12466.74 182.58 o 4 7 0 1701.60 1671.51 33.10 o 5 7 0 5871.01 6345.54 102.47 o 6 7 0 9054.38 8900.55 149.45 o 7 7 0 7916.84 8037.50 136.26 o 8 7 0 1464.89 1514.29 32.75 o 9 7 0 1190.57 1155.22 31.79 o 10 7 0 1772.75 1916.44 47.99 o 11 7 0 1268.37 1207.38 36.41 o 12 7 0 155.09 203.53 16.85 o 13 7 0 2144.31 2224.18 59.93 o 14 7 0 36.45 58.48 19.50 o 15 7 0 2372.14 2390.79 62.28 o 16 7 0 154.45 125.14 22.05 o 17 7 0 640.28 553.13 36.06 o 18 7 0 81.38 44.07 25.92 o 19 7 0 667.42 651.94 53.40 o 20 7 0 22.59 -22.20 28.40 o 0 8 0 32.60 125.18 12.74 o 1 8 0 7259.15 7545.95 120.70 o 2 8 0 3923.87 3596.93 62.21 o 3 8 0 3812.12 3562.40 58.53 o 4 8 0 1775.17 1768.00 33.54 o 5 8 0 59.90 108.11 9.75 o 6 8 0 14.88 32.26 8.00 o 7 8 0 5450.58 5700.84 95.70 o 8 8 0 552.64 592.63 22.65 o 9 8 0 211.66 238.46 16.25 o 10 8 0 194.05 202.35 17.32 o 11 8 0 2.01 10.50 13.17 o 12 8 0 548.82 651.13 31.18 o 13 8 0 38.63 38.67 16.33 o 14 8 0 155.89 114.45 18.12 o 15 8 0 356.58 346.48 28.64 o 16 8 0 36.70 21.94 21.47 o 17 8 0 67.48 37.99 22.91 o 18 8 0 117.42 115.29 28.37 o 19 8 0 49.42 5.87 28.66 o 1 9 0 2786.99 2781.42 50.80 o 2 9 0 1799.10 1669.76 34.37 o 3 9 0 1.69 325.59 41.16 o 4 9 0 4434.99 4540.39 77.66 o 5 9 0 997.36 1068.32 25.23 o 6 9 0 146.92 416.09 22.98 o 7 9 0 197.34 202.33 13.99 o 8 9 0 436.52 414.81 19.79 o 9 9 0 130.63 129.82 15.56 o 10 9 0 1019.95 1089.02 35.94 o 11 9 0 1175.86 1256.29 39.36 o 12 9 0 951.56 922.82 40.35 o 13 9 0 5206.21 5451.45 109.05 o 14 9 0 1189.23 1123.65 40.65 o 15 9 0 2010.81 2092.64 56.21 o 16 9 0 219.03 227.31 26.01 o 17 9 0 884.25 929.60 46.02 o 18 9 0 3.67 -31.60 34.60 o 19 9 0 200.11 84.61 31.33 o 0 10 0 84.60 117.44 14.91 o 1 10 0 2484.06 2461.03 47.42 o 2 10 0 163.56 124.78 10.52 o 3 10 0 3020.74 3244.44 59.46 o 4 10 0 13512.88 13639.85 213.53 o 5 10 0 1516.57 1592.08 35.70 o 6 10 0 396.24 464.70 19.85 o 7 10 0 1076.56 1056.96 30.94 o 8 10 0 498.49 514.27 23.48 o 9 10 0 8.04 -16.18 16.18 o 10 10 0 8.78 2.00 17.92 o 11 10 0 67.18 66.91 16.96 o 12 10 0 184.20 174.92 19.92 o 13 10 0 211.44 213.32 21.69 o 14 10 0 262.40 308.12 26.72 o 15 10 0 2.88 40.14 22.18 o 16 10 0 268.06 297.30 28.56 o 17 10 0 70.28 49.10 27.09 o 18 10 0 42.46 9.31 29.40 o 1 11 0 208.03 210.29 13.76 o 2 11 0 137.90 143.27 11.54 o 3 11 0 1.16 13.36 8.69 o 4 11 0 48.32 78.01 10.71 o 5 11 0 9.43 54.54 10.89 o 6 11 0 1352.20 1443.89 35.28 o 7 11 0 0.54 9.10 10.56 o 8 11 0 2571.59 2573.48 67.89 o 9 11 0 240.53 180.71 22.95 o 10 11 0 1737.65 1893.56 53.35 o 11 11 0 45.93 54.91 19.75 o 12 11 0 426.26 453.12 28.77 o 13 11 0 2.91 33.05 19.84 o 14 11 0 1861.83 2039.59 57.99 o 15 11 0 57.69 69.36 23.00 o 16 11 0 1775.46 1910.64 55.23 o 17 11 0 4.30 -18.82 33.39 o 0 12 0 213.10 342.87 32.21 o 1 12 0 0.57 -9.35 10.75 o 2 12 0 2882.50 2727.26 54.80 o 3 12 0 3288.59 3411.24 71.21 o 4 12 0 3478.06 3612.20 69.75 o 5 12 0 385.41 424.52 23.52 o 6 12 0 15.48 39.12 12.00 o 7 12 0 17.36 11.14 11.73 o 8 12 0 22.85 29.21 17.60 o 9 12 0 698.87 790.21 47.86 o 10 12 0 885.80 844.59 57.03 o 11 12 0 16.36 79.44 23.82 o 12 12 0 1568.73 1833.95 75.50 o 13 12 0 1110.13 1081.51 58.48 o 14 12 0 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0.27 9.87 16.08 o 3 15 0 171.95 157.64 19.09 o 4 15 0 28.14 51.15 18.78 o 5 15 0 363.33 378.23 24.73 o 6 15 0 808.72 799.68 38.26 o 7 15 0 278.19 296.37 25.41 o 8 15 0 32.08 63.08 25.56 o 9 15 0 205.00 232.51 31.28 o 10 15 0 30.17 74.21 30.17 o 11 15 0 410.28 380.18 45.42 o 12 15 0 9.59 30.80 31.43 o 0 16 0 51.48 31.02 25.09 o 1 16 0 305.34 251.27 22.19 o 2 16 0 276.66 224.33 23.59 o 3 16 0 10.00 -11.93 29.91 o 4 16 0 67.64 41.03 24.57 o 5 16 0 11.76 18.04 20.84 o 6 16 0 768.15 747.32 47.91 o 7 16 0 177.36 221.51 25.09 o 8 16 0 28.88 56.59 27.25 o 9 16 0 1044.20 954.86 56.96 o 10 16 0 19.73 3.70 32.16 o 1 17 0 348.60 252.80 25.22 o 2 17 0 308.98 283.32 36.58 o 3 17 0 285.30 321.08 39.85 o 4 17 0 1.31 -3.74 22.52 o 5 17 0 38.12 70.27 23.49 o 6 17 0 370.66 323.21 27.78 o 7 17 0 274.96 308.01 32.42 o 0 18 0 140.24 6.01 78.52 o 1 18 0 447.04 366.25 39.27 o 2 18 0 63.90 54.77 30.68 o -21 0 1 329.42 400.40 48.32 o -19 0 1 61.08 93.01 46.01 o -17 0 1 474.25 560.77 45.47 o -15 0 1 520.62 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40.00 o -5 1 1 6.00 63.50 8.64 o -4 1 1 5976.30 5864.36 95.15 o -3 1 1 436.07 460.48 10.56 o -2 1 1 5667.22 4954.01 101.25 o 2 1 1 717.13 1116.83 23.49 o 4 1 1 1287.28 2088.91 42.18 o 5 1 1 19256.03 18276.18 335.96 o 6 1 1 1275.78 1269.57 28.63 o 7 1 1 265.04 240.42 10.97 o 8 1 1 110.13 203.30 13.50 o 9 1 1 59.46 210.37 21.02 o 10 1 1 748.19 812.35 23.93 o 11 1 1 4776.41 4708.19 105.56 o 12 1 1 6.24 -2.83 10.95 o 13 1 1 353.87 298.92 20.57 o 14 1 1 13.22 -1.87 13.12 o 15 1 1 550.26 532.11 32.61 o 16 1 1 1216.37 1161.24 41.13 o 17 1 1 414.32 501.68 45.47 o 18 1 1 65.07 86.57 20.31 o 19 1 1 22.34 60.31 21.93 o 20 1 1 17.46 98.37 29.39 o 21 1 1 49.25 130.00 29.52 o 22 1 1 27.79 153.91 41.72 o -22 2 1 571.26 617.75 56.07 o -21 2 1 385.34 401.11 52.16 o -20 2 1 1.14 13.05 27.59 o -19 2 1 406.29 410.05 60.61 o -18 2 1 0.28 -13.07 33.92 o -17 2 1 267.58 311.72 25.09 o -16 2 1 332.01 347.50 23.77 o -15 2 1 667.02 597.12 22.94 o -14 2 1 279.37 309.87 17.79 o -13 2 1 33.21 37.92 10.37 o -12 2 1 49.30 82.71 10.65 o -11 2 1 292.49 298.40 15.91 o -10 2 1 2.29 13.34 7.58 o -9 2 1 1464.84 1427.59 31.95 o -8 2 1 1174.78 1024.32 23.81 o -7 2 1 10151.32 10415.31 180.32 o -6 2 1 1327.26 1549.92 31.31 o -5 2 1 4428.74 4702.86 77.85 o -4 2 1 5461.91 4703.46 77.47 o -3 2 1 269.32 267.97 9.30 o -2 2 1 1881.38 1660.53 30.78 o 0 2 1 19781.69 17295.72 318.35 o 1 2 1 6725.18 7442.58 119.82 o 2 2 1 547.86 444.11 12.80 o 3 2 1 3624.33 3958.34 70.66 o 4 2 1 2129.36 2216.25 41.80 o 5 2 1 2292.45 2361.16 41.68 o 6 2 1 95.30 87.70 5.86 o 7 2 1 3525.64 3749.19 69.39 o 8 2 1 17.79 91.70 7.79 o 9 2 1 1419.94 1543.37 36.95 o 10 2 1 4457.54 4677.10 94.30 o 11 2 1 346.15 351.41 18.19 o 12 2 1 153.51 169.71 16.35 o 13 2 1 1572.14 1742.97 43.84 o 14 2 1 28.84 33.31 14.37 o 15 2 1 118.90 115.50 19.11 o 16 2 1 246.27 270.20 23.08 o 17 2 1 1374.93 1338.77 47.95 o 18 2 1 967.60 1175.87 56.58 o 19 2 1 1226.93 1384.08 56.72 o 20 2 1 412.68 662.85 61.47 o 21 2 1 1559.90 1867.25 108.64 o -21 3 1 942.20 796.34 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